CN107418705A - A kind of method that aqueous enzymatic method prepares capsicum seed oil - Google Patents
A kind of method that aqueous enzymatic method prepares capsicum seed oil Download PDFInfo
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- CN107418705A CN107418705A CN201710358072.7A CN201710358072A CN107418705A CN 107418705 A CN107418705 A CN 107418705A CN 201710358072 A CN201710358072 A CN 201710358072A CN 107418705 A CN107418705 A CN 107418705A
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- Prior art keywords
- capsicum
- zymolyte
- seed oil
- filtrate
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Classifications
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/02—Pretreatment
- C11B1/025—Pretreatment by enzymes or microorganisms, living or dead
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/02—Pretreatment
- C11B1/04—Pretreatment of vegetable raw material
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B1/00—Production of fats or fatty oils from raw materials
- C11B1/10—Production of fats or fatty oils from raw materials by extracting
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Biochemistry (AREA)
- Microbiology (AREA)
- Fats And Perfumes (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
Abstract
The invention discloses a kind of method that aqueous enzymatic method prepares capsicum seed oil, comprise the following steps：(1) chilli seed is gone into the removal of impurity, dry, pulverize sieving, obtain capsicum powder of seeds；(2) add water to mix capsicum powder of seeds, obtain mixture；(3) food-grade complex enzyme is added, pH is adjusted, enzymolysis, water-bath enzyme deactivation, obtains zymolyte；(4) zymolyte is dried；(5) absolute ethyl alcohol is added in the zymolyte obtained to step (4), extracts, isolated filtrate, filtrate is rotated, reclaimed ethanol, obtain capsicum seed oil.The present invention is pre-processed using aqueous enzymatic method to chilli seed, alcohol steep assisted extraction capsicum seed oil.Aqueous enzymatic method, which carries out pre-treatment, can improve oil quality, harmful substance is removed, and the addition of the green solvent in later stage can effectively improve oil yield, and avoid problem of solvent residual, the method category green processes craft of the present invention, safety and sanitation, have the characteristics that energy consumption is low, process operations are simple.
Description
Technical field
The present invention relates to the method for plant extract capsicum seed oil, belong to field of food industry.
Background technology
Capsicum (Capsicum annuum L.) is Solanaceae capsicum plants, is about occurred in the Ming Dynasty in China.At present, capsicum
Plantation spreads all over the world, world's pepper planting area about 4,000,000 hm2, the t of yield about 40,000,000, year, sown area was about 1,500,000
hm2, the 40% of world's cultivated area is accounted for, total output about 30,000,000 t, accounts for the 46% of Gross World Product, the output value about 2000
Hundred million yuan, occupy first of vegetables, account for the 16.67% of world's vegetables gross output value.The consumption figure of capsicum ranks forefront in the whole world, and global is peppery
Green pepper and its product up to more than 1000 are planted, and peppery crowd is eaten more than 20% in the whole world, and China eats peppery crowd and is up to 40%, it is seen that capsicum and
Its product yield is huge, it is meant that accessory substance yield is also extremely more.The part that people most often utilize, i.e., the pericarp of dry full capsicum account for
50%, and seed accounts for 39%, stalk accounts for 11% with other, and such accessory substance generally goes out of use, it is seen that capsicum accessory substance resource wave
Take seriously,
The content of the invention
The purpose of the present invention is overcome the deficiencies in the prior art, there is provided a kind of method that aqueous enzymatic method prepares capsicum seed oil.
Technical scheme is summarized as follows：
A kind of method that aqueous enzymatic method prepares capsicum seed oil, comprises the following steps：
(1) chilli seed is gone into the removal of impurity, is dried at 30~50 DEG C to water quality≤10% is contained, crushed 20~60 mesh sieves,
Obtain capsicum powder of seeds；
(2) it is 1 according to material-water ratio:Capsicum powder of seeds is added water to mix by 3~8 ratio, obtains mixture；
(3) 0.5%-2% of chilli seed powder quality food-grade complex enzyme is added, pH=4.0~7.0 are adjusted, 40
At~65 DEG C, 3~6h is digested, water-bath 5~10min of enzyme deactivation, obtains zymolyte；The complex enzyme is 3~7 by mass ratio:7~3
Pectase and neutral proteinase composition；
(4) by zymolyte dry to containing water quality be 50%~60%；
(5) absolute ethyl alcohol of 4~8 times of volumes is added in the zymolyte obtained to step (4), 2 are extracted at 40~70 DEG C
~7h, isolated filtrate, filtrate is rotated, and is reclaimed ethanol, is obtained capsicum seed oil.
Preferably, complex enzyme is 3 by mass ratio:7 pectase and neutral proteinase composition.
