CN107495126A - A kind of calcareous nourishing reinforced food oxidative rancidity Control Technology of beans base - Google Patents
A kind of calcareous nourishing reinforced food oxidative rancidity Control Technology of beans base Download PDFInfo
- Publication number
- CN107495126A CN107495126A CN201710827287.9A CN201710827287A CN107495126A CN 107495126 A CN107495126 A CN 107495126A CN 201710827287 A CN201710827287 A CN 201710827287A CN 107495126 A CN107495126 A CN 107495126A
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- CN
- China
- Prior art keywords
- calcium
- microencapsulation
- calcareous
- homogenization
- beans base
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- 235000010627 Phaseolus vulgaris Nutrition 0.000 title claims abstract description 14
- 244000046052 Phaseolus vulgaris Species 0.000 title claims abstract description 14
- 235000013305 food Nutrition 0.000 title claims abstract description 12
- 238000005516 engineering process Methods 0.000 title claims abstract description 9
- 230000001590 oxidative effect Effects 0.000 title claims abstract description 7
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims abstract description 25
- 239000011575 calcium Substances 0.000 claims abstract description 25
- 229910052791 calcium Inorganic materials 0.000 claims abstract description 25
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims abstract description 20
- 239000000463 material Substances 0.000 claims abstract description 14
- 229910000019 calcium carbonate Inorganic materials 0.000 claims abstract description 10
- 238000000265 homogenisation Methods 0.000 claims abstract description 10
- 239000007787 solid Substances 0.000 claims abstract description 10
- 235000012054 meals Nutrition 0.000 claims abstract description 8
- 229920002774 Maltodextrin Polymers 0.000 claims abstract description 7
- 235000020429 malt syrup Nutrition 0.000 claims abstract description 7
- 150000001875 compounds Chemical class 0.000 claims abstract description 5
- 239000000843 powder Substances 0.000 claims description 15
- 239000011162 core material Substances 0.000 claims description 12
- 238000003756 stirring Methods 0.000 claims description 5
- 238000009826 distribution Methods 0.000 claims description 4
- 238000002360 preparation method Methods 0.000 claims description 4
- 239000002002 slurry Substances 0.000 claims description 4
- 239000003643 water by type Substances 0.000 claims description 2
- 235000016709 nutrition Nutrition 0.000 abstract description 16
- 230000035764 nutrition Effects 0.000 abstract description 16
- 230000003647 oxidation Effects 0.000 abstract description 10
- 238000007254 oxidation reaction Methods 0.000 abstract description 10
- 238000000034 method Methods 0.000 abstract description 5
- 238000001694 spray drying Methods 0.000 abstract description 4
- BHPQYMZQTOCNFJ-UHFFFAOYSA-N Calcium cation Chemical compound [Ca+2] BHPQYMZQTOCNFJ-UHFFFAOYSA-N 0.000 abstract description 3
- 229910001424 calcium ion Inorganic materials 0.000 abstract description 3
- 230000002265 prevention Effects 0.000 abstract description 3
- 239000003795 chemical substances by application Substances 0.000 abstract description 2
- 239000007788 liquid Substances 0.000 abstract 2
- 238000010438 heat treatment Methods 0.000 abstract 1
- 239000003925 fat Substances 0.000 description 8
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 description 6
- 235000019197 fats Nutrition 0.000 description 6
- OVBPIULPVIDEAO-LBPRGKRZSA-N folic acid Chemical compound C=1N=C2NC(N)=NC(=O)C2=NC=1CNC1=CC=C(C(=O)N[C@@H](CCC(O)=O)C(O)=O)C=C1 OVBPIULPVIDEAO-LBPRGKRZSA-N 0.000 description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
- 239000005913 Maltodextrin Substances 0.000 description 4
- 235000007144 ferric diphosphate Nutrition 0.000 description 4
- 239000011706 ferric diphosphate Substances 0.000 description 4
- CADNYOZXMIKYPR-UHFFFAOYSA-B ferric pyrophosphate Chemical compound [Fe+3].[Fe+3].[Fe+3].[Fe+3].[O-]P([O-])(=O)OP([O-])([O-])=O.[O-]P([O-])(=O)OP([O-])([O-])=O.[O-]P([O-])(=O)OP([O-])([O-])=O CADNYOZXMIKYPR-UHFFFAOYSA-B 0.000 description 4
