CN107629584A - The halogen-free flameproof canvas that a kind of halogen-free flameproof Weak solvent coating paste, preparation method and coating obtain - Google Patents
The halogen-free flameproof canvas that a kind of halogen-free flameproof Weak solvent coating paste, preparation method and coating obtain Download PDFInfo
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- CN107629584A CN107629584A CN201710911151.6A CN201710911151A CN107629584A CN 107629584 A CN107629584 A CN 107629584A CN 201710911151 A CN201710911151 A CN 201710911151A CN 107629584 A CN107629584 A CN 107629584A
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- halogen
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- free flameproof
- slurries
- weak solvent
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Abstract
The invention discloses the halogen-free flameproof canvas that a kind of halogen-free flameproof Weak solvent coating paste, preparation method and coating obtain, coating paste includes halogen-free flameproof A slurries and B slurries, and blotting surface layer slurry；A slurries include：Poly- 120~140 parts of ethyl acetate ethylene copolymer, 10~20 parts of calcium carbonate, 10~20 parts of kaolin, 5~10 parts of titanium dioxide, 10~20 parts of deionized water；B slurries include：60~80 parts of ammonium polyphosphate, 10~20 parts of pentaerythrite, 10~20 parts of melamine, 80~100 parts of deionized water；Blotting surface layer slurry includes：140~160 parts of acrylic latex, 0.2~0.5 part of organic amine pH adjusting agent, 9~12 parts of silica, 40~60 parts of deionized water.Halogen-free flameproof coating is respectively coated in the obverse and reverse of base fabric；Front is coated one layer of ink-absorbed coated layer and obtains halogen-free flameproof and the high fire-retardant canvas of durability degree.
Description
Technical field
The present invention relates to show and colour technical field, and in particular to a kind of halogen-free flameproof show and colour technology.
Background technology
Painting advertisement material is more and more applied in recent years, including house fitting-up, market publicity and some its
Its indoor and outdoor advertisement.But the not fire-retardant characteristic of its easy firing also result in its limitation used.Later stage is to be adapted to market
Demand, engendered halogen fire-retardant Weak solvent chemical fabric.But when really running into fire, although halogen flame
There is good flame retardant effect, but can also discharge substantial amounts of toxic smog simultaneously, and these poisonous smogs will be to precision
Instrument or human body directly produce corrosion and toxic action.Except the application aspect the shortcomings that, when scrapping processing, containing in the later stage
The show and colour of halogen can produce a large amount of hydrogen halides, heavy metal etc. by burning, thus natural environment can be produced serious
Harm.And the research and development of halogen-free flameproof show and colour, it will not produce a large amount of cigarettes when not only having prevented burning during fire, and having toasted
Mist causes secondary hazards to the people in fire, and the processing of scrapping on the later stage will not also cause to seriously endanger to environment.Therefore,
Halogen-free flameproof show and colour is the direction that national following fire-retardant development in science and technology is advocated.
The content of the invention
First technical problem to be solved by this invention be：Can in view of the deficienciess of the prior art, providing one kind
It is effectively fire-retardant and do not contain halogen, and the halogen-free flameproof Weak solvent with excellent coating color developing effect and durability degree effect applies
Layer slurry.
Second technical problem to be solved by this invention be：Can in view of the deficienciess of the prior art, providing one kind
It is effectively fire-retardant and do not contain halogen, and the halogen-free flameproof Weak solvent with excellent coating color developing effect and durability degree effect applies
The preparation method of layer slurry.
3rd technical problem to be solved by this invention be：Can in view of the deficienciess of the prior art, providing one kind
It is effectively fire-retardant and do not contain halogen, and the halogen-free flameproof canvas with excellent coating color developing effect and durability degree.
To solve above-mentioned first technical problem, the technical scheme is that：
A kind of halogen-free flameproof Weak solvent coating paste, the coating paste include halogen-free flameproof water borne base slurry and weak molten
Agent blotting surface layer slurry；It is 1 that the halogen-free flameproof water borne base slurry includes weight proportion again:1~1.2 A slurries and B slurry
Material；
The A slurries include the material component of following parts by weight：Poly- 120~140 parts of ethyl acetate-ethylene copolymer,
10~20 parts of calcium carbonate, 10~20 parts of kaolin, 5~10 parts of titanium dioxide, 10~20 parts of deionized water；
The B slurries include the material component of following parts by weight：60~80 parts of ammonium polyphosphate, pentaerythrite 10~20
Part, 10~20 parts of melamine, 80~100 parts of deionized water；
The Weak solvent blotting surface layer slurry includes the material component of following parts by weight：Acrylic latex 140~160
Part, 0.2~0.5 part of organic amine pH adjusting agent, 9~12 parts of Superfine Silica Dioxide, 40~60 parts of deionized water.
