CN107421824A - A kind of composite polycrystal-diamond shock resistance test equipment and evaluation method - Google Patents

A kind of composite polycrystal-diamond shock resistance test equipment and evaluation method Download PDF

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Publication number
CN107421824A
CN107421824A CN201710366912.4A CN201710366912A CN107421824A CN 107421824 A CN107421824 A CN 107421824A CN 201710366912 A CN201710366912 A CN 201710366912A CN 107421824 A CN107421824 A CN 107421824A
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CN
China
Prior art keywords
diamond
impact
composite polycrystal
shock resistance
block
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Pending
Application number
CN201710366912.4A
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Chinese (zh)
Inventor
张春林
牛同健
赵东鹏
李英豪
马姗姗
方海江
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
HENAN SIFANG SUPER HARD MATERIAL CO Ltd
Henan SF Diamond Co Ltd
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HENAN SIFANG SUPER HARD MATERIAL CO Ltd
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Priority to CN201710366912.4A priority Critical patent/CN107421824A/en
Publication of CN107421824A publication Critical patent/CN107421824A/en
Pending legal-status Critical Current

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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N3/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N3/32Investigating strength properties of solid materials by application of mechanical stress by applying repeated or pulsating forces
    • G01N3/38Investigating strength properties of solid materials by application of mechanical stress by applying repeated or pulsating forces generated by electromagnetic means
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2203/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N2203/0001Type of application of the stress
    • G01N2203/001Impulsive
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2203/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N2203/0058Kind of property studied
    • G01N2203/006Crack, flaws, fracture or rupture
    • G01N2203/0067Fracture or rupture

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  • Physics & Mathematics (AREA)
  • Electromagnetism (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Investigating Strength Of Materials By Application Of Mechanical Stress (AREA)

Abstract

The invention provides a kind of detection of composite polycrystal-diamond shock resistance and evaluation method, including motor, disk, fixture and impact hardness block and its fixing device, described motor is connected to main shaft by transmission device, main shaft is provided with disk, and the edge of disk is provided with the fixture for loading composite polycrystal-diamond;Described impact hardness block is set on the securing means, and impact hardness block can contact with the composite polycrystal-diamond in rotation.The present invention evaluates the impact resistance of composite polycrystal-diamond by number of shocks and polycrystalline diamond surface damage area to solve the existing impulse detection that continuous high-efficient can not be carried out to composite polycrystal-diamond.

