CN107619953A - A kind of reduction distillation reaction unit in titanium sponge production - Google Patents
A kind of reduction distillation reaction unit in titanium sponge production Download PDFInfo
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- CN107619953A CN107619953A CN201710827262.9A CN201710827262A CN107619953A CN 107619953 A CN107619953 A CN 107619953A CN 201710827262 A CN201710827262 A CN 201710827262A CN 107619953 A CN107619953 A CN 107619953A
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- sieve plate
- titanium sponge
- reactor
- reaction unit
- intersecting parallels
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Abstract
The invention discloses the reduction distillation reaction unit in a kind of titanium sponge production, mainly by reactor, cone-type tower frame, magnesium chloride pipe, sieve plate forms, magnesium chloride pipe is arranged on the side in reactor, sieve plate is arranged on the bottom of reactor, cone-type tower frame is welded on sieve plate, the sieve plate by connection below support panel and support panel intersecting parallels supporting framework into, support panel is provided with several holes, intersecting parallels support frame is formed by some risers are crisscross, every piece of riser is provided with through hole, intersecting parallels support frame bottom is nearly dome-type shape, distilling path can be formed using the device of the present invention in the titanium sponge internal and reactor bottom that sticks together, improve distillation efficiency, titanium sponge is reduced in distillation time, reduce the titanium sponge production cycle, reduce energy consumption.
Description
Technical field
The invention belongs to technical field of production of sponge titanium, reduction distillation in more particularly to a kind of magnesium reduction production titanium sponge
Reaction unit.
Background technology
Industrial production titanium sponge uses magnesium metal reduction titanium tetrachloride method mostly both at home and abroad at present, i.e., in reduction distillation work
In sequence, sieve plate first is set in reaction unit bottom, titanium sponge and magnesium chloride, magnesium chloride are obtained using magnesium metal reduction titanium tetrachloride
Discharge on time, titanium sponge, which is gradually deposited on sieve plate, to be formed titanium and stick together, and after reduction terminates, titanium is sticked together interior chlorination using distillation mode
The impurity such as magnesium remove, so as to obtain pure titanium sponge.To reduce production cost, each state is all sent out equipment enlarging as technology
Direction is opened up, still, with the increase of the type of furnace, its titanium sponge titanium sticks together, and structural base is fine and close, and center portion has sandwich lump, to ensure sponge
Titanium titanium sticks together without sandwich magnesium chloride, general to distill high constant temperature time using increase, but is so easily caused titanium sponge titanium and sticks together and distilling
Journey has a strong impact on the quality of titanium sponge because deadweight and high temperature cause its structure more and more finer and close.
After being maximized due to the type of furnace, titanium sponge sticks together, and dead weight is big, and titanium sponge sticks together bottoms by middle and upper part product
Under pressure effect, its structure is still comparatively dense, therefore, a kind of titanium sponge reduction distillation is have developed in applicant's prior art
Reaction unit（Patent applied for, application number 201710329279.1）, cone-type tower frame device is devised to support titanium sponge
Stick together, although the technology can solve the problems, such as compact product structure, but still have distillation time length, the problems such as high energy consumption.
The content of the invention
To solve problems of the prior art, invention proposes providing a kind of steaming of the reduction in titanium sponge production
Reaction unit is evaporated, distillation efficiency can be improved using this reaction unit, and can improves product compact texture problem, reduces energy consumption.
Technical scheme is as described below：
Reduction distillation reaction unit in a kind of titanium sponge production, mainly by reactor, cone-type tower frame, magnesium chloride pipe, sieve plate
Composition, magnesium chloride pipe are arranged on the side in reactor, and sieve plate is arranged on the bottom of reactor, and cone-type tower frame is welded on sieve plate
On, the sieve plate is by the intersecting parallels supporting framework of connection below support panel and support panel into support panel is provided with some
Individual hole, intersecting parallels support frame are formed by some risers are crisscross, and every piece of riser is provided with through hole, and intersecting parallels support frame bottom is
Nearly dome-type shape.
Further, the support panel is provided with liftout attachment, to take out sieve plate and tapered tower after facilitating product to come out of the stove
Frame.
Further, it is welding connection structure between described intersecting parallels support frame and support panel, intersecting parallels support frame
For the steel cast member of entirety, the intensity of sieve plate can be lifted.