As a kind of improved technical scheme, the viscosity of the halogen-free flameproof water borne base slurry for 1200~
1400mPa·s；The viscosity of the Weak solvent blotting surface layer slurry is 1800~2200mPas.
As a kind of preferable technical scheme, the particle diameter of the Superfine Silica Dioxide is 6~8um.
As a kind of preferable technical scheme, the organic amine pH adjusting agent is AMP-95.
To solve above-mentioned second technical problem, the technical scheme is that：
The preparation method of halogen-free flameproof Weak solvent coating paste, comprises the following steps：
(1) halogen-free flameproof water borne base slurry is prepared：
Prepare A slurries：Deionized water, ethyl acetate-ethylene copolymer, kaolin, calcium carbonate, titanium dioxide are added respectively
Scattered stirring more than 30min is carried out into high speed dispersion tank, waits to be uniformly dispersed, using 140~160 mesh filter screens filter standby
With；
Prepare B slurries：Deionized water, ammonium polyphosphate, pentaerythrite, melamine are added in agitator tank respectively,
Speed of agitator stirs 20~30min in 600~800R/min, using 140~160 mesh filter screens filter after stirring standby
With；
According to weight proportion it is 1 by the A slurries prepared and B slurries:1~1.2 mixing, 300~400R/ of control rotating speed
Min, more than 20min is stirred, it is 1200~1400mPas to add thickener adjustment viscosity；
The weight proportion of A slurries and B slurries is that the applicant tries according to both performance and compounding effect by multiple
Verify that what is obtained most adds proportioning, if A usage of sizing agent increases, B usage of sizing agent reduces and do not have good flame retardant effect then；Instead
It, A usage of sizing agent is reduced, and B usage of sizing agent increases, and cost can be caused to improve, while the product after being coated with do not reach it is preferably full
Full scale.
(2) Weak solvent blotting surface layer slurry is prepared：Respectively by deionized water, organic amine pH adjusting agent, ultra tiny titanium dioxide
Silicon is added in dispersion tank, and 15~20min and then reduction of speed are quickly stirred with 1200~1400R/min to 400~500R/min, is added
Enter acrylic latex, and be kept stirring for more than 20min, to be mixed uniform, it is 1800- to add thickener adjustment viscosity
2200mPas, filtered using 140~160 mesh filter screens.
As a kind of preferable technical scheme, the thickener is polyurethane thickener or alkali soluble rises thickener.
To solve above-mentioned 3rd technical problem, the technical scheme is that：
A kind of halogen-free flameproof canvas, the halogen-free flameproof canvas are coated respectively with above-mentioned in the obverse and reverse of base fabric
Halogen-free flameproof water borne base slurry halogen-free flameproof coating；It is further coated with the positive halogen-free flameproof coating above-mentioned weak
The ink-absorbed coated layer of solvent blotting surface layer slurry.
As a kind of improved technical scheme, the halogen-free flameproof coating grammes per square metre is 40~50g/ ㎡ and dried by high temperature
Crosslinking Treatment；The ink-absorbed coated layer grammes per square metre is 15~20g/ ㎡ and dries crosslinking Treatment by high temperature.
As a kind of improved technical scheme, the high temperature drying crosslinking Treatment temperature is 100~120 DEG C.
By adopting the above-described technical solution, the beneficial effects of the invention are as follows：
The halogen-free flameproof Weak solvent coating paste of the present invention includes halogen-free flameproof water borne base slurry and Weak solvent blotting face
Layer slurry；It is 1 that the halogen-free flameproof water borne base slurry includes weight proportion again:1~1.2 A slurries and B slurries；Wherein A is starched
Material includes the material component of following parts by weight：Poly- 120~140 parts of ethyl acetate-ethylene copolymer, 10~20 parts of calcium carbonate,
10~20 parts of kaolin, 5~10 parts of titanium dioxide, 10~20 parts of deionized water；B slurries include the raw material group of following parts by weight
Part：60~80 parts of ammonium polyphosphate, 10~20 parts of pentaerythrite, 10~20 parts of melamine, 80~100 parts of deionized water；Institute
Stating Weak solvent blotting surface layer slurry includes the material component of following parts by weight：140~160 parts of acrylic latex, organic amine pH
0.2~0.5 part of conditioning agent, 9~12 parts of Superfine Silica Dioxide, 40~60 parts of deionized water.Halogen-free flameproof water borne base slurry
In A slurries primarily serve covering, filling and the effect such as bottoming, ammonium polyphosphate, pentaerythrite and melamine in B slurries
Mutually collaboration, plays good fire retardation；And one layer of ink-absorbed coated layer is coated in flame retardant coating top, not only increase colour developing
Effect, also improve color fastness and durability degree.