Description

A kind of composite polycrystal-diamond shock resistance test equipment and evaluation method
Technical field
The invention belongs to super-hard compound material technical field, and in particular to a kind of composite polycrystal-diamond shock resistance test Equipment and test and evaluation methods.
Background technology
Composite polycrystal-diamond (polycrystalline diamond compact, PDC) belongs to new function material Material, it is to sinter to form under high pressure and high temperature condition with cemented carbide substrate using diadust, and it both has diamond High rigidity, high-wearing feature and thermal conductivity, there is the intensity and toughness of hard alloy again, be manufacture cutting tool, drilling well The ideal material of drill bit and other wear resistant tools.Weighing the good and bad index of PDC performances has impact resistance, wearability and heat resistance. The quality of impact resistance is directly connected to PDC service life, and therefore, among production process, its impact resistance need to be made Precisely detection, and the performance of composite polycrystal-diamond is judged according to result, and existing detection method can not be right Composite polycrystal-diamond carries out the shock resistance detection of continuous high-efficient, it is therefore necessary to which exploitation is a kind of simple to operation and adopts With with actual drilling process similar in analogy method, to composite polycrystal-diamond carry out continuous high-efficient shock resistance detect, and Accurate evaluation is made to the impact resistance of composite polycrystal-diamond.
The content of the invention
It is existing to solve the invention provides a kind of detection of composite polycrystal-diamond shock resistance and evaluation method Can not to composite polycrystal-diamond carry out continuous high-efficient impulse detection, pass through number of shocks and polycrystalline diamond surface Damage area carrys out the impact resistance of evaluating combined.
The technical solution adopted by the present invention is:A kind of composite polycrystal-diamond shock resistance detection device, including electricity Motivation, disk, fixture and impact hardness block and its fixing device, described motor are connected to main shaft by transmission device, main Axle is provided with disk, and the edge of disk is provided with the fixture for loading composite polycrystal-diamond;Described impact hardness block is set On the securing means, impact hardness block can contact with the composite polycrystal-diamond in rotation.
Further, described fixing device includes the impact support frame being arranged on lathe base, and impact rotating bar is located at The middle part of support frame is impacted, is provided with limited block above described impact rotating bar, lower section is provided with elastomer, described Impact hardness block be arranged on the front end of impact rotating bar, force cell is housed below impact hardness block.
Further, described motor is also connected with frequency-variable controller and pulsed data logger;Described pulsed Data logger and force cell are connected with computer.
Further, described impact rotating bar can keep being horizontal in the presence of limited block and elastomer.
Further, one end of described impact rotating bar is connected by be hinged with impact support frame.
Further, described impact rotating bar in the presence of no limited block and elastomer can around pin joint carry out- 50 °~50 ° of rotation.
Further, described limited block is block rubber;Described elastomer is spring.
Further, described force cell is resistance-strain chip force cell.
The invention further relates to a kind of composite polycrystal-diamond shock resistance evaluation method, comprise the following steps:
The first step, composite polycrystal-diamond is put into the fixture of disk border, impact hardness block is arranged on impact The front end of pivoted lever;
Second step, the straight line registration between composite polycrystal-diamond and impact hardness block is adjusted in 0.3mm-3mm Between;
3rd step, the range of speeds of disk is adjusted between 60r/min-220r/min;
4th step, impact hardness is changed after composite polycrystal-diamond and impact hardness block impact 500 or 1000 times times The impact position of block;
5th step, measure the damaged area on composite polycrystal-diamond and record number of shocks.
Further, the Rockwell hardness of described impact hardness block is HRC58-HRC64.
The beneficial effect comprise that:Drive main shaft to be rotated by the motion of motor, and then drive on main shaft Disk and the composite polycrystal-diamond that is loaded on disk clamp move in a circle, composite polycrystal-diamond is hard with impact Block is spent in same level, and both have certain registration, composite polycrystal-diamond is by before to impacting pivoted lever The block of hardness at end is impacted, and in the presence of limited block and elastomer, pivoted lever is carried out within the very short time in impact space Reset, and then carry out next Secondary Shocks, ultimately form bump.Its frequency of impact is finally by the VFC in control system Device is controlled, and number of shocks is recorded by pulsed data logger, and is shown in control main screen, meanwhile, during impact Impulsive force by force cell signal collection and export, can intuitively see very much each impulsive force on computers Numerical value.This test machine can also carry out multi-point shock-testing to composite polycrystal-diamond, can be continuous, efficiently, Than the shock resistance of more comprehensively reflection composite polycrystal-diamond.
Brief description of the drawings
Fig. 1 is the structural representation of the present invention.
Embodiment
As shown in figure 1, a kind of composite polycrystal-diamond shock resistance detection device, is driven, motor by motor 1 Frequency-variable controller 2 and pulsed data logger 3 are connected with, for controlling the power of motor 1 and turning for record motor 1 Speed.The rotation of motor 1 is by belt or gear drive to main shaft 15, being provided with disk 4, the edge of disk on main shaft 15 Provided with the fixture 5 for installing composite polycrystal-diamond 6.Composite polycrystal-diamond 6 moves in a circle with disk, make its with Impact hardness block 11 collides.
Impact hardness block 11 is arranged on one end of impact rotating bar 8, and resistance is provided with the lower section of impact hardness block 11 should Become chip force cell 12, force cell 12 is transferred data in computer 13.Impact rotating bar 8 is arranged on base 14 On support frame 7 in, the top of impact rotating bar 8 is provided with limited block 9, and lower section is provided with elastomer 10, and limited block and elastomer make The keep level position of impact rotating bar 8.In the present embodiment, limited block 9 uses block rubber, and elastomer 10 uses spring.
Before impact starts, make that there is certain registration between composite polycrystal-diamond 6 and impact hardness block 11, electricity Motivation 1 drives disk 4 on main shaft and the composite polycrystal-diamond 6 that is loaded on fixture 5 to move in a circle, polycrystalline diamond The each rotation of composite sheet 6, impact block of hardness 11 is impacted once, in impact process, letter that force cell 12 will be collected into Number be converted to the numerical value of impulsive force and be real-time transmitted in computer 13.
When testing the shock resistance of composite polycrystal-diamond, the course of work of above-described embodiment is:
Composite polycrystal-diamond 6 is installed in the fixture 5 in rotating circular disc 4, meanwhile, it is HRC60 by Rockwell hardness Impact hardness block 11 be installed to the front end of impact rotating bar 8, and fasten, rotating circular disc 4, make the He of composite polycrystal-diamond 6 Impact hardness block 11 contacts and in same level, adjusts both positions, and setting them has 2mm registration, adjusts The working frequency of whole frequency-variable controller 2, the rotating speed for making output main shaft 15 are 100r/min, open operating switch, polycrystalline diamond Composite sheet 6 carries out rotation bump to impact block of hardness 11, and pulsed data logger 3 then records to number of shocks, The signal being collected into is converted to the numerical value of impulsive force and is real-time transmitted in computer 13 by force cell 12, can be intuitively See impulsive force numerical value.
In test process, often impacting 500 times or 1000 times need to change to the impact position of block of hardness, to ensure to rush The stability hit, until composite polycrystal-diamond is damaged, stop impact, record number of shocks, composite sheet breakage area and punching Hit power numerical value.
The table is the experimental data of the present embodiment:
Composite sheet sample Rotating speed (r/min) Registration (mm) Damaged number of shocks Damaged area Impulsive force
1# 100 2 14537 1/2 320N-360N
2# 100 2 13982 1/4 320N-360N
3# 100 2 9302 1/4 320N-360N
The evaluation method of the present invention can provide foundation for the shock resistance of composite polycrystal-diamond, and then be glomerocryst The selection of diamond compact uses offer reference.Test result such as the present embodiment can see:No. 1 sample shock resistance number Highest, but damaged area is larger, and No. 2 are identical with No. 3 damaged areas, and No. 2 sample shock resistance numbers are higher, and No. 1 and No. 2 Shock resistance number is very nearly the same, and if being selected from shock resistance, No. 2 samples are appropriate.