- 229940036404 ferric pyrophosphate Drugs 0.000 description 4
- 229940035034 maltodextrin Drugs 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- 239000013589 supplement Substances 0.000 description 4
- FPIPGXGPPPQFEQ-UHFFFAOYSA-N 13-cis retinol Natural products OCC=C(C)C=CC=C(C)C=CC1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-UHFFFAOYSA-N 0.000 description 3
- OVBPIULPVIDEAO-UHFFFAOYSA-N N-Pteroyl-L-glutaminsaeure Natural products C=1N=C2NC(N)=NC(=O)C2=NC=1CNC1=CC=C(C(=O)NC(CCC(O)=O)C(O)=O)C=C1 OVBPIULPVIDEAO-UHFFFAOYSA-N 0.000 description 3
- FPIPGXGPPPQFEQ-BOOMUCAASA-N Vitamin A Natural products OC/C=C(/C)\C=C\C=C(\C)/C=C/C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-BOOMUCAASA-N 0.000 description 3
- 229930003316 Vitamin D Natural products 0.000 description 3
- QYSXJUFSXHHAJI-XFEUOLMDSA-N Vitamin D3 Natural products C1(/[C@@H]2CC[C@@H]([C@]2(CCC1)C)[C@H](C)CCCC(C)C)=C/C=C1\C[C@@H](O)CCC1=C QYSXJUFSXHHAJI-XFEUOLMDSA-N 0.000 description 3
- FPIPGXGPPPQFEQ-OVSJKPMPSA-N all-trans-retinol Chemical compound OC\C=C(/C)\C=C\C=C(/C)\C=C\C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-OVSJKPMPSA-N 0.000 description 3
- 239000001506 calcium phosphate Substances 0.000 description 3
- 229960000304 folic acid Drugs 0.000 description 3
- 235000019152 folic acid Nutrition 0.000 description 3
- 239000011724 folic acid Substances 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- DPJRMOMPQZCRJU-UHFFFAOYSA-M thiamine hydrochloride Chemical compound Cl.[Cl-].CC1=C(CCO)SC=[N+]1CC1=CN=C(C)N=C1N DPJRMOMPQZCRJU-UHFFFAOYSA-M 0.000 description 3
- QORWJWZARLRLPR-UHFFFAOYSA-H tricalcium bis(phosphate) Chemical compound [Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O QORWJWZARLRLPR-UHFFFAOYSA-H 0.000 description 3
- 229940078499 tricalcium phosphate Drugs 0.000 description 3
- 229910000391 tricalcium phosphate Inorganic materials 0.000 description 3
- 235000019731 tricalcium phosphate Nutrition 0.000 description 3
- 235000019155 vitamin A Nutrition 0.000 description 3
- 239000011719 vitamin A Substances 0.000 description 3
- 239000011691 vitamin B1 Substances 0.000 description 3
- 235000019166 vitamin D Nutrition 0.000 description 3
- 239000011710 vitamin D Substances 0.000 description 3
- 150000003710 vitamin D derivatives Chemical class 0.000 description 3
- 229940045997 vitamin a Drugs 0.000 description 3
- 229940046008 vitamin d Drugs 0.000 description 3
- 239000011787 zinc oxide Substances 0.000 description 3
- 229960001296 zinc oxide Drugs 0.000 description 3
- 235000014692 zinc oxide Nutrition 0.000 description 3
- IIZPXYDJLKNOIY-JXPKJXOSSA-N 1-palmitoyl-2-arachidonoyl-sn-glycero-3-phosphocholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCC\C=C/C\C=C/C\C=C/C\C=C/CCCCC IIZPXYDJLKNOIY-JXPKJXOSSA-N 0.000 description 2
- 229920000858 Cyclodextrin Polymers 0.000 description 2
- 102000004407 Lactalbumin Human genes 0.000 description 2
- 108090000942 Lactalbumin Proteins 0.000 description 2
- 235000010489 acacia gum Nutrition 0.000 description 2
- 239000001785 acacia senegal l. willd gum Substances 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- WHGYBXFWUBPSRW-FOUAGVGXSA-N beta-cyclodextrin Chemical compound OC[C@H]([C@H]([C@@H]([C@H]1O)O)O[C@H]2O[C@@H]([C@@H](O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O[C@H]3O[C@H](CO)[C@H]([C@@H]([C@H]3O)O)O3)[C@H](O)[C@H]2O)CO)O[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@@H]3O[C@@H]1CO WHGYBXFWUBPSRW-FOUAGVGXSA-N 0.000 description 2
- 235000011175 beta-cyclodextrine Nutrition 0.000 description 2
- 239000001202 beta-cyclodextrine Substances 0.000 description 2
- FDJOLVPMNUYSCM-WZHZPDAFSA-L cobalt(3+);[(2r,3s,4r,5s)-5-(5,6-dimethylbenzimidazol-1-yl)-4-hydroxy-2-(hydroxymethyl)oxolan-3-yl] [(2r)-1-[3-[(1r,2r,3r,4z,7s,9z,12s,13s,14z,17s,18s,19r)-2,13,18-tris(2-amino-2-oxoethyl)-7,12,17-tris(3-amino-3-oxopropyl)-3,5,8,8,13,15,18,19-octamethyl-2 Chemical compound [Co+3].N#[C-].N([C@@H]([C@]1(C)[N-]\C([C@H]([C@@]1(CC(N)=O)C)CCC(N)=O)=C(\C)/C1=N/C([C@H]([C@@]1(CC(N)=O)C)CCC(N)=O)=C\C1=N\C([C@H](C1(C)C)CCC(N)=O)=C/1C)[C@@H]2CC(N)=O)=C\1[C@]2(C)CCC(=O)NC[C@@H](C)OP([O-])(=O)O[C@H]1[C@@H](O)[C@@H](N2C3=CC(C)=C(C)C=C3N=C2)O[C@@H]1CO FDJOLVPMNUYSCM-WZHZPDAFSA-L 0.000 description 2