The present invention each coating coating after by high temperature dry crosslinking Treatment, by crosslinking, allow the powders such as calcium carbonate with
Acrylic latex is bonded together, and increases the weather resistance and adhesive force of coating.The present inventor confirms by test of many times：Do not hand over
The durability of coating of connection is poor, and peeling is broken once week or one-month period, and the coating being crosslinked according to the inventive method can be protected
Hold more than 2 years and remain in that good adhesion effect and color developing effect.
Brief description of the drawings
The present invention is further described with reference to the accompanying drawings and examples.
Fig. 1 is the structure sectional view of halogen-free flameproof canvas of the present invention；
In figure, 1. base fabrics；2. halogen-free flameproof coating；3. ink-absorbed coated layer.
Embodiment
With reference to the accompanying drawings and examples, the present invention is expanded on further.It should be understood that these embodiments are merely to illustrate this hair
Bright rather than limitation the scope of the present invention.In addition, it is to be understood that after the content of the invention lectured has been read, art technology
Personnel can make various changes or modifications to the present invention, and these equivalent form of values equally fall within the application appended claims and limited
Fixed scope.
As shown in Figure 1, halogen-free flameproof canvas of the invention, the halogen-free flameproof canvas base fabric 1 front and
Reverse side is coated respectively with halogen-free flameproof coating 2；Ink-absorbed coated layer 3 is further coated with the positive halogen-free flameproof coating 2.
Embodiment 1
A kind of halogen-free flameproof Weak solvent coating paste, the coating paste include halogen-free flameproof water borne base slurry and weak molten
Agent blotting surface layer slurry；It is 1 that the halogen-free flameproof water borne base slurry includes weight proportion again:1 A slurries and B slurries；It is described
The viscosity of halogen-free flameproof water borne base slurry is 1300mPas；
The A slurries include the material component of following parts by weight：Poly- 130 parts of ethyl acetate-ethylene copolymer, calcium carbonate
15 parts, 15 parts of kaolin, 8 parts of titanium dioxide, 15 parts of deionized water；The B slurries include the material component of following parts by weight：It is more
70 parts of APP, 15 parts of pentaerythrite, 15 parts of melamine, 90 parts of deionized water.
The Weak solvent blotting surface layer slurry includes the material component of following parts by weight：It is 150 parts of acrylic latex, organic
0.3 part of amine pH adjusting agent, 11 parts of Superfine Silica Dioxide, 50 parts of deionized water；The viscosity of the Weak solvent blotting surface layer slurry
For 2000mPas.
Embodiment 2
A kind of halogen-free flameproof Weak solvent coating paste, the coating paste include halogen-free flameproof water borne base slurry and weak molten
Agent blotting surface layer slurry；It is 1 that the halogen-free flameproof water borne base slurry includes weight proportion again:1.2 A slurries and B slurries；Institute
The viscosity for stating halogen-free flameproof water borne base slurry is 1350mPas；
The A slurries include the material component of following parts by weight：Poly- 135 parts of ethyl acetate-ethylene copolymer, calcium carbonate
12 parts, 16 parts of kaolin, 9 parts of titanium dioxide, 18 parts of deionized water；The B slurries include the material component of following parts by weight：It is more
75 parts of APP, 16 parts of pentaerythrite, 13 parts of melamine, 86 parts of deionized water.
The Weak solvent blotting surface layer slurry includes the material component of following parts by weight：It is 155 parts of acrylic latex, organic
0.4 part of amine pH adjusting agent, particle diameter are 6~8um 10 parts of Superfine Silica Dioxide, 55 parts of deionized water；The Weak solvent blotting
The viscosity of surface layer slurry is 2100mPas.
Embodiment 3
According to the proportioning of embodiment 1：
(1) halogen-free flameproof water borne base slurry is prepared：
Prepare A slurries：Deionized water, ethyl acetate-ethylene copolymer, kaolin, calcium carbonate, titanium dioxide are added respectively
Scattered stirring 35min is carried out into high speed dispersion tank, waits to be uniformly dispersed, using 150 mesh filter screens filter standby；Prepare B slurries
Material：Deionized water, ammonium polyphosphate, pentaerythrite, melamine are added in agitator tank respectively, speed of agitator is in 700R/
Min, 25min is stirred, using 150 mesh filter screens filter after stirring standby；
According to weight proportion it is 1 by the A slurries prepared and B slurries:1 mixing, control rotating speed 350R/min, stirring
25min, it is 1300mPas to add polyurethane thickener adjustment viscosity；
(2) Weak solvent blotting surface layer slurry is prepared：Respectively by deionized water, organic amine pH adjusting agent, ultra tiny titanium dioxide
Silicon is added in dispersion tank, and 18min and then reduction of speed are quickly stirred with 1300R/min to 450R/min, adds acrylic latex, and
25min is kept stirring for, to be mixed uniformly it is 2000mPas that addition thickener, which adjusts viscosity, uses the filtering of 150 mesh filter screens.
