CN107418031A - A kind of compounded lubricant and preparation method thereof - Google Patents
A kind of compounded lubricant and preparation method thereof Download PDFInfo
- Publication number
- CN107418031A CN107418031A CN201710444783.6A CN201710444783A CN107418031A CN 107418031 A CN107418031 A CN 107418031A CN 201710444783 A CN201710444783 A CN 201710444783A CN 107418031 A CN107418031 A CN 107418031A
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- China
- Prior art keywords
- reactant
- fischer
- ope
- tissuemat
- stearic acid
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L23/00—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers
- C08L23/02—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers not modified by chemical after-treatment
- C08L23/04—Homopolymers or copolymers of ethene
- C08L23/06—Polyethene
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Lubricants (AREA)
Abstract
The present invention relates to a kind of compounded lubricant and preparation method thereof.Including following components, the weight ratio of each component is：Stearic acid 5 15, Fischer-Tropsch wax 10 30, OPE 5 15, Tissuemat E 60 70.The good combination that the present invention will lubricate outside lubrication in stearic acid and Tissuemat E, add Fischer-Tropsch wax and OPE improves the needle penetration and polarity of lubrication prescription, make fusion time and the plasticizing moment of torsion of plastic products stable, the again easy use of client of integral lubricating system.Production equipment is simple, and economic well-being of workers and staff is good.
Description
Technical field
The present invention relates to a kind of compounded lubricant and preparation method thereof, belong to technical field of lubricant preparation.
Background technology
Lubricant as plastics needs lubricant to possess good needle penetration and polarity, is turned round with improving plastic products plasticizing
The stability of square, while for the metachromatism for preventing plastics from occurring in process, lubricant is preferably while possess good
Thermal stability；And in order to keep the production efficiency of plastic products and product quality, preferably require that lubricant possesses preferably
Dispersiveness and the features such as low viscosity；And existing lubricant does not possess above feature, therefore it have impact on the life of plastic products
The quality of efficiency and plastic products is produced, it is necessary to be improved.
The content of the invention
The present invention is directed to drawbacks described above, and it is an object of the present invention to provide one kind possesses multiple performance, ensures plastic products quality and life
Produce a kind of compounded lubricant of efficiency and preparation method thereof.
It is for this technical solution adopted by the present invention：The present invention includes following components, and the weight ratio of each component is：Stearic acid
5-15, Fischer-Tropsch wax 10-30, OPE 5-15, Tissuemat E 60-70.
The weight ratio of each component is：Stearic acid 5-10, Fischer-Tropsch wax 20-30, OPE 10-15, Tissuemat E
60-70。
A kind of preparation method of compounded lubricant, by various components by component than input reactor, reaction temperature 150-200
Degree, hour time 1-2, through steel band granulating and forming.
The present invention further follows the steps below：Stearic acid, OPE and Tissuemat E are mixed and made
For reactant A, using Fischer-Tropsch wax as reactant B, A and B is alternately squeezed into hybrid reaction is carried out in reactor.
Reactant B is specifically first squeezed into, then squeezes into reactant A, so alternately squeezes into and hybrid reaction is carried out in reactor.
It is an advantage of the invention that：1）The good combination that the present invention will lubricate outside lubrication in stearic acid and Tissuemat E, adds
Enter Fischer-Tropsch wax and OPE improves the needle penetration and polarity of lubrication prescription, make the fusion time and plasticizing moment of torsion of plastic products
It is stable, the again easy use of client of integral lubricating system.Production equipment is simple, and economic well-being of workers and staff is good.
2）The present invention reactant A and reactant B squeezed into using alternative expression by the way of in reactor so that reactant A with
Reactant B mixing be more uniformly distributed, using Fischer-Tropsch wax viscosity it is relatively low the characteristics of, both, which are well mixed, can guarantee that product viscosity
Uniformity, uniformity, improve the production efficiency of product and the quality of product, avoid viscosity differ caused by speed of production inequality
It is even, so as to influence the unstability of the quality of product and equipment operation.
Embodiment
Embodiment one：
The present invention includes following components, and the weight ratio of each component is：Stearic acid 6, Fischer-Tropsch wax 22, OPE 12, poly- second
Alkene wax 60.
