CN107599255A - The vulcanization manufacture of glue sample and the method for inspection - Google Patents
The vulcanization manufacture of glue sample and the method for inspection Download PDFInfo
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- CN107599255A CN107599255A CN201710769201.1A CN201710769201A CN107599255A CN 107599255 A CN107599255 A CN 107599255A CN 201710769201 A CN201710769201 A CN 201710769201A CN 107599255 A CN107599255 A CN 107599255A
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- glue sample
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Abstract
The invention discloses a kind of vulcanization manufacture of glue sample and the method for inspection, comprise the following steps：（1）Parameter setting：Computer is opened, connects air pressure pump, while the switch in terminal box is allocated to vulcanization side；185 DEG C of the temperature of experiment is set, the time is arranged to 6 minutes；（2）Heating and preheating：Cavity closed pattern is selected, carries out heating preheating；Preheating time is first powered on more than 15 minutes；（3）Reset：After temperature stabilization, reset, rise die cavity；（4）Sampling test：The 8g of glue sample 5 is taken to cover top and bottom as glue sample test piece with high temperature resistant barrier paper, be placed on lower mould center and test；（5）Data record：Record data value MH peak torques, ML minimal torques, scorch time and cure time；（6）Subsequent treatment：Take out glue sample test piece, clear up die cavity, should not scratch rubber washer, terminate.Data are true, quick, easy, efficient；Top and bottom are covered with high temperature resistant barrier paper, Jiao Yang local heatings is avoided, influences result of the test.
Description
Technical field
The invention belongs to technical field of rubber preparation, vulcanization manufacture and the method for inspection more particularly, to a kind of glue sample.
Background technology
Rubber（Rubber）Refer to the strong flexible polymer material with reversible deformation, high resilience at room temperature, very
Small external force effect is lower to be produced compared with large deformation, remove resilient after external force.Rubber belongs to entirely without styling polymer, it
Glass transition temperature（T g）Low, molecular weight is often very big, more than hundreds of thousands.It is the cold resistance of butadiene rubber after vulcanization, resistance to
Mill property and elasticity are especially excellent, are generated heat under dynamic load few, and ageing-resistant performance is good, easily with natural rubber, neoprene, nitrile rubber
Deng being used in combination.
But it is existing also without a kind of method of the performance after preferably inspection vulcanization of rubber, therefore, it is necessary to develop
A kind of manufacture of new vulcanization of rubber and the method for inspection.
The content of the invention
The problem to be solved in the present invention is to propose vulcanization manufacture and the inspection party of a kind of quick, easy, efficient glue sample
Method.
In order to solve the above technical problems, the technical solution adopted by the present invention is：The vulcanization manufacture of the glue sample and the method for inspection,
Comprise the following steps：
（1）Parameter setting：Computer is opened, connects air pressure pump, while the switch in terminal box is allocated to vulcanization side；Setting experiment
185 DEG C of temperature, the time is arranged to 6 minutes；
（2）Heating and preheating：Cavity closed pattern is selected, carries out heating preheating；Preheating time is first powered on more than 15 minutes；
（3）Reset：After temperature stabilization, reset, rise die cavity；
（4）Sampling test：Glue sample 5-8g is taken to cover top and bottom as glue sample test piece with high temperature resistant barrier paper, be placed in lower mould
Test heart position；
（5）Data record：Record data value MH peak torques, ML minimal torques, scorch time and cure time；
（6）Subsequent treatment：Take out glue sample test piece, clear up die cavity, should not scratch rubber washer, terminate.
Using above-mentioned technical proposal, the real data of rubber glue sample are can obtain, discovery is repeatedly studied through inventor, experiment
Optimum temperature is 185 degree, and the time is arranged to 6 minutes；Preheating time is more than 15 minutes, primarily to so that vulcameter is in
Optimum state；Cavity closed pattern, carry out heating preheating so that die cavity forms closed-system, and vulcanization effect is best；Use high temperature resistant
Barrier paper covers top and bottom, avoids Jiao Yang local heatings, influences result of the test.
Embodiment
Embodiment 1：The vulcanization manufacture of glue sample and the method for inspection, comprise the following steps：
（1）Parameter setting：Computer is opened, connects air pressure pump, while the switch in terminal box is allocated to vulcanization side；Setting experiment
185 DEG C of temperature, the time is arranged to 6 minutes；
（2）Heating and preheating：Cavity closed pattern is selected, carries out heating preheating；Preheating time is first powered on more than 15 minutes；
（3）Reset：After temperature stabilization, reset, rise die cavity；
（4）Sampling test：Glue sample 5-8g is taken to cover top and bottom as glue sample test piece with high temperature resistant barrier paper, be placed in lower mould
Test heart position；
（5）Data record：Record data value MH peak torques, ML minimal torques, scorch time and cure time；
（6）Subsequent treatment：Take out glue sample test piece, clear up die cavity, should not scratch rubber washer, terminate.
