CN107595672B - Chromonic paste compositions and methods of making and using the same - Google Patents
Chromonic paste compositions and methods of making and using the same Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8152—Homopolymers or copolymers of esters, e.g. (meth)acrylic acid esters; Compositions of derivatives of such polymers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/25—Silicon; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/26—Aluminium; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/29—Titanium; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/87—Polyurethanes
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/06—Preparations for styling the hair, e.g. by temporary shaping or colouring
- A61Q5/065—Preparations for temporary colouring the hair, e.g. direct dyes
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Abstract
The invention relates to a color developing paste composition, a preparation method and a using method thereof. The color developing paste composition comprises water and the following raw material components in percentage by weight: 1-20% of pigment, 1-30% of film-forming agent and 0.1-6% of matrix; wherein the film forming agent is one or more of acrylic acid (ester) copolymer, polyurethane-14/acrylic acid (ester) copolymer AMP salt; the pigment is a cosmetic grade paint. The hair color cream composition can uniformly and completely cover the whole hair at 360 degrees, is convenient to remove, can be removed by only adopting a shampoo article containing a surfactant, restores the original hair color, can be conveniently colored, removed or replaced according to needs, realizes one-time temporary coloring, has a better coloring effect, has no strong shaping effect, and has a natural and smooth colored hair style.
Description
Technical Field
This invention relates to hair coloring products and, in particular, to a hair color paste composition that temporarily conceals the original color (e.g., covering white hair) in an amorphous, one-time process, and methods of making and using the same.
Background
Along with the improvement of living standard of people, the requirements of people on the aspect of exterior decoration are higher and higher, and more people dye hair to beautify the hair. There is also an increasing focus on health and care in product selection.
Permanent hair dyeing belongs to hair dyeing with chemical reaction, although the hair dyeing is safe, some people still have concerns about the hair dyeing, and the hair color can not be randomly replaced and washed off at any time when the permanent hair dyeing is used.
The existing disposable temporary hair dye, such as color hair mud and hair wax, belongs to the strong shaping class, has the characteristic of over-strong shaping effect, and the hair is generally hard after being used, can only coat the hair on the surface (can not be colored every time), can not meet the requirement of consumers pursuing hair smoothness, and is not suitable for longer hair. Additional disposable temporary hair dyes include dye sprays and solid or liquid stick types: dyeing spray contains the propellant, and is not environmental protection also not safe, has explosion hidden danger can not carry and to take vehicles such as aircraft, and dyeing coloring effect is poor and the safety difference, and it is also inconvenient to operate, and the operation carelessly makes face and neck dyeing easily, causes the awkwardness, and dyeing spray only has better effect to the hair top layer, can not color every hair, and simultaneously, to the operation of coloring in lower floor's hair or hair middle section not convenient, can't guarantee coloring and graceful of every hair. The solid or liquid stick type complementary dyeing product has the defects that the volume component is small, the large-area complementary dyeing product is not easy to be uniformly coated, only each new white hair is coated, the operation is inconvenient, the hair is difficult to cover at 360 ℃, a user needs to spend more time to carry out local complementary dyeing on a part (such as a white hair part) of each new hair, the time and the labor are wasted, the product is not suitable for longer hair, if the product is based on gel cream or gel water type setting products, the product has stronger setting function and cannot be smooth, if the capacity is increased, the full-head complementary dyeing product cannot carry out each dyeing, the full-head hair is changed into full-head hair plastic hardening, and if white powder (starch) is attached to the hair by forced loosening after the product is coated, the product is not practical.
Therefore, none of the above-mentioned disposable temporary hair dye products can color the entire or large area of hair or simultaneously apply various colors, and it is difficult to completely cover each hair, and the setting effect is strong, and it is impossible to maintain a smooth hairstyle.
Disclosure of Invention
Accordingly, there is a need for a hair color paste composition which is suitable for coloring all or a large area or simultaneously coloring a plurality of colors, can cover the entire hair, has an excellent effect of covering the original color (e.g., white hair), can maintain the natural and smooth hairstyle, and can conveniently remove the color by using a shampoo containing a surfactant as required to achieve a temporary one-time coloring effect.
The color developing paste composition comprises water and the following raw material components in percentage by weight:
1 to 20 percent of pigment
1 to 30 percent of film forming agent
0.1 to 6 percent of matrix; wherein the content of the first and second substances,
the film forming agent is one or more of acrylic acid (ester) copolymer, polyurethane-14/acrylic acid (ester) copolymer AMP salt;
the pigment is a cosmetic grade paint.