Embodiment 3
According to the proportioning of embodiment 2：
(1) halogen-free flameproof water borne base slurry is prepared：
Prepare A slurries：Deionized water, ethyl acetate-ethylene copolymer, kaolin, calcium carbonate, titanium dioxide are added respectively
Scattered stirring 40min is carried out into high speed dispersion tank, waits to be uniformly dispersed, using 140 mesh filter screens filter standby；Prepare B slurries
Material：Deionized water, ammonium polyphosphate, pentaerythrite, melamine are added in agitator tank respectively, speed of agitator is in 800R/
Min, 20min is stirred, using 140 mesh filter screens filter after stirring standby；
According to weight proportion it is 1 by the A slurries prepared and B slurries:1.2 mixing, control rotating speed 400R/min, stirring
20min, it is 1350mPas to add thickener adjustment viscosity；
(2) Weak solvent blotting surface layer slurry is prepared：Respectively by deionized water, organic amine pH adjusting agent, ultra tiny titanium dioxide
Silicon is added in dispersion tank, and 15min and then reduction of speed are quickly stirred with 1400R/min to 500R/min, adds acrylic latex, and
More than 20min is kept stirring for, to be mixed uniform, it is 2100mPas to add thickener adjustment viscosity, uses 140 mesh filter screen mistakes
Filter.
Embodiment 5
Coating machine drying temperature is set as 120 DEG C, and is fixed base fabric to be coated by coating machine, sets Coating Speed
16m/min, the halogen-free flameproof water borne base slurry that embodiment 3 is prepared is affixed to by base fabric in a manner of scratching scraper
Positive and negative two surface, by passing through oven for drying crosslinking Treatment (coating grammes per square metre 50g/ ㎡) after continuous coating.
Treat, by after halogen-free flameproof coated and dried, one layer of ink-absorbed coated layer to be scratched again in positive halogen-free flameproof coating surface
(coating grammes per square metre 20g/ ㎡), by being halogen-free flameproof Weak solvent chemical fibre canvas finished product after oven for drying and crosslinking Treatment.
Embodiment 6
Coating machine drying temperature is set as 110 DEG C, and is fixed base fabric to be coated by coating machine, sets Coating Speed
18m/min, the halogen-free flameproof water borne base slurry that embodiment 4 is prepared is affixed to by base fabric in a manner of scratching scraper
Positive and negative two surface, by passing through oven for drying crosslinking Treatment (coating grammes per square metre 45g/ ㎡) after continuous coating.
Treat, by after halogen-free flameproof coated and dried, one layer of ink-absorbed coated layer to be scratched again in positive halogen-free flameproof coating surface
(coating grammes per square metre 16g/ ㎡), by being halogen-free flameproof Weak solvent chemical fibre canvas finished product after oven for drying and crosslinking Treatment.
Comparative example 1
Unlike embodiment 5：Melamine is not contained in the B slurries used, remaining is identical.
Comparative example 2
Unlike embodiment 5：Ammonium polyphosphate is not contained in the B slurries used, remaining is identical.
Comparative example 3
Unlike embodiment 5：Pentaerythrite is not contained in the B slurries used, remaining is identical.
Comparative example 4
Unlike embodiment 5：Without using B slurries, remaining is identical.
Embodiment 5, embodiment 6, comparative example 1-4 are prepared fire-retardant canvas and respectively take 2.5 × 15cm cloth to test,
Its flame retardant effect see the table below 1.
Table 1
It can be seen that in comparative example 1, comparative example 2 and comparative example 3 in the case where only adding a kind of fire retardant less, its fire-retardant effect
Fruit declines a lot, and the flame retardant effect of the comparative example 4 with being not added with fire retardant is similar, almost without flame retardant effect, illustrates this hair
The three kinds of fire retardants used in bright B slurries are implicitly present in the effect mutually cooperateed with.
