CN107573650A - A kind of preparation method of polyester filling mattress - Google Patents
A kind of preparation method of polyester filling mattress Download PDFInfo
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- CN107573650A CN107573650A CN201710774914.7A CN201710774914A CN107573650A CN 107573650 A CN107573650 A CN 107573650A CN 201710774914 A CN201710774914 A CN 201710774914A CN 107573650 A CN107573650 A CN 107573650A
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Abstract
This application discloses a kind of preparation method of polyester filling mattress, polyester, triethylenediamine, dibutyl tin laurate, organic tin stabilizer, distilled water, AC foaming agents, glycerine, dimethyl cyclohexyl amine, EP rubbers, dioctyl phthalate, talcum powder, citric acid, benzophenone, absolute ethyl alcohol and tricresyl phosphate are weighed；Relative density is low, the 320kPa of compressive strength 260；From fiery self-extinguishment, product is soft, is not easy collapse-deformation, support performance is high, and heat-resist, 120 DEG C of 24h of constant temperature 12 are indeformable in baking oven；Water absorption rate is low, and 7 days water absorption rates of soak at room temperature are 0.01 0.1kg/m3, antibacterial and mouldproof, it is not easy to damage by worms, percent opening is high；Elongation 440 500%, the 360MPa of tensile strength 330, the 320MPa of adhesion strength 280.
Description
Technical field
The application belongs to mattress material field, more particularly to a kind of preparation method of polyester filling mattress.
Background technology
Mattress be in order to ensure consumer secure good health and comfortably sleep and use it is a kind of between human body and bed it
Between article, mattress material is various, different materials make mattress can give people to bring different sleeper effects.
1881, one, Texas, USA Houston countryside small town, a ginning machine for being named as Daniel Haynes
Craftsman has started a kind of production of tampon mattress.
1900, beautiful simons this, bagged-spring bed mattress, earlier 1900s, Dan Luofu, rubber pange cushion, 1932,
Italy, Malian Georg Aberg are recorded, and are used for mat with polyurethane foam, during World War II, German, Louis
Koala Buddhist nun, a kind of oval mattress is have also been devised, and the body pressure of different parts on mattress is lain in by human body, be divided into soft, medium, hard
Three parts, skeleton is set to keep optimum state, foreign countries have also appeared a kind of " actively responding spring system ", change in the past
Usual spring structural form, make one more comfortable, elasticity is sustained；Some sping mattresses are soft also with polyester foamed combination
Hardness can select with people.
Modern commonly use, the performance preferably mattress of sping mattress category, its bedding core are made up of spring.It is elastic good that this is lined with, and holds
Support property preferably, gas permeability it is stronger, durable etc. excellent.
Sping mattress point.The present age is thin with the entrance of advanced foreign technology and the extensive application of patent, sping mattress
It is divided into many classifications, such as independent bag bed net, five area's patent bed nets, spring adds latex system etc. etc., is greatly enriched
The selection of people.
Except working, live, body, psychology etc. the reason in addition to, possess the health of " hygienic, comfortable, attractive in appearance, durable "
Bedding is the key point for obtaining high quality sleep.
With the continuous progress of material progress and technical matters, the mattress species that modern people use gradually tends to polynary
Change, mainly have：Sping mattress, palm mattress, latex bed mattress, water bed mattress, pneumatic mattress, magnetic mattress etc., in these mattresses, spring
Mattress accounts for larger proportion.
Soft durometer requirement to mattress, Chinese and western consumer have very big difference, and Chinese Consumer's tend to harder mattress,
Western customers then prefer soft mattress.Science proves, mattress pad can reduce spine support, and the comfort level of hard mattress is again not
Reach, so excessively all unfavorable to healthy sleep as hard as soft mattress.The soft durometer of mattress directly affects the quality of sleep, and partially hard
Plank mattress is compared with partially soft sponge bed, and neither too hard, nor too soft sping mattress is more beneficial for obtaining good sleep.
Flexible mattress is most important to the level of comfort and sleep quality of human body.Sping mattress is to body-support power
Distribution rationally can play sufficient supporting role than more uniform, and can ensures rational backbone physiological bending degree；Use bullet
The sleep of spring mattress is more stable, improves total Sleep efficiency, physical comfort and the state of mind are preferable after wakeing up.Use sping mattress
It can obtain than using plank or the higher-quality sleep of sponge matress.