- 239000008367 deionised water Substances 0.000 description 2
- 229910021641 deionized water Inorganic materials 0.000 description 2
- 239000000839 emulsion Substances 0.000 description 2
- 235000010445 lecithin Nutrition 0.000 description 2
- 239000000787 lecithin Substances 0.000 description 2
- 229940067606 lecithin Drugs 0.000 description 2
- 235000013336 milk Nutrition 0.000 description 2
- 239000008267 milk Substances 0.000 description 2
- 210000004080 milk Anatomy 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 235000015097 nutrients Nutrition 0.000 description 2
- -1 reserve temperature Substances 0.000 description 2
- 239000011715 vitamin B12 Substances 0.000 description 2
- 239000011647 vitamin D3 Substances 0.000 description 2
- OYHQOLUKZRVURQ-NTGFUMLPSA-N (9Z,12Z)-9,10,12,13-tetratritiooctadeca-9,12-dienoic acid Chemical compound C(CCCCCCC\C(=C(/C\C(=C(/CCCCC)\[3H])\[3H])\[3H])\[3H])(=O)O OYHQOLUKZRVURQ-NTGFUMLPSA-N 0.000 description 1
- 102000045595 Phosphoprotein Phosphatases Human genes 0.000 description 1
- 108700019535 Phosphoprotein Phosphatases Proteins 0.000 description 1
- AUNGANRZJHBGPY-SCRDCRAPSA-N Riboflavin Chemical compound OC[C@@H](O)[C@@H](O)[C@@H](O)CN1C=2C=C(C)C(C)=CC=2N=C2C1=NC(=O)NC2=O AUNGANRZJHBGPY-SCRDCRAPSA-N 0.000 description 1
- JETSKDPKURDVNI-UHFFFAOYSA-N [C].[Ca] Chemical compound [C].[Ca] JETSKDPKURDVNI-UHFFFAOYSA-N 0.000 description 1
- 125000001931 aliphatic group Chemical group 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 238000006701 autoxidation reaction Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 150000001732 carboxylic acid derivatives Chemical class 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 230000000295 complement effect Effects 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 239000007884 disintegrant Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000001804 emulsifying effect Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 125000002485 formyl group Chemical class [H]C(*)=O 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 150000002632 lipids Chemical class 0.000 description 1
- 239000000314 lubricant Substances 0.000 description 1
- 239000011159 matrix material Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 229910021645 metal ion Inorganic materials 0.000 description 1
- 239000011785 micronutrient Substances 0.000 description 1
- 235000013369 micronutrients Nutrition 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 235000010755 mineral Nutrition 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 150000002978 peroxides Chemical class 0.000 description 1
- 235000020777 polyunsaturated fatty acids Nutrition 0.000 description 1
- 238000007348 radical reaction Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000002893 slag Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 235000021081 unsaturated fats Nutrition 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 239000011716 vitamin B2 Substances 0.000 description 1
- 150000003722 vitamin derivatives Chemical class 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L11/00—Pulses, i.e. fruits of leguminous plants, for production of food; Products from legumes; Preparation or treatment thereof
- A23L11/05—Mashed or comminuted pulses or legumes; Products made therefrom
- A23L11/07—Soya beans, e.g. oil-extracted soya bean flakes
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
- A23L29/30—Foods or foodstuffs containing additives; Preparation or treatment thereof containing carbohydrate syrups; containing sugars; containing sugar alcohols, e.g. xylitol; containing starch hydrolysates, e.g. dextrin
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
