CN107459924A - A kind of woven bag surface flame-retardant dope layer - Google Patents
A kind of woven bag surface flame-retardant dope layer Download PDFInfo
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- CN107459924A CN107459924A CN201710850490.8A CN201710850490A CN107459924A CN 107459924 A CN107459924 A CN 107459924A CN 201710850490 A CN201710850490 A CN 201710850490A CN 107459924 A CN107459924 A CN 107459924A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D179/00—Coating compositions based on macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing nitrogen, with or without oxygen, or carbon only, not provided for in groups C09D161/00 - C09D177/00
- C09D179/04—Polycondensates having nitrogen-containing heterocyclic rings in the main chain; Polyhydrazides; Polyamide acids or similar polyimide precursors
- C09D179/08—Polyimides; Polyester-imides; Polyamide-imides; Polyamide acids or similar polyimide precursors
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/18—Fireproof paints including high temperature resistant paints
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/02—Elements
- C08K2003/026—Phosphorus
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/02—Flame or fire retardant/resistant
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
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- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Compositions Of Macromolecular Compounds (AREA)
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Abstract
The present invention provides a kind of woven bag surface flame-retardant dope layer, and mass fraction shared by its constituent and each composition is respectively:Resin base:34~52 parts, surfactant:2~5 parts, fire retardant:5~7 parts, renovation agent:5~9 parts, carbonized agent:3~7 parts, expansible graphite:3~7 parts;Resin base includes M-and P-cresols, polyester imine resin, polyhydroxy acrylic resin;Fire retardant includes acidic silicasol, acidifying castor oil, tetrahydrochysene methylsulfuric acid, Wrapped up Phosphorus Fire Retardant;Renovation agent includes mineral oil, repairing activity agent, nano-sized carbon.Constituent of the present invention and proportioning are unique, while preparation method simple and fast;Also there is obvious repairing performance while outstanding anti-flammability is ensured, for maintaining the every mechanical performance and anti-flammability of woven bag bodies that there is remarkable result;Component easily obtains, lower cost, is adapted to promote in medium-sized and small enterprises.
Description
Technical field
The invention belongs to technical field of coatings, and in particular to a kind of woven bag surface flame-retardant dope layer.
Background technology
Woven bag is also known as snakeskin bag, is one kind of polybag, and for packing, its raw material is usually polyethylene, polypropylene etc.
Various Xylonite raw materials, it is mainly used in storage transport article;The fusing point of existing woven bag is relatively low, easily by kindling material, very
Burnt under to hot environment, the article in woven bag is caused to damage;
Therefore, it is art technology to develop the flame retardant coating on a kind of flame retardant woven bag or woven bag surface for problem above
Personnel institute urgent need to solve the problem.
The content of the invention
To solve the above problems, the invention discloses a kind of woven bag surface flame-retardant dope layer;
In order to achieve the above object, the present invention provides following technical scheme:
Mass fraction shared by a kind of woven bag surface flame-retardant dope layer, its constituent and each composition is respectively:Resin base:
34~52 parts, surfactant:2~5 parts, fire retardant:5~7 parts, renovation agent:5~9 parts, carbonized agent:3~7 parts, inflatable stone
Ink:3~7 parts;The number of resin base quality is respectively shared by the constituent of resin base and each composition:M-and P-cresols:4
~7 parts, polyester imine resin:3~7 parts, polyhydroxy acrylic resin:2~5 parts;The constituent of fire retardant and each composition
The number of shared fire retardant quality is respectively:Acidic silicasol:3~7 parts, acidifying castor oil:2~5 parts, tetrahydrochysene methylsulfuric acid:1
~3 parts, Wrapped up Phosphorus Fire Retardant:2~5 parts;The number of renovation agent quality shared by the constituent of renovation agent and each composition point
It is not:Mineral oil:7~15 parts, repairing activity agent:2~5 parts, nano-sized carbon:3~5 parts;
Further, its preparation method is:
(1)Polyester imine resin in resin base, polyhydroxy acrylic resin are mixed with surfactant and fire retardant,