The content of the invention
The technical problem of solution：
The application is directed to above-mentioned technical problem, there is provided a kind of preparation method of polyester filling mattress, solves existing polyester packed bed
Pad quality is hard, robustness is poor, easy collapse-deformation, support poor performance, maintenance are bad easily damages by worms or the technical problem such as mouldy.
Technical scheme：
A kind of preparation method of polyester filling mattress, comprises the following steps：
The first step：100 parts of polyester, triethylenediamine 0.3-0.7 parts, di lauric dibutyl are weighed according to parts by weight proportioning
Tin 1-5 parts, organic tin stabilizer 0.45-0.85 parts, distilled water 6-10 parts, AC foaming agent 0.5-4.5 parts, glycerine 1.1-1.5 parts,
Dimethyl cyclohexyl amine 1-5 parts, EP rubbers 23-27 parts, dioctyl phthalate 2-6 parts, talcum powder 1.2-1.6 parts, lemon
Sour 0.1-0.5 parts, benzophenone 0.2-0.6 parts, absolute ethyl alcohol 5-25 parts and tricresyl phosphate 3-7 parts；
Second step：Polyester, triethylenediamine, dibutyl tin laurate and organic tin stabilizer are put into reactor,
Temperature is 80-100 DEG C, and rotating speed is under 2700-2900r/min speed, stirs 4-8s, adds distilled water, AC foaming agents, glycerine
And dimethyl cyclohexyl amine, 100-120 DEG C is warming up to, 15-25s is stirred, adds EP rubbers, dioctyl phthalate and cunning
Stone flour, 140-150 DEG C is warming up to, mixes 1-3min；
3rd step：Surplus stock is added, 180-200 DEG C is warming up to, regulation mixing speed to 4000-6000 r/min, mixes 3-
5min, finally well mixed product is fitted into mould, nitrogen 0.25mol/kg is poured, is warming up to 200-280 DEG C, pressure control
0.6-1MPa is made, 6-15min is heated, is produced after cooling.
As a preferred technical solution of the present invention：The raw materials by weight portion of polyester filling mattress in the first step
Proportioning is as follows：100 parts of polyester, 0.3 part of triethylenediamine, 1 part of dibutyl tin laurate, 0.45 part of organic tin stabilizer,
6 parts of distilled water, 0.5 part of AC foaming agents, 1.1 parts of glycerine, 1 part of dimethyl cyclohexyl amine, 23 parts of EP rubbers, phthalic acid two are pungent
3 parts of 2 parts of ester, 1.2 parts of talcum powder, 0.1 part of citric acid, 0.2 part of benzophenone, 5 parts of absolute ethyl alcohol and tricresyl phosphate.
As a preferred technical solution of the present invention：The raw materials by weight portion of polyester filling mattress in the first step
Proportioning is as follows：100 parts of polyester, 0.7 part of triethylenediamine, 5 parts of dibutyl tin laurate, 0.85 part of organic tin stabilizer,
10 parts of distilled water, 4.5 parts of AC foaming agents, 1.5 parts of glycerine, 5 parts of dimethyl cyclohexyl amine, 27 parts of EP rubbers, phthalic acid two
7 parts of 6 parts of monooctyl ester, 1.6 parts of talcum powder, 0.5 part of citric acid, 0.6 part of benzophenone, 25 parts of absolute ethyl alcohol and tricresyl phosphate.
As a preferred technical solution of the present invention：The raw materials by weight portion of polyester filling mattress in the first step
Proportioning is as follows：100 parts of polyester, 0.3 part of triethylenediamine, 1 part of dibutyl tin laurate, 0.85 part of organic tin stabilizer,
10 parts of distilled water, 0.5 part of AC foaming agents, 1.5 parts of glycerine, 5 parts of dimethyl cyclohexyl amine, 23 parts of EP rubbers, phthalic acid two
3 parts of 6 parts of monooctyl ester, 1.2 parts of talcum powder, 0.5 part of citric acid, 0.6 part of benzophenone, 5 parts of absolute ethyl alcohol and tricresyl phosphate.