A kind of preparation method of compounded lubricant, various components are compared by component and put into reactor, 185 degree of reaction temperature,
The 1.8 hours time, through steel band granulating and forming.
The present invention further follows the steps below：Stearic acid, OPE and Tissuemat E are mixed and made
For reactant A, using Fischer-Tropsch wax as reactant B, A and B is alternately squeezed into hybrid reaction is carried out in reactor.
Reactant B is specifically first squeezed into, then squeezes into reactant A, so alternately squeezes into and hybrid reaction is carried out in reactor.
Embodiment two：
The present invention includes following components, and the weight ratio of each component is：Stearic acid 12, Fischer-Tropsch wax 12, OPE 8, poly- second
Alkene wax 68.
A kind of preparation method of compounded lubricant, various components are compared by component and put into reactor, 160 degree of reaction temperature,
Time 2 h, through steel band granulating and forming.
The present invention further follows the steps below：Stearic acid, OPE and Tissuemat E are mixed and made
For reactant A, using Fischer-Tropsch wax as reactant B, A and B is alternately squeezed into hybrid reaction is carried out in reactor.
Reactant B is specifically first squeezed into, then squeezes into reactant A, so alternately squeezes into and hybrid reaction is carried out in reactor.
Embodiment three：
The present invention includes following components, and the weight ratio of each component is：Stearic acid 12, Fischer-Tropsch wax 20, OPE 5, poly- second
Alkene wax 63.
A kind of preparation method of compounded lubricant, various components are compared by component and put into reactor, 200 degree of reaction temperature,
The 1 hour time, through steel band granulating and forming.
The present invention further follows the steps below：Stearic acid, OPE and Tissuemat E are mixed and made
For reactant A, using Fischer-Tropsch wax as reactant B, A and B is alternately squeezed into hybrid reaction is carried out in reactor.
Reactant B is specifically first squeezed into, then squeezes into reactant A, so alternately squeezes into and hybrid reaction is carried out in reactor.
The mechanism of action of each component of the present invention is described in detail below：Stearic acid be widely used in PVC plastic pipe,
The manufacture of sheet material, section bar, film.It is PVC heat stabilizer, there is good lubricity and preferable light, heat stabilization.Moulding
Expect in pvc pipe, " coking " that stearic acid helps to prevent in process, addition is a kind of effective in PVC film processing
Heat stabilizer, while can defend to be placed in finished films discoloration caused in sulfide cruelly.
Fischer-Tropsch wax may apply in plastic processing, such as injection, extrusion and granulation industry.Fischer-Tropsch wax is in Masterbatch and changes
Property plastics-production during, contribute to the scattered and outstanding slipping of filler in batch mixing.PVC external lubricant is may be used as,
Low-viscosity can improve the speed of production of product, contribute to the scattered especially in the extrusion of high viscosity systems of color stuffing in batch mixing
Have and preferably appoint, it is fewer 40--50% than common PE wax addition, and product surface gloss can be significantly improved.Using heavy colour
When, the Fischer-Tropsch wax of fusing can effectively soak dyestuff, reduce extrusion viscosity.
OPE is excellent new polar waxes, because OPE strand carries a certain amount of carbonyl
And hydroxyl, so just being significantly improved with the intermiscibility of filler, pigment, polar resin.Wetability in polar system, point
Dissipate property and be better than Tissuemat E, while also have concurrently coupled, balance is compared to PVC inside and outside lubrication；In hard transparent, no
Its lubricity of addition OPE is better than other lubricants in transparent PVC formulas.It is widely used in PE, PVC cable
Making, PVC profile, tubing make, the novel plastic lubricant that can yet be regarded as excellent.
Tissuemat E（PE waxes）, also known as macromolecule wax abbreviation Tissuemat E.Because of its excellent cold resistance, heat resistance, resistance toization
Learn property and wearability and be widely used.In normal production, this part wax can be applied directly to polyene as a kind of additive
In hydrocarbon processing, it can increase the gloss and processing characteristics of product.As lubricant, its chemical property is stable, electrical property is good.
