CN107488387A - A kind of waterproof color paint and preparation method thereof - Google Patents

A kind of waterproof color paint and preparation method thereof Download PDF

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Publication number
CN107488387A
CN107488387A CN201710864510.7A CN201710864510A CN107488387A CN 107488387 A CN107488387 A CN 107488387A CN 201710864510 A CN201710864510 A CN 201710864510A CN 107488387 A CN107488387 A CN 107488387A
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parts
preparation
mixture
oxide
powder
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CN201710864510.7A
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Chinese (zh)
Inventor
施享
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Maanshan Songhe Information Technology Co Ltd
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Maanshan Songhe Information Technology Co Ltd
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Priority to CN201710864510.7A priority Critical patent/CN107488387A/en
Publication of CN107488387A publication Critical patent/CN107488387A/en
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    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D131/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an acyloxy radical of a saturated carboxylic acid, of carbonic acid, or of a haloformic acid; Coating compositions based on derivatives of such polymers
    • C09D131/02—Homopolymers or copolymers of esters of monocarboxylic acids
    • C09D131/04—Homopolymers or copolymers of vinyl acetate
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/18—Fireproof paints including high temperature resistant paints
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/16—Halogen-containing compounds
    • C08K2003/162—Calcium, strontium or barium halides, e.g. calcium, strontium or barium chloride
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
    • C08K3/20—Oxides; Hydroxides
    • C08K3/22—Oxides; Hydroxides of metals
    • C08K2003/2237—Oxides; Hydroxides of metals of titanium
    • C08K2003/2241—Titanium dioxide
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
    • C08K3/20—Oxides; Hydroxides
    • C08K3/22—Oxides; Hydroxides of metals
    • C08K2003/2265—Oxides; Hydroxides of metals of iron
    • C08K2003/2268—Ferrous oxide (FeO)
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
    • C08K3/20—Oxides; Hydroxides
    • C08K3/22—Oxides; Hydroxides of metals
    • C08K2003/2296—Oxides; Hydroxides of metals of zinc
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K2201/00—Specific properties of additives
    • C08K2201/011—Nanostructured additives
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2201/00—Properties
    • C08L2201/02—Flame or fire retardant/resistant
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2201/00—Properties
    • C08L2201/08—Stabilised against heat, light or radiation or oxydation
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00—Polymer mixtures characterised by other features
    • C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
    • C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Paints Or Removers (AREA)
  • Compositions Of Macromolecular Compounds (AREA)

Abstract

The present invention relates to a kind of waterproof color paint and preparation method thereof, raw material constituent is made up of following ratio in parts by weight：15 20 parts of acrylic resin, 10 15 parts of alkyd resin, 48 parts of silicone resin powder, 35 parts of mica powder, 25 parts of ferrous oxide, 36 parts of nano zine oxide, 24 parts of nano titanium oxide, 30 45 parts of acrylate and vinyl acetate emulsion, 24 parts of polyoxyethylene polyoxypropylene polyethers, 23 parts of lauryl sodium sulfate, 13 parts of calcium sulphoaluminate, 23 parts of calcium chloride, 10 20 parts of deionized water.Material of the present invention is easy to get, and cost is low, environment-friendly and green, and color is full, glossiness is high, and abrasion resistant effect is good, insulation fire prevention, fire-proof and damp-proof, has excellent light resistance, and ageing resistance is strong, increases the service life, and construction is convenient, applied widely.

