CN107383925A - A kind of preparation method of enhanced environment-friendlyinsulation insulation material - Google Patents

A kind of preparation method of enhanced environment-friendlyinsulation insulation material Download PDF

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Publication number
CN107383925A
CN107383925A CN201710823444.9A CN201710823444A CN107383925A CN 107383925 A CN107383925 A CN 107383925A CN 201710823444 A CN201710823444 A CN 201710823444A CN 107383925 A CN107383925 A CN 107383925A
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China
Prior art keywords
parts
temperature
area
preparation
insulation material
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Pending
Application number
CN201710823444.9A
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Chinese (zh)
Inventor
唐正华
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RUGAO CITY LEHENG CHEMICAL Co Ltd
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RUGAO CITY LEHENG CHEMICAL Co Ltd
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Priority to CN201710823444.9A priority Critical patent/CN107383925A/en
Publication of CN107383925A publication Critical patent/CN107383925A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L101/00Compositions of unspecified macromolecular compounds
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29CSHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C45/00Injection moulding, i.e. forcing the required volume of