Preparation method for the pure titanium hollow billet of TA2
Technical field
The present invention relates to a kind of preparation methods to belong to gold more particularly, to a kind of preparation method for the pure titanium hollow billet of TA2
Belong to pipe manufacturing process technical field.
Background technique
Pure titanium is extremely active metal, is heated to 890 DEG C or more and is easy for reacting with O, N, H in air and generate
Compound forms brittle layer, influences the defects of being plastically deformed or cracking after deforming.Due to contract and Equipment, early period
Pure titanium hollow billet roll piercing mainly with barrel shaped roll roll piercing, specification also mostly in Φ 100mm hereinafter, rare Φ 200mm with
On hollow billet preparation.As certain contract requirements of military project pipe and marine worker pipe occur, the pure titanium hollow billet of Φ 200mm or more is needed to be
Cold rolling titanium tube provides blank, promotes to prepare pure titanium hollow billet using the roll piercing with rolling angle and possibility occurs.But due to oblique
The pure titanium blank of perforation procedure is rolled by more complicated alternate stress, and the axial rolling that the strain of generation is more common is increasingly complex, rolling
Process stability is poor, causes the above hollow billet preparation of Φ 200mm more difficult, fails effectively to carry out roll piercing always, also have no
There is the report of bulk production.
It perforates relative to squeezing, the synthesis production cost of roll piercing is lower, and is able to produce equivalent specifications outer diameter condition
The lower longer hollow billet of length, for this purpose, effectively realizing that pure titanium heavy caliber hollow billet oblique rolling perforated process just seems more necessary.
Summary of the invention
The technical problems to be solved by the present invention are: providing a kind of diameter that can effectively produce greater than 100 ㎜, and can guarantee
The preparation method for the pure titanium hollow billet of TA2 of the quality of production.
Used technical solution is to solve above-mentioned technical problem: a kind of preparation method for the pure titanium hollow billet of TA2, institute
The preparation method stated is based on ordinary carbon steel hollow billet oblique rolling perforated process, using the titanium base heated under micro-oxygenation atmospheric condition
For blank, the pure titanium hollow billet that outer diameter is not less than 115 ㎜ is made by following piercing process parameters,
It is 11%~13% that the piercing process parameter, which is overall diameter reduction ratio, top front reduction ratio be 5.5%~
7.5%, oval coefficient is 1.16~1.22, and feed angle is 8.5 °, and rolling angle is 14.2 °, punching rate 0.20m/s, godet
Speed is 0.60m/s.
The beneficial effects of the present invention are: by using above-mentioned technological parameter provided by the present application, it can be with ordinary carbon steel
Based on hollow billet oblique rolling perforated process, uses the titanium base heated under micro-oxygenation atmospheric condition that outer diameter is made for blank and be not less than
The pure titanium hollow billet of 180 ㎜.And since titanium base blank is heated under micro-oxygenation atmospheric condition, it can also be ensured that
A large amount of oxygen layer will not be generated in heating process, to guarantee the quality of the pure titanium hollow billet of production.
Further, first carrying out machine end to end in blank before carrying out the heating under micro-oxygenation atmospheric condition to titanium base
Tool drilling centering.
The preferred mode of the above solution is that parameter is when carrying out machine drilling centering end to end to blank,
Head end centering bore dia d=50 ± 2mm, depth h=40 ± 2mm;Tail end centering bore dia d=50 ± 2mm, depth
H=100 ± 2mm, and internal point bottom needs rounding off.
Further, coming directly towards when the blank completed to heating carries out roll piercing as in three small hole for water sprayings of band
Water cooling top, top outer surface carry out hanging mould processing;Roll is cutting and the half new roll that annular knurl cutter trade is just ground off;It leads
Disk is the half new godet that surface cutter trade is just ground off.
The preferred mode of the above solution is that cooling down operation process of interior water cooling top during apical pore is, water cooling mandril,
Cooling water is opened when top is in state to be rolled, cooling water is closed when retracting in top, and cooling water pressure after booster pump is maintained at
Between 0.7-1.0MPa.
Further: before perforation procedure, godet is first coated into special lube, to upper and lower godet in the operation of rolling
It applies slip coating and keeps lubrication;It is secondary bite foundation after perforating roller cooling water is reached into big water state be lubricated and cool down;It leads
Disk cooling water is opened again after the completion of perforation and is cooled down.
The preferred mode of the above solution is that being by following when being heated using micro-oxygenation atmospheric condition to titanium base
What work step was operated,
Annular furnace bringing-up section burner is closed, only opens soaking zone burner, air-fuel ratio is kept micro-oxygenation atmosphere by 12:1;?
The carbon steel stopper material of 2 same outer diameter scales of arrangement before and after titanium base, to guarantee that titanium base temperature is uniform;Annular furnace soaking zone instrument temperature
Degree control is at 890~900 DEG C.