The addition of food-grade complex enzyme is preferably the 1% of chilli seed powder quality.
The temperature of step (3) is 50 DEG C.
Step (3) enzymolysis time is 5h.
Step (3) pH is 5.0.
Preferably, step (5) is：The absolute ethyl alcohol of 5 times of volumes is added in the zymolyte obtained to step (4), at 60 DEG C
Lower extraction 3h, isolated filtrate, filtrate is rotated, and is reclaimed ethanol, is obtained capsicum seed oil.
Advantages of the present invention：
The present invention is pre-processed using aqueous enzymatic method to chilli seed, alcohol steep assisted extraction capsicum seed oil.Aqueous enzymatic method enters
Row pre-treatment can improve oil quality, remove harmful substance, and the addition of the green solvent in later stage can effectively improve it is fuel-displaced
Rate, and avoid problem of solvent residual, method category green processes craft of the invention, safety and sanitation have that energy consumption is low, process operations
The features such as simple.
Embodiment
With reference to specific embodiment, the present invention is further illustrated.The following examples are in order that this area
Technical staff is not imposed any restrictions to the present invention it will be appreciated that the present invention.
Embodiment 1
A kind of method that aqueous enzymatic method prepares capsicum seed oil, comprises the following steps：
(1) chilli seed is gone into the removal of impurity, is dried at 40 DEG C to being 9% containing water quality, crushed 40 mesh sieves, obtain chilli seed powder
End；(2) it is 1 according to material-water ratio:Capsicum powder of seeds is added water to mix by 5 ratio, obtains mixture；
(3) 1% food-grade complex enzyme of chilli seed powder quality is added, adjusts pH=5.0, at 50 DEG C, digests 5h,
Water-bath enzyme deactivation 8min, obtains zymolyte；The complex enzyme is 3 by mass ratio:7 pectase and neutral proteinase composition；
(4) by zymolyte dry to containing water quality be 55%；
(5) absolute ethyl alcohol of 5 times of volumes is added in the zymolyte obtained to step (4), 3h is extracted at 60 DEG C, separates
To filtrate, filtrate is rotated, ethanol is reclaimed, obtains capsicum seed oil.
Capsicum seed oil oil yield is up to 70%.
Embodiment 2
A kind of method that aqueous enzymatic method prepares capsicum seed oil, comprises the following steps：
(1) chilli seed is gone into the removal of impurity, is dried at 30 DEG C to water quality=10% is contained, crushed 20 mesh sieves, obtain chilli seed
Powder；
(2) it is 1 according to material-water ratio:Capsicum powder of seeds is added water to mix by 3 ratio, obtains mixture；
(3) 0.5% food-grade complex enzyme of chilli seed powder quality is added, adjusts pH=4.0, at 40 DEG C, enzymolysis
6h, water-bath enzyme deactivation 5min, obtains zymolyte；The complex enzyme is 3 by mass ratio:7 pectase and neutral proteinase composition；
(4) by zymolyte dry to containing water quality be 50%；
(5) absolute ethyl alcohol of 4 times of volumes is added in the zymolyte obtained to step (4), 7h is extracted at 40 DEG C, separates
To filtrate, filtrate is rotated, ethanol is reclaimed, obtains capsicum seed oil.
Capsicum seed oil oil yield is up to 51%.
Embodiment 3
A kind of method that aqueous enzymatic method prepares capsicum seed oil, comprises the following steps：
(1) chilli seed is gone into the removal of impurity, is dried at 50 DEG C to being 8% containing water quality, crushed 60 mesh sieves, obtain chilli seed powder
End；
(2) it is 1 according to material-water ratio:Capsicum powder of seeds is added water to mix by 8 ratio, obtains mixture；
(3) 2% food-grade complex enzyme of chilli seed powder quality is added, adjusts pH=7.0, at 65 DEG C, digests 3h,
Water-bath enzyme deactivation 10min, obtains zymolyte；The complex enzyme is 7 by mass ratio:3 pectase and neutral proteinase composition；
(4) by zymolyte dry to containing water quality be 60%；
(5) absolute ethyl alcohol of 8 times of volumes is added in the zymolyte obtained to step (4), 2h is extracted at 70 DEG C, separates
To filtrate, filtrate is rotated, ethanol is reclaimed, obtains capsicum seed oil.
Capsicum seed oil oil yield is up to 60.8%.
Sample chilli seed passes through petroleum ether (60~90 DEG C of boiling range) surname extraction, oil yield 25g/100g, defines fuel-displaced
Rate is 100%.
