CN107389564A - A kind of method for differentiating stir-baked RHIZOMA ATRACTYLDIS MACROCEPHALAE in bran and processing the duration and degree of heating - Google Patents
A kind of method for differentiating stir-baked RHIZOMA ATRACTYLDIS MACROCEPHALAE in bran and processing the duration and degree of heating Download PDFInfo
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- CN107389564A CN107389564A CN201710620282.9A CN201710620282A CN107389564A CN 107389564 A CN107389564 A CN 107389564A CN 201710620282 A CN201710620282 A CN 201710620282A CN 107389564 A CN107389564 A CN 107389564A
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- 238000000034 method Methods 0.000 title claims abstract description 43
- 238000012545 processing Methods 0.000 title claims abstract description 36
- 238000010438 heat treatment Methods 0.000 title claims abstract description 29
- 239000003610 charcoal Substances 0.000 claims description 6
- 241000132012 Atractylodes Species 0.000 abstract description 17
- 230000007812 deficiency Effects 0.000 abstract description 3
- 239000003814 drug Substances 0.000 description 14
- 238000001514 detection method Methods 0.000 description 6
- 239000000523 sample Substances 0.000 description 5
- 239000000463 material Substances 0.000 description 4
- 229940079593 drug Drugs 0.000 description 3
- 230000001953 sensory effect Effects 0.000 description 3
- 241000092665 Atractylodes macrocephala Species 0.000 description 2
- 235000008495 Chrysanthemum leucanthemum Nutrition 0.000 description 2
- 235000000604 Chrysanthemum parthenium Nutrition 0.000 description 2
- 240000004460 Tanacetum coccineum Species 0.000 description 2
- 125000003118 aryl group Chemical group 0.000 description 2
- 230000007547 defect Effects 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 235000008384 feverfew Nutrition 0.000 description 2
- 235000012907 honey Nutrition 0.000 description 2
- 210000000952 spleen Anatomy 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 235000015099 wheat brans Nutrition 0.000 description 2
- 206010012735 Diarrhoea Diseases 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 206010062717 Increased upper airway secretion Diseases 0.000 description 1
- 206010022998 Irritability Diseases 0.000 description 1
- 244000174681 Michelia champaca Species 0.000 description 1
- 206010030113 Oedema Diseases 0.000 description 1
- 206010033557 Palpitations Diseases 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- 208000019790 abdominal distention Diseases 0.000 description 1
- 206010003549 asthenia Diseases 0.000 description 1
- 210000001124 body fluid Anatomy 0.000 description 1
- 239000010839 body fluid Substances 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 208000002173 dizziness Diseases 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000002708 enhancing effect Effects 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 230000001605 fetal effect Effects 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 241000411851 herbal medicine Species 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 239000006101 laboratory sample Substances 0.000 description 1
- 239000012567 medical material Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000000149 penetrating effect Effects 0.000 description 1
- 208000026435 phlegm Diseases 0.000 description 1
- 238000011002 quantification Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 238000005464 sample preparation method Methods 0.000 description 1
- 210000000697 sensory organ Anatomy 0.000 description 1
- 230000002269 spontaneous effect Effects 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 238000002604 ultrasonography Methods 0.000 description 1
- 238000012795 verification Methods 0.000 description 1
Classifications
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/17—Systems in which incident light is modified in accordance with the properties of the material investigated
- G01N21/25—Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
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- Spectroscopy & Molecular Physics (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
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- Analytical Chemistry (AREA)
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- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Spectrometry And Color Measurement (AREA)
Abstract
The invention provides a kind of method for differentiating stir-baked RHIZOMA ATRACTYLDIS MACROCEPHALAE in bran and processing the duration and degree of heating, it comprises the following steps：A) detected sample is taken；B) sample space colorimetric parameter L*, b* value is processed with measure；C) bring L*, b* value measured in step b) into discriminate, calculate A and B value, wherein A=0.614 × L*+0.705 × b*, 0.724 × b* of B=0.803 × L*；D) the different processing duration and degree of heating are determined according to discriminant score.The inventive method will can process color standard objectify, precision, make up the deficiency of traditional duration and degree of heating method of discrimination, the setting for bighead atractylodes rhizome processing procedure parameter provides scientific basis.