As a preferred technical solution of the present invention：The raw materials by weight portion of polyester filling mattress in the first step
Proportioning is as follows：100 parts of polyester, 0.5 part of triethylenediamine, 3 parts of dibutyl tin laurate, 0.65 part of organic tin stabilizer,
8 parts of distilled water, 2.5 parts of AC foaming agents, 1.3 parts of glycerine, 3 parts of dimethyl cyclohexyl amine, 25 parts of EP rubbers, phthalic acid two are pungent
5 parts of 4 parts of ester, 1.4 parts of talcum powder, 0.3 part of citric acid, 0.4 part of benzophenone, 15 parts of absolute ethyl alcohol and tricresyl phosphate.
Beneficial effect：
A kind of preparation method of polyester filling mattress of the present invention using above technical scheme compared with prior art, have with
Lower technique effect：1st, relative density is low, and preparation method is simple, and cost is cheap, workable, compressive strength 260-320kPa；
2nd, from fiery self-extinguishment, product is soft, and robustness is high, is not easy collapse-deformation, support performance is high, heat-resist, 120 DEG C of perseverances in baking oven
Warm 12-24h is indeformable；3rd, water absorption rate is low, and 7 days water absorption rates of soak at room temperature are 0.01-0.1kg/m3, antibacterial and mouldproof, process stabilizing
Property good, service life length, be not easy to damage by worms, percent opening is high；4th, elongation 440-500%, tensile strength 330-360MPa, bond strong
280-320MPa is spent, raw material sources are extensive, can extensively produce and constantly replace current material.
Embodiment
Embodiment 1:
100 parts of polyester, 0.3 part of triethylenediamine, 1 part of dibutyl tin laurate, organic is weighed according to parts by weight proportioning
0.45 part of tin stabilizer, 6 parts of distilled water, 0.5 part of AC foaming agents, 1.1 parts of glycerine, 1 part of dimethyl cyclohexyl amine, EP rubbers 23
Part, 2 parts of dioctyl phthalate, 1.2 parts of talcum powder, 0.1 part of citric acid, 0.2 part of benzophenone, 5 parts of absolute ethyl alcohol and phosphorus
Sour 3 parts of front three phenolic ester.
Polyester, triethylenediamine, dibutyl tin laurate and organic tin stabilizer are put into reactor, in temperature
For 80 DEG C, rotating speed is under 2700r/min speed, stirs 4s, adds distilled water, AC foaming agents, glycerine and dimethyl cyclohexyl amine,
100 DEG C are warming up to, 15s is stirred, adds EP rubbers, dioctyl phthalate and talcum powder, is warming up to 140 DEG C, mixing
1min。
Surplus stock is added, 180 DEG C is warming up to, regulation mixing speed to 4000r/min, mixes 3min, finally will mixing
Uniform product is fitted into mould, pours nitrogen 0.25mol/kg, is warming up to 200 DEG C, Stress control to 0.6MPa, heats 6-
15min, produced after cooling.
Relative density is low, and preparation method is simple, and cost is cheap, workable, compressive strength 260kPa；From fiery self-extinguishment,
Product is soft, and robustness is high, is not easy collapse-deformation, support performance is high, and heat-resist, 120 DEG C of constant temperature 12h are constant in baking oven
Shape；Water absorption rate is low, and 7 days water absorption rates of soak at room temperature are 0.1kg/m3, antibacterial and mouldproof, technology stability is good, service life length, is not easy
Damage by worms, percent opening is high；Elongation 440%, tensile strength 330MPa, adhesion strength 280MPa, raw material sources are extensive, can be extensive
Produce and constantly replace current material.
Embodiment 2:
100 parts of polyester, 0.7 part of triethylenediamine, 5 parts of dibutyl tin laurate, organic is weighed according to parts by weight proportioning
0.85 part of tin stabilizer, 10 parts of distilled water, 4.5 parts of AC foaming agents, 1.5 parts of glycerine, 5 parts of dimethyl cyclohexyl amine, EP rubbers 27
Part, 6 parts of dioctyl phthalate, 1.6 parts of talcum powder, 0.5 part of citric acid, 0.6 part of benzophenone, 25 parts of absolute ethyl alcohol and phosphorus
Sour 7 parts of front three phenolic ester.