- A23L29/30—Foods or foodstuffs containing additives; Preparation or treatment thereof containing carbohydrate syrups; containing sugars; containing sugar alcohols, e.g. xylitol; containing starch hydrolysates, e.g. dextrin
- A23L29/35—Degradation products of starch, e.g. hydrolysates, dextrins; Enzymatically modified starches
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/16—Inorganic salts, minerals or trace elements
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23P—SHAPING OR WORKING OF FOODSTUFFS, NOT FULLY COVERED BY A SINGLE OTHER SUBCLASS
- A23P10/00—Shaping or working of foodstuffs characterised by the products
- A23P10/30—Encapsulation of particles, e.g. foodstuff additives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Abstract
The invention provides a kind of oxidative rancidity prevention and control new technology of the calcareous nourishing reinforced food of beans base, it is core by 20 50% calcium carbonate, using 40 85% soy meals, 10 20% maltodextrins, 5 15% malt syrups as compound wall materialses, 70 90 DEG C dissolve by heating and are well mixed, material liquid solid content 15 40%, the 25min of feed liquid homogenization 15 after dissolving, the 30MPa of homogenization pressure 25, microencapsulation calcium is finally prepared using spray drying technology, embedding rate is up to more than 90%.Microencapsulation calcium prepared by this technology method, it can effectively prevent that free calcium ions caused by hardening agent from directly contacting with fat in nutrition bag and accelerates its oxidation, the rance generation of nutrition bag fat oxidation is prevented or alleviates, so as to ensure that nutrition is contracted for fixed output quotas the stability of quality.
Description
One, technical fields
Nourishing reinforced food oxidative rancidity Control Technology field.
Two, background technologies
（1）Infant's diatery supplement nutrition bag, it is a kind of (vitamin and mineral of nutrient containing lot of trace referred to as " nutrition bag "
Deng) complementary goods, wherein with or without food matrix or other auxiliary materials, add and eaten in the instant diatery supplement of (6 ~ 36) monthly age infant
With, it can also be used to (37 ~ 60) monthly age children.
Nutrition bag is by the instant bean no less than 70%, adds lot of trace nutrient, adds or does not add whole-fat milk powder
The hybrid packed product formed.Due to containing a certain amount of polyunsaturated fatty acid (linoleic acid, Asia in raw material bean powder and whole-fat milk powder
Numb acid), radical reaction easily occurs in storage for these unsaturated fats causes oxidation deterioration, produce peroxide,
The material such as aldehyde or carboxylic acid, nutrition is contracted for fixed output quotas and give birth to unpleasant rancidity, high risks also are caused simultaneously to infant's body
The quality of product is had a strong impact on, huge loss is brought to manufacturing enterprise.Therefore, finding out influences infant's diatery supplement nutrition bag fat
The key factor of oxidation is simultaneously controlled to these factors, and have become that each infant's diatery supplement nutrition bag manufacturing enterprise faces works as
Business is anxious.
According to the literature, the degree of unsaturation of aliphatic acid, reserve temperature, oxygen, moisture, metal class, pH are
Influence the principal element of fat oxidation.Metal ion is the good catalyst of lipid autoxidation, in accelerated oxidation experiment, is added
The formula of carbon calcium and (or) ferric pyrophosphate is added rancidity occur.And the formula of calcium carbonate is added rancid once occurring in week
Taste, show that calcium carbonate has large effect to the stability of nutrition bag.
（2）Application for a patent for invention number 201510766034.6：
A kind of children pregnant woman's calcium tablet, it contains following component：Microencapsulation calcium 200-500 parts by weight, the weight of casein phosphatase 11-10
Measure part, vitamin D30.1-1 parts by weight.