Claims (10)

  1. A kind of 1. composite polycrystal-diamond shock resistance detection device, it is characterised in that:Including motor, disk, fixture With impact hardness block and its fixing device, described motor is connected to main shaft by transmission device, and main shaft is provided with disk, circle The edge of disk is provided with the fixture for loading composite polycrystal-diamond;Described impact hardness block is set on the securing means, punching Hitting block of hardness can contact with the composite polycrystal-diamond in rotation.
  2. A kind of 2. composite polycrystal-diamond shock resistance detection device according to claim 1, it is characterised in that:Institute The fixing device stated includes the impact support frame being arranged on lathe base, and impact rotating bar is located at the pars intermedia of impact support frame , limited block is provided with above described impact rotating bar, lower section is provided with elastomer, and described impact hardness block is arranged on The front end of impact rotating bar, impact hardness block lower section are equipped with force cell.
  3. A kind of 3. composite polycrystal-diamond shock resistance detection device according to claim 1, it is characterised in that:Institute The motor stated also is connected with frequency-variable controller and pulsed data logger;Described pulsed data logger and dynamometry pass Sensor is connected with computer.
  4. A kind of 4. composite polycrystal-diamond shock resistance detection device according to claim 2, it is characterised in that:Institute The impact rotating bar stated can keep being horizontal in the presence of limited block and elastomer.
  5. A kind of 5. composite polycrystal-diamond shock resistance detection device according to claim 2, it is characterised in that:Institute The one end for the impact rotating bar stated is connected by be hinged with impact support frame.
  6. A kind of 6. composite polycrystal-diamond shock resistance detection device according to claim 2, it is characterised in that:Institute The impact rotating bar stated can carry out -50 ° ~ 50 ° of rotation in the presence of no limited block and elastomer around pin joint.
  7. A kind of 7. composite polycrystal-diamond shock resistance detection device according to claim 2, it is characterised in that:Institute The limited block stated is block rubber;Described elastomer is spring.
  8. A kind of 8. composite polycrystal-diamond shock resistance detection device according to claim 2, it is characterised in that:Institute The force cell stated is resistance-strain chip force cell.
  9. 9. a kind of composite polycrystal-diamond shock resistance evaluation method, comprises the following steps:
    The first step, composite polycrystal-diamond is put into the fixture of disk border, impact hardness block is arranged on impact rotating The front end of bar;
    Second step, the straight line registration between composite polycrystal-diamond and impact hardness block is adjusted between 0.3mm-3mm;
    3rd step, the range of speeds of disk is adjusted between 60 r/min -220r/min;
    4th step, impacted in composite polycrystal-diamond and impact hardness block and impact hardness block is changed after 500 or 1000 times times Impact position;
    5th step, measure the damaged area on composite polycrystal-diamond and record number of shocks.
  10. A kind of 10. composite polycrystal-diamond shock resistance detection device according to claim 9, it is characterised in that: The Rockwell hardness of described impact hardness block is HRC58-HRC64.
CN201710366912.4A 2017-05-19 2017-05-19 A kind of composite polycrystal-diamond shock resistance test equipment and evaluation method Pending CN107421824A (en)

