CN107446420A - A kind of environmental protection heat preservation thermal insulation material and preparation method thereof - Google Patents
A kind of environmental protection heat preservation thermal insulation material and preparation method thereof Download PDFInfo
- Publication number
- CN107446420A CN107446420A CN201710796502.3A CN201710796502A CN107446420A CN 107446420 A CN107446420 A CN 107446420A CN 201710796502 A CN201710796502 A CN 201710796502A CN 107446420 A CN107446420 A CN 107446420A
- Authority
- CN
- China
- Prior art keywords
- parts
- thermal insulation
- preparation
- stirred
- deionized water
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D125/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an aromatic carbocyclic ring; Coating compositions based on derivatives of such polymers
- C09D125/02—Homopolymers or copolymers of hydrocarbons
- C09D125/04—Homopolymers or copolymers of styrene
- C09D125/06—Polystyrene
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/18—Fireproof paints including high temperature resistant paints
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2237—Oxides; Hydroxides of metals of titanium
- C08K2003/2241—Titanium dioxide
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/014—Additives containing two or more different additives of the same subgroup in C08K
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/02—Flame or fire retardant/resistant
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Curing Cements, Concrete, And Artificial Stone (AREA)
- Building Environments (AREA)
Abstract
The present invention relates to a kind of environmental protection heat preservation thermal insulation material and preparation method thereof, raw material constituent is made up of following ratio in parts by weight：10 15 parts of Portland cement, 15 20 parts of granular polystyrene, 20 30 parts of expanded and vitrified small ball, 10 15 parts of expansion vitrification bead heat-preserving rubber powder material, 8 12 parts of white carbon, 25 parts of titanium dioxide, 24 parts of 2,4 dimethyl, 6 tert-butyl phenol, 34 parts of cocoanut fatty acid diethanolamide, 23 parts of ethoxylated dodecyl alcohol, 24 parts of higher fatty acids, 40 50 parts of deionized water.Material of the present invention is easy to get, and cost is low, easy for construction, can be smeared directly on original wall without tying layer；Good heat-insulation effect, insulation rate are high；High temperature resistant, low temperature performance well, temperature are resistant to as 80 120 DEG C, compressive resistance is strong；It is stable with good hot-face insulation property, chemical property；With good water resistance, hydrophobic layer is formed on surface, improves heat insulation effect and ageing resistace；It is capable of the drying of quick-hardening, improves efficiency of construction；It is nontoxic, tasteless, green.
Description
Technical field
The present invention relates to field of heat insulating materials, and in particular to a kind of environmental protection heat preservation thermal insulation material and preparation method thereof.
Background technology
With continuing deeply for national propulsion energy-saving environmental protection, the implementation of Regulation of building energy-saving, future architecture energy-saving heat preserving material
Wide market development space be present in material.Now, global heat preserving and insulating material is just towards efficient, energy-conservation, thin layer, heat-insulated, waterproof
The outer integrated direction of shield is developed, and in Development of Novel heat preserving and insulating material and meets structural thermal insulation power-saving technology simultaneously, has more emphasized
Specific aim uses heat-insulation material, by standard criterion design and construction, makes great efforts to improve insulating efficiency and reduces cost.
The content of the invention
A kind of environmental protection heat preservation thermal insulation material and its preparation are provided the invention aims to overcome the shortcomings of the above
Method.
Technical scheme includes：A kind of environmental protection heat preservation thermal insulation material and preparation method thereof, raw material constituent
It is made up of in parts by weight following ratio：Portland cement 10-15 parts, granular polystyrene 15-20 parts, expanded and vitrified small ball
20-30 parts, expansion vitrification bead heat-preserving rubber powder material 10-15 parts, white carbon 8-12 parts, titanium dioxide 2-5 parts, 2,4- dimethyl -6-
Tert-butyl phenol 2-4 parts, cocoanut fatty acid diethanolamide 3-4 parts, ethoxylated dodecyl alcohol 2-3 parts, higher fatty acids
2-4 parts, deionized water 40-50 parts.
Further improvement of the present invention is：Its preparation method is as follows：
A, expanded and vitrified small ball and expansion vitrification bead heat-preserving rubber powder material are added by being necessarily relatively stirred in whipping process
Appropriate granular polystyrene and deionized water, stir speed (S.S.) 500-700r/min, obtain mixture A；
B, will white carbon, titanium dioxide and deionized water add Portland cement in be stirred, add 2,4- dimethyl-
6- tert-butyl phenols and cocoanut fatty acid diethanolamide are mixed to thick, stir speed (S.S.) 650-800r/min,
Obtain mixture B；
C, ethoxylated dodecyl alcohol and mixture B will be added in mixture A be stirred, and be evenly stirred until thick, adding
Add higher fatty acids to stir, be put into deionizing water machine and handle, frequency 5000-6000HZ, time 10-15min, remove more
Remaining moisture, obtains product.