Tissuemat E and polyethylene, polypropylene, poly- cerinic acid ethene, EP rubbers, butyl rubber intermiscibility are good.Polyethylene can be improved, gathered
Propylene, ABS mobility and polymethyl methacrylate, the release property of makrolon.For PVC and other exterior lubricants
Compare, Tissuemat E has stronger internal lubrication effect.
Claims (5)
1. a kind of compounded lubricant, it is characterised in that including following components, the weight ratio of each component is：Stearic acid 5-15, Fischer-Tropsch
Wax 10-30, OPE 5-15, Tissuemat E 60-70.
2. a kind of compounded lubricant according to claim 1, it is characterised in that the weight ratio of each component is：Stearic acid 5-
10, Fischer-Tropsch wax 20-30, OPE 10-15, Tissuemat E 60-70.
3. a kind of preparation method of compounded lubricant, it is characterised in that by various components by component than input reactor, reaction temperature
Spend 150-200 degree, hour time 1-2, through steel band granulating and forming.
4. the preparation method of a kind of compounded lubricant according to claim 3, it is characterised in that enter according to following steps
OK：Stearic acid, OPE and Tissuemat E are mixed as reactant A, using Fischer-Tropsch wax as reactant B, by A and B
Alternating, which is squeezed into, carries out hybrid reaction in reactor.
A kind of 5. preparation method of compounded lubricant according to claim 4, it is characterised in that reactant B is first squeezed into, then
Reactant A is squeezed into, so alternately squeezes into and hybrid reaction is carried out in reactor.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710444783.6A CN107418031A (en) | 2017-06-13 | 2017-06-13 | A kind of compounded lubricant and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710444783.6A CN107418031A (en) | 2017-06-13 | 2017-06-13 | A kind of compounded lubricant and preparation method thereof |
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| Publication Number | Publication Date |
|---|---|
| CN107418031A true CN107418031A (en) | 2017-12-01 |
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| CN201710444783.6A Pending CN107418031A (en) | 2017-06-13 | 2017-06-13 | A kind of compounded lubricant and preparation method thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109929193A (en) * | 2019-03-15 | 2019-06-25 | 青岛中塑高新材料有限公司 | A kind of PVC rigid tube lubrication brightener and preparation method thereof |
| CN110305584A (en) * | 2019-07-15 | 2019-10-08 | 内蒙古曜园材料科技有限公司 | A kind of heat molten type road gage mark coating PE wax and preparation method thereof |
| CN111607238A (en) * | 2020-07-03 | 2020-09-01 | 江苏法迩蜡业有限公司 | Composite wax for PVC (polyvinyl chloride) stone-plastic floor and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103265818A (en) * | 2013-05-28 | 2013-08-28 | 广州赫尔普化工有限公司 | Compound lubricant for wood-plastic composite material |
| CN103304881A (en) * | 2013-06-26 | 2013-09-18 | 山东阳谷华泰化工股份有限公司 | Novel carbon black dispersing agent for rubber and preparation method thereof |
-
2017
- 2017-06-13 CN CN201710444783.6A patent/CN107418031A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103265818A (en) * | 2013-05-28 | 2013-08-28 | 广州赫尔普化工有限公司 | Compound lubricant for wood-plastic composite material |
| CN103304881A (en) * | 2013-06-26 | 2013-09-18 | 山东阳谷华泰化工股份有限公司 | Novel carbon black dispersing agent for rubber and preparation method thereof |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109929193A (en) * | 2019-03-15 | 2019-06-25 | 青岛中塑高新材料有限公司 | A kind of PVC rigid tube lubrication brightener and preparation method thereof |
| CN110305584A (en) * | 2019-07-15 | 2019-10-08 | 内蒙古曜园材料科技有限公司 | A kind of heat molten type road gage mark coating PE wax and preparation method thereof |
| CN111607238A (en) * | 2020-07-03 | 2020-09-01 | 江苏法迩蜡业有限公司 | Composite wax for PVC (polyvinyl chloride) stone-plastic floor and preparation method thereof |
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| PB01 | Publication | ||
| PB01 | Publication | ||
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| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20171201 |