CN107568226A - A kind of miticide composition containing Spiromesifen and plant growth regulator - Google Patents
A kind of miticide composition containing Spiromesifen and plant growth regulator Download PDFInfo
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- CN107568226A CN107568226A CN201710718963.9A CN201710718963A CN107568226A CN 107568226 A CN107568226 A CN 107568226A CN 201710718963 A CN201710718963 A CN 201710718963A CN 107568226 A CN107568226 A CN 107568226A
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- spiromesifen
- plant growth
- growth regulator
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- miticide composition
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Abstract
The invention discloses a kind of miticide composition containing Spiromesifen and plant growth regulator, miticide composition in the present invention has fine prevention effect to harmful mite class on vegetables, strawberry, flowers, melon, nursery, orchard, tea place, vineyard, forest, Chinese herbal medicine, this several plant growth regulator of abscisic acid, brassin lactones, auxin, gibberellin, the basic element of cell division has synergistic effect to Spiromesifen, to putting forward the resistance such as the high drought resisting of crop, high temperature resistance, regulating crop growth, Accelerate bloom, raising fruit yield and quality have good effect.
Description
Technical field
The invention belongs to technical field of pesticide, is related to a kind of containing the combination of the mite killing of Spiromesifen and plant growth regulator
Thing, have very well to harmful mite class on vegetables, strawberry, flowers, melon, nursery, orchard, tea place, vineyard, forest, Chinese herbal medicine
Prevention effect.
Background technology
Spiromesifen category tetronic acid class acaricide, chemical name:(3- mesitylene base -2- oxo -1- oxaspiros [4.4]
Nonyl- 3- alkene -4- bases) -3,3- dimethyl butyrate acid esters.Molecular formula is:
Abscisic acid, brassin lactones, auxin, gibberellin, the basic element of cell division are that people exist as plant growth regulator
After the structurally and functionally mechanism for understanding natural phytohormone, there is similar physiology and biology with plant hormone by artificial synthesized
The material of effect, is used in agricultural production, is effectively adjusted the growing process of crop, is reached stable yields volume increase, improving quality, enhancing
The purpose of crop anti-adversity.
In the real process of agricultural production, controlling disease is easiest to generate the problem that the generation of disease drug resistance.No
Compounded with kind composition, be to prevent and treat the very common method of resistance disease.Heterogeneity is compounded, and is imitated according to practical application
Fruit, to judge that certain compounding is synergy plus and or antagonism.Rational Chemical acaricide compounding or mixture are killed with expansion
Mite compose, improve prevention effect, extend the optimum period for applying fertilizer, reduce dosage, reduce poisoning, reduce residual, delay mite class drug resistance and
The positive features such as drug-fast generation and development, acaricide compounding are one of maximally efficient methods to solve the above problems.Mesh
Before, application of the Spiromesifen as acaricide in crop protection is a lot, and the application of plant growth regulator class compound is special
Profit, document are relatively fewer, and Spiromesifen and plant growth regulator mixture are combined and its application is at home and abroad not yet disclosed.
The content of the invention
The present invention provides a kind of containing Spiromesifen and plant growth regulator aiming at above-mentioned defect
Miticide composition, available on preventing and treating vegetables, strawberry, flowers, melon, nursery, orchard, tea place, vineyard, forest, Chinese herbal medicine
Harmful mite class have fine prevention effect, this several plant growth regulator has synergistic effect to Spiromesifen, to carrying crop height
The resistance such as drought resisting, high temperature resistance, regulating crop growth, Accelerate bloom, raising fruit yield and quality have good effect.With list
One medicament drug effect is compared, and has good synergistic effect after two kinds of composite reagents.
A kind of miticide composition technical scheme containing Spiromesifen and plant growth regulator of the present invention is, described
Plant growth regulator is one kind in abscisic acid, brassin lactones, auxin, gibberellin, the basic element of cell division.
The weight of Spiromesifen and plant growth regulator ratio is:1:0.0001~9:1.
The weight of Spiromesifen and plant growth regulator ratio is:1:0.001~50:1.
The percentage composition that Spiromesifen and plant growth regulator account for total Ingredients Weight is 7%~68%.