Polyester, triethylenediamine, dibutyl tin laurate and organic tin stabilizer are put into reactor, in temperature
For 80-100 DEG C, rotating speed is under 2700-2900r/min speed, stirs 4-8s, adds distilled water, AC foaming agents, glycerine and two
Methyl cyclohexylamine, 100-120 DEG C is warming up to, stirs 15-25s, add EP rubbers, dioctyl phthalate and talcum
Powder, 140-150 DEG C is warming up to, mixes 1-3min.
Surplus stock is added, 180-200 DEG C is warming up to, regulation mixing speed to 4000-6000 r/min, mixes 3-
5min, finally well mixed product is fitted into mould, nitrogen 0.25mol/kg is poured, is warming up to 200-280 DEG C, pressure control
0.6-1MPa is made, 6-15min is heated, is produced after cooling.
Relative density is low, and preparation method is simple, and cost is cheap, workable, compressive strength 260-320kPa；From fire certainly
Put out, product is soft, and robustness is high, is not easy collapse-deformation, support performance is high, heat-resist, 120 DEG C of constant temperature 12-24h in baking oven
It is indeformable；Water absorption rate is low, and 7 days water absorption rates of soak at room temperature are 0.01-0.1kg/m3, antibacterial and mouldproof, technology stability is good, uses the longevity
Life length, is not easy to damage by worms, and percent opening is high；Elongation 440-500%, tensile strength 330-360MPa, adhesion strength 280-320MPa,
Raw material sources are extensive, can extensively produce and constantly replace current material.
Embodiment 3:
100 parts of polyester, 0.3 part of triethylenediamine, 1 part of dibutyl tin laurate, organic is weighed according to parts by weight proportioning
0.85 part of tin stabilizer, 10 parts of distilled water, 0.5 part of AC foaming agents, 1.5 parts of glycerine, 5 parts of dimethyl cyclohexyl amine, EP rubbers 23
Part, 6 parts of dioctyl phthalate, 1.2 parts of talcum powder, 0.5 part of citric acid, 0.6 part of benzophenone, 5 parts of absolute ethyl alcohol and phosphorus
Sour 3 parts of front three phenolic ester.
Polyester, triethylenediamine, dibutyl tin laurate and organic tin stabilizer are put into reactor, in temperature
For 80-100 DEG C, rotating speed is under 2700-2900r/min speed, stirs 4-8s, adds distilled water, AC foaming agents, glycerine and two
Methyl cyclohexylamine, 100-120 DEG C is warming up to, stirs 15-25s, add EP rubbers, dioctyl phthalate and talcum
Powder, 140-150 DEG C is warming up to, mixes 1-3min.
Surplus stock is added, 180-200 DEG C is warming up to, regulation mixing speed to 4000-6000 r/min, mixes 3-
5min, finally well mixed product is fitted into mould, nitrogen 0.25mol/kg is poured, is warming up to 200-280 DEG C, pressure control
0.6-1MPa is made, 6-15min is heated, is produced after cooling.
Relative density is low, and preparation method is simple, and cost is cheap, workable, compressive strength 260-320kPa；From fire certainly
Put out, product is soft, and robustness is high, is not easy collapse-deformation, support performance is high, heat-resist, 120 DEG C of constant temperature 12-24h in baking oven
It is indeformable；Water absorption rate is low, and 7 days water absorption rates of soak at room temperature are 0.01-0.1kg/m3, antibacterial and mouldproof, technology stability is good, uses the longevity
Life length, is not easy to damage by worms, and percent opening is high；Elongation 440-500%, tensile strength 330-360MPa, adhesion strength 280-320MPa,
Raw material sources are extensive, can extensively produce and constantly replace current material.
Embodiment 4:
100 parts of polyester, 0.5 part of triethylenediamine, 3 parts of dibutyl tin laurate, organic is weighed according to parts by weight proportioning
0.65 part of tin stabilizer, 8 parts of distilled water, 2.5 parts of AC foaming agents, 1.3 parts of glycerine, 3 parts of dimethyl cyclohexyl amine, EP rubbers 25
Part, 4 parts of dioctyl phthalate, 1.4 parts of talcum powder, 0.3 part of citric acid, 0.4 part of benzophenone, 15 parts of absolute ethyl alcohol and phosphorus
Sour 5 parts of front three phenolic ester.
