CN107457408A - The sensing atomization of continous way cold crucible prepares titanium valve equipment - Google Patents

The sensing atomization of continous way cold crucible prepares titanium valve equipment Download PDF

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Publication number
CN107457408A
CN107457408A CN201710976948.4A CN201710976948A CN107457408A CN 107457408 A CN107457408 A CN 107457408A CN 201710976948 A CN201710976948 A CN 201710976948A CN 107457408 A CN107457408 A CN 107457408A
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CN
China
Prior art keywords
crucible
heater
cold
continous way
charging
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Pending
Application number
CN201710976948.4A
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Chinese (zh)
Inventor
牟鑫
马海玲
王勃
陈鼎
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SHENYANG VACUUM TECHNOLOGY INSTITUTE
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SHENYANG VACUUM TECHNOLOGY INSTITUTE
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Priority to CN201710976948.4A priority Critical patent/CN107457408A/en
Publication of CN107457408A publication Critical patent/CN107457408A/en
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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00Making metallic powder or suspensions thereof
    • B22F9/02Making metallic powder or suspensions thereof using physical processes
    • B22F9/06Making metallic powder or suspensions thereof using physical processes starting from liquid material
    • B22F9/08Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying
    • B22F9/082Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying atomising using a fluid
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22FWORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00Making metallic powder or suspensions thereof
    • B22F9/02Making metallic powder or suspensions thereof using physical processes
    • B22F9/06Making metallic powder or suspensions thereof using physical processes starting from liquid material
    • B22F9/08Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying
    • B22F9/082Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying atomising using a fluid
    • B22F2009/0844Making metallic powder or suspensions thereof using physical processes starting from liquid material by casting, e.g. through sieves or in water, by atomising or spraying atomising using a fluid in controlled atmosphere

Abstract

The invention belongs to vacuum metallurgy apparatus field, more particularly to a kind of sensing atomization of continous way cold crucible to prepare titanium valve equipment, including body of heater(1), high-pressure pipe(11), atomization storehouse(12)And vacuum system(3);Body of heater(1)Including material alloying mechanism(4), safety valve(5), infrared measurement of temperature mechanism(6), gravity material pawl charging mechanism(7), screw feed mechanism(8), explosion tapping equipment(10), smelting electrode(20), rising pouring electrode(21), cold-crucible system(13), melting induction coil(14), rising pouring induction coil(15)And annular distance shape spray disk(18);Gravity material pawl charging mechanism(7)Charging chamber on be transversely provided with pneumatic gate valve(22).The present invention can continuous production, flour extraction elevated oxygen level is low, and powder constitution and size tunable, device structure is simple, fabricates, easy for installation, energy-conserving and environment-protective low with maintenance cost, security is good.