In composition auxiliary agent be dispersant, wetting agent, emulsifying agent, antifreezing agent, defoamer, thickener, disintegrant, filler,
At least one of solvent, described solvent are organic solvent or water.
Its formulation of composition is one kind in wettable powder, suspending agent, aqueous emulsion, water dispersible granules and missible oil.
Described miticide composition is cream preparation, and the mass fraction of each component is:1~60 part of Spiromesifen, plant life
Long 1~60 part of conditioning agent, 10 parts of 1-METHYLPYRROLIDONE, 60 parts of methyl oleate;The specific production stage of the cream preparation is will
Spiromesifen, plant growth regulator, 1-METHYLPYRROLIDONE, methyl oleate are added sequentially in reactor, stirring, treat activity
Composition adds methyl oleate after fully dissolving, and stirs;Emulsifying agent is added in reactor, stirs and produces missible oil
Product.
Described miticide composition is suspending agent, and the mass fraction of each component is:1~60 part of Spiromesifen, plant growth
1~60 part of conditioning agent, APES 0.5-3 parts, pull open powder 1-3 parts, xanthans 0.1-0.5 parts, SAG622
0.01-0.05 parts, glycerine 1-3 parts, sodium benzoate 0.1-0.3 parts, remainder are supplied with deionized water;Surplus is supplemented with water;Should
The specific production stage of suspending agent is first mixes other auxiliary agents in addition to except Spiromesifen with plant growth regulator, through high speed
Shear-mixed is uniform, adds active ingredient Spiromesifen and plant growth regulator, abrading-ball 2~3 hours, make grain in ball crusher
Footpath is in below 5mm, you can aqueous suspension formulations are made.
Described miticide composition is wettable powder, and the mass fraction of each component is:1~60 part of Spiromesifen;Plant
1~60 part of growth regulator;4~10 parts of dispersant;1~3 part of wetting agent;Surplus filler polishing;The tool of the wettable powder
Body production stage is:Active ingredient Spiromesifen is mixed with plant growth regulator and dispersant, wetting agent and filler,
Uniform stirring in stirred tank, well mixed after airslide disintegrating mill, you can wettable powder is made.
Described miticide composition is water dispersible granules, and the mass fraction of each component is:1~60 part of Spiromesifen;Plant
1~60 part of growth regulator;2~12 parts of dispersant;1~8 part of wetting agent;1.5~4.5 parts of disintegrant;Surplus filler polishing;
The specific production stage of the water dispersible granules is:By active ingredient Spiromesifen and plant growth regulator and dispersant, wetting
Agent, disintegrant and filler are well mixed, and are crushed with micro jet, through mediating, are then added fluidized bed prilling and are dried
Be granulated, dried in machine, sieve after through sampling analysis, you can water dispersible granules are made.
Described miticide composition is aqueous emulsion, and the mass fraction of each component is:1~60 part of Spiromesifen;Plant growth
1~60 part of conditioning agent;2.5~34 parts of emulsifying agent;4~16 parts of solvent;0.5~5 part of antifreezing agent;0.1~8 part of defoamer;Thickening
0.3~1.8 part of agent;Surplus is supplied with water;The specific production stage of the aqueous emulsion is:Spiromesifen and plant growth are adjusted first
Section agent, solvent and emulsifying agent are added together, and make to be dissolved into uniform oil phase;By part water, antifreezing agent and other insecticides adjuvants
Mix into uniform aqueous phase;Oil phase is added into aqueous phase while high-speed stirred in a kettle, slowly plus water is until reach
To phase inversion point, open cutter and carry out high speed shear, and add remaining water, shear about half an hour, form the water of oil-in-water type
Emulsion, you can aqueous emulsion is made.