Further, each section of rotary heating furnace of heating temperature and heating time are as follows,
Specific embodiment
In order to solve the above technical problems existing in the prior art, diameter can effectively be produced the present invention provides a kind of
Greater than 100 ㎜, and it can guarantee the preparation method for the pure titanium hollow billet of TA2 of the quality of production.The preparation method is with common carbon
Based on steel wool pipe oblique rolling perforated process, use the titanium base heated under micro-oxygenation atmospheric condition for blank, by following perforation
The pure titanium hollow billet that outer diameter is not less than 180 ㎜ is made in technological parameter, and it is 11% that the piercing process parameter, which is overall diameter reduction ratio,
~13%, top front reduction ratio is 5.5%~7.5%, and oval coefficient is 1.16~1.22, and feed angle is 8.5 °, and rolling angle is
14.2 °, punching rate 0.20m/s, godet speed is 0.60m/s.By using above-mentioned technological parameter provided by the present application, just
The titanium base heated under micro-oxygenation atmospheric condition can be used for blank system based on ordinary carbon steel hollow billet oblique rolling perforated process
Obtain the pure titanium hollow billet that outer diameter is not less than 180 ㎜.And since titanium base blank is heated under micro-oxygenation atmospheric condition,
It can also guarantee that a large amount of oxygen layer will not be generated during heating, to guarantee the quality of the pure titanium hollow billet of production.
In above embodiment, in order to avoid pure titanium blank to generate oxide layer in heating process to greatest extent, using
It when micro-oxygenation atmospheric condition heats titanium base, is operated by following work steps, closes annular furnace bringing-up section burner,
Soaking zone burner is only opened, air-fuel ratio is kept micro-oxygenation atmosphere by 12:1;2 same outer diameter scales are arranged before and after titanium base
Carbon steel stopper material, to guarantee that titanium base temperature is uniform;Annular furnace soaking zone instrument temperature is controlled at 890~900 DEG C;And annular adds
The heating temperature and heating time that each section of hot stove are as follows,
In order to guarantee the quality of production of the pure titanium hollow billet of major diameter to greatest extent, this application provides further technique limits
Determine parameter and first carries out machine drilling centering end to end in blank that is, before carrying out the heating under micro-oxygenation atmospheric condition to titanium base;
Particularly, when carrying out machine drilling centering end to end to blank, parameter is, head end centering bore dia d=50 ± 2mm, depth h
=40 ± 2mm;Tail end centering bore dia d=50 ± 2mm, depth h=100 ± 2mm, and internal point bottom needs rounding off.
When the blank completed to heating carries out roll piercing, the interior water cooling top for three small hole for water sprayings of band is come directly towards, outer surface is come directly towards
It carries out hanging mould processing;Roll is cutting and the half new roll that annular knurl cutter trade is just ground off;Godet is that surface cutter trade is rigid
The half new godet ground off well;Cooling down operation process of interior water cooling top during apical pore is that water cooling mandril, top are in be rolled
Open cooling water when state, cooling water is closed in top when retracting, cooling water pressure after booster pump be maintained at 0.7-1.0MPa it
Between;Before perforation procedure, godet is first coated into special lube, slip coating is applied to upper and lower godet in the operation of rolling and keeps profit
It is sliding;It is secondary bite foundation after perforating roller cooling water is reached into big water state be lubricated and cool down;Godet cooling water is being perforated
Cheng Houzai opening is cooled down.
Embodiment
Specifically operating procedure is
The heating temperature and heating time that each section of rotary heating furnace
TA2 quickly arrives punch after coming out of the stove and perforates, and perforation is carried out by designed technological parameter.
Cooling water (cooling water is closed when retracting in top), cooling water warp are opened when water cooling mandril, top are in state to be rolled
Pressure is maintained between 0.7-1.0MPa after booster pump.
With 340 adhesion resistant steel slip coatings (i.e. with 159 red oil+ink-consolidating agent 1:1 exchange), first godet is coated before perforation dedicated
Lubricating oil applies slip coating to upper and lower godet in the operation of rolling and keeps lubrication;It is secondary bite foundation after perforating roller cooling water is opened
To big water state, led to be lubricated and to cool down;Godet cooling water is opened again after the completion of perforation and is cooled down.
Embodiment 1
Roll piercing is the hollow billet of Φ 212 × 16 after the pure titanium blank heating of the TA2 of Φ 200.
Embodiment 2
Roll piercing is the hollow billet of Φ 179 × 18.5 after the pure titanium blank heating of the TA2 of Φ 160.
Embodiment 3
Roll piercing is the hollow billet of Φ 118 × 9.5 after the pure titanium blank heating of the TA2 of Φ 115.