The pigment is a cosmetic-grade paint, namely a pigment with pigment, namely a substrate with pigment, which does not need to be oxidized to generate color development with hair through an oxidation chemical reaction, such as the substrate with pigment which can be used in cosmetics such as lipstick, nail polish, eye shadow and the like. Depending on the actual requirements, existing pigmented substrates, such as mica, aluminum powder, titanium dioxide, sodium calcium borosilicate, ferric oxide, tin oxide or other pigmented substrates, among others, can be combined to obtain the desired color.
In one embodiment, the color paste composition comprises water and the following raw material components in percentage by weight:
3 to 18 percent of pigment
5 to 25 percent of film forming agent
0.1 to 6 percent of matrix.
In one embodiment, the color paste composition comprises water and the following raw material components in percentage by weight:
5 to 15 percent of pigment
15 to 25 percent of film forming agent
0.1 to 6 percent of matrix.
In one embodiment, the film former is an acrylic copolymer.
In one embodiment, the matrix comprises at least one of an emulsifier, a thickener. It is understood that in other embodiments, other adjuvants that can assist in forming the paste may be used.
In one embodiment, the thickener is at least one of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, fatty alcohol emulsifying thickener, acrylic acid (ester)/steareth-20 methacrylate copolymer.
In one embodiment, the thickener is an acrylate/steareth-20 methacrylate copolymer.
In one embodiment, the emulsifier is a nonionic emulsifier.
In one embodiment, the emulsifier is at least one of oleyl polyether-5, polysorbate-20, ceteareth-6, rose-eth-4, oleic acid.
In one embodiment, the emulsifier is polysorbate-20.
In one embodiment, the fabric further comprises 0.2-5 wt% of a humectant.
In one embodiment, the humectant is at least one of 1, 3-butylene glycol, propylene glycol, and glycerin. Preferred are glycerol and propylene glycol.
In one embodiment, the functional paint also comprises 0.01-55 wt% of functional additives; the functional additive is at least one of cosolvent, plant extract, hair care nutrient, protein, sunscreen agent, antioxidant, pH regulator, metal chelating agent, antiseptic and essence.
In one embodiment, the functional additive comprises a pH adjuster and a cosolvent; the pH regulator is aminomethyl propanol, so as to regulate the pH of the system to 5.5-7.5; the cosolvent is ethanol.
Other functional additives may also be added to the hair color paste composition of the present invention as desired: if one or more of plant extract (such as tea extract), hair care nutrient and protein (such as hydrolyzed keratin) are added to obtain better hair care effect, the weight percentage is preferably 0.1-2%; adding sunscreen agent to provide sunscreen function, such as methoxy cinnamyl ethylhexyl ester and benzophenone-4, preferably 0.1-0.5% by weight; adding antioxidant to provide antioxidant and free radical preventing functions, such as butylated hydroxytoluene, preferably 0.1-0.5 wt%; adding a metal chelating agent to form a relatively stable chelate with metal ions, so that the chelate cannot catalyze oxidation reaction, such as EDTA disodium, and the weight percentage is preferably 0.05-0.1%; the preservative is added to provide a preservative function, such as methyl hydroxybenzoate and/or propyl hydroxybenzoate, and the weight percentage is preferably 0.01-0.3%.
In one embodiment, the color paste composition comprises water and the following raw material components in percentage by weight:
the film forming agent is acrylic acid (ester) copolymer;
the thickening agent is acrylic acid (ester)/stearyl alcohol polyether-20 methacrylate copolymer;
the emulsifier is polysorbate-20;
the humectant is glycerol and propylene glycol;
the functional additive comprises a pH regulator and a cosolvent, wherein the pH regulator is aminomethyl propanol, and the pH of a regulating system is 5.5-7.5; the cosolvent is ethanol.
The invention also provides a preparation method of the color developing paste composition, which comprises the following steps:
adding a proper amount of water into the pigment for dispersion to obtain dispersion liquid;
and adding the rest water, the matrix and the film forming agent into the dispersion, then adding or not adding the humectant or the humectant and the functional additive, and stirring to obtain the water-based dispersion.