Claims (7)
- A kind of 1. halogen-free flameproof Weak solvent coating paste, it is characterised in that：The coating paste includes halogen-free flameproof water borne base Slurry and Weak solvent blotting surface layer slurry；It is 1 that the halogen-free flameproof water borne base slurry includes weight proportion again:1~1.2 A Slurry and B slurries；The A slurries include the material component of following parts by weight：Poly- 120~140 parts of ethyl acetate-ethylene copolymer, carbonic acid 10~20 parts of calcium, 10~20 parts of kaolin, 5~10 parts of titanium dioxide, 10~20 parts of deionized water；The B slurries include the material component of following parts by weight：60~80 parts of ammonium polyphosphate, 10~20 parts of pentaerythrite, 10~20 parts of melamine, 80~100 parts of deionized water；The Weak solvent blotting surface layer slurry includes the material component of following parts by weight：140~160 parts of acrylic latex, have 0.2~0.5 part of machine amine pH adjusting agent, 9~12 parts of Superfine Silica Dioxide, 40~60 parts of deionized water.
- 2. halogen-free flameproof Weak solvent coating paste as claimed in claim 1, it is characterised in that：The halogen-free flameproof water borne base The viscosity of slurry is 1200~1400mPas；The viscosity of the Weak solvent blotting surface layer slurry is 1800~2200mPas.
- 3. halogen-free flameproof Weak solvent coating paste as claimed in claim 1, it is characterised in that：The Superfine Silica Dioxide Particle diameter is 6~8um.
- 4. the preparation method of halogen-free flameproof Weak solvent coating paste as claimed in claim 1, it is characterised in that including following step Suddenly：(1) halogen-free flameproof water borne base slurry is prepared：Prepare A slurries：Deionized water, ethyl acetate-ethylene copolymer, kaolin, calcium carbonate, titanium dioxide are added to height respectively Scattered stirring more than 30min is carried out in fast dispersion tank, waits to be uniformly dispersed, using 140~160 mesh filter screens filter standby；Prepare B slurries：Deionized water, ammonium polyphosphate, pentaerythrite, melamine are added in agitator tank respectively, stirred Rotating speed stirs 20~30min in 600~800R/min, using 140~160 mesh filter screens filter after stirring standby；According to weight proportion it is 1 by the A slurries prepared and B slurries:1~1.2 mixing, controls 300~400R/min of rotating speed, stirs More than 20min is mixed, it is 1200~1400mPas to add thickener adjustment viscosity；(2) Weak solvent blotting surface layer slurry is prepared：Deionized water, organic amine pH adjusting agent, Superfine Silica Dioxide are added respectively Enter into dispersion tank, 15~20min and then reduction of speed are quickly stirred with 1200~1400R/min to 400~500R/min, adds third Olefin(e) acid latex, and more than 20min is kept stirring for, it is to be mixed that uniformly it is 1800-2200mPas to add thickener adjustment viscosity, Filtered using 140~160 mesh filter screens.
- A kind of 5. halogen-free flameproof canvas, it is characterised in that：The halogen-free flameproof canvas is distinguished in the obverse and reverse of base fabric The halogen-free flameproof coating for the halogen-free flameproof water borne base slurry being coated with described in claim 1；The positive halogen-free flameproof applies The ink-absorbed coated layer for the Weak solvent blotting surface layer slurry being further coated with layer described in claim 1.
- 6. halogen-free flameproof canvas as claimed in claim 5, it is characterised in that：The halogen-free flameproof coating grammes per square metre be 40~ 50g/ ㎡ simultaneously dry crosslinking Treatment by high temperature；The ink-absorbed coated layer grammes per square metre is 15~20g/ ㎡ and dried by high temperature at crosslinking Reason.
- 7. halogen-free flameproof canvas as claimed in claim 6, it is characterised in that：The high temperature dries crosslinking Treatment temperature 100~120 DEG C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710911151.6A CN107629584A (en) | 2017-09-29 | 2017-09-29 | The halogen-free flameproof canvas that a kind of halogen-free flameproof Weak solvent coating paste, preparation method and coating obtain |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710911151.6A CN107629584A (en) | 2017-09-29 | 2017-09-29 | The halogen-free flameproof canvas that a kind of halogen-free flameproof Weak solvent coating paste, preparation method and coating obtain |
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| CN107629584A true CN107629584A (en) | 2018-01-26 |
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| CN201710911151.6A Pending CN107629584A (en) | 2017-09-29 | 2017-09-29 | The halogen-free flameproof canvas that a kind of halogen-free flameproof Weak solvent coating paste, preparation method and coating obtain |
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Cited By (1)
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| CN110983804A (en) * | 2019-12-27 | 2020-04-10 | 江苏华峰超纤材料有限公司 | Heat-preservation water-repellent high-color-fastness microfiber clothing leather and preparation method thereof |
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Application publication date: 20180126 |