CN107499754A - A kind of phosphorus trichloride storage tank breathes Flash Gas Compression Skid System - Google Patents

A kind of phosphorus trichloride storage tank breathes Flash Gas Compression Skid System Download PDF

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Publication number
CN107499754A
CN107499754A CN201710777634.1A CN201710777634A CN107499754A CN 107499754 A CN107499754 A CN 107499754A CN 201710777634 A CN201710777634 A CN 201710777634A CN 107499754 A CN107499754 A CN 107499754A
Authority
CN
China
Prior art keywords
phosphorus trichloride
storage tank
skid system
gas compression
trichloride storage
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710777634.1A
Other languages
Chinese (zh)
Inventor
张广辉
罗朝林
李俊峰
孟庆红
朱晓兵
张彦伟
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Luohe New Flourishing Chemical Co Ltd
Original Assignee
Luohe New Flourishing Chemical Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Luohe New Flourishing Chemical Co Ltd filed Critical Luohe New Flourishing Chemical Co Ltd
Priority to CN201710777634.1A priority Critical patent/CN107499754A/en
Publication of CN107499754A publication Critical patent/CN107499754A/en
Pending legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B65CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
    • B65DCONTAINERS FOR STORAGE OR TRANSPORT OF ARTICLES OR MATERIALS, e.g. BAGS, BARRELS, BOTTLES, BOXES, CANS, CARTONS, CRATES, DRUMS, JARS, TANKS, HOPPERS, FORWARDING CONTAINERS; ACCESSORIES, CLOSURES, OR FITTINGS THEREFOR; PACKAGING ELEMENTS; PACKAGES
    • B65D90/00Component parts, details or accessories for large containers
    • B65D90/22Safety features
    • B65D90/32Arrangements for preventing, or minimising the effect of, excessive or insufficient pressure
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/26Drying gases or vapours
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/34Chemical or biological purification of waste gases
    • B01D53/74General processes for purification of waste gases; Apparatus or devices specially adapted therefor
    • B01D53/77Liquid phase processes
    • B01D53/78Liquid phase processes with gas-liquid contact
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B65CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
    • B65DCONTAINERS FOR STORAGE OR TRANSPORT OF ARTICLES OR MATERIALS, e.g. BAGS, BARRELS, BOTTLES, BOXES, CANS, CARTONS, CRATES, DRUMS, JARS, TANKS, HOPPERS, FORWARDING CONTAINERS; ACCESSORIES, CLOSURES, OR FITTINGS THEREFOR; PACKAGING ELEMENTS; PACKAGES
    • B65D90/00Component parts, details or accessories for large containers
    • B65D90/22Safety features
    • B65D90/30Recovery of escaped vapours
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2257/00Components to be removed
    • B01D2257/80Water

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  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Mechanical Engineering (AREA)
  • Analytical Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Environmental & Geological Engineering (AREA)
  • Health & Medical Sciences (AREA)
  • Biomedical Technology (AREA)
  • Respiratory Apparatuses And Protective Means (AREA)

Abstract

The invention discloses a kind of phosphorus trichloride storage tank to breathe Flash Gas Compression Skid System, including phosphorus trichloride storage tank and automaton, also include storing up tank connected breath device and getter device with phosphorus trichloride respectively by the first pipeline and second pipe, present device is simple, it is practical and convenient, cost is low, getter device solves the moisture brought into storage tank air-breathing body, prevent that phosphorus trichloride is contaminated in storage tank, breath device is efficiently solved due to uncontrollable discharge caused by phosphorus trichloride storage tank discharge gas, improve work on the spot environment, alleviate environmental protection pressure, expiration automatic stop valve can completely cut off aqueous vapor and touch phosphorus trichloride, phosphorus trichloride is prevented to be contaminated.