Further, the cone-type tower frame, the outer surface of sieve plate are provided with and ooze titanium layer, avoid polluted product.
The advantages of the present invention mainly have：
1st, distilling path can be formed in the titanium sponge internal and reactor bottom that sticks together, improves distillation efficiency, reduce sponge titanium and distilling
Time, the titanium sponge production cycle is reduced, reduce energy consumption.
2nd, improve titanium sponge compactness structure, particularly titanium sponge titanium to stick together bottom, the structure of center portion；
3rd, distillation vacuum-pumping tube is used as using magnesium chloride pipe in the present invention, the evacuation tube that pre-existing reactors cover greatly can be cancelled,
Simplify the big lid structure of reactor, reduce air leakage point.
Brief description of the drawings
Fig. 1 is the reaction unit schematic diagram of the present invention；
Fig. 2 is that the sieve plate master in the present invention cuts open schematic diagram；
Fig. 3 is Fig. 2 upward view；
In figure：1- reactors, 2- cone-type tower frames, 3- magnesium chloride pipes, 4- sieve plates, 401- liftout attachments, 402- support panels, 403-
Through hole, 404- risers.
Embodiment
The present invention is described in further detail below in conjunction with accompanying drawing, but not theme of the present invention should not be interpreted as with regard to this
Scope is only limitted to following embodiment, without departing from the idea case in the present invention described above, all according to ordinary skill
Various modifications, replacement and the change that knowledge and customary means are made, are included within the scope of the present invention.
Embodiment one
As shown in Figure 1, Figure 2, Figure 3 shows, the reduction distillation reaction unit in a kind of titanium sponge production, mainly by reactor 1, tapered
Pylon 2, magnesium chloride pipe 3, sieve plate 4 form, and magnesium chloride pipe 3 is arranged on the side in reactor 1, and sieve plate 4 is arranged on reactor 1
Bottom, cone-type tower frame 2 are welded on sieve plate 4, and the sieve plate 4 is by support panel 402 and the well word of the lower section of support panel 402 connection
Type supporting framework into, support panel 402 is provided with several holes, and intersecting parallels support frame is formed by some risers 404 are crisscross,
Every piece of riser 404 is provided with through hole 403, and intersecting parallels support frame bottom is nearly dome-type shape.
The support panel 402 is provided with liftout attachment 401.
It is welding connection structure between described intersecting parallels support frame and support panel 402, intersecting parallels support frame is overall
Steel cast member.
The cone-type tower frame 2, the outer surface of sieve plate 4 are provided with and ooze titanium layer.
Claims (4)
- A kind of 1. reduction distillation reaction unit in titanium sponge production, mainly by reactor（1）, cone-type tower frame（2）, magnesium chloride Pipe（3）, sieve plate（4）Composition, magnesium chloride pipe（3）It is arranged on reactor（1）Interior side, sieve plate（4）It is arranged on reactor（1）'s Bottom, cone-type tower frame（2）It is welded on sieve plate（4）On, it is characterised in that the sieve plate（4）By support panel（402）And supporting surface Plate（402）The intersecting parallels supporting framework of lower section connection is into support panel（402）Be provided with several holes, intersecting parallels support frame by Some risers（404）Crisscross composition, every piece of riser（404）It is provided with through hole（403）, intersecting parallels support frame bottom is nearly half Globular shape.
- 2. the reduction distillation reaction unit in a kind of titanium sponge production according to claim 1, it is characterised in that described Support panel（402）It is provided with liftout attachment（401）.
- 3. the reduction distillation reaction unit in a kind of titanium sponge production according to claim 1 or 2, it is characterised in that institute The intersecting parallels support frame and support panel stated（402）Between be welding connection structure, intersecting parallels support frame is overall steel casting Part.