Polyester, triethylenediamine, dibutyl tin laurate and organic tin stabilizer are put into reactor, in temperature
For 100 DEG C, rotating speed is under 2900r/min speed, stirs 8s, adds distilled water, AC foaming agents, glycerine and dimethyleyelohexane
Amine, 120 DEG C are warming up to, stir 25s, add EP rubbers, dioctyl phthalate and talcum powder, be warming up to 150 DEG C, mixed
Close 3min.
Surplus stock is added, 200 DEG C is warming up to, regulation mixing speed to 6000 r/min, mixes 5min, finally will mixing
Uniform product is fitted into mould, pours nitrogen 0.25mol/kg, is warming up to 280 DEG C, Stress control to 1MPa, heats 15min,
Produced after cooling.
Relative density is low, and preparation method is simple, and cost is cheap, workable, compressive strength 320kPa；From fiery self-extinguishment,
Product is soft, and robustness is high, is not easy collapse-deformation, support performance is high, and heat-resist, 120 DEG C of constant temperature 24h are constant in baking oven
Shape；Water absorption rate is low, and 7 days water absorption rates of soak at room temperature are 0.01kg/m3, antibacterial and mouldproof, technology stability is good, service life length, no
Easily damage by worms, percent opening is high；Elongation 500%, tensile strength 360MPa, adhesion strength 320MPa, raw material sources are extensive, Ke Yiguang
It is general to produce and constantly replace current material.
Composition all components in above example can be with commercially available.
The above embodiments are intended to illustrate the present invention, rather than limitation, therefore with the present invention's
Any change in claims suitable implication and scope, all it is considered as being included within the scope of the claims.
Claims (5)
1. a kind of preparation method of polyester filling mattress, it is characterised in that comprise the following steps：
The first step：100 parts of polyester, triethylenediamine 0.3-0.7 parts, di lauric dibutyl are weighed according to parts by weight proportioning
Tin 1-5 parts, organic tin stabilizer 0.45-0.85 parts, distilled water 6-10 parts, AC foaming agent 0.5-4.5 parts, glycerine 1.1-1.5 parts,
Dimethyl cyclohexyl amine 1-5 parts, EP rubbers 23-27 parts, dioctyl phthalate 2-6 parts, talcum powder 1.2-1.6 parts, lemon
Sour 0.1-0.5 parts, benzophenone 0.2-0.6 parts, absolute ethyl alcohol 5-25 parts and tricresyl phosphate 3-7 parts；
Second step：Polyester, triethylenediamine, dibutyl tin laurate and organic tin stabilizer are put into reactor,
Temperature is 80-100 DEG C, and rotating speed is under 2700-2900r/min speed, stirs 4-8s, adds distilled water, AC foaming agents, glycerine
And dimethyl cyclohexyl amine, 100-120 DEG C is warming up to, 15-25s is stirred, adds EP rubbers, dioctyl phthalate and cunning
Stone flour, 140-150 DEG C is warming up to, mixes 1-3min；
3rd step：Surplus stock is added, 180-200 DEG C is warming up to, regulation mixing speed to 4000-6000 r/min, mixes 3-
5min, finally well mixed product is fitted into mould, nitrogen 0.25mol/kg is poured, is warming up to 200-280 DEG C, pressure control
0.6-1MPa is made, 6-15min is heated, is produced after cooling.
A kind of 2. preparation method of polyester filling mattress according to claim 1, it is characterised in that：Gather in the first step
The raw materials by weight portion proportioning of ester filling mattress is as follows：100 parts of polyester, 0.3 part of triethylenediamine, di lauric dibutyl
1 part of tin, 0.45 part of organic tin stabilizer, 6 parts of distilled water, 0.5 part of AC foaming agents, 1.1 parts of glycerine, 1 part of dimethyl cyclohexyl amine, second
Third 23 parts of rubber, 2 parts of dioctyl phthalate, 1.2 parts of talcum powder, 0.1 part of citric acid, 0.2 part of benzophenone, absolute ethyl alcohol
5 parts and 3 parts of tricresyl phosphate.