Description
Technical field
The present invention relates to a kind of method for differentiating and processing the duration and degree of heating, specifically, being related to a kind of discriminating stir-baked RHIZOMA ATRACTYLDIS MACROCEPHALAE in bran processes the duration and degree of heating
Method.
Background technology
The bighead atractylodes rhizome is feverfew bighead atractylodes rhizome Atractylodes macrocephala Koidz. dry rhizome, is " tonifying Qi
The key medicine of invigorating the spleen first ", clinically for diseases such as spleen eating less, abdominal distention diarrhea, phlegm and retained fluid, feel dizzy and heart palpitations, oedema, spontaneous perspiration, fetal irritabilities.Pass
System thinks that bighead atractylodes rhizome health product eliminating dampness power is strong, has certain dry property, the dry thirsty and yin asthenia generating intrinsic heat person of all body fluid losses should not take, through bran
The property of medicine relaxes after stir-fry, curative effect enhancing, can also expand function by the work(of auxiliary material, expand clinical application range.
Ming Dynasty's Chen Jia plans exist《Book on Chinese herbal medicine covers an aromatic plant metioned in ancient books》In point out that " pharmacy is valued for moderate, and too late then effect is hard to find, too then smell is anti-
Lose ... ", it is seen that the processing of medical material duration and degree of heating is that the clinical efficacy of Chinese medicine is directly affected an important factor for determining to process quality.
Version Chinese Pharmacopoeia one in 2015 processes the duration and degree of heating to stir-baked RHIZOMA ATRACTYLDIS MACROCEPHALAE in bran and is described as " frying to yellowish-brown, effusion burnt odor gas "；2015 editions《Four
River province prepared slices of Chinese crude drugs concocted specification》Description thereof is " frying to surface buff, aromatic spilling ", it is seen that color is that the duration and degree of heating judges
One of important indicator.In addition, Li Xuelian etc. (during bighead atractylodes rhizome bran is fried color and material base change correlation research [D] into
All:Chengdu University of Traditional Chinese Medicine, 2015.) find that stir-baked RHIZOMA ATRACTYLDIS MACROCEPHALAE in bran medicine materical crude slice color value and material base have significant correlation.But so far
Color judgement is still more to combine macroscopic sensory judgments with subjective description, and objectivity and accuracy are difficult to ensure that.Meanwhile with
" yellowish-brown ", " buff " are used as duration and degree of heating criterion, and its color standard scope is excessively broad, it is impossible to atractylodes slice is effectively ensured
Quality stable homogeneous.
The content of the invention
To solve the above problems, differentiate the different objective quantification sides for processing the duration and degree of heating of stir-baked RHIZOMA ATRACTYLDIS MACROCEPHALAE in bran the invention provides a kind of
Method.
The invention provides a kind of method for differentiating stir-baked RHIZOMA ATRACTYLDIS MACROCEPHALAE in bran and processing the duration and degree of heating, it comprises the following steps：
A) detected sample is taken；
B) sample space colorimetric parameter L*, b* value is processed with measure；
C) L*, b* value measured in step b) will be brought into discriminate, calculate A and B value, wherein A=0.614 × L*+
0.705 × b*, B=0.803 × L*-0.724 × b*；
D) according to standardization allusion quotation, then functional value scope determines the different processing duration and degree of heating.
Wherein, L*, b* value in step b are that the bighead atractylodes rhizome is processed into medicine materical crude slice number of colours value:Wherein L* represents atractylodes slice face
The brightness of color, L* values are bigger, then illustrate that the color of atractylodes slice is brighter, and b* values represent the champac degree of medicine materical crude slice color, when b* values
Illustrate that medicine materical crude slice color is more yellow when bigger, when b* values are smaller, show that color is more blue.
Wherein, in step a, the sample is that bran is fried and obtained at a temperature of 280~330 DEG C.
Wherein, in step b, space chromacity parameter L*, b* value is determined with color evaluating.
Preferably, in step d, determine that the mode of the different processing duration and degree of heating is as follows：
When the scope that A scope is 56.6031~60.4934, B is 20.0038~24.7614, it is determined that the degree of processing is
Fry light；
When the scope that A scope is 42.8153~59.2535, B is 10.0264~18.8925, it is determined that the degree of processing is
Stir-bake to yellowish；
When the scope that A scope is 16.4152~41.2825, B is 8.4903~14.8910, it is determined that the degree of processing is stir-fry
It is burnt；
When the scope that A scope is 11.8896~15.8316, B is 10.7985~15.3658, it is determined that the degree of processing is
Fry charcoal；
6th, preferably, the processing duration and degree of heating is：It is below 4min to fry the light time；The stir-bake to yellowish time is 8-16min；During stir-bake to brown
Between be 20-24min；It is more than 28min to fry the charcoal time.