- 4. the reduction distillation reaction unit in a kind of titanium sponge production according to claim 1 or 2, it is characterised in that institute State cone-type tower frame（2）, sieve plate（4）Outer surface be provided with ooze titanium layer.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710827262.9A CN107619953A (en) | 2017-09-14 | 2017-09-14 | A kind of reduction distillation reaction unit in titanium sponge production |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710827262.9A CN107619953A (en) | 2017-09-14 | 2017-09-14 | A kind of reduction distillation reaction unit in titanium sponge production |
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| CN107619953A true CN107619953A (en) | 2018-01-23 |
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| CN201710827262.9A Pending CN107619953A (en) | 2017-09-14 | 2017-09-14 | A kind of reduction distillation reaction unit in titanium sponge production |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110055431A (en) * | 2019-06-19 | 2019-07-26 | 遵义钛业股份有限公司 | A kind of titanium produced during titanium sponge reduction sticks together centre automated hole generation device |
| CN110093516A (en) * | 2019-06-19 | 2019-08-06 | 遵义钛业股份有限公司 | Make during titanium sponge reduction distillation titanium stick together between the device that is mutually communicated of air-flow |
| CN110747356A (en) * | 2019-12-04 | 2020-02-04 | 遵义钛业股份有限公司 | Titanium lump center pore-forming and separating device for producing titanium sponge |
| CN110885929A (en) * | 2019-12-17 | 2020-03-17 | 遵义钛业股份有限公司 | Titanium lump separation device |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN201305617Y (en) * | 2008-12-05 | 2009-09-09 | 遵义钛业股份有限公司 | Sieve plate of reactor of combined furnace |
| CN201459220U (en) * | 2009-10-30 | 2010-05-12 | 朝阳百盛锆钛股份有限公司 | Reducing and distilling reactor sieve plate component for use in titanium sponge production |
| CN201678718U (en) * | 2010-04-27 | 2010-12-22 | 四川恒为制钛科技有限公司 | Reactor sieve plate used for producing titanium sponge |
| CN201857418U (en) * | 2010-11-10 | 2011-06-08 | 攀枝花钢城集团有限公司 | Sieve plate of titanium sponge reduction reactor |
| CN104152722A (en) * | 2014-08-13 | 2014-11-19 | 四川恒为制钛科技有限公司 | Titanium sponge double-magnesium chloride tube reactor and production method of titanium sponge |
| CN104357686A (en) * | 2014-12-09 | 2015-02-18 | 遵义钛业股份有限公司 | Titanium heap separation device for producing titanium sponge |
| CN104831088A (en) * | 2015-05-21 | 2015-08-12 | 罗时雨 | Sponge titanium reduction distillation reactor and production technique thereof |
-
2017
- 2017-09-14 CN CN201710827262.9A patent/CN107619953A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN201305617Y (en) * | 2008-12-05 | 2009-09-09 | 遵义钛业股份有限公司 | Sieve plate of reactor of combined furnace |
| CN201459220U (en) * | 2009-10-30 | 2010-05-12 | 朝阳百盛锆钛股份有限公司 | Reducing and distilling reactor sieve plate component for use in titanium sponge production |
| CN201678718U (en) * | 2010-04-27 | 2010-12-22 | 四川恒为制钛科技有限公司 | Reactor sieve plate used for producing titanium sponge |
| CN201857418U (en) * | 2010-11-10 | 2011-06-08 | 攀枝花钢城集团有限公司 | Sieve plate of titanium sponge reduction reactor |
| CN104152722A (en) * | 2014-08-13 | 2014-11-19 | 四川恒为制钛科技有限公司 | Titanium sponge double-magnesium chloride tube reactor and production method of titanium sponge |
| CN104357686A (en) * | 2014-12-09 | 2015-02-18 | 遵义钛业股份有限公司 | Titanium heap separation device for producing titanium sponge |
| CN104831088A (en) * | 2015-05-21 | 2015-08-12 | 罗时雨 | Sponge titanium reduction distillation reactor and production technique thereof |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110055431A (en) * | 2019-06-19 | 2019-07-26 | 遵义钛业股份有限公司 | A kind of titanium produced during titanium sponge reduction sticks together centre automated hole generation device |
| CN110093516A (en) * | 2019-06-19 | 2019-08-06 | 遵义钛业股份有限公司 | Make during titanium sponge reduction distillation titanium stick together between the device that is mutually communicated of air-flow |
| CN110747356A (en) * | 2019-12-04 | 2020-02-04 | 遵义钛业股份有限公司 | Titanium lump center pore-forming and separating device for producing titanium sponge |
| CN110885929A (en) * | 2019-12-17 | 2020-03-17 | 遵义钛业股份有限公司 | Titanium lump separation device |
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