Beneficial effects of the present invention：
1st, material is easy to get, and cost is low, easy for construction, can be smeared directly on original wall without tying layer；
2nd, good heat-insulation effect, insulation rate are high；
3rd, high temperature resistant, low temperature performance well, temperature are resistant to as -80-120 DEG C, compressive resistance is strong；
4th, there is good hot-face insulation property, chemical property stabilization；
5th, there is good water resistance, hydrophobic layer is formed on surface, improve heat insulation effect and ageing resistace；
6th, it is capable of the drying of quick-hardening, improves efficiency of construction；
7th, it is nontoxic, tasteless, green.
Embodiment：
In order to deepen the understanding of the present invention, below in conjunction with embodiment, the invention will be further described, and the embodiment is only used
In explaining the present invention, it is not intended to limit the scope of the present invention..
Embodiment 1
A kind of environmental protection heat preservation thermal insulation material and preparation method thereof, raw material constituent are made up of following ratio in parts by weight：
12 parts of Portland cement, 18 parts of granular polystyrene, 25 parts of expanded and vitrified small ball, 12 parts of expansion vitrification bead heat-preserving rubber powder material,
10 parts of white carbon, 3 parts of titanium dioxide, 4 parts of 2,4 dimethyl 6 tert butyl phenol, cocoanut fatty acid diethanolamide 3 part, month
3 parts of cinnamic alcohol APEO, 4 parts of higher fatty acids, 50 parts of deionized water.
Its preparation method is as follows：
A, expanded and vitrified small ball and expansion vitrification bead heat-preserving rubber powder material are added by being necessarily relatively stirred in whipping process
Appropriate granular polystyrene and deionized water, stir speed (S.S.) 550r/min, obtain mixture A；
B, will white carbon, titanium dioxide and deionized water add Portland cement in be stirred, add 2,4- dimethyl-
6- tert-butyl phenols and cocoanut fatty acid diethanolamide are mixed to thick, stir speed (S.S.) 750r/min, are obtained mixed
Compound B；
C, ethoxylated dodecyl alcohol and mixture B will be added in mixture A be stirred, and be evenly stirred until thick, adding
Add higher fatty acids to stir, be put into deionizing water machine and handle, frequency 5600HZ, time 14min, remove excessive moisture,
Obtain product.
Embodiment 2
A kind of environmental protection heat preservation thermal insulation material and preparation method thereof, raw material constituent are made up of following ratio in parts by weight：
15 parts of Portland cement, 15 parts of granular polystyrene, 30 parts of expanded and vitrified small ball, 15 parts of expansion vitrification bead heat-preserving rubber powder material,
8 parts of white carbon, 2 parts of titanium dioxide, 2 parts of 2,4 dimethyl 6 tert butyl phenol, 4 parts of cocoanut fatty acid diethanolamide, bay
2 parts of alcohol APEO, 2 parts of higher fatty acids, 50 parts of deionized water.
Its preparation method is as follows：
A, expanded and vitrified small ball and expansion vitrification bead heat-preserving rubber powder material are added by being necessarily relatively stirred in whipping process
Appropriate granular polystyrene and deionized water, stir speed (S.S.) 700r/min, obtain mixture A；
B, will white carbon, titanium dioxide and deionized water add Portland cement in be stirred, add 2,4- dimethyl-
6- tert-butyl phenols and cocoanut fatty acid diethanolamide are mixed to thick, stir speed (S.S.) 650r/min, are obtained mixed
Compound B；
C, ethoxylated dodecyl alcohol and mixture B will be added in mixture A be stirred, and be evenly stirred until thick, adding
Add higher fatty acids to stir, be put into deionizing water machine and handle, frequency 5200HZ, time 13min, remove excessive moisture,
Obtain product.
Embodiment 3
A kind of environmental protection heat preservation thermal insulation material and preparation method thereof, raw material constituent are made up of following ratio in parts by weight：
10 parts of Portland cement, 15 parts of granular polystyrene, 20 parts of expanded and vitrified small ball, 10 parts of expansion vitrification bead heat-preserving rubber powder material,
9 parts of white carbon, 3 parts of titanium dioxide, 3 parts of 2,4 dimethyl 6 tert butyl phenol, 3 parts of cocoanut fatty acid diethanolamide, bay
3 parts of alcohol APEO, 4 parts of higher fatty acids, 40 parts of deionized water.