The invention also provides a method of using the hair color paste composition, comprising the steps of:
(1) coating the hair color cream composition on hair, and combing;
(2) repeating or not repeating step (1) and covering each hair desired to be covered with the hair cream composition;
(3) combing until the hair is dry.
In one embodiment, in step (1), the amount of the color paste composition is 1-10 g.
In one embodiment, in the step (3), blowing by using artificial wind is performed simultaneously with the carding.
In one embodiment, in step (3), after the drying, the carding is performed in a direction consistent with the coating direction in step (1).
In one embodiment, in the step (1) and/or the step (3), the combing method is combing by using a hair dyeing comb;
the hair dyeing comb comprises a comb body and a comb handle, wherein the comb body is provided with a first tooth part used for cream feeding and initial dyeing, the first tooth part comprises a bottom plate and a plurality of rows of teeth, the plurality of rows of teeth are perpendicularly arranged on the bottom plate, the peripheral tooth height of the plurality of rows of teeth is larger than that of the inner teeth to form a groove, a second tooth part used for fine hair dyeing is further arranged on the back side of the first tooth part, the second tooth part is a single row of teeth, and the tooth space of the plurality of rows of teeth is larger than that of the single row of teeth.
In one embodiment, the carding method in the step (1) is as follows:
putting the hair color paste composition into the groove, combing and coating the hair color paste composition on hair; then combing by adopting the first tooth part, and combing by adopting the second tooth part;
the carding method in the step (3) comprises the following steps: and combing by adopting the second tooth part.
In one embodiment, the method of using the hair color paste composition comprises the steps of:
(1) taking 1-10 g of the hair color paste composition in the groove, and coating the hair color paste composition on hair; then combing by adopting the first tooth part, and combing by adopting the second tooth part;
(2) repeating or not repeating step (1) and covering each hair desired to be covered with the hair cream composition;
(3) and combing by adopting the second tooth part, and blowing by using artificial wind while combing.
The principle and advantages of the invention are as follows:
on the basis of reasonably controlling the raw materials and weight percentage of each component, the invention creatively adopts the cosmetic-grade coating as the pigment to be matched with the specific film-forming agent to prepare the hair color paste composition, wherein the cosmetic-grade coating is adopted as the pigment, and the coloring of the hair is realized by utilizing the color of the cosmetic-grade coating. Meanwhile, in order to ensure the covering effect of the pigment on the original color, at least one of acrylic acid (ester) copolymer and polyurethane-14/acrylic acid (ester) copolymer AMP salt is used as a film forming agent, the film forming agent can be well combined with the pigment, a uniform protective film can be formed during coloring, the pigment can uniformly and completely cover the whole hair at 360 degrees, the removal is convenient, and the protective film can be destroyed, the pigment can be removed, the original color can be restored by only adopting a shampoo containing a surfactant, so that the temporary one-time coloring effect is realized.
In addition, by adopting the film forming agent and reasonably controlling the weight ratio of the raw material components in the color developing paste composition, the strong setting effect can be avoided, so that the color developing paste composition can be suitable for coloring all over the hair or a large area, and the hair style after use is natural and elegant. The acrylic acid (ester) copolymer is preferably used as the film forming agent, so that the strong setting prevention and coloring effect are better. In addition, the acrylic acid (ester) copolymer can also ensure that the color paste composition has better waterproof effect, and when a user is in a hot or outdoor rainy environment, the pigment is not easy to fall off due to sweating or damp and rainy environment.
Compared with the prior art, the invention has the following beneficial effects:
the color developing paste composition disclosed by the invention adopts a cosmetic grade coating as a pigment to be matched with a specific type of film forming agent on the basis of reasonably controlling the raw materials and the weight percentages of the components: (1) the hair color restoring agent can be uniformly and completely applied to the whole head from small to large in 360 degrees, particularly can be applied to the whole head and covers the whole hair, is convenient to remove, can be removed by only adopting a shampoo article containing a surfactant, restores the original hair color, can be conveniently colored, removed or replaced according to needs, and really realizes one-time temporary coloring; (2) the hair can be colored locally, or can be colored on the whole head or a large area of hair, and can be colored with various colors simultaneously, and long or short hair can be used; (3) no strong setting effect exists, and the colored hairstyle is natural and smooth and is basically the same as that before the hair is not colored; (4) the cosmetic-grade paint is adopted as the pigment, the raw materials are safe, the cosmetic-grade paint can be used by consumers at ease, and the hair flakes on the surface layer of the hair are not opened like the traditional hair dye adopting the oxidation pigment, so that the damage of coloring to the hair is further reduced. Furthermore, a certain proportion of humectant is added, so that the hair can be moisturized and nursed while being colored, and the pH of the system can be controlled by adding specific functional additives, particularly a pH regulator and a cosolvent, and the dissolution and dispersion of the raw material components are promoted, so that a better coloring effect is obtained.