Description

A kind of waterproof color paint and preparation method thereof
Technical field
The present invention relates to paint field, and in particular to a kind of waterproof color paint and preparation method thereof.
Background technology
Paint belongs to high-molecular organic material, and the film category formed is with high-molecular compound type, with the hair of science and technology Exhibition, existing coating are progressively turning into the engineering material of a kind of more effects, are an important industries in Chemical Engineering.But Existing paint is not very excellent in the performance of anti-aging, glossiness, the waterproof of dyeing etc., and has with substantial amounts of formaldehyde etc. Evil material, is unfavorable for health, is not suitable for long-run development, is phased out, so needing raising performance more excellent Paint.
The content of the invention
A kind of waterproof color paint and preparation method thereof is provided the invention aims to overcome the shortcomings of the above.
Technical scheme includes：A kind of waterproof color paint and preparation method thereof, raw material constituent is by weight Number is made up of following ratio：Acrylic resin 15-20 parts, alkyd resin 10-15 parts, silicone resin powder 4-8 parts, mica powder 3-5 parts, ferrous oxide 2-5 parts, nano zine oxide 3-6 parts, nano titanium oxide 2-4 parts, acrylate and vinyl acetate emulsion 30-45 parts, polyoxy second Alkene polyoxypropylene polyether 2-4 parts, lauryl sodium sulfate 2-3 parts, calcium sulphoaluminate 1-3 parts, calcium chloride 2-3 parts, deionized water 10- 20 parts.
Further improvement of the present invention is：Its preparation method is as follows：
A, mica powder, ferrous oxide, nano zine oxide and nano titanium oxide are added in deionized water by suitable proportion, become It is scattered through high speed in frequency high-speed dispersing kettle, then uniform extender paste is made after being ground in colloid mill, then move into and mix slowly in kettle, add Entering acrylate and vinyl acetate emulsion, polyoxyethylene polyoxypropylene polyethers, lauryl sodium sulfate, calcium sulphoaluminate and calcium chloride, stir speed (S.S.) is 450-550r/min, mixture A is obtained after stirring；
B, acrylic resin and alkyd resin are allocated, adds silicone resin powder and carry out dissolving copolymerization, temperature is set to 250-280 DEG C, pressure is set to 1.6-1.8MPa, obtains mixture B；
C, mixture B is put into mixture A and be stirred, stir speed (S.S.) 600-750r/min, by the production after stirring Thing is distilled, and vapo(u)rizing temperature is 100-120 DEG C, leaves and takes viscous liquid, obtains product.
Beneficial effects of the present invention：Material of the present invention is easy to get, and cost is low, environment-friendly and green, and color is full, glossiness is high, resistance to It is good to grind effect, insulation fire prevention, fire-proof and damp-proof, there is excellent light resistance, ageing resistance is strong, increases the service life, and construction is just Victory, it is applied widely.
Embodiment：
In order to deepen the understanding of the present invention, below in conjunction with embodiment, the invention will be further described, and the embodiment is only used In explaining the present invention, it is not intended to limit the scope of the present invention..
Embodiment 1
A kind of waterproof color paint and preparation method thereof, raw material constituent is made up of following ratio in parts by weight：Acrylic acid 15 parts of resin, 15 parts of alkyd resin, 4 parts of silicone resin powder, 5 parts of mica powder, 2 parts of ferrous oxide, 6 parts of nano zine oxide, receive 2 parts of titanium dioxide of rice, 45 parts of acrylate and vinyl acetate emulsion, 2 parts of polyoxyethylene polyoxypropylene polyethers, 3 parts of lauryl sodium sulfate, calcium sulphoaluminate 1 part, 3 parts of calcium chloride, 10 parts of deionized water.
Its preparation method is as follows：
A, mica powder, ferrous oxide, nano zine oxide and nano titanium oxide are added in deionized water by suitable proportion, become It is scattered through high speed in frequency high-speed dispersing kettle, then uniform extender paste is made after being ground in colloid mill, then move into and mix slowly in kettle, add Entering acrylate and vinyl acetate emulsion, polyoxyethylene polyoxypropylene polyethers, lauryl sodium sulfate, calcium sulphoaluminate and calcium chloride, stir speed (S.S.) is 450r/min, mixture A is obtained after stirring；
B, acrylic resin and alkyd resin are allocated, adds silicone resin powder and carry out dissolving copolymerization, temperature is set to 280 DEG C, pressure is set to 1.6MPa, obtains mixture B；
C, mixture B is put into mixture A and be stirred, stir speed (S.S.) 750r/min, the product after stirring entered Row distillation, vapo(u)rizing temperature are 100 DEG C, leave and take viscous liquid, obtain product.
Embodiment 2