Preferably, the calcium tablet contains following component：The parts by weight of microencapsulation calcium 350, the weight of CPP 6
Part, vitamin D30.2 parts by weight.
It is further preferred that the microencapsulation calcium is prepared in accordance with the following methods：
1) by the powder that tricalcium phosphate ultramicro grinding to particle diameter is 10-50 microns, then plus water stirs, and weight concentration is made
For 10-30% tricalcium phosphate slip；2) Arabic gum, β-cyclodextrine, lecithin, lactalbumin are added to the water, stirred
The emulsion that solid content is 5-20%, the Arabic gum, β-cyclodextrine, lecithin, the weight of lactalbumin are made after mixing
Than being followed successively by (0.5-2)：(2-8)：(5-15)：(0.5-2) ；
The tricalcium phosphate slip and the emulsion are pressed 1：2-5 volume ratio mixing, emulsifying, is then sprayed
Dry, obtained white solid powder is microencapsulation calcium.It is further preferred that the calcium tablet is also containing pharmaceutically acceptable
Auxiliary material, the auxiliary material include filler, lubricant, disintegrant, flavouring.
The three, content of the invention
（1）The problem of existing for prior art, the invention provides a kind of oxidative rancidity of the calcareous nourishing reinforced food of beans base
Prevention and control new technology, to prevent Creta Preparata produces free calcium ion and directly contacted with fat in nutrition bag from accelerating its oxidation.
（2）To solve the problems, such as set forth above adopted the technical scheme that：
A kind of calcareous nourishing reinforced food of beans base of calcium microencapsulation, it uses bean powder, maltodextrin, malt syrup as wall material, right
Calcium carbonate carries out microencapsulation, so as to effectively prevent or mitigate the rance generation of nutrition bag fat oxidation, effectively extends nutrition bag
Shelf-life, increase product stability.
The calcareous nourishing reinforced food of beans base contains following component：Soy meal 50 ~ 85%, microencapsulation calcium 20 ~ 50%, premix
0.5-1%, premix contain embedding ferric pyrophosphate, zinc oxide, vitamin A, vitamin D, vitamin B1, vitamin B2, folic acid, dimension
Raw plain B12。
To realize the purpose of the oxidative rancidity prevention and control of the calcareous nourishing reinforced food of beans base, its microencapsulation calcium method includes following
Step：
1. prepare core：By 20-50% calcium carbonate, add in 5-20% deionized waters, stir, obtain core material solution；2. prepare
Wall material：40-85% soy meals, 10-20% maltodextrins, 5-15% malt syrups are compound wall materialses；
It is 3. high-pressure homogeneous：It is 70-90% in mass ratio by above-mentioned core material solution and wall material solution：10-30% is mixed and heated dissolving,
Solution temperature is 70-90 DEG C, then adds homogenizer and carries out homogenization 15-25min, homogenization pressure 20-30mpa, solid content
15-40%；
4. spray drying：The slurry of above-mentioned gained is spray-dried, 180-200 DEG C of EAT, leaving air temp 75-85
DEG C, vacuum pressure maintains 2.3-3.7kpa, flow velocity 10-15ml/min, obtain it is aqueous be divided into 3-6% dried powders, obtain granularity
Distribution is 80-120 mesh, and obtained solid powder is microencapsulation calcium, and embedding rate is up to more than 90%.
（3）Beneficial effects of the present invention：
1. microencapsulation calcium prepared by the inventive method, it can effectively prevent free calcium ions caused by hardening agent and fat in nutrition bag
Directly contact and accelerate its oxidation, the rance generation of nutrition bag fat oxidation is prevented or alleviate, so as to ensure that nutrition bag
The stability of product quality.
It is made 2. microencapsulation calcium prepared by the present invention is calcium carbonate through bean powder, maltodextrin and malt syrup microencapsulation, with
Other calcium sources are compared, and micronutrient levels is high, and bioavilability is more preferable, and water solubility significantly improves, and have good point in water
Dissipate property, in good taste, no granulated slag sense, free from extraneous odour.
3. preparation method technique of the present invention is simple, simple to operate, power consumption is low, and cost is low, easily realizes industrialized production.