The preparation method of the color developing paste composition is simple to operate and convenient for practical production and application.
The application method of the color developing paste composition is simple, convenient and practical to operate, and a user can carry out DIY operation.
Furthermore, when combing and drying, the hair is dispersed by matching with artificial wind blowing, the hair can be combed and opened into every independently colored hair without being adhered together, so that the colored hair style is natural and comfortable, meanwhile, the drying time can be shortened, and the coloring efficiency is improved. Furthermore, the hair dyeing comb is matched with a specific hair dyeing comb for use, and the first tooth part and the second tooth part of the hair dyeing comb are combined for combing, so that a better coloring effect can be obtained, and the hair style obtained by combing can be further natural and smooth.
Drawings
FIG. 1 is a schematic structural view of a hair comb as set forth in example 21;
fig. 2 is a schematic structural view of a first tooth portion of the hair-dyeing comb shown in fig. 1.
Detailed Description
The inventive chromonic paste compositions, methods of making and methods of using the same are described in further detail in connection with specific examples below.
The film-forming agents adopted in the embodiment of the invention are acrylic acid (ester) copolymer, polyurethane-14/acrylic acid (ester) copolymer AMP salt; the thickening agent acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, fatty alcohol emulsifying thickening agent and acrylic acid (ester)/stearyl alcohol polyether-20 methacrylate copolymer are all commercial products. The above name is INCI Chinese name.
The pigments adopted in the embodiment of the invention are all cosmetic-grade coatings, wherein the pigments with the models of Earis4602, Earis3310, M6004, Earis7422, M4102 and SM3015 are purchased from Cambo chemical Co., Ltd; the pigment type T30D was obtained from BASF. Some of the parameters are shown in the following table:
examples 1 to 5
The five color developing paste compositions of this example comprise the following raw material components in percentage by weight:
the preparation method of the color developing paste composition comprises the following steps:
adding a proper amount of water into the pigment for dispersion to obtain dispersion liquid;
mixing the rest water, the emulsifier and the thickener, heating for emulsification, stirring and cooling to obtain an emulsion;
and adding the film forming agent and the dispersion into the emulsion, and stirring to obtain the emulsion.
Examples 6 to 11
The six color paste compositions described in this example comprise the following raw material components in percentage by weight:
the above-described chromonic paste compositions were prepared in the same manner as in examples 1-5.
Examples 12 to 15
The four color paste compositions of this example comprise, in weight percent, the following raw material components:
the preparation method of the color developing paste composition comprises the following steps:
adding a proper amount of water into the pigment for dispersion to obtain dispersion liquid;
mixing the rest water, the emulsifier and the thickener, heating for emulsification, stirring and cooling to obtain an emulsion;
and sequentially adding the film forming agent and the dispersion into the emulsion, then adding the humectant, and stirring to obtain the water-based emulsion.
Examples 16 to 19
The four color paste compositions described in this example comprise, in weight percent, the following raw material components:
the process for preparing the above-described hair color paste composition comprises the steps of:
adding a proper amount of water into the pigment for dispersion to obtain dispersion liquid;
mixing the rest water, the emulsifier and the thickener, heating for emulsification, stirring and cooling to obtain an emulsion;
and sequentially adding the film forming agent and the dispersion into the emulsion, then adding the humectant and the functional additive, and stirring to obtain the water-based emulsion.
Example 20
The color developing paste composition described in this embodiment includes, by weight, the following raw material components:
the above-described hair color paste compositions were prepared in a manner analogous to examples 16-19.
Example 21
This example is a method of using the hair color paste composition of any of examples 1-20, comprising the steps of:
(1) coating the hair color cream composition on hair, and combing;
(2) repeating or not repeating step (1) and covering each hair desired to be covered with the hair cream composition;
(3) combing until the hair is dry.
Specifically, in the step (1), the amount of the color development paste composition is 1-10 g. Proper control of the amount of each application provides for more uniform application of the color paste composition.