And be dissolved in M-and P-cresols, 65~80 DEG C are warming up to, stirs and is incubated 0.5~1h;After being warming up to 85~90 DEG C, add
Renovation agent, it is again stirring for uniformly, and is incubated 1~2h, obtains paint-based bottom;
(2)Expansible graphite is ground into homogeneous;
(3)Successively by step(2)Expansible graphite and carbonized agent after the grinding homogeneous of middle acquisition are added to step(1)In
In paint-based bottom, stir, obtain anti-flaming dope;
Further, the meta content of M-and P-cresols is not less than 50%;Surfactant is fluorocarbon surfactant;Carbonized agent is
Polyphosphoric acid amine;Fire retardant is Wrapped up Phosphorus Fire Retardant;
Further, repairing activity agent is the chain compound containing siloxanes or the chain compound containing succimide
In any one;
Preferably, mass fraction shared by constituent and each composition is respectively:Resin base:40~48 parts, surface-active
Agent:3~5 parts, fire retardant:6~7 parts, renovation agent:6~8 parts, carbonized agent:4~5 parts, expansible graphite:4~6 parts;
The number of resin base quality is respectively shared by the constituent of resin base and each composition:M-and P-cresols:4~7 parts,
Polyester imine resin:3~7 parts, polyhydroxy acrylic resin:2~5 parts;The constituent of fire retardant and the shared resistance of each composition
Combustion agent quality number be respectively:Acidic silicasol:3~7 parts, acidifying castor oil:2~5 parts, tetrahydrochysene methylsulfuric acid:1~3 part,
Wrapped up Phosphorus Fire Retardant:2~5 parts;The number of renovation agent quality is respectively shared by the constituent of renovation agent and each composition:Ore deposit
Thing oil:7~15 parts, repairing activity agent:2~5 parts, nano-sized carbon:3~5 parts;
Preferably, mass fraction shared by constituent and each composition is respectively:Resin base:44 parts, surfactant:4
Part, fire retardant:6 parts, renovation agent:7 parts, carbonized agent:5 parts, expansible graphite:5 parts;The constituent of resin base and respectively into
The number of resin base quality is respectively shared by point:M-and P-cresols:6 parts, polyester imine resin:5 parts, polyhydroxy acrylic acid tree
Fat:4 parts;The number of fire retardant quality is respectively shared by the constituent of fire retardant and each composition:Acidic silicasol:5 parts, acid
Change castor oil:3 parts, tetrahydrochysene methylsulfuric acid:2 parts, Wrapped up Phosphorus Fire Retardant:4 parts;The constituent of renovation agent and each composition institute
The number for accounting for renovation agent quality is respectively:Mineral oil:11 parts, repairing activity agent:4 parts, nano-sized carbon:4 parts;
The invention provides a kind of woven bag surface flame-retardant dope layer, by resin base, surfactant, fire retardant, renovation agent,
Carbonized agent and expansible graphite composition, wherein resin base is by M-and P-cresols, polyester imine resin and polyhydroxy acrylic acid
Resin is formed, and based on polyester imine resin, is dissolved in together with polyhydroxy acrylic resin in M-and P-cresols, as the present invention
Coating vehicles, on the one hand can ensure mechanical performance, electrical insulating property, heat-resisting quantity and wear-resisting after anti-flaming dope shaping
Property, the properties and security of woven bag are effectively ensured, while can be used in dissolving mixing the present invention in fire retardant with
And renovation agent;Fire retardant can effectively strengthen the present invention anti-flammability, while the innovation being added in the present invention of renovation agent it
Place, is made up of mineral oil, repairing activity agent and nano-sized carbon, can ensure when certain of anti-flaming dope layer occurs damaged,
Effective diaphragm can be formed within a certain period of time by renovation agent, persistently carry out fire-resisting protection, be woven bag surface fracture
Detection and woven bag in the transfer of reserve provide valuable time;
And present invention also offers the preparation method of anti-flaming dope, method is simple, producing efficiency is high, is adapted to carry out the present invention
It is widely popularized;
Compared with prior art, constituent and proportioning are unique, while preparation method simple and fast by the present invention;It is outstanding in guarantee
Also there is obvious repairing performance, for maintaining the every mechanical performance and anti-flammability of woven bag bodies to have while anti-flammability
Remarkable result;Component easily obtains, lower cost, is adapted to promote in medium-sized and small enterprises.