The invention provides a kind of method for differentiating stir-baked RHIZOMA ATRACTYLDIS MACROCEPHALAE in bran and processing the duration and degree of heating, overcomes main using master in the prior art
See description the process of preparing with reference to caused by visually observing the subjective factors such as sensory judgments' method it is too late with too the defects of.Can be by big gun
Color standard processed objectifies, precision, makes up the deficiency of traditional duration and degree of heating method of discrimination, is carried for the setting of bighead atractylodes rhizome processing procedure parameter
For scientific basis.
According to the above of the present invention, according to the ordinary technical knowledge and customary means of relevant art, not
Under the premise of departing from the above-mentioned basic fundamental thought of the present invention, the modification, replacement or change of other diversified forms can also be made.
Embodiment
The detection method of the present invention of embodiment 1
Detection method comprises the following steps：
1. take sample：Taking processed products of Rhizoma Atractylodis Macrocephalae to be checked, (processed product can be according to 2015 editions Chinese Pharmacopoeias (0213 processes general rule)
Bran is fried concocting method and processed under.Using temperature in the pot of two-dimensional infrared imager detection machine for stir-frying Chinese medicine, temperature in concocting process
When degree reaches 280~330 DEG C, add honey and process wheat bran, when smoldering, be rapidly added the net bighead atractylodes rhizome).
2. determine space chromacity parameter L*, b* value with color evaluating.
3. into discriminate will be brought L*, b* for being measured in step 2 value, A and B value, wherein A=0.614 × L*+ are calculated
0.705 × b*, B=0.803 × L*-0.724 × b*；.
As a result：
Determine that the mode of the different processing duration and degree of heating is as follows：
When the scope that A scope is 56.6031~60.4934, B is 20.0038~24.7614, it is determined that the degree of processing is
Fry light；
When the scope that A scope is 42.8153~59.2535, B is 10.0264~18.8925, it is determined that the degree of processing is
Stir-bake to yellowish；
When the scope that A scope is 16.4152~41.2825, B is 8.4903~14.8910, it is determined that the degree of processing is stir-fry
It is burnt；
When the scope that A scope is 11.8896~15.8316, B is 10.7985~15.3658, it is determined that the degree of processing is
Fry charcoal；
7th, preferably, the processing duration and degree of heating is：It is below 4min to fry the light time；The stir-bake to yellowish time is 8-16min；During stir-bake to brown
Between be 20-24min；It is more than 28min to fry the charcoal time.
The verification method of the present invention of embodiment 2
1. experiment material
1.1 instrument
CM-5-Spectrophotometer color evaluatings (Konica Minolta Co., Ltd), 380Lc type two dimensions are red
Outer imager (German DIAS companies), CY-900 types machine for stir-frying Chinese medicine (the grand steel in Nanjing contains mechanical equipment factory), SB-5200DT ultrasounds are clear
Wash device (500W, 50KHz).
1.2 laboratory sample
Atractylodes slice is provided by certain medicine materical crude slice company, is awarded through Lu elder generation of Chengdu University of Traditional Chinese Medicine penetrating judgment and is accredited as the feverfew bighead atractylodes rhizome
Atractylodes macrocephala Koidz. dry rhizome, meets through quality inspection《Chinese Pharmacopoeia》Version is white within 2015
Provided under art item.
Sample is made using the sample preparation methods of embodiment 1, i.e., according to 2015 editions Chinese Pharmacopoeias (0213 processes general rule)
Bran is fried concocting method and processed under.Using temperature in the pot of two-dimensional infrared imager detection machine for stir-frying Chinese medicine, temperature in concocting process
When degree reaches 280~330 DEG C, add honey and process wheat bran, when smoldering, be rapidly added the net bighead atractylodes rhizome, take different concocted time point samples
15.
2. detection method
Detected using the method for embodiment 1.