Described emulsifying agent is APES, is one of the most frequently used nonionic emulsifier, is had excellent
Emulsification, wetting, diffusion and antistatic behaviour;
Described dispersant is pull open powder, can significantly reduce the surface tension of water, has excellent penetration and wetability,
And with emulsification, diffusion and frothiness energy;
Described thickener is xanthans, has the highly viscous characteristic of low concentration, is a kind of efficient thickener;
Described defoamer is SAG622, is a kind of high temperature resistant, the fast durability organosilicon foam inhibitor of antifoaming speed;
Described antifreezing agent is glycerine, prevents product from the problems such as flocculation, caking, severe delamination occur;
A kind of described miticide composition containing Spiromesifen and plant growth regulator, it is characterised in that to vegetables,
Strawberry, flowers, melon, nursery, orchard, tea place, vineyard, forest, harmful mite class on Chinese herbal medicine have fine prevention effect, right
The resistance such as the high drought resisting of crop, high temperature resistance, regulating crop growth are put forward, Accelerate bloom, raising fruit yield and quality have well
Effect.
Beneficial effects of the present invention are:The active component or composition of the present invention, which has, virtuous kills microbial activity simultaneously
And it can be used for preventing and treating for example true mite of undesired microorganism and thin mite in crop protection and material protection.
The present invention has bright using Spiromesifen with Compositional acaricide of the plant growth regulator class compound as active ingredient
Aobvious synergistic effect, delay the drug-fast generation in key, and reduce into production cost and use cost, and adjust plant life
It is long, reach the purpose for improving yield and quality.To vegetables, strawberry, flowers, melon, nursery, orchard, tea place, vineyard, forest,
Harmful mite class on Chinese herbal medicine has a fine prevention effect, abscisic acid, brassin lactones, auxin, gibberellin, the basic element of cell division this
Several plant growth regulator has synergistic effect to Spiromesifen, to putting forward the resistance such as the high drought resisting of crop, high temperature resistance, adjusts crop
Growth, Accelerate bloom, raising fruit yield and quality have good effect.
Embodiment:
For a better understanding of the present invention, technical scheme is described in detail with instantiation below, but originally
Invention is not limited thereto.
Emulsifying agent described in following examples is APES, is one of the most frequently used nonionic emulsifier,
With excellent emulsification, wetting, diffusion and antistatic behaviour;
Embodiment 1
A kind of miticide composition suspending agent containing Spiromesifen and brassin lactones, is made up of the component of following parts by weight,
24 parts of active component, 1 part of APES, 1 part of pull open powder, 0.2 part of xanthans, 0.02 part of SAG622, glycerine 2
Part, 0.1 part of sodium benzoate, remainder are supplied with deionized water;Active component is the mixture of Spiromesifen and brassin lactones, and
Both weight ratio is:100:1;
The technique containing Spiromesifen and brassin lactones miticide composition suspending agent is prepared, is comprised the following steps that:
First other auxiliary agents in addition to except Spiromesifen with brassin lactones are mixed, are well mixed through high speed shear, are added
Active ingredient Spiromesifen and brassin lactones, abrading-ball 2~3 hours in ball crusher, make particle diameter in below 5mm, you can system
Into aqueous suspension formulations.
Embodiment 2
A kind of miticide composition suspending agent containing Spiromesifen and abscisic acid, is made up of the component of following parts by weight, activity
36 parts of component, 2 parts of APES, 2.2 parts of pull open powder, 0.4 part of xanthans, 0.04 part of SAG622,1 part of glycerine,
0.2 part of sodium benzoate, remainder are supplied with deionized water;Active component is the mixture of Spiromesifen and abscisic acid, and both
Weight ratio is:20:1;
The technique for preparing the miticide composition suspending agent containing Spiromesifen and abscisic acid, is comprised the following steps that:
First other auxiliary agents in addition to except Spiromesifen with abscisic acid are mixed, are well mixed through high speed shear, are added effective
Composition Spiromesifen and abscisic acid, abrading-ball 2~3 hours in ball crusher, make particle diameter in below 5mm, you can suspending agent is made
Preparation.
Embodiment 3
A kind of miticide composition suspending agent containing Spiromesifen and auxin, is made up of the component of following parts by weight, activity
56 parts of component, 0.5 part of APES, 2 parts of pull open powder, 0.2 part of xanthans, 0.01 part of SAG622, glycerine 1.5
Part, 0.1 part of sodium benzoate, remainder are supplied with deionized water;Active component is the mixture of Spiromesifen and auxin, and both
Weight ratio be:50:1;
The technique containing Spiromesifen and auxin miticide composition suspending agent is prepared, is comprised the following steps that:
First other auxiliary agents in addition to except Spiromesifen with auxin are mixed, are well mixed through high speed shear, are added effective
Composition Spiromesifen and auxin, abrading-ball 2~3 hours in ball crusher, make particle diameter in below 5mm, you can suspending agent is made
Preparation.