Description

A kind of phosphorus trichloride storage tank breathes Flash Gas Compression Skid System
Technical field
The invention belongs to chemical field, and in particular to a kind of phosphorus trichloride storage tank breathes Flash Gas Compression Skid System.
Background technology
Phosphorus trichloride, relative molecular weight 137.33, density 1.574, fusing point are -112 DEG C, 76 DEG C of boiling point, and outward appearance is Colourless transparent liquid, it is dissolved in benzene, ether, carbon disulfide, carbon tetrachloride.Phosphorus trichloride meets water and plays hydrolysis, and phosphorus trichloride exists Salt acid mist can be generated in air, has stimulation corrosiveness to skin, mucous membrane.
When temperature Change, material transfer, Volume Changes can occur phosphorus trichloride storage tank for the gas-phase space in storage tank, cause Gas pressure changes in storage tank, may cause the flat tank of storage tank or quick-fried tank.Due to the tri-chlorination of storage tank internal respiration discharge Phosphorus gas is less, and treating capacity is small, if a set of elution Tower System of independent configuration, construction cost is higher, and utilization rate is not again high, increases Construction cost and operating cost are added, but if without processing, phosphorus trichloride gas can impact to environment again, damage people How member's health, therefore, realize low-cost processes phosphorus trichloride storage tank tidal air, need to solve the problems, such as it into the art One.
The content of the invention
It is easy to use it is an object of the invention to provide a kind of simple in construction, the air-breathing of phosphorus trichloride storage tank can be handled simultaneously Flash Gas Compression Skid System is breathed with the phosphorus trichloride storage tank of discharge gas.
The object of the present invention is achieved like this:
A kind of phosphorus trichloride storage tank breathes Flash Gas Compression Skid System, including phosphorus trichloride storage tank and automaton, in addition to passes through First pipeline and second pipe store up tank connected breath device and getter device with phosphorus trichloride respectively.
First pipeline and second pipe are connected by total pipeline with phosphorus trichloride storage tank, and the total pipeline is provided with pressure Power transmitter, pressure transmitter are connected with the automaton.
The getter device includes the air-breathing automatic stop valve being arranged on the first pipeline and is connected with the first pipe end Moisture dryer.
Expiration automatic stop valve that the breath device includes being arranged on second pipe, it is connected with second pipe end Injector, circulating tank and circulating pump,
The injector includes gas access, liquid inlet and liquid outlet, and the gas access is connected with second pipe end, The liquid outlet is located in the liquid of circulating tank, and the liquid inlet is connected by circulating pump with circulation pot bottom.
The injector interior is provided with sleeve pipe, and described sleeve pipe port of export horizontal level is less than gas access.
The air-breathing automatic stop valve, expiration automatic stop valve and circulating pump are connected with automaton.
The beneficial effects of the invention are as follows:Present device is simple, practical and convenient, and cost is low, and getter device solves storage tank The moisture brought into air-breathing body, prevent that phosphorus trichloride is contaminated in storage tank, breath device is efficiently solved due to phosphorus trichloride Uncontrollable discharge caused by storage tank discharge gas, improves work on the spot environment, alleviates environmental protection pressure, expiration automatic stop valve can completely cut off Aqueous vapor touches phosphorus trichloride, prevents phosphorus trichloride to be contaminated.
Brief description of the drawings
Fig. 1 is the structural representation of the present invention;
Fig. 2 is the structural representation of injector;
In figure:Phosphorus trichloride storage tank 1, moisture dryer 2, air-breathing automatic stop valve 3, pressure transmitter 4, injector 5, exhale certainly Dynamic stop valve 6, circulating tank 7, circulating pump 8, the first pipeline 9, second pipe 10, gas access 11, liquid inlet 12, liquid outlet 13, total pipeline 14.
Embodiment
Below in conjunction with accompanying drawing, the invention will be further described.
As shown in Figure 1 and Figure 2, a kind of phosphorus trichloride storage tank breathing Flash Gas Compression Skid System, including phosphorus trichloride storage tank 1 and automatic Control device, in addition to the breath device being connected respectively with phosphorus trichloride storage tank 1 by the first pipeline 9 and second pipe 10 and suction Device of air.First pipeline 9 and second pipe 10 are connected by total pipeline 14 with phosphorus trichloride storage tank 1, the total pipeline 14 Pressure transmitter 4 is provided with, pressure transmitter 4 is connected with the automaton.
The getter device includes the air-breathing automatic stop valve being arranged on the first pipeline 9 and 3 and the end of the first pipeline 9 company The moisture dryer 2 connect, moisture dryer 2 are avoided in the gas of suction with the gas in moisture contamination phosphorus trichloride storage tank.
The breath device includes the expiration automatic stop valve 6 being arranged on second pipe 10 and the end of second pipe 10 Injector 5, circulating tank 7 and the circulating pump 8 of connection, injector 5 include gas access 11, liquid inlet 12 and liquid outlet 13, The gas access 11 is connected with the end of second pipe 10, and the liquid outlet 13 is located in the liquid of circulating tank 7, the liquid Entrance 12 is connected by circulating pump 8 with the bottom of circulating tank 7, the air-breathing automatic stop valve 3, expiration automatic stop valve 6 and circulation Pump 8 is connected with automaton.When phosphorus trichloride 1 exhaled gas of storage tank, the gas of exhalation enters injector 5, simultaneously Automaton control circulating pump 8 is worked, and the exhaled gas entered in injector 5 is reacted and removed, prevents from polluting Air.
The inside of the injector 5 is provided with sleeve pipe, and described sleeve pipe port of export horizontal level is less than gas access, be easy to gas with Liquid is sufficiently mixed.
When the show value of pressure transmitter 4 is in setting range, expiration automatic stop valve 6 and air-breathing automatic stop valve 3 are equal In dissengaged positions, phosphorus trichloride storage tank breath device and getter device do not work;Set when the show value of pressure transmitter 4 is higher than When determining scope, automaton control expiration automatic stop valve 6 is opened, and circulating pump 8 starts, phosphorus trichloride storage tank tidal air dress Put start-up operation;When the show value of pressure transmitter 4 is less than setting range, air-breathing automatic stop valve 3 is opened, until pressure inverting The show value of device 4 is in setting range.
Present device is simple, practical and convenient, and cost is low, and getter device solves the moisture brought into storage tank air-breathing body, Prevent that phosphorus trichloride is contaminated in storage tank, breath device is efficiently solved because phosphorus trichloride storage tank is discharged caused by gas without group Discharge to be knitted, improves work on the spot environment, alleviates environmental protection pressure, expiration automatic stop valve can completely cut off aqueous vapor and touch phosphorus trichloride, Phosphorus trichloride is prevented to be contaminated.