A kind of 3. preparation method of polyester filling mattress according to claim 1, it is characterised in that：Gather in the first step
The raw materials by weight portion proportioning of ester filling mattress is as follows：100 parts of polyester, 0.7 part of triethylenediamine, di lauric dibutyl
5 parts of tin, 0.85 part of organic tin stabilizer, 10 parts of distilled water, 4.5 parts of AC foaming agents, 1.5 parts of glycerine, 5 parts of dimethyl cyclohexyl amine,
27 parts of EP rubbers, 6 parts of dioctyl phthalate, 1.6 parts of talcum powder, 0.5 part of citric acid, 0.6 part of benzophenone, anhydrous second
7 parts of 25 parts of alcohol and tricresyl phosphate.
A kind of 4. preparation method of polyester filling mattress according to claim 1, it is characterised in that：Gather in the first step
The raw materials by weight portion proportioning of ester filling mattress is as follows：100 parts of polyester, 0.3 part of triethylenediamine, di lauric dibutyl
1 part of tin, 0.85 part of organic tin stabilizer, 10 parts of distilled water, 0.5 part of AC foaming agents, 1.5 parts of glycerine, 5 parts of dimethyl cyclohexyl amine,
23 parts of EP rubbers, 6 parts of dioctyl phthalate, 1.2 parts of talcum powder, 0.5 part of citric acid, 0.6 part of benzophenone, anhydrous second
3 parts of 5 parts of alcohol and tricresyl phosphate.
A kind of 5. preparation method of polyester filling mattress according to claim 1, it is characterised in that：Gather in the first step
The raw materials by weight portion proportioning of ester filling mattress is as follows：100 parts of polyester, 0.5 part of triethylenediamine, di lauric dibutyl
3 parts of tin, 0.65 part of organic tin stabilizer, 8 parts of distilled water, 2.5 parts of AC foaming agents, 1.3 parts of glycerine, 3 parts of dimethyl cyclohexyl amine, second
Third 25 parts of rubber, 4 parts of dioctyl phthalate, 1.4 parts of talcum powder, 0.3 part of citric acid, 0.4 part of benzophenone, absolute ethyl alcohol
15 parts and 5 parts of tricresyl phosphate.
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| CN201710774914.7A CN107573650A (en) | 2017-08-31 | 2017-08-31 | A kind of preparation method of polyester filling mattress |
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| CN201710774914.7A CN107573650A (en) | 2017-08-31 | 2017-08-31 | A kind of preparation method of polyester filling mattress |
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Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101469076A (en) * | 2007-12-29 | 2009-07-01 | 黄仕颖 | Method for manufacturing special foam material |
| CN101535405A (en) * | 2006-12-22 | 2009-09-16 | 尤尼吉可株式会社 | Biodegradable polyester resin composition, and molded body, foamed body and molded container obtained from the biodegradable polyester resin composition |
| CN104194282A (en) * | 2014-08-28 | 2014-12-10 | 太仓力九和塑胶工业有限公司 | Shock absorbing material, cushion body made of same and preparation method of cushion body |
| CN106317443A (en) * | 2015-06-19 | 2017-01-11 | 罗建光 | Production technology of bamboo charcoal and sponge cushion |
-
2017
- 2017-08-31 CN CN201710774914.7A patent/CN107573650A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101535405A (en) * | 2006-12-22 | 2009-09-16 | 尤尼吉可株式会社 | Biodegradable polyester resin composition, and molded body, foamed body and molded container obtained from the biodegradable polyester resin composition |
| CN101469076A (en) * | 2007-12-29 | 2009-07-01 | 黄仕颖 | Method for manufacturing special foam material |
| CN104194282A (en) * | 2014-08-28 | 2014-12-10 | 太仓力九和塑胶工业有限公司 | Shock absorbing material, cushion body made of same and preparation method of cushion body |
| CN106317443A (en) * | 2015-06-19 | 2017-01-11 | 罗建光 | Production technology of bamboo charcoal and sponge cushion |
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Application publication date: 20180112 |
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