Embodiment 4
A kind of miticide composition water dispersible granules containing Spiromesifen and the basic element of cell division, by the component group of following parts by weight
Into 1~60 part of Spiromesifen, 1~60 part of the basic element of cell division, 5~15 parts of dispersant, 5~10 parts of wetting agent, disintegrant 1~10
Part, filler complements to 100 parts.Active component is the mixture of Spiromesifen and the basic element of cell division, and both weight ratios are:
20:1;Specifically production stage is:Active ingredient and other auxiliary agents are well mixed, crushed with micro jet, through mediating,
Then add in fluidized-bed granulation dryer and be granulated, dry, sieve, water dispersible granules are made.
Embodiment 5
A kind of miticide composition wettable powder containing Spiromesifen and gibberellin, is made up of the component of following parts by weight,
1~50 part of Spiromesifen, 1~60 part of gibberellin, filler complements to 100 parts.Active component is the mixed of Spiromesifen and gibberellin
Compound, and both weight ratios are:100:1.Specifically production stage is:Active ingredient and other auxiliary agents are mixed, mechanical crushing
It is well mixed again through air-flow crushing afterwards, wettable powder is made.
Embodiment 6
A kind of miticide composition wettable powder containing Spiromesifen and auxin, is made up of the component of following parts by weight,
1~50 part of Spiromesifen, 1~30 part of auxin, filler complement to 100 parts.Active component is the mixed of Spiromesifen and auxin
Compound, and both weight ratios are:20:1.Specifically production stage is:Active ingredient and other auxiliary agents are mixed, after mechanical crushing
Again through air-flow crushing, it is well mixed, wettable powder is made.
Embodiment 7
A kind of miticide composition aqueous emulsion containing Spiromesifen and brassin lactones, is made up of the component of following parts by weight,
1~25 part of Spiromesifen, 1~30 part of brassin lactones, 5~30 parts of emulsifying agent, 5~15 parts of solvent, 2~5 parts of antifreezing agent, defoaming
0.1~5 part of agent, 0.1~2 part of thickener, deionized water complements to 100 parts.Active component is that Spiromesifen and plant growth are adjusted
The mixture of agent is saved, and both weight ratios are:50:1.First active ingredient, solvent, emulsifying agent are mixed, are dissolved into
For uniform oil phase.Part water and other auxiliary agents are mixed again, dissolving turns into uniform aqueous phase.Then in a kettle
Aqueous phase is added into oil phase while high-speed stirred, slowly adds water to and reaches phase inversion point, carries out high speed shear afterwards, and add residue
Water, shear about 30min, be made aqueous emulsion.
Embodiment 8
A kind of miticide composition cream preparation containing Spiromesifen and brassin lactones, by the component group of following parts by weight
Into, 1~30 part of Spiromesifen, 1~25 part of plant growth regulator, 10 parts of 1-METHYLPYRROLIDONE, 60 parts of methyl oleate.Activity
Component is the mixture of Spiromesifen and plant growth regulator, and both weight ratios are:30:1.Its specific preparation process
For:Each raw material for standby is weighed in proportion;Spiromesifen, brassin lactones, 1-METHYLPYRROLIDONE, methyl oleate are sequentially added
Into reactor, stirring, treat that active component adds methyl oleate after fully dissolving, stir;Emulsifying agent is added to instead
Answer in kettle, stir and produce missible oil product.
Experimental example
The present composition is verified as follows to tomato acarid field efficacy:
Field test embodiment one:The field medicine of Spiromesifen and plant growth regulator composition to tomato Tetranychus urticae
Effect experiment measure
After Spiromesifen and plant growth regulator are re-dubbed 5 kinds of different dosage forms under different proportion, in the variegated leaf of tomato two
Mite early stage is sprayed, and every mu is watered 15L, and two kinds of total active ingredients of medicament are 3g, and comparison medicament is 24% spiral shell first mite
Ester suspending agent.As a result show:Spiromesifen and each mixture of plant growth regulator processing preventive effect are above comparison medicament, 5d after medicine
Preventive effect be up to 80.66%~91.05%.