A kind of waterproof color paint and preparation method thereof, raw material constituent is made up of following ratio in parts by weight：Acrylic acid 20 parts of resin, 10 parts of alkyd resin, 8 parts of silicone resin powder, 3 parts of mica powder, 5 parts of ferrous oxide, 3 parts of nano zine oxide, receive 4 parts of titanium dioxide of rice, 30 parts of acrylate and vinyl acetate emulsion, 4 parts of polyoxyethylene polyoxypropylene polyethers, 2 parts of lauryl sodium sulfate, calcium sulphoaluminate 3 parts, 2 parts of calcium chloride, 20 parts of deionized water.
Its preparation method is as follows：
A, mica powder, ferrous oxide, nano zine oxide and nano titanium oxide are added in deionized water by suitable proportion, become It is scattered through high speed in frequency high-speed dispersing kettle, then uniform extender paste is made after being ground in colloid mill, then move into and mix slowly in kettle, add Entering acrylate and vinyl acetate emulsion, polyoxyethylene polyoxypropylene polyethers, lauryl sodium sulfate, calcium sulphoaluminate and calcium chloride, stir speed (S.S.) is 550r/min, mixture A is obtained after stirring；
B, acrylic resin and alkyd resin are allocated, adds silicone resin powder and carry out dissolving copolymerization, temperature is set to 250 DEG C, pressure is set to 1.8MPa, obtains mixture B；
C, mixture B is put into mixture A and be stirred, stir speed (S.S.) 600r/min, the product after stirring entered Row distillation, vapo(u)rizing temperature are 120 DEG C, leave and take viscous liquid, obtain product.
Embodiment 3
A kind of waterproof color paint and preparation method thereof, raw material constituent is made up of following ratio in parts by weight：Acrylic acid 18 parts of resin, 14 parts of alkyd resin, 6 parts of silicone resin powder, 4 parts of mica powder, 4 parts of ferrous oxide, 5 parts of nano zine oxide, receive 3 parts of titanium dioxide of rice, 40 parts of acrylate and vinyl acetate emulsion, 3 parts of polyoxyethylene polyoxypropylene polyethers, 3 parts of lauryl sodium sulfate, calcium sulphoaluminate 2 parts, 2 parts of calcium chloride, 18 parts of deionized water.
Its preparation method is as follows：
A, mica powder, ferrous oxide, nano zine oxide and nano titanium oxide are added in deionized water by suitable proportion, become It is scattered through high speed in frequency high-speed dispersing kettle, then uniform extender paste is made after being ground in colloid mill, then move into and mix slowly in kettle, add Entering acrylate and vinyl acetate emulsion, polyoxyethylene polyoxypropylene polyethers, lauryl sodium sulfate, calcium sulphoaluminate and calcium chloride, stir speed (S.S.) is 500r/min, mixture A is obtained after stirring；
B, acrylic resin and alkyd resin are allocated, adds silicone resin powder and carry out dissolving copolymerization, temperature is set to 260 DEG C, pressure is set to 1.7MPa, obtains mixture B；
C, mixture B is put into mixture A and be stirred, stir speed (S.S.) 720r/min, the product after stirring entered Row distillation, vapo(u)rizing temperature are 140 DEG C, leave and take viscous liquid, obtain product.
Embodiment 4
A kind of waterproof color paint and preparation method thereof, raw material constituent is made up of following ratio in parts by weight：Acrylic acid 17 parts of resin, 12 parts of alkyd resin, 5 parts of silicone resin powder, 4 parts of mica powder, 3 parts of ferrous oxide, 5 parts of nano zine oxide, receive 3 parts of titanium dioxide of rice, 40 parts of acrylate and vinyl acetate emulsion, 3 parts of polyoxyethylene polyoxypropylene polyethers, 2 parts of lauryl sodium sulfate, calcium sulphoaluminate 1 part, 2 parts of calcium chloride, 15 parts of deionized water.
Its preparation method is as follows：
A, mica powder, ferrous oxide, nano zine oxide and nano titanium oxide are added in deionized water by suitable proportion, become It is scattered through high speed in frequency high-speed dispersing kettle, then uniform extender paste is made after being ground in colloid mill, then move into and mix slowly in kettle, add Entering acrylate and vinyl acetate emulsion, polyoxyethylene polyoxypropylene polyethers, lauryl sodium sulfate, calcium sulphoaluminate and calcium chloride, stir speed (S.S.) is 490r/min, mixture A is obtained after stirring；
B, acrylic resin and alkyd resin are allocated, adds silicone resin powder and carry out dissolving copolymerization, temperature is set to 270 DEG C, pressure is set to 1.7MPa, obtains mixture B；
C, mixture B is put into mixture A and be stirred, stir speed (S.S.) 650r/min, the product after stirring entered Row distillation, vapo(u)rizing temperature are 110 DEG C, leave and take viscous liquid, obtain product.
In above example, embodiment 3 is most preferred embodiment, and chroma-luminance is high, antiageing effect is good, and water proofing property is strong；On Energy waste can effectively be reduced using frequency-conversion high-speed Scattered Kettle by stating in step A, improve dispersing uniformity.
Explanation embodiments of the present invention are the foregoing is only, are not intended to limit the invention, for the technology of this area For personnel, within the spirit and principles of the invention, any modification, equivalent substitution and improvements made etc., it should be included in Within protection scope of the present invention.