Embodiment
Technical scheme provided by the invention is described in detail below with reference to specific embodiment, it should be understood that following specific
Embodiment is only illustrative of the invention and is not intended to limit the scope of the invention;
Embodiment 1:
Mass fraction shared by a kind of woven bag surface flame-retardant dope layer, its constituent and each composition is respectively:Resin base:
34 parts, surfactant:5 parts, fire retardant:7 parts, renovation agent:9 parts, carbonized agent:7 parts, expansible graphite:3 parts, wherein carbonizing
Agent is polyphosphoric acid amine;Fire retardant is Wrapped up Phosphorus Fire Retardant;Resin base shared by the constituent of resin base and each composition
The number of substrate amount is respectively:M-and P-cresols:4 parts, polyester imine resin:7 parts, polyhydroxy acrylic resin:5 parts, among it
The meta content of paracresol is not less than 50%;The number difference of fire retardant quality shared by the constituent of fire retardant and each composition
For:Acidic silicasol:3 parts, acidifying castor oil:5 parts, tetrahydrochysene methylsulfuric acid:3 parts, Wrapped up Phosphorus Fire Retardant:5 parts;Renovation agent
The number of renovation agent quality is respectively shared by constituent and each composition:Mineral oil:7 parts, repairing activity agent:5 part, nanometers
Carbon:5 parts, surfactant is fluorocarbon surfactant;Repairing activity agent is the chain compound containing siloxanes;
Its preparation method is:
(1)Polyester imine resin in resin base, polyhydroxy acrylic resin are mixed with surfactant and fire retardant,
And be dissolved in M-and P-cresols, 65 DEG C are warming up to, stirs and is incubated 0.5h;After being warming up to 85 DEG C, renovation agent is added, again
Stir, and be incubated 1h, obtain paint-based bottom;
(2)Expansible graphite is ground into homogeneous;
(3)Successively by step(2)Expansible graphite and carbonized agent after the grinding homogeneous of middle acquisition are added to step(1)In
In paint-based bottom, stir, obtain anti-flaming dope;
Embodiment 2:
Mass fraction shared by a kind of woven bag surface flame-retardant dope layer, its constituent and each composition is respectively:Resin base:
52 parts, surfactant:2 parts, fire retardant:5 parts, renovation agent:5 parts, carbonized agent:3 parts, expansible graphite:3 parts, wherein carbonizing
Agent is polyphosphoric acid amine;Fire retardant is Wrapped up Phosphorus Fire Retardant;Resin base shared by the constituent of resin base and each composition
The number of substrate amount is respectively:M-and P-cresols:7 parts, polyester imine resin:3 parts, polyhydroxy acrylic resin:2 parts, among it
The meta content of paracresol is not less than 50%;The number difference of fire retardant quality shared by the constituent of fire retardant and each composition
For:Acidic silicasol:7 parts, acidifying castor oil:2 parts, tetrahydrochysene methylsulfuric acid:1 part, Wrapped up Phosphorus Fire Retardant:2 parts;Renovation agent
The number of renovation agent quality is respectively shared by constituent and each composition:Mineral oil:15 parts, repairing activity agent:2 part, nanometers
Carbon:3 parts, surfactant is fluorocarbon surfactant;Repairing activity agent is in the chain compound containing succimide
Any one;
Its preparation method is:
(1)Polyester imine resin in resin base, polyhydroxy acrylic resin are mixed with surfactant and fire retardant,
And be dissolved in M-and P-cresols, 80 DEG C are warming up to, stirs and is incubated 1h;After being warming up to 90 DEG C, renovation agent is added, is stirred again
Mix uniformly, and be incubated 2h, obtain paint-based bottom;
(2)Expansible graphite is ground into homogeneous;
(3)Successively by step(2)Expansible graphite and carbonized agent after the grinding homogeneous of middle acquisition are added to step(1)In
In paint-based bottom, stir, obtain anti-flaming dope;
Embodiment 3:
Mass fraction shared by a kind of woven bag surface flame-retardant dope layer, its constituent and each composition is respectively:Resin base:
44 parts, surfactant:4 parts, fire retardant:6 parts, renovation agent:7 parts, carbonized agent:5 parts, expansible graphite:5 parts, wherein carbonizing
Agent is polyphosphoric acid amine;Fire retardant is Wrapped up Phosphorus Fire Retardant;Resin base shared by the constituent of resin base and each composition
The number of substrate amount is respectively:M-and P-cresols:6 parts, polyester imine resin:5 parts, polyhydroxy acrylic resin:4 parts, among it
The meta content of paracresol is not less than 50%;The number difference of fire retardant quality shared by the constituent of fire retardant and each composition
For:Acidic silicasol:5 parts, acidifying castor oil:3 parts, tetrahydrochysene methylsulfuric acid:2 parts, Wrapped up Phosphorus Fire Retardant:4 parts;Renovation agent
The number of renovation agent quality is respectively shared by constituent and each composition:Mineral oil:11 parts, repairing activity agent:4 part, nanometers
Carbon:4 parts, surfactant is fluorocarbon surfactant;Repairing activity agent is the chain compound containing siloxanes;
Its preparation method is:
(1)Polyester imine resin in resin base, polyhydroxy acrylic resin are mixed with surfactant and fire retardant,
And be dissolved in M-and P-cresols, 65~80 DEG C are warming up to, stirs and is incubated 0.5~1h;After being warming up to 85~90 DEG C, add
Renovation agent, it is again stirring for uniformly, and is incubated 1~2h, obtains paint-based bottom;
(2)Expansible graphite is ground into homogeneous;
(3)Successively by step(2)Expansible graphite and carbonized agent after the grinding homogeneous of middle acquisition are added to step(1)In
In paint-based bottom, stir, obtain anti-flaming dope;
The anti-flaming dope obtained by three above embodiment is respectively coated to not existing together on same woven bag surface, and simultaneously
Carry out combustion test, coat the three of anti-flaming dope be in just start experiment preceding 2min in it is unburned;It is fire-retardant in embodiment 1
Coating gradually melts after 2min, until during 2min5s, woven bag starts to burn;Anti-flaming dope in embodiment 2 is in 2min10s
When start to melt, until during 2min15s, woven bag starts to burn;Anti-flaming dope in embodiment 3 just starts to melt in 3min
Change, while can substantially observe fusing birth into thin film, until during 3min30s, film ruptures, and woven bag starts to fire
Burn;The anti-flaming dope that to sum up three above embodiment obtains has significant flame retardant effect, and the resistance of embodiment 3 to woven bag
Fuel efficiency fruit is optimal, and embodiment 3 is the optimum embodiment in three embodiments;
It is last it should be noted that the above embodiments are merely illustrative of the technical solutions of the present invention and non-limiting technical scheme,
It will be understood by those within the art that technical scheme is modified for those or equivalent substitution, without
Depart from the objective and scope of the technical program, all should cover among scope of the presently claimed invention.
Claims (6)
- A kind of 1. woven bag surface flame-retardant dope layer, it is characterised in that:Mass fraction shared by its constituent and each composition point It is not:Resin base:34~52 parts,Surfactant:2~5 parts,Fire retardant:5~7 parts,Renovation agent:5~9 parts,Carbonized agent:3~7 parts,Expansible graphite:3~7 parts;The number of resin base quality is respectively shared by the constituent of the resin base and each composition:M-and P-cresols:4~ 7 parts, polyester imine resin:3~7 parts, polyhydroxy acrylic resin:2~5 parts;The number of fire retardant quality is respectively shared by the constituent of the fire retardant and each composition:Acidic silicasol:3~7 Part, acidifying castor oil:2~5 parts, tetrahydrochysene methylsulfuric acid:1~3 part, Wrapped up Phosphorus Fire Retardant:2~5 parts;The number of renovation agent quality is respectively shared by the constituent of the renovation agent and each composition:Mineral oil:7~15 parts, Repairing activity agent:2~5 parts, nano-sized carbon:3~5 parts.