The Spiromesifen of table 1 and plant growth regulator composition are to tomato Tetranychus urticae test of pesticide effectiveness result
Field test embodiment two:The field efficacy of Spiromesifen and plant growth regulator composition to wheat red spider
Experiment measure
After Spiromesifen and plant growth regulator are re-dubbed 5 kinds of different dosage forms under different proportion, in wheat red spider
Early stage carries out cauline leaf spraying treatment, and comparison medicament is 24% Spiromesifen suspending agent.As a result show:Spiromesifen and plant
Each mixture spraying treatment of growth regulator is above comparison medicament to the preventive effect of wheat red spider, and 10d preventive effect is up to after medicine
73.03%~80.92%.
The Spiromesifen of table 2 and plant growth regulator composition are to wheat red spider test of pesticide effectiveness result
Field test embodiment three:The field efficacy of Spiromesifen and plant growth regulator composition to watermelon red spider
Experiment measure
After Spiromesifen and plant growth regulator are re-dubbed 5 kinds of different dosage forms under different proportion, in watermelon red spider
Early stage carries out spraying treatment, and comparison medicament is 24% Spiromesifen suspending agent.As a result show:Spiromesifen and plant growth
Each mixture spraying treatment of conditioning agent is above comparison medicament to watermelon red spider preventive effect, after medicine 10d preventive effect be up to 70.12%~
85.96%.
The Spiromesifen of table 3 and plant growth regulator composition are to watermelon red spider test of pesticide effectiveness result
By three experiments Spiromesifen and plant growth regulator compounding can be drawn to preventing and treating tomato Tetranychus urticae, small
Wheat red mite, watermelon red spider have good effect.In addition to vegetables, strawberry, flowers, melon, nursery, orchard, tea place, grape
Garden, forest, harmful mite class on Chinese herbal medicine have fine prevention effect, and this several plant growth regulator has synergy to Spiromesifen
Effect, to putting forward the resistance such as the high drought resisting of crop, high temperature resistance, regulating crop growth, Accelerate bloom, raising fruit yield and quality have
Effect well.
Spiromesifen mite killing spectrum is wide, acaricidal activity is high, quick, and resistance of rainwater washing against, the lasting period length, category efficiently, low toxicity,
Less-persistent pesticide, there is good prospect with plant growth regulator compounding.
Claims (10)
- A kind of 1. miticide composition containing Spiromesifen and plant growth regulator, it is characterised in that described plant growth Conditioning agent is one kind in abscisic acid, brassin lactones, auxin, gibberellin, the basic element of cell division.
- 2. a kind of miticide composition containing Spiromesifen and plant growth regulator according to claim 1, its feature It is, the weight ratio of Spiromesifen and plant growth regulator is:1:0.0001~9:1.
- 3. a kind of miticide composition containing Spiromesifen and plant growth regulator according to claim 1, its feature It is, the weight ratio of Spiromesifen and plant growth regulator is:1:0.001~50:1.
- 4. a kind of miticide composition containing Spiromesifen and plant growth regulator according to claim 1, its feature It is, the percentage composition that Spiromesifen and plant growth regulator account for total Ingredients Weight is 7%~68%.
- 5. a kind of miticide composition containing Spiromesifen and plant growth regulator according to claim 1, its feature It is, described miticide composition is cream preparation, and the mass fraction of each component is:1~60 part of Spiromesifen, plant growth are adjusted Save 1~60 part of agent, 10 parts of 1-METHYLPYRROLIDONE, 60 parts of methyl oleate;The specific production stage of the cream preparation is by Luo Jia Mite ester, plant growth regulator, 1-METHYLPYRROLIDONE, methyl oleate are added sequentially in reactor, stirring, treat active component Methyl oleate fully is added after dissolving, is stirred;Emulsifying agent is added in reactor, stirs and produces missible oil production Product.