Its preparation method is as follows：
A, expanded and vitrified small ball and expansion vitrification bead heat-preserving rubber powder material are added by being necessarily relatively stirred in whipping process
Appropriate granular polystyrene and deionized water, stir speed (S.S.) 550r/min, obtain mixture A；
B, will white carbon, titanium dioxide and deionized water add Portland cement in be stirred, add 2,4- dimethyl-
6- tert-butyl phenols and cocoanut fatty acid diethanolamide are mixed to thick, stir speed (S.S.) 750r/min, are obtained mixed
Compound B；
C, ethoxylated dodecyl alcohol and mixture B will be added in mixture A be stirred, and be evenly stirred until thick, adding
Add higher fatty acids to stir, be put into deionizing water machine and handle, frequency 5400HZ, time 12min, remove excessive moisture,
Obtain product.
Embodiment 4
A kind of environmental protection heat preservation thermal insulation material and preparation method thereof, raw material constituent are made up of following ratio in parts by weight：
13 parts of Portland cement, 18 parts of granular polystyrene, 28 parts of expanded and vitrified small ball, 13 parts of expansion vitrification bead heat-preserving rubber powder material,
11 parts of white carbon, 4 parts of titanium dioxide, 3 parts of 2,4 dimethyl 6 tert butyl phenol, cocoanut fatty acid diethanolamide 3 part, month
3 parts of cinnamic alcohol APEO, 4 parts of higher fatty acids, 48 parts of deionized water.
Its preparation method is as follows：
A, expanded and vitrified small ball and expansion vitrification bead heat-preserving rubber powder material are added by being necessarily relatively stirred in whipping process
Appropriate granular polystyrene and deionized water, stir speed (S.S.) 500r/min, obtain mixture A；
B, will white carbon, titanium dioxide and deionized water add Portland cement in be stirred, add 2,4- dimethyl-
6- tert-butyl phenols and cocoanut fatty acid diethanolamide are mixed to thick, stir speed (S.S.) 800r/min, are obtained mixed
Compound B；
C, ethoxylated dodecyl alcohol and mixture B will be added in mixture A be stirred, and be evenly stirred until thick, adding
Add higher fatty acids to stir, be put into deionizing water machine and handle, frequency 6000HZ, time 15min, remove excessive moisture,
Obtain product.
In above example, embodiment 1 is most preferred embodiment, and insulation rate is high, good heat-insulation effect, good water-proof effect, fine and smooth
Lubrication, it is easy for construction.Higher fatty acids is finally added in step C, its water resistance can be effectively ensured, it is ensured that uniformity.
Explanation embodiments of the present invention are the foregoing is only, are not intended to limit the invention, for the technology of this area
For personnel, within the spirit and principles of the invention, any modification, equivalent substitution and improvements made etc., it should be included in
Within protection scope of the present invention.
Claims (2)
- A kind of 1. environmental protection heat preservation thermal insulation material and preparation method thereof, it is characterised in that：Raw material constituent in parts by weight by Following ratio composition：Portland cement 10-15 parts, granular polystyrene 15-20 parts, expanded and vitrified small ball 20-30 parts, expansion glass Change micro-sphere thermal insulation rubber powder material 10-15 parts, white carbon 8-12 parts, titanium dioxide 2-5 parts, 2,4 dimethyl 6 tert butyl phenol 2-4 Part, cocoanut fatty acid diethanolamide 3-4 parts, ethoxylated dodecyl alcohol 2-3 parts, higher fatty acids 2-4 parts, deionized water 40-50 parts.
- A kind of 2. environmental protection heat preservation thermal insulation material according to claim 1 and preparation method thereof, it is characterised in that：It is prepared Method is as follows：A, expanded and vitrified small ball and expansion vitrification bead heat-preserving rubber powder material are added by being necessarily relatively stirred in whipping process Appropriate granular polystyrene and deionized water, stir speed (S.S.) 500-700r/min, obtain mixture A；B, will white carbon, titanium dioxide and deionized water add Portland cement in be stirred, add 2,4- dimethyl- 6- tert-butyl phenols and cocoanut fatty acid diethanolamide are mixed to thick, stir speed (S.S.) 650-800r/min, Obtain mixture B；C, ethoxylated dodecyl alcohol and mixture B will be added in mixture A be stirred, and be evenly stirred until thick, adding Add higher fatty acids to stir, be put into deionizing water machine and handle, frequency 5000-6000HZ, time 10-15min, remove more Remaining moisture, obtains product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710796502.3A CN107446420A (en) | 2017-09-06 | 2017-09-06 | A kind of environmental protection heat preservation thermal insulation material and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710796502.3A CN107446420A (en) | 2017-09-06 | 2017-09-06 | A kind of environmental protection heat preservation thermal insulation material and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107446420A true CN107446420A (en) | 2017-12-08 |