For the ordinary skill in the art, simply the present invention is exemplarily described for specific embodiment,
Obviously present invention specific implementation is not subject to the restrictions described above, and is entered as long as employing the inventive concept and technical scheme of the present invention
The improvement of capable various unsubstantialities, or it is not improved by the present invention design and technical scheme directly apply to other occasions
, within protection scope of the present invention.
Claims (1)
1. vulcanization manufacture and the method for inspection of a kind of glue sample, it is characterised in that comprise the following steps：
（1）Parameter setting：Computer is opened, connects air pressure pump, while the switch in terminal box is allocated to vulcanization side；Setting experiment
185 DEG C of temperature, the time is arranged to 6 minutes；
（2）Heating and preheating：Cavity closed pattern is selected, carries out heating preheating；Preheating time is first powered on more than 15 minutes；
（3）Reset：After temperature stabilization, reset, rise die cavity；
（4）Sampling test：Glue sample 5-8g is taken to cover top and bottom as glue sample test piece with high temperature resistant barrier paper, be placed in lower mould
Test heart position；
（5）Data record：Record data value MH peak torques, ML minimal torques, scorch time and cure time；
（6）Subsequent treatment：Take out glue sample test piece, clear up die cavity, should not scratch rubber washer, terminate.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710769201.1A CN107599255A (en) | 2017-08-31 | 2017-08-31 | The vulcanization manufacture of glue sample and the method for inspection |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710769201.1A CN107599255A (en) | 2017-08-31 | 2017-08-31 | The vulcanization manufacture of glue sample and the method for inspection |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107599255A true CN107599255A (en) | 2018-01-19 |
Family
ID=61056643
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710769201.1A Pending CN107599255A (en) | 2017-08-31 | 2017-08-31 | The vulcanization manufacture of glue sample and the method for inspection |
Country Status (1)
| Country | Link |
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| CN (1) | CN107599255A (en) |
Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102199355A (en) * | 2011-04-23 | 2011-09-28 | 茂名市信翼化工有限公司 | Preparation method for room temperature vulcanized silicon rubber |
| CN102634046A (en) * | 2012-04-26 | 2012-08-15 | 邹德荣 | Vulcanization method for improving bonding quality of adhesive |
| CN102977471A (en) * | 2012-12-10 | 2013-03-20 | 无锡绿缘汽车零部件有限公司 | Low-emission and low-pollution EPDM (Ethylene-Propylene-Diene Monomer) rubber and preparation method thereof |
| CN103353520A (en) * | 2013-05-31 | 2013-10-16 | 南京群力运动器材有限公司 | Vulkameter operation technology |
| CN205538971U (en) * | 2015-12-25 | 2016-08-31 | 青岛科技大学 | Experimental device for measure thick goods cure time of rubber |
| CN106188698A (en) * | 2016-08-29 | 2016-12-07 | 樊之雄 | A kind of heat-resisting oil resistant rubber sealing ring and preparation method thereof |
| CN106378893A (en) * | 2016-08-31 | 2017-02-08 | 柳州元吉兴工业技术有限公司 | Rubber vulcanization process |
| CN106696115A (en) * | 2016-12-15 | 2017-05-24 | 陕西高华知本化工科技有限公司 | Preparation method for AES resin |
| CN106945091A (en) * | 2017-05-18 | 2017-07-14 | 山东盛润胶带有限公司 | Automatic cutting sheet devices are used in a kind of vulcanization of rubber experiment |
-
2017
- 2017-08-31 CN CN201710769201.1A patent/CN107599255A/en active Pending
Patent Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102199355A (en) * | 2011-04-23 | 2011-09-28 | 茂名市信翼化工有限公司 | Preparation method for room temperature vulcanized silicon rubber |
| CN102634046A (en) * | 2012-04-26 | 2012-08-15 | 邹德荣 | Vulcanization method for improving bonding quality of adhesive |
| CN102977471A (en) * | 2012-12-10 | 2013-03-20 | 无锡绿缘汽车零部件有限公司 | Low-emission and low-pollution EPDM (Ethylene-Propylene-Diene Monomer) rubber and preparation method thereof |
| CN103353520A (en) * | 2013-05-31 | 2013-10-16 | 南京群力运动器材有限公司 | Vulkameter operation technology |
| CN205538971U (en) * | 2015-12-25 | 2016-08-31 | 青岛科技大学 | Experimental device for measure thick goods cure time of rubber |
| CN106188698A (en) * | 2016-08-29 | 2016-12-07 | 樊之雄 | A kind of heat-resisting oil resistant rubber sealing ring and preparation method thereof |
| CN106378893A (en) * | 2016-08-31 | 2017-02-08 | 柳州元吉兴工业技术有限公司 | Rubber vulcanization process |
| CN106696115A (en) * | 2016-12-15 | 2017-05-24 | 陕西高华知本化工科技有限公司 | Preparation method for AES resin |
| CN106945091A (en) * | 2017-05-18 | 2017-07-14 | 山东盛润胶带有限公司 | Automatic cutting sheet devices are used in a kind of vulcanization of rubber experiment |
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| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20180119 |
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| RJ01 | Rejection of invention patent application after publication |