Description

The sensing atomization of continous way cold crucible prepares titanium valve equipment
Technical field
The invention belongs to vacuum metallurgy apparatus field, more particularly to a kind of sensing atomization of continous way cold crucible to prepare titanium valve and set It is standby.
Background technology
Induction Melting Technology is a kind of advanced melting means, and it eliminates in fusion process atmosphere and heating source to furnace charge Pollution.It is especially vivaciously golden in melting but in general process for vacuum induction smelting can not prevent the reaction between furnace charge and crucible When category or high purity metal, this influence is very serious.There is a kind of more advanced cold crucible vacuum induction in last century end Melting technique.It is that one kind utilizes cold-crucible(Predominantly fine copper, also useful other alloys)To carry out vacuum induction melting Method.Such a method can exclude pollution of the crucible to furnace charge completely.
Cold crucible induction melting device mainly has three kinds of casting modes:Topple over casting (tilt-tapping) technology, uphill casting (bottom-tapping) technology, the uphill casting technology of floating type (lavitation type) cold crucible.
Topple over foundry engieering advantage be it is simple in construction be easy to implement, problem is, melt is the same as crucible wall when verting Contact area increases, and scull is significantly grown up, and the melt amount cast out is reduced.So casting should be as fast (generally at 3 seconds as possible Within).In addition, casting is just grown up rapidly once interrupting scull, need crucible going back to fusing scull in situ to recover casting, Repeatedly.
The problem of uphill casting technology of floating type cold crucible, is that the very big melt quality of suspension is had any problem, and only suspends at present Melting 5kg device, industrialized scale can't to be used for.
Therefore, uphill casting technology has the advantage of application.But its structure and technique are extremely complex.Require further study.
The content of the invention
It is contemplated that being provided in place of overcome the deficiencies in the prior art, a kind of energy consumption simple in construction is low, and operating efficiency is high, Powder quality is good and grain diameter of components is controllable, and security is good, and can realize and not destroy in stove under vacuum or atmosphere, not similar shape The addition of shape material, the powder by atomization equipment of continuous smelting is reached.
In order to solve the above technical problems, what the present invention was realized in:
A kind of continous way cold crucible sensing atomization prepares titanium valve equipment, including body of heater, high-pressure pipe, atomization storehouse and vacuum system System;The port of the vacuum system communicates with body of heater working chamber;The body of heater includes material alloying mechanism, safety valve, infrared survey Warm mechanism, gravity material pawl charging mechanism, screw feed mechanism, explosion tapping equipment, smelting electrode, rising pouring electrode, cold-crucible System, melting induction coil, rising pouring induction coil and annular distance shape spray disk;The material alloying mechanism, safety valve, infrared measurement of temperature machine Structure, gravity material pawl charging mechanism, the working end of screw feed mechanism and explosion tapping equipment communicate with body of heater working chamber respectively;Institute State melting induction coil and be fixed at cold-crucible system external wall of upper portion;The rising pouring induction coil is fixed at cold-crucible system System bottom outer wall;Ceramic spray pipe is provided with the cold-crucible system bottom;Ceramic conduit is provided with the ceramic spray pipe bottom; The ceramic conduit upper port is vertical with ceramic spray pipe base opening to be socketed, and sprays disk through annular distance shape;High pressure low temperature argon gas passes through The annular distance shape spray disk that high-pressure pipe enters in body of heater;Pneumatic insert is transversely provided with the charging chamber of the gravity material pawl charging mechanism Plate valve.
As a kind of preferred scheme, body of heater of the present invention can use vertical Kazakhstan shell Double water-cooled jacket structured.
Further, infrared measurement of temperature mechanism of the present invention can use ball pivot chain structure;The material alloying is in-house There are multiple independent charging cups.
Further, the present invention is connected in the body of heater inner chamber by pneumatic ball valve with screw feed mechanism cavity;Institute State screw feed mechanism bottom and be provided with blanking chute.
Further, the taper of ceramic spray pipe of the present invention is 90 °;The caliber of the ceramic spray pipe is DN20.
The present invention is simple in construction, and processing and manufacturing is low with maintenance cost, and easy for installation, security is easy to well equipment batch raw Production, due to, as atomization gas, saving source of the gas heating cost using high pressure low temperature argon gas and rapid improve of powder cooling is received Powder efficiency;The big scull of suspending power is few(Less than 10%)Flour extraction is high and scull repeats fusing, does not waste raw material;It can be achieved continuous Production reduces evacuation inflation link, substantially increases operating efficiency, reduces the wasting of resources, not strict to melting raw material shape It is required that different-alloy can be called in fusion process and the violent liquation composition of stirring is uniform;Powder diameter can be by adjusting nozzle Diameter is adjusted with admission pressure, and powder sphericity is high, oxygen content is low(Less than 600ppm);The present invention can also meet a variety of The powder by atomization requirement of refractory active metal.
Brief description of the drawings
The invention will be further described with reference to the accompanying drawings and detailed description.Protection scope of the present invention not only office It is limited to the statement of following content.
Fig. 1 is invention overall structure diagram.
Fig. 2 is invention top view.
Fig. 3 is interior views of the present invention.
Fig. 4 is gravity pawl charging mechanism of the present invention.
Fig. 5 is screw feed mechanism of the present invention.
In figure:1st, body of heater;2nd, fire door;3rd, vacuum system;4th, material alloying mechanism;5th, safety valve;6th, infrared measurement of temperature mechanism; 7th, gravity pawl charging mechanism;8th, screw feed mechanism;9th, power-supply system;10th, explosion tapping equipment;11st, high-pressure pipe;12、 It is atomized storehouse;13rd, cold-crucible system;14th, melting induction coil;15th, rising pouring induction coil;16th, ceramic spray pipe;17th, ceramics are led Pipe;18th, annular distance shape spray disk;19th, support frame;20th, smelting electrode;21st, rising pouring electrode;22nd, pneumatic gate valve;23rd, Pneumatic ball Valve;24th, blanking chute.
Embodiment
As illustrated, the sensing atomization of continous way cold crucible prepares titanium valve equipment, including body of heater 1, high-pressure pipe 11, atomization Storehouse 12 and vacuum system 3;The port of the vacuum system 3 communicates with the working chamber of body of heater 1;The body of heater 1 includes material alloying machine Structure 4, safety valve 5, infrared measurement of temperature mechanism 6, gravity material pawl charging mechanism 7, screw feed mechanism 8, explosion tapping equipment 10, melting Electrode 20, rising pouring electrode 21, cold-crucible system 13, melting induction coil 14, rising pouring induction coil 15 and annular distance shape spray disk 18; The material alloying mechanism 4, safety valve 5, infrared measurement of temperature mechanism 6, gravity material pawl charging mechanism 7, screw feed mechanism 8 and explosion The working end of tapping equipment 10 communicates with the working chamber of body of heater 1 respectively;The melting induction coil 14 is fixed at cold-crucible system Unite 13 external wall of upper portion;The rising pouring induction coil 15 is fixed at the bottom outer wall of cold-crucible system 13;In the cold-crucible The bottom of system 13 is provided with ceramic spray pipe 16;Ceramic conduit 17 is provided with the bottom of ceramic spray pipe 16;On the ceramic conduit 17 Portion port is vertical with the base opening of ceramic spray pipe 16 to be socketed, and sprays disk 18 through annular distance shape;High pressure low temperature argon gas passes through high-pressure pipe The 11 annular distance shape spray disks 18 entered in body of heater 1;Pneumatic gate valve is transversely provided with the charging chamber of the gravity material pawl charging mechanism 7 22。