Specifically, in the step (3), the artificial wind is used for drying while carding. The hair drier is matched with wind blowing to disperse hair, so that the colored hair style can be natural and smooth, the drying time can be shortened, the coloring efficiency can be improved, and if the drying is further accelerated, the hair drier can be heated and dried by using hot air (the general temperature is not lower than 30 ℃) of the hair drier. After being dried, the hair can be combed to be opened into each independently colored hair without adhesion, and a natural and smooth effect is obtained.
Specifically, in the step (3), after the drying, carding is carried out in a direction consistent with the coating direction in the step (1). So as to disperse the hair and make the hair style natural and smooth.
Further, in the above using method, combing can be performed in combination with a specific hair comb to obtain a more excellent coloring effect and make the hairstyle more natural. The hair dyeing comb comprises a comb body and a comb handle 10, wherein the comb body is provided with a first tooth part 20 used for cream feeding and primary dyeing, the first tooth part 20 comprises a bottom plate 22 and a plurality of rows of teeth 21, the plurality of rows of teeth 21 are vertically arranged on the bottom plate 22, the height of the peripheral teeth of the plurality of rows of teeth 21 is larger than that of the internal teeth to form a groove 221, a second tooth part 30 used for fine hair dyeing is further arranged on the back side of the first tooth part 20, the second tooth part 30 is a single row of teeth 31, and the tooth space of the plurality of rows of teeth 21 is larger than that of the single row of teeth 31. In the present embodiment, the first tooth portion 20 further includes temple teeth 23 for coloring the temple hair.
Specifically, when the hair is colored in a long hair, a full hair, a large area or a small area, the steps of the using method are as follows:
(1) taking 1-10 g of the hair color paste composition, placing the hair color paste composition on inner teeth of a plurality of rows of teeth 21, namely grooves 21, and coating the hair color paste composition on hair; then, combing 3-5 times in the same direction by adopting the first tooth part 20, combing 3-5 times in the same direction by adopting the second tooth part 30, and combing 3-5 times in different directions;
(2) when coloring hair with small area (such as temple and short hair), coating and combing once according to the step (1); when the hair is colored for longer hair or large area to the whole hair, the step (1) can be repeated for a plurality of times according to the requirement, the coloring condition of the hair is observed, and each hair required to be covered is covered by the hair cream composition;
(3) while waiting for the hair color paste composition to dry, repeatedly combing the hair to which the hair color paste composition has been applied with the second teeth 30 and blowing with artificial wind while combing until completely dry; then, the second teeth 30 are used to comb the hairs 1-2 times in the same direction as the direction of applying the hair cream composition in step (1) until each hair is combed open, and each independently colored hair is not stuck together, so that a natural and smooth effect can be obtained.
When multiple colors are simultaneously used, the steps of the using method are as follows:
(1) taking 1-10 g of the color developing cream composition to be placed on inner teeth of a plurality of rows of teeth 21, namely grooves 21, picking out hair strands to be colored, and coating the color developing cream composition on the hair strands by using the plurality of rows of teeth 21; then, combing 3-5 times in the same direction by adopting the first tooth part 20, combing 3-5 times in the same direction by adopting the second tooth part 30, and combing 3-5 times in different directions;
(2) repeating or not repeating step (1) and covering each hair of the bundle with the hair cream composition;
(3) while waiting for the hair color paste composition to dry, repeatedly combing the tress of hair to which the hair color paste composition has been applied with the second teeth 30 and blowing with artificial wind while combing until completely dry; then combing the hair bundle for 1-2 times along the direction consistent with the coating direction in the step (1) by using the second tooth part 30 until each hair in the hair bundle is combed open, and each independently colored hair is not adhered together, so that a natural and smooth effect can be obtained;
(4) and (4) selecting hair strands with other colors, and repeating the steps (1) to (3) until the selected hair cream compositions with various colors are finished.
After the coloring is finished by the using method, when a user needs to replace the color or reduce the original color (such as several hours or several days after coloring), the user can wash the hair with the shampoo containing the conventional surfactant for 1-2 times according to the conventional hair washing method, and then the hair cream composition can be removed.
Comparative example 1
This comparative example is a hair color paste composition having similar raw material components and preparation method as example 1, except that: the adopted film-forming agent is VP/VA copolymer.