Obviously, the above embodiment of the present invention is only intended to clearly illustrate example of the present invention, and is not pair
The restriction of embodiments of the present invention, for those of ordinary skill in the field, may be used also on the basis of the above description
To make other changes in different forms, all embodiments can not be exhaustive here, it is every to belong to this hair
Row of the obvious changes or variations that bright technical scheme is extended out still in protection scope of the present invention.
Claims (7)
1. a kind of aqueous enzymatic method prepares the method for capsicum seed oil, it is characterized in that comprising the following steps：
(1) chilli seed is gone into the removal of impurity, is dried at 30~50 DEG C to water quality≤10% is contained, crushed 20~60 mesh sieves, obtain peppery
Green pepper powder of seeds；
(2) it is 1 according to material-water ratio:Capsicum powder of seeds is added water to mix by 3~8 ratio, obtains mixture；
(3) 0.5%-2% of chilli seed powder quality food-grade complex enzyme is added, pH=4.0~7.0 are adjusted, 40~65
At DEG C, 3~6h is digested, water-bath 5~10min of enzyme deactivation, obtains zymolyte；The complex enzyme is 3~7 by mass ratio:7~3 pectin
Enzyme and neutral proteinase composition；
(4) by zymolyte dry to containing water quality be 50%~60%；
(5) absolute ethyl alcohol of 4~8 times of volumes is added in the zymolyte obtained to step (4), 2~7h is extracted at 40~70 DEG C,
Isolated filtrate, filtrate is rotated, and is reclaimed ethanol, is obtained capsicum seed oil.
2. the method according to claim 11, it is characterized in that the complex enzyme is 3 by mass ratio:7 pectase and neutral egg
White enzyme composition.
3. according to the method for claim 1, it is characterized in that the addition of food-grade complex enzyme is chilli seed powder quality
1%.
4. according to the method for claim 1, it is characterized in that step (3) temperature is 50 DEG C.
5. according to the method for claim 1, it is characterized in that step (3) enzymolysis time is 5h.
6. according to the method for claim 1, it is characterized in that step (3) pH is 5.0.
7. according to the method for claim 1, it is characterized in that the step (5) is：Add in the zymolyte obtained to step (4)
Enter the absolute ethyl alcohol of 5 times of volumes, 3h is extracted at 60 DEG C, isolated filtrate, filtrate is rotated, reclaim ethanol, obtain capsicum
Seed oil.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201710358072.7A CN107418705A (en) | 2017-05-19 | 2017-05-19 | A kind of method that aqueous enzymatic method prepares capsicum seed oil |
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| CN201710358072.7A CN107418705A (en) | 2017-05-19 | 2017-05-19 | A kind of method that aqueous enzymatic method prepares capsicum seed oil |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108060009A (en) * | 2017-12-25 | 2018-05-22 | 石河子大学 | A kind of extracting method of aqueous enzymatic extraction tomato seed oil |
| CN114947104A (en) * | 2022-05-23 | 2022-08-30 | 青岛天祥食品集团调味品有限公司 | Production process of fresh chilli sauce and fresh chilli sauce |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105779117A (en) * | 2016-05-18 | 2016-07-20 | 吉林省鑫生物质新能源发展有限公司 | Method for extracting chilli seed oil in chilies |
| CN106350198A (en) * | 2016-08-26 | 2017-01-25 | 施蕊 | Method for simultaneously extracting capsicol, pigment and alkaloid from chilies and application of method |
-
2017
- 2017-05-19 CN CN201710358072.7A patent/CN107418705A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105779117A (en) * | 2016-05-18 | 2016-07-20 | 吉林省鑫生物质新能源发展有限公司 | Method for extracting chilli seed oil in chilies |
| CN106350198A (en) * | 2016-08-26 | 2017-01-25 | 施蕊 | Method for simultaneously extracting capsicol, pigment and alkaloid from chilies and application of method |
Non-Patent Citations (3)
| Title |
|---|
| 徐丹丹，等: "辣椒籽油提取工艺研究", 《湖南农业科学》 * |
| 袁唯，等: "云南丘北辣椒籽油酶法提取条件优化研究", 《食品科技》 * |
| 马自超，等: "《天然食用色素化学》", 31 January 2016, 中国轻工业出版社 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108060009A (en) * | 2017-12-25 | 2018-05-22 | 石河子大学 | A kind of extracting method of aqueous enzymatic extraction tomato seed oil |
| CN114947104A (en) * | 2022-05-23 | 2022-08-30 | 青岛天祥食品集团调味品有限公司 | Production process of fresh chilli sauce and fresh chilli sauce |
| CN114947104B (en) * | 2022-05-23 | 2023-05-12 | 青岛天祥食品集团调味品有限公司 | Production process of fresh chilli sauce and fresh chilli sauce |
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