Claims (2)

  1. A kind of 1. waterproof color paint and preparation method thereof, it is characterised in that：Raw material constituent in parts by weight by comparing below Example composition：Acrylic resin 15-20 parts, alkyd resin 10-15 parts, silicone resin powder 4-8 parts, mica powder 3-5 parts, oxidation are sub- Iron 2-5 parts, nano zine oxide 3-6 parts, nano titanium oxide 2-4 parts, acrylate and vinyl acetate emulsion 30-45 parts, polyoxyethylene polyoxypropylene gather Ether 2-4 parts, lauryl sodium sulfate 2-3 parts, calcium sulphoaluminate 1-3 parts, calcium chloride 2-3 parts, deionized water 10-20 parts.
  2. A kind of 2. waterproof color paint according to claim 1 and preparation method thereof, it is characterised in that：Its preparation method is such as Under：
    A, mica powder, ferrous oxide, nano zine oxide and nano titanium oxide are added in deionized water by suitable proportion, become It is scattered through high speed in frequency high-speed dispersing kettle, then uniform extender paste is made after being ground in colloid mill, then move into and mix slowly in kettle, add Entering acrylate and vinyl acetate emulsion, polyoxyethylene polyoxypropylene polyethers, lauryl sodium sulfate, calcium sulphoaluminate and calcium chloride, stir speed (S.S.) is 450-550r/min, mixture A is obtained after stirring；
    B, acrylic resin and alkyd resin are allocated, adds silicone resin powder and carry out dissolving copolymerization, temperature is set to 250-280 DEG C, pressure is set to 1.6-1.8MPa, obtains mixture B；
    C, mixture B is put into mixture A and be stirred, stir speed (S.S.) 600-750r/min, by the production after stirring Thing is distilled, and vapo(u)rizing temperature is 100-120 DEG C, leaves and takes viscous liquid, obtains product.
CN201710864510.7A 2017-09-22 2017-09-22 A kind of waterproof color paint and preparation method thereof Withdrawn CN107488387A (en)

Priority Applications (1)

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Application Number Priority Date Filing Date Title
CN201710864510.7A CN107488387A (en) 2017-09-22 2017-09-22 A kind of waterproof color paint and preparation method thereof

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109705691A (en) * 2019-01-22 2019-05-03 段小宁 A kind of preparation method of fast, waterproof the aqueous, environmental protective paint of film forming

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109705691A (en) * 2019-01-22 2019-05-03 段小宁 A kind of preparation method of fast, waterproof the aqueous, environmental protective paint of film forming

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Application publication date: 20171219

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