Effect testing on the hair color paste compositions of examples and comparative examples:
the test method comprises the following steps: selecting 20 trained testers (all of which are full-length hair in shoulder) for trial, and coloring the whole heads according to the trial method in the embodiment 21; each of the test subjects tried the hair color cream compositions described in examples 1 to 20 and comparative examples 1 to 2 and scored, and the results were averaged over the scores of 20 test subjects.
Degree of comfort: 1-10 minutes; 1 minute-strong shaping effect, not smooth and comfortable; 10 minutes-almost amorphous effect, very smooth;
coloring effect: 1-10 minutes; 1 min-poor, difficult to color; 10 min-good, uniform coloring;
the unloading effect is as follows: 1-10 minutes; 1 minute, namely shampoo containing the surfactant is used for cleaning, and almost no falling off exists; and 10 minutes, namely the shampoo containing the surfactant is used for cleaning for 1 time and can be easily removed.
The test results are shown in the following table.
The technical features of the embodiments described above may be arbitrarily combined, and for the sake of brevity, all possible combinations of the technical features in the embodiments described above are not described, but should be considered as being within the scope of the present specification as long as there is no contradiction between the combinations of the technical features.
The above-mentioned embodiments only express several embodiments of the present invention, and the description thereof is more specific and detailed, but not construed as limiting the scope of the invention. It should be noted that, for a person skilled in the art, several variations and modifications can be made without departing from the inventive concept, which falls within the scope of the present invention. Therefore, the protection scope of the present patent shall be subject to the appended claims.
Claims (21)
1. The color developing paste composition is characterized by comprising water and the following raw material components in percentage by weight:
1 to 20 percent of pigment
1 to 30 percent of film forming agent
0.1 to 6 percent of matrix; wherein the content of the first and second substances,
the film forming agent is at least one of acrylic acid (ester) copolymer and polyurethane-14/acrylic acid (ester) copolymer AMP salt;
the pigment is a cosmetic grade paint;
the matrix comprises an emulsifier and a thickener;
wherein the thickening agent is acrylic acid (ester)/steareth-20 methacrylate copolymer;
the emulsifier is polysorbate-20.
2. The hair color paste composition according to claim 1, comprising water, and the following raw material components in percentage by weight:
3 to 18 percent of pigment
5 to 25 percent of film forming agent
0.1 to 6 percent of matrix.
3. The hair color paste composition according to claim 2, comprising water, and the following raw material components in percentage by weight:
5 to 15 percent of pigment
15 to 25 percent of film forming agent
0.1 to 6 percent of matrix.
4. The hair color paste composition of claim 1, wherein the film forming agent is an acrylic copolymer.
5. The hair color paste composition of claim 1, further comprising 0.2 to 5 weight percent of a humectant.
6. The hair color paste composition of claim 5, wherein the humectant is at least one of 1, 3-butylene glycol, propylene glycol, glycerin.
7. The hair color paste composition of claim 6, wherein the humectant is glycerin and propylene glycol.
8. The hair color paste composition according to any one of claims 1 to 7, further comprising 0.01 to 55% by weight of a functional additive; the functional additive is at least one of cosolvent, plant extract, hair care nutrient, protein, sunscreen agent, antioxidant, pH regulator, metal chelating agent, antiseptic and essence.
9. The hair color paste composition of claim 8, wherein the plant extract is a tea extract; the protein is hydrolyzed keratin.
10. The hair color paste composition of claim 8, wherein the sunscreen agent is methoxycinnamyl ethylhexyl benzoate, benzophenone-4.
11. The hair color paste composition of claim 8, wherein the antioxidant is butylated hydroxytoluene.
12. The hair color paste composition of claim 8, wherein the metal chelating agent is disodium EDTA.
13. The hair color paste composition of claim 8, wherein the functional additive comprises a pH adjuster and a co-solvent; the pH regulator is aminomethyl propanol; the cosolvent is ethanol.
14. The hair color paste composition according to claim 13, comprising water, and the following raw material components in percentage by weight:
the film forming agent is acrylic acid (ester) copolymer;
the thickening agent is acrylic acid (ester)/stearyl alcohol polyether-20 methacrylate copolymer;
the emulsifier is polysorbate-20;
the humectant is glycerol and propylene glycol;
the functional additive comprises a pH regulator and a cosolvent, wherein the pH regulator is aminomethyl propanol, and the pH of a regulating system is 5.5-7.5; the cosolvent is ethanol.