3. testing result
The testing result of 1 different processed products of table
Learnt by table 1, the different bighead atractylodes rhizomes for processing the duration and degree of heating of present invention detection work well, rate of accuracy reached to 100%.Conventional big gun
Using " yellowish-brown ", " buff " as duration and degree of heating criterion in method of discrimination processed, combined using subjective description and visually observe sense organ
Evaluation method, objectivity and accuracy are difficult to ensure that.Simultaneously as color standard scope is excessively broad, it is impossible to is effectively ensured white
Art prepared slice quality stable homogeneous.The present invention can objectify color standard, precision, make up traditional duration and degree of heating method of discrimination not
Foot, the setting for bighead atractylodes rhizome processing procedure parameter provide scientific basis.
To sum up, the invention provides a kind of method for differentiating stir-baked RHIZOMA ATRACTYLDIS MACROCEPHALAE in bran and processing the duration and degree of heating, overcome main in the prior art
Using subjective description process of preparing with reference to caused by visually observing the subjective factors such as sensory judgments' method it is too late with too the defects of.
To can process color standard objectify, precision, make up the deficiency of traditional duration and degree of heating method of discrimination, be bighead atractylodes rhizome processing procedure parameter
Setting provides scientific basis.
Claims (5)
- A kind of 1. method for differentiating stir-baked RHIZOMA ATRACTYLDIS MACROCEPHALAE in bran and processing the duration and degree of heating, it is characterised in that：It comprises the following steps：A) detected sample is taken；B) sample space colorimetric parameter L*, b* value is processed with measure；C) bring L*, b* value measured in step b) into discriminate, calculate A and B value, wherein A=0.614 × L*+0.705 × B*, B=0.803 × L*-0.724 × b*；D) the different processing duration and degree of heating are determined according to discriminant score.
- 2. according to the method for claim 1, it is characterised in that：In step a, the sample is at a temperature of 280~330 DEG C Bran is fried and obtained.
- 3. according to the method for claim 1, it is characterised in that：In step b, space chromacity parameter L*, b* value color color Difference meter measure.
- 4. according to the method for claim 1, it is characterised in that：In step d, determine that the mode of the different processing duration and degree of heating is as follows：When the scope that A scope is 56.6031~60.4934, B is 20.0038~24.7614, it is determined that the degree of processing is light to fry；When the scope that A scope is 42.8153~59.2535, B is 10.0264~18.8925, it is determined that the degree of processing is stir-bake to yellowish；When the scope that A scope is 16.4152~41.2825, B is 8.4903~14.8910, it is determined that the degree of processing is stir-bake to brown；When the scope that A scope is 11.8896~15.8316, B is 10.7985~15.3658, it is determined that the degree of processing is stir-fry charcoal.
- 5. the method according to claim 1 or 4, it is characterised in that：It is described processing the duration and degree of heating be：Fry the light time for 4min with Under；The stir-bake to yellowish time is 8-16min；The stir-bake to brown time is 20-24min；It is more than 28min to fry the charcoal time.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN111323379A (en) * | 2020-04-23 | 2020-06-23 | 山东省中医药研究院 | Method for judging processing quality of platycladus orientalis charcoal |
| CN111487202A (en) * | 2019-01-29 | 2020-08-04 | 沈阳药科大学 | Method for controlling processing process of cattail pollen on line |
| CN111795877A (en) * | 2020-07-09 | 2020-10-20 | 重庆市中药研究院 | Digital quality control method for chromaticity of fructus psoraleae |
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| CN104931433A (en) * | 2015-07-01 | 2015-09-23 | 西北农林科技大学 | CIELAB color space based method for determining apple color |
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2017
- 2017-07-26 CN CN201710620282.9A patent/CN107389564B/en not_active Expired - Fee Related
Patent Citations (1)
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| CN104931433A (en) * | 2015-07-01 | 2015-09-23 | 西北农林科技大学 | CIELAB color space based method for determining apple color |
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| 李旻等: "基于颜色客观化的陈皮药材鉴别", 《中国实验方剂学杂质》 * |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111487202A (en) * | 2019-01-29 | 2020-08-04 | 沈阳药科大学 | Method for controlling processing process of cattail pollen on line |
| CN111323379A (en) * | 2020-04-23 | 2020-06-23 | 山东省中医药研究院 | Method for judging processing quality of platycladus orientalis charcoal |
| CN111795877A (en) * | 2020-07-09 | 2020-10-20 | 重庆市中药研究院 | Digital quality control method for chromaticity of fructus psoraleae |
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