- 6. a kind of miticide composition containing Spiromesifen and plant growth regulator according to claim 1, its feature It is, described miticide composition is suspending agent, and the mass fraction of each component is:1~60 part of Spiromesifen, plant growth regulating 1~60 part of agent, APES 0.5-3 parts, pull open powder 1-3 parts, xanthans 0.1-0.5 parts, SAG6220.01-0.05 Part, glycerine 1-3 parts, sodium benzoate 0.1-0.3 parts, remainder are supplied with deionized water;Surplus is supplemented with water;The tool of the suspending agent Other auxiliary agents in addition to except Spiromesifen with plant growth regulator is first mixs by body production stage, through high speed shear mixing It is even, active ingredient Spiromesifen and plant growth regulator are added, abrading-ball 2~3 hours in ball crusher, makes particle diameter in 5mm Below, you can aqueous suspension formulations are made.
- 7. a kind of miticide composition containing Spiromesifen and plant growth regulator according to claim 1, its feature It is, described miticide composition is wettable powder, and the mass fraction of each component is:1~60 part of Spiromesifen;Plant growth 1~60 part of conditioning agent;4~10 parts of dispersant;1~3 part of wetting agent;Surplus filler polishing;The specific life of the wettable powder Producing step is:Active ingredient Spiromesifen is mixed with plant growth regulator and dispersant, wetting agent and filler, stirred Uniform stirring in kettle, well mixed after airslide disintegrating mill, you can wettable powder is made.
- 8. a kind of miticide composition containing Spiromesifen and plant growth regulator according to claim 1, its feature It is, described miticide composition is water dispersible granules, and the mass fraction of each component is:1~60 part of Spiromesifen;Plant growth 1~60 part of conditioning agent;2~12 parts of dispersant;1~8 part of wetting agent;1.5~4.5 parts of disintegrant;Surplus filler polishing;The water The specific production stage of dispersible granule is:By active ingredient Spiromesifen and plant growth regulator and dispersant, wetting agent, collapse Solution agent and filler are well mixed, and are crushed with micro jet, through mediating, then add in fluidized-bed granulation dryer Through sampling analysis after row granulation, dry, screening, you can water dispersible granules are made.
- 9. a kind of miticide composition containing Spiromesifen and plant growth regulator according to claim 1, its feature It is, described miticide composition is aqueous emulsion, and the mass fraction of each component is:1~60 part of Spiromesifen;Plant growth regulating 1~60 part of agent;2.5~34 parts of emulsifying agent;4~16 parts of solvent;0.5~5 part of antifreezing agent;0.1~8 part of defoamer;Thickener 0.3 ~1.8 parts;Surplus is supplied with water;The specific production stage of the aqueous emulsion is:First by Spiromesifen and plant growth regulator, Solvent and emulsifying agent are added together, and make to be dissolved into uniform oil phase;By part water, antifreezing agent and other insecticides adjuvants are blended in Together into uniform aqueous phase;Oil phase is added into aqueous phase while high-speed stirred in a kettle, slowly plus water is until reach phase inversion Point, open cutter and carry out high speed shear, and add remaining water, shear about half an hour, form the aqueous emulsion of oil-in-water type, i.e., It can be made into aqueous emulsion.
- 10. a kind of miticide composition containing Spiromesifen and plant growth regulator according to claim 1, its feature It is have very to harmful mite class on vegetables, strawberry, flowers, melon, nursery, orchard, tea place, vineyard, forest, Chinese herbal medicine Good prevention effect, to putting forward the resistance such as the high drought resisting of crop, high temperature resistance, regulating crop growth, Accelerate bloom, improve fruit yield and Quality has good effect.
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CN114642206A (en) * | 2022-03-29 | 2022-06-21 | 贵州省烟草公司贵阳市公司 | Tobacco bud inhibitor suspending agent, preparation method and application thereof |
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CN105961378A (en) * | 2009-08-07 | 2016-09-28 | 加特微胶囊有限公司 | Macrolide-containing microcapsules |
CN102177891A (en) * | 2011-03-22 | 2011-09-14 | 浙江大学 | Spiromesifen water dispersant |
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Application publication date: 20180112 |