Family
ID=60496132
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710796502.3A Pending CN107446420A (en) | 2017-09-06 | 2017-09-06 | A kind of environmental protection heat preservation thermal insulation material and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107446420A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110510918A (en) * | 2019-04-25 | 2019-11-29 | 四川陆亨能源科技有限公司 | A kind of heat preservation filler and preparation method thereof applied to heat exchanger |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101575193A (en) * | 2009-06-25 | 2009-11-11 | 北京立高科技有限公司 | Waterproof, heat preservation and thermal insulation building material and preparation method thereof |
| CN102010166A (en) * | 2010-11-18 | 2011-04-13 | 重庆思贝肯节能技术开发有限公司 | Method for preparing micro expanded inorganic heat insulation mortar |
| CN102746763A (en) * | 2011-04-22 | 2012-10-24 | 北京建筑技术发展有限责任公司 | Steel structure fireproof paint by taking expanded and vitrified small ball as base material |
| CN103553480A (en) * | 2013-09-27 | 2014-02-05 | 安唛杰节能建材科技（上海）有限公司 | A1-grade fireproof insulation mortar and preparation method thereof |
| CN105367024A (en) * | 2015-12-04 | 2016-03-02 | 南阳理工学院 | Heat-preserving material for outer wall |
-
2017
- 2017-09-06 CN CN201710796502.3A patent/CN107446420A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101575193A (en) * | 2009-06-25 | 2009-11-11 | 北京立高科技有限公司 | Waterproof, heat preservation and thermal insulation building material and preparation method thereof |
| CN102010166A (en) * | 2010-11-18 | 2011-04-13 | 重庆思贝肯节能技术开发有限公司 | Method for preparing micro expanded inorganic heat insulation mortar |
| CN102746763A (en) * | 2011-04-22 | 2012-10-24 | 北京建筑技术发展有限责任公司 | Steel structure fireproof paint by taking expanded and vitrified small ball as base material |
| CN103553480A (en) * | 2013-09-27 | 2014-02-05 | 安唛杰节能建材科技（上海）有限公司 | A1-grade fireproof insulation mortar and preparation method thereof |
| CN105367024A (en) * | 2015-12-04 | 2016-03-02 | 南阳理工学院 | Heat-preserving material for outer wall |
Non-Patent Citations (1)
| Title |
|---|
| 胡飞燕等: "《涂料基础配方与工艺》", 30 June 2013, 东华大学出版社 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110510918A (en) * | 2019-04-25 | 2019-11-29 | 四川陆亨能源科技有限公司 | A kind of heat preservation filler and preparation method thereof applied to heat exchanger |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN105272042B (en) | A kind of antifreeze anti-crack concrete | |
| CN103304187B (en) | Thermal insulation material and preparation method thereof | |
| CN103553421B (en) | A kind of environmentally friendly compounding coagulation soil whipping agent and preparation method thereof | |
| CN103922628B (en) | A kind of high performance water reducing agent of polyocarboxy acid of anti-freeze type and preparation method thereof | |
| CN107446404A (en) | A kind of external thermal insulation wall surface water proof flexible material | |
| CN101318789A (en) | Concrete air-entrainer and preparation method thereof | |
| CN104844258A (en) | Aerating block with waste rubber | |
| CN104673087A (en) | Anti-flaking waterproof coating material for buildings and preparation method thereof | |
| CN107446420A (en) | A kind of environmental protection heat preservation thermal insulation material and preparation method thereof | |
| CN110194643A (en) | A kind of preparation method of high-efficiency environment friendly gypsum mortar | |
| CN107954629A (en) | A kind of environment-friendly type concrete antifreezing agent | |
| CN109650797A (en) | A kind of preparation method of waterproof expanded perlite thermal-nsulation plate | |
| CN100404453C (en) | Environment-friendly type energy-saving house heat-insulating material | |
| CN104909626A (en) | Fire retardant insulation mortar for building's exterior and preparation method thereof | |
| CN105271878A (en) | Preparation method of montmorillonite-modified curing agent in cement-based material | |
| CN115073084A (en) | Environment-friendly high-performance light foaming cement and use method thereof | |
| CN107118456A (en) | A kind of novel environment friendly sheet material and preparation method thereof | |
| CN106431135A (en) | Preparation method of foamed concrete | |
| CN102786246A (en) | Concrete antifreezer | |
| CN102390971B (en) | Building outer wall thermal insulation material assistant, preparation and use methods thereof | |
| CN105110733A (en) | Adhesive mortar for phenolic insulation board | |
| CN111662038A (en) | Concrete surface reinforcing agent | |
| CN108410248A (en) | A kind of exterior wall putty and preparation method thereof being modified based on aerating aluminium powder | |
| CN104609793A (en) | Thermal-insulating and energy-saving wall material and preparation method thereof | |
| CN104529372A (en) | Composite silicate heat insulation coating and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20171208 |
|
| WD01 | Invention patent application deemed withdrawn after publication |