Four, embodiments
Specific embodiment one：
A kind of calcareous nourishing reinforced food of beans base of calcium microencapsulation, it is consisted of the following composition：Soy meal 50 ~ 85%, microencapsulation calcium
20 ~ 50%, premix 0.5-1%, premix contain embedding ferric pyrophosphate, zinc oxide, vitamin A, vitamin D, vitamin B1, dimension
Raw plain B2, folic acid, vitamin B12.Microencapsulation calcium is that main preparation methods are as follows：
1. prepare core：By 20% calcium carbonate, add in 5% deionized water, stir, obtain core material solution；2. prepare wall material：
40% soy meal, 10% maltodextrin, 5% malt syrup are compound wall materialses；
It is 3. high-pressure homogeneous：It is 70% in mass ratio by above-mentioned core material solution and wall material solution：10% is mixed and heated dissolving, dissolving temperature
Spend for 70 DEG C, then add homogenizer and carry out homogenization 15min, homogenization pressure 20mpa, solid content 15%；
4. spray drying：The slurry of above-mentioned gained is spray-dried, 180 DEG C of EAT, 75 DEG C of leaving air temp, vacuum pressure
Power maintains 2.3kpa, flow velocity 10ml/min, obtain it is aqueous be divided into 3% dried powder, it is 80 mesh to obtain particle size distribution, is obtained
To solid powder be microencapsulation calcium, embedding rate is up to more than 90%.
Specific embodiment two：
A kind of calcareous nourishing reinforced food of beans base of calcium microencapsulation, it is consisted of the following composition：Soy meal 50 ~ 85%, microencapsulation calcium
20 ~ 50%, premix 0.5-1%, premix contain embedding ferric pyrophosphate, zinc oxide, vitamin A, vitamin D, vitamin B1, dimension
Raw plain B2, folic acid, vitamin B12.Microencapsulation calcium is that main preparation methods are as follows：
1. prepare core：By 50% calcium carbonate, add in 20% deionized water, stir, obtain core material solution；2. prepare wall material：
85% soy meal, 20% maltodextrin, 15% malt syrup are compound wall materialses；
It is 3. high-pressure homogeneous：It is 90% in mass ratio by above-mentioned core material solution and wall material solution：30% is mixed and heated dissolving, dissolving temperature
Spend for 90 DEG C, then add homogenizer and carry out homogenization 25min, homogenization pressure 30mpa, solid content 40%；
4. spray drying：The slurry of above-mentioned gained is spray-dried, 200 DEG C of EAT, 85 DEG C of leaving air temp, vacuum pressure
Power maintains 3.7kpa, flow velocity 15ml/min, obtain it is aqueous be divided into 6% dried powder, it is 120 mesh to obtain particle size distribution, is obtained
To solid powder be microencapsulation calcium, embedding rate is up to more than 90%.
Claims (1)
1. a kind of oxidative rancidity Control Technology of the calcareous nourishing reinforced food of beans base, it is characterised in that by calcium carbonate microencapsulation, system
Preparation Method is as follows：
（1）Core is prepared：By 20-50% calcium carbonate, add in 5-20% deionized waters, stir, obtain core material solution；（2）.
Prepare wall material：40-85% soy meals, 10-20% maltodextrins, 5-15% malt syrups are compound wall materialses；
（3）It is high-pressure homogeneous：It is 70-90% in mass ratio by above-mentioned core material solution and wall material solution：10-30% is mixed and heated molten
Solution, solution temperature are 70-90 DEG C, then add homogenizer and carry out homogenization 15-25min, homogenization pressure 20-30mpa, admittedly contain
Measure 15-40%；
（4）It is spray-dried：The slurry of above-mentioned gained is spray-dried, 180-200 DEG C of EAT, leaving air temp 75-85
DEG C, vacuum pressure maintains 2.3-3.7kpa, flow velocity 10-15ml/min, obtain it is aqueous be divided into 3-6% dried powders, obtain granularity
Distribution is 80-120 mesh, and obtained solid powder is microencapsulation calcium, and embedding rate is up to more than 90%.
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| CN108851155A (en) * | 2018-07-11 | 2018-11-23 | 天添爱(青岛)生物科技有限公司 | A kind of technique extending the diatery supplement nutrient supplement shelf-life |
| CN109645493A (en) * | 2018-11-29 | 2019-04-19 | 郑州瑞普生物工程有限公司 | A kind of ferric pyrophosphate production method made an addition in vegetable protein based food |
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| CN109645493A (en) * | 2018-11-29 | 2019-04-19 | 郑州瑞普生物工程有限公司 | A kind of ferric pyrophosphate production method made an addition in vegetable protein based food |
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Application publication date: 20171222 |