Claims (7)

1. a kind of phosphorus trichloride storage tank breathes Flash Gas Compression Skid System, including phosphorus trichloride storage tank(1)And automaton, its feature It is:Also include passing through the first pipeline(9)And second pipe(10)Respectively with phosphorus trichloride storage tank(1)The breath device of connection and Getter device.
2. phosphorus trichloride storage tank according to claim 1 breathes Flash Gas Compression Skid System, it is characterised in that:First pipeline (9)And second pipe(10)Pass through total pipeline(14)With phosphorus trichloride storage tank(1)Connection, the total pipeline(14)It is provided with pressure Transmitter(4), pressure transmitter(4)It is connected with the automaton.
3. phosphorus trichloride storage tank according to claim 1 breathes Flash Gas Compression Skid System, it is characterised in that:The getter device bag Include and be arranged on the first pipeline(9)On air-breathing automatic stop valve(3)With with the first pipeline(9)The moisture dryer of end connection (2).
4. phosphorus trichloride storage tank according to claim 1 breathes Flash Gas Compression Skid System, it is characterised in that:The breath device bag Include and be arranged on second pipe(10)On expiration automatic stop valve(6)With second pipe(10)The injector of end connection(5)、 Circulating tank(7)And circulating pump(8).
5. phosphorus trichloride storage tank according to claim 4 breathes Flash Gas Compression Skid System, it is characterised in that:The injector(5) Including gas access(11), liquid inlet(12)And liquid outlet(13), the gas access(11)With second pipe(10)End End connection, the liquid outlet(13)Positioned at circulating tank(7)Liquid in, the liquid inlet(12)Pass through circulating pump(8)With Circulating tank(7)Bottom connects.
6. the phosphorus trichloride storage tank breathing Flash Gas Compression Skid System according to claim 4 or 5, it is characterised in that:The injector (5)Inside is provided with sleeve pipe, and described sleeve pipe port of export horizontal level is less than gas access(11).
7. the phosphorus trichloride storage tank breathing Flash Gas Compression Skid System according to claim 3 or 4, it is characterised in that:The air-breathing is certainly Dynamic stop valve(3), expiration automatic stop valve(6)And circulating pump(8)It is connected with automaton.
CN201710777634.1A 2017-09-01 2017-09-01 A kind of phosphorus trichloride storage tank breathes Flash Gas Compression Skid System Pending CN107499754A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201710777634.1A CN107499754A (en) 2017-09-01 2017-09-01 A kind of phosphorus trichloride storage tank breathes Flash Gas Compression Skid System

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201710777634.1A CN107499754A (en) 2017-09-01 2017-09-01 A kind of phosphorus trichloride storage tank breathes Flash Gas Compression Skid System

Publications (1)

Publication Number Publication Date
CN107499754A true CN107499754A (en) 2017-12-22

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Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1915795A (en) * 2006-09-06 2007-02-21 山西佳新能源化工实业有限公司 Storage equipment in fillingup station of fuel in alcohols
CN203345509U (en) * 2013-06-17 2013-12-18 浙江优创材料科技股份有限公司 Antioxidant protecting device for heat transfer oil
CN103758616A (en) * 2014-02-20 2014-04-30 山东申普交通科技有限公司 Motor vehicle exhaust purifying device
CN203886516U (en) * 2013-12-24 2014-10-22 梧州三和新材料科技有限公司 Jet self-suction type gas and liquid contact reaction device
CN106185095A (en) * 2016-08-25 2016-12-07 聂麒曌 In vehicle-mounted groove tank of tank car breather valve tail gas and absorption system
CN207417627U (en) * 2017-09-01 2018-05-29 漯河市新旺化工有限公司 A kind of phosphorus trichloride storage tank breathes Flash Gas Compression Skid System

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1915795A (en) * 2006-09-06 2007-02-21 山西佳新能源化工实业有限公司 Storage equipment in fillingup station of fuel in alcohols
CN203345509U (en) * 2013-06-17 2013-12-18 浙江优创材料科技股份有限公司 Antioxidant protecting device for heat transfer oil
CN203886516U (en) * 2013-12-24 2014-10-22 梧州三和新材料科技有限公司 Jet self-suction type gas and liquid contact reaction device
CN103758616A (en) * 2014-02-20 2014-04-30 山东申普交通科技有限公司 Motor vehicle exhaust purifying device
CN106185095A (en) * 2016-08-25 2016-12-07 聂麒曌 In vehicle-mounted groove tank of tank car breather valve tail gas and absorption system
CN207417627U (en) * 2017-09-01 2018-05-29 漯河市新旺化工有限公司 A kind of phosphorus trichloride storage tank breathes Flash Gas Compression Skid System

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
张玉秀: "《化工仪表及自动化(工艺专业及分析专业适用)》", 30 June 1986, 化学工业出版社, pages: 12 *

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