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CN201710366912.4A CN107421824A (en) 2017-05-19 2017-05-19 A kind of composite polycrystal-diamond shock resistance test equipment and evaluation method

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CN201710366912.4A CN107421824A (en) 2017-05-19 2017-05-19 A kind of composite polycrystal-diamond shock resistance test equipment and evaluation method

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Citations (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH09210890A (en) * 1996-01-30 1997-08-15 Shin Etsu Polymer Co Ltd Method and apparatus for testing impact of plastic sheet
US20020035865A1 (en) * 1999-02-22 2002-03-28 Luk Allan Kai Disc drive component level shock tester
JP2005056990A (en) * 2003-08-01 2005-03-03 Nikko Materials Co Ltd Shock-resistance testing method for semiconductor wafer and method of manufacturing semiconductor device
JP2006125845A (en) * 2004-10-26 2006-05-18 Mitsubishi Heavy Ind Ltd Shock testing apparatus and shock testing method of surface treatment material
JP2010283151A (en) * 2009-06-04 2010-12-16 Shin Etsu Handotai Co Ltd Evaluation device for semiconductor wafer
DE102010027817A1 (en) * 2010-04-15 2011-11-24 Skz - Kfe Ggmbh Kunststoff-Forschung Und -Entwicklung Measuring system for determining impact strength properties of parameter e.g. rotation speed, of plastic material, has control device determining impact strength properties of plastic strand, measured with respect to material index
CN203287267U (en) * 2013-04-27 2013-11-13 北京远东恒嘉新材料有限公司 Impact resistance tester for polycrystalline diamond compacts
CN103698234A (en) * 2013-12-03 2014-04-02 常州深倍超硬材料有限公司 Impact testing machine for composite sheet
CN204044011U (en) * 2014-09-11 2014-12-24 莆田学院 Shock resistance detector at the bottom of a kind of footwear hardness
CN106574885A (en) * 2014-09-16 2017-04-19 横滨橡胶株式会社 Impact test device and method
CN207114346U (en) * 2017-05-19 2018-03-16 河南四方达超硬材料股份有限公司 A kind of composite polycrystal-diamond shock resistance test equipment

Patent Citations (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH09210890A (en) * 1996-01-30 1997-08-15 Shin Etsu Polymer Co Ltd Method and apparatus for testing impact of plastic sheet
US20020035865A1 (en) * 1999-02-22 2002-03-28 Luk Allan Kai Disc drive component level shock tester
JP2005056990A (en) * 2003-08-01 2005-03-03 Nikko Materials Co Ltd Shock-resistance testing method for semiconductor wafer and method of manufacturing semiconductor device
JP2006125845A (en) * 2004-10-26 2006-05-18 Mitsubishi Heavy Ind Ltd Shock testing apparatus and shock testing method of surface treatment material
JP2010283151A (en) * 2009-06-04 2010-12-16 Shin Etsu Handotai Co Ltd Evaluation device for semiconductor wafer
DE102010027817A1 (en) * 2010-04-15 2011-11-24 Skz - Kfe Ggmbh Kunststoff-Forschung Und -Entwicklung Measuring system for determining impact strength properties of parameter e.g. rotation speed, of plastic material, has control device determining impact strength properties of plastic strand, measured with respect to material index
CN203287267U (en) * 2013-04-27 2013-11-13 北京远东恒嘉新材料有限公司 Impact resistance tester for polycrystalline diamond compacts
CN103698234A (en) * 2013-12-03 2014-04-02 常州深倍超硬材料有限公司 Impact testing machine for composite sheet
CN204044011U (en) * 2014-09-11 2014-12-24 莆田学院 Shock resistance detector at the bottom of a kind of footwear hardness
CN106574885A (en) * 2014-09-16 2017-04-19 横滨橡胶株式会社 Impact test device and method
CN207114346U (en) * 2017-05-19 2018-03-16 河南四方达超硬材料股份有限公司 A kind of composite polycrystal-diamond shock resistance test equipment

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