- A kind of 2. woven bag surface flame-retardant dope layer according to claim 1, it is characterised in that:Its preparation method is:(1)Polyester imine resin in resin base, polyhydroxy acrylic resin are mixed with surfactant and fire retardant, And be dissolved in M-and P-cresols, 65~80 DEG C are warming up to, stirs and is incubated 0.5~1h;After being warming up to 85~90 DEG C, add Renovation agent, it is again stirring for uniformly, and is incubated 1~2h, obtains paint-based bottom;(2)Expansible graphite is ground into homogeneous;(3)Successively by step(2)Expansible graphite and carbonized agent after the grinding homogeneous of middle acquisition are added to step(1)In In paint-based bottom, stir, obtain anti-flaming dope.
- A kind of 3. woven bag surface flame-retardant dope layer according to claim 1, it is characterised in that:Between the M-and P-cresols Position content is not less than 50%;The surfactant is fluorocarbon surfactant;The carbonized agent is polyphosphoric acid amine;The resistance Combustion agent is Wrapped up Phosphorus Fire Retardant.
- A kind of 4. woven bag surface flame-retardant dope layer according to claim 1, it is characterised in that:The repairing activity agent is Any one in chain compound containing siloxanes or the chain compound containing succimide.
- A kind of 5. woven bag surface flame-retardant dope layer according to claim 1, it is characterised in that:Its constituent and each Mass fraction is respectively shared by composition:Resin base:40~48 parts,Surfactant:3~5 parts,Fire retardant:6~7 parts,Renovation agent:6~8 parts,Carbonized agent:4~5 parts,Expansible graphite:4~6 parts;The number of resin base quality is respectively shared by the constituent of the resin base and each composition:M-and P-cresols:4~ 7 parts, polyester imine resin:3~7 parts, polyhydroxy acrylic resin:2~5 parts;The number of fire retardant quality is respectively shared by the constituent of the fire retardant and each composition:Acidic silicasol:3~7 Part, acidifying castor oil:2~5 parts, tetrahydrochysene methylsulfuric acid:1~3 part, Wrapped up Phosphorus Fire Retardant:2~5 parts;The number of renovation agent quality is respectively shared by the constituent of the renovation agent and each composition:Mineral oil:7~15 parts, Repairing activity agent:2~5 parts, nano-sized carbon:3~5 parts.
- A kind of 6. woven bag surface flame-retardant dope layer according to claim 1, it is characterised in that:Its constituent and each Mass fraction is respectively shared by composition:Resin base:44 parts,Surfactant:4 parts,Fire retardant:6 parts,Renovation agent:7 parts,Carbonized agent:5 parts,Expansible graphite:5 parts;The number of resin base quality is respectively shared by the constituent of the resin base and each composition:M-and P-cresols:6 Part, polyester imine resin:5 parts, polyhydroxy acrylic resin:4 parts;The number of fire retardant quality is respectively shared by the constituent of the fire retardant and each composition:Acidic silicasol:5 parts, It is acidified castor oil:3 parts, tetrahydrochysene methylsulfuric acid:2 parts, Wrapped up Phosphorus Fire Retardant:4 parts;The number of renovation agent quality is respectively shared by the constituent of the renovation agent and each composition:Mineral oil:11 parts, reparation Activating agent:4 parts, nano-sized carbon:4 parts.
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109166945A (en) * | 2018-08-17 | 2019-01-08 | 安徽英发三友新能源科技有限公司 | A kind of solar battery sheet sintering process |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN104293101A (en) * | 2014-09-25 | 2015-01-21 | 安徽蓝翔电器成套设备有限公司 | High-temperature-resistant insulating paint composition and preparation method thereof |
CN106633141A (en) * | 2016-12-28 | 2017-05-10 | 南京协和助剂有限公司 | Treatment technology for improving fire resistance of plastic surface |
-
2017
- 2017-09-20 CN CN201710850490.8A patent/CN107459924A/en active Pending
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN104293101A (en) * | 2014-09-25 | 2015-01-21 | 安徽蓝翔电器成套设备有限公司 | High-temperature-resistant insulating paint composition and preparation method thereof |
CN106633141A (en) * | 2016-12-28 | 2017-05-10 | 南京协和助剂有限公司 | Treatment technology for improving fire resistance of plastic surface |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN109166945A (en) * | 2018-08-17 | 2019-01-08 | 安徽英发三友新能源科技有限公司 | A kind of solar battery sheet sintering process |
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