15. A method of making the chromonic paste composition of any of claims 1-14, comprising the steps of:
adding a proper amount of water into the pigment for dispersion to obtain dispersion liquid;
and adding the rest water, the matrix and the film forming agent into the dispersion, then adding or not adding the humectant or the humectant and the functional additive, and stirring to obtain the water-based dispersion.
16. A method of using the hair color paste composition of any of claims 1-14, comprising the steps of:
(1) coating the hair color cream composition on hair, and combing;
(2) repeating or not repeating step (1) and covering each hair desired to be covered with the hair cream composition;
(3) combing until the hair is dry.
17. The method of using the hair color paste composition according to claim 16, wherein in step (3), the hair is blown dry with an artificial air while combing.
18. The method of using the hair color paste composition according to claim 17, wherein in step (3), after said drying, carding is performed in a direction that coincides with the direction of said coating in step (1).
19. The method of using the hair color paste composition according to any of claims 16-18, wherein in step (1) and/or step (3), the combing is performed with a hair dye comb;
the hair dyeing comb comprises a comb body and a comb handle, wherein the comb body is provided with a first tooth part used for cream feeding and initial dyeing, the first tooth part comprises a bottom plate and a plurality of rows of teeth, the plurality of rows of teeth are perpendicularly arranged on the bottom plate, the peripheral tooth height of the plurality of rows of teeth is larger than that of the inner teeth to form a groove, a second tooth part used for fine hair dyeing is further arranged on the back side of the first tooth part, the second tooth part is a single row of teeth, and the tooth space of the plurality of rows of teeth is larger than that of the single row of teeth.
20. The method of using the hair color paste composition of claim 19, wherein the combing in step (1) is by:
putting the hair color paste composition into the groove, combing and coating the hair color paste composition on hair; then combing by adopting the first tooth part, and combing by adopting the second tooth part;
the carding method in the step (3) comprises the following steps: and combing by adopting the second tooth part.
21. The method of using the hair color paste composition of claim 19, comprising the steps of:
(1) taking 1-10 g of the hair color paste composition in the groove, and coating the hair color paste composition on hair; then combing by adopting the first tooth part, and combing by adopting the second tooth part;
(2) repeating or not repeating step (1) and covering each hair desired to be covered with the hair cream composition;
(3) and combing by adopting the second tooth part, and blowing by using artificial wind while combing.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PCT/CN2017/103416 WO2018133442A1 (en) | 2017-01-22 | 2017-09-26 | Hair dye cream composition and preparation and use methods thereof |
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| CN201710047556 | 2017-01-22 | ||
| CN201710047556X | 2017-01-22 | ||
| CN201710538397 | 2017-07-04 | ||
| CN2017105383973 | 2017-07-04 |
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| CN107595672A CN107595672A (en) | 2018-01-19 |
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| CN201710822488.XA Active CN107595672B (en) | 2017-01-22 | 2017-09-13 | Chromonic paste compositions and methods of making and using the same |
| CN201710822487.5A Pending CN107496199A (en) | 2017-01-22 | 2017-09-13 | Color development elastin composition and preparation method thereof and application method |
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| CN108096065A (en) * | 2017-12-25 | 2018-06-01 | 广州温雅日用化妆品有限公司 | Foam type color development hair wax composition and preparation method thereof and application method |
| CN108379125B (en) * | 2018-04-19 | 2021-07-09 | 中原工学院 | Environment-friendly nail polish with repairability and preparation method thereof |
| CN108514525A (en) * | 2018-04-20 | 2018-09-11 | 安徽大学 | A kind of disposable colored hair care dying gel and preparation method thereof |
| CN109602628A (en) * | 2018-12-25 | 2019-04-12 | 钟卫敏 | A kind of hair dyeing rear complementary color color protection shampoo and preparation method thereof |
| CN111012681B (en) * | 2019-12-31 | 2022-12-02 | 娇时日化（杭州）股份有限公司 | Hair dyeing spray, preparation method and application method thereof |
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- 2017-09-26 WO PCT/CN2017/103415 patent/WO2018133441A1/en active Application Filing
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Also Published As
| Publication number | Publication date |
|---|---|
| CN107595672A (en) | 2018-01-19 |
| WO2018133442A1 (en) | 2018-07-26 |
| CN107496199A (en) | 2017-12-22 |
| WO2018133441A1 (en) | 2018-07-26 |
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