Body of heater 1 of the present invention can use vertical Kazakhstan shell Double water-cooled jacket structured.Infrared measurement of temperature mechanism 6 of the present invention Ball pivot chain structure can be used;There are multiple independent charging cups inside the material alloying mechanism 4.The present invention is in the body of heater 1 Chamber is connected by pneumatic ball valve 23 with the cavity of screw feed mechanism 8;Blanking chute is provided with the bottom of screw feed mechanism 8 24.The taper of ceramic spray pipe 16 of the present invention is 90 °;The caliber of the ceramic spray pipe 16 is DN20.
Body of heater of the present invention is using vertical Kazakhstan hull shape formula, after opening fire door, it is internal overall expose be easy to dress to take furnace charge and daily Installation is safeguarded.In specific design, the present invention includes vacuum system, material alloying mechanism, safety valve, infrared measurement of temperature mechanism, again Power material pawl charging mechanism, screw feed mechanism, power-supply system, explosion tapping equipment, high-pressure pipe and atomization storehouse;Said units Module communicates with body of heater working cavity.Body of heater of the present invention includes cold-crucible system, melting induction coil, the rising pouring line of induction Circle, ceramic spray pipe, ceramic conduit, the installation of annular distance shape spray disk on the support frame, are fixedly connected as overall structure with body of heater;It is molten Refining electrode and rising pouring electrode are connected with the melting induction coil in body of heater and rising pouring induction coil respectively by sealing structure, electricity It is extremely outside to be connected by copper bar with power-supply system.
The present invention is jacket structured using vertical Kazakhstan shell Double water-cooled in the body of heater;The infrared measurement of temperature mechanism uses ball pivot Chain structure can realize the measurement of liquation optional position and can realize the argon gas cleaning to infrared lens;In the material alloying mechanism There are multiple independent charging cups in portion, and the addition of a variety of alloy material independences in fusion process can be achieved.The present invention is on the body of heater It is connected by pneumatic gate valve with gravity material pawl charging mechanism, its cavity is provided with vacuum interface and inflation inlet, may be implemented in and does not break The addition of rod shaped materials under bad body of heater vacuum or atmosphere.The present invention passes through pneumatic ball valve and screw feeding on the body of heater Mechanism is connected, and its cavity is provided with vacuum interface and inflation inlet, and there is swingable blanking chute bottom, not only may be implemented in and do not destroy The addition of fragment or titanium sponge under body of heater vacuum or atmosphere, it can also realize that continuous and quantitative adds in fusion process.The present invention Induction melting part is made up of upper and lower two groups of coils, and its top is passed through electric current of intermediate frequency for melting induction coil and is used for melting materialss, Its underpart is passed through high frequency electric for taper rising pouring induction coil makes liquation be flowed out from crucible bottom for heated nozzle;Power-supply system By in Medium frequency induction system and high-frequency induction system combination to same power cabinet, by smelting electrode and rising pouring electrode respectively with two Group coil is connected.High pressure low temperature argon gas of the present invention enters annular distance shape by high-pressure pipe and sprays disk atomization, saves source of the gas and adds Hot cost and raising powder quality shortening work period.
Water jacketed copper crucible wall in cold-crucible system of the present invention is designed with water jacketed copper crucible bottom using split, is possessed respectively Independent circulation, sidewall of crucible are spliced by the copper crucible valve of independent loops water channel;Crucible bottom is joint-cutting pyramidal structure Liner yttrium jet pipe, due to yittrium oxide and Titanium liquation minor response, and stable soakage layer is generated after reacting Prevent reaction continue to occur, therefore yttrium can be used as be atomized titanium valve when jet pipe;The taper and caliber of ceramic spray pipe with Whether cold crucible rising pouring successfully has direct relation.Taper by testing ceramic spray pipe chooses 90 °, and jet pipe caliber chooses DN20.
The present invention can be passed through the pressure of spray disk gas by changing and change ceramic spray pipe end aperture to obtain difference The powder of particle diameter.Source of the gas heating cost is saved as atomizing gas using high pressure low temperature argon gas due to of the invention, it is average every Second goes out powder 0.25kg and powder cooling is rapid, and atomization can take powder after completing 30 minutes, improve operating efficiency.
Present invention can be implemented in the addition for not destroying different shape material under body of heater vacuum or atmosphere, rod-like material uses The feeding of gravity pawl mechanism, its principle are conducted oneself with dignity by material to provide clamping force, and material pawl will by push-pull valve by winding mechanism Material is sent into crucible, and when material contacts with crucible bottom, material pawl unclamps automatically to be withdrawn by winding mechanism again;When need add fragment Blanking chute is swung during material, the ball valve being connected with body of heater is opened, material is continuously sent into by earthenware by screw feed mechanism Crucible, and the adjustment of feeding amount can be realized by adjusting motor speed.It not only may be implemented in and do not destroy body of heater vacuum or atmosphere The addition of lower fragment or titanium sponge, it can also realize that continuous and quantitative adds in fusion process.
Vent gas of the present invention can just eventually enter into mechanical pump vacuum system after dry filter filters, and can effectively receive Collect caused volatile matter, grease, dust etc. in fusion process, avoid scuffing of the dust granules to mechanical pump rotor, slow down to pump The pollution of oil.Meanwhile to prevent in fusion process because water jacketed copper crucible burn through cooling water caused by accident connects with melt liquid Raw unpredictable reaction condition is triggered, body of heater sets the diaphragm explosion-proof decompression device of independent safety valve and big orifice.
Above with respect to the specific descriptions of the present invention, it is merely to illustrate the present invention and is not limited to the embodiment of the present invention and is retouched The technical scheme stated.It will be understood by those within the art that still the present invention can be modified or equivalent substitution, To reach identical technique effect.As long as satisfaction uses needs, all in the protection domain of invention.

Claims (5)

1. a kind of continous way cold crucible sensing atomization prepares titanium valve equipment, it is characterised in that including body of heater(1), high-pressure pipe (11), atomization storehouse(12)And vacuum system(3);The vacuum system(3)Port and body of heater(1)Working chamber communicates;The stove Body(1)Including material alloying mechanism(4), safety valve(5), infrared measurement of temperature mechanism(6), gravity material pawl charging mechanism(7), spiral gives Expect mechanism(8), explosion tapping equipment(10), smelting electrode(20), rising pouring electrode(21), cold-crucible system(13), melting sense Answer coil(14), rising pouring induction coil(15)And annular distance shape spray disk(18);The material alloying mechanism(4), safety valve(5), it is red Outer temperature measuring mechanism(6), gravity material pawl charging mechanism(7), screw feed mechanism(8)And explosion tapping equipment(10)Working end point Not and body of heater(1)Working chamber communicates;The melting induction coil(14)It is fixed at cold-crucible system(13)External wall of upper portion;Institute State rising pouring induction coil(15)It is fixed at cold-crucible system(13)Bottom outer wall;In the cold-crucible system(13)Bottom Provided with ceramic spray pipe(16);In the ceramic spray pipe(16)Bottom is provided with ceramic conduit(17);The ceramic conduit(17)Top Port and ceramic spray pipe(16)Base opening is vertically socketed, and sprays disk through annular distance shape(18);High pressure low temperature argon gas passes through high pressure admission Pipe(11)Into body of heater(1)Interior annular distance shape spray disk(18);The gravity material pawl charging mechanism(7)Charging chamber on be transversely provided with Pneumatic gate valve(22).
2. continous way cold crucible sensing atomization according to claim 1 prepares titanium valve equipment, it is characterised in that:The body of heater (1)It is jacket structured using vertical Kazakhstan shell Double water-cooled.
3. continous way cold crucible sensing atomization according to claim 2 prepares titanium valve equipment, it is characterised in that:It is described infrared Temperature measuring mechanism(6)Using ball pivot chain structure;The material alloying mechanism(4)There are multiple independent charging cups inside.
4. continous way cold crucible sensing atomization according to claim 3 prepares titanium valve equipment, it is characterised in that:In the stove Body(1)Inner chamber passes through pneumatic ball valve(23)With screw feed mechanism(8)Cavity is connected;In the screw feed mechanism(8)Bottom Provided with blanking chute(24).
5. continous way cold crucible sensing atomization according to claim 4 prepares titanium valve equipment, it is characterised in that:The ceramics Jet pipe(16)Taper be 90 °;The ceramic spray pipe(16)Caliber be DN20.
CN201710976948.4A 2017-10-19 2017-10-19 The sensing atomization of continous way cold crucible prepares titanium valve equipment Pending CN107457408A (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109405546A (en) * 2018-12-18 2019-03-01 沈阳真空技术研究所有限公司 Variable clamping range band bottoms out the pneumatic charging mechanism of protection
CN109764676A (en) * 2019-01-14 2019-05-17 合肥科晶材料技术有限公司 A kind of multiple feeding device of induction heater vacuum state
CN114734047A (en) * 2022-06-15 2022-07-12 沈阳欧特真空科技有限公司 Continuous preparation equipment for hydrogen storage metal magnesium powder
WO2024016488A1 (en) * 2022-07-16 2024-01-25 南京尚吉增材制造研究院有限公司 Continuous feeding mechanism for rotating electrode atomization powder preparation, powder preparation device, and powder preparation method

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CN205869473U (en) * 2016-08-04 2017-01-11 浙江亚通焊材有限公司 Preparation vibration material disk metal powder's no crucible gas atomizing device
CN106334800A (en) * 2016-11-22 2017-01-18 沈阳真空技术研究所 The induction atomization titanium powder preparation equipment of cold crucible bottom injection
CN107234245A (en) * 2017-08-12 2017-10-10 长沙唯特冶金工程技术有限公司 The equipment that a kind of use bar continuous feed produces spherical powder
CN208178424U (en) * 2017-10-19 2018-12-04 沈阳真空技术研究所 The induction atomization of continous way cold crucible prepares titanium valve equipment

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Publication number Priority date Publication date Assignee Title
US20040105483A1 (en) * 2002-12-02 2004-06-03 Shuang-Shii Lian Method and apparatus for solidification-controllable induction melting of alloy with cold copper crucible
CN1486806A (en) * 2003-06-02 2004-04-07 湖南省顶立新材料工程中心有限公司 Atomizing formation apparatus for producing spherical casting WC powder
CN204545419U (en) * 2015-03-10 2015-08-12 沈阳好智多新材料制备技术有限公司 A kind of high vacuum induction is without crucible and have crucible inert gas atomizer powder manufacturing apparatus
CN205869473U (en) * 2016-08-04 2017-01-11 浙江亚通焊材有限公司 Preparation vibration material disk metal powder's no crucible gas atomizing device
CN106334800A (en) * 2016-11-22 2017-01-18 沈阳真空技术研究所 The induction atomization titanium powder preparation equipment of cold crucible bottom injection
CN107234245A (en) * 2017-08-12 2017-10-10 长沙唯特冶金工程技术有限公司 The equipment that a kind of use bar continuous feed produces spherical powder
CN208178424U (en) * 2017-10-19 2018-12-04 沈阳真空技术研究所 The induction atomization of continous way cold crucible prepares titanium valve equipment

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109405546A (en) * 2018-12-18 2019-03-01 沈阳真空技术研究所有限公司 Variable clamping range band bottoms out the pneumatic charging mechanism of protection
CN109405546B (en) * 2018-12-18 2023-12-19 沈阳真空技术研究所有限公司 Pneumatic feeding mechanism with variable clamping range and bottoming protection
CN109764676A (en) * 2019-01-14 2019-05-17 合肥科晶材料技术有限公司 A kind of multiple feeding device of induction heater vacuum state
CN109764676B (en) * 2019-01-14 2023-09-08 合肥科晶材料技术有限公司 Multiple feeding device for induction heating furnace in vacuum state
CN114734047A (en) * 2022-06-15 2022-07-12 沈阳欧特真空科技有限公司 Continuous preparation equipment for hydrogen storage metal magnesium powder
WO2024016488A1 (en) * 2022-07-16 2024-01-25 南京尚吉增材制造研究院有限公司 Continuous feeding mechanism for rotating electrode atomization powder preparation, powder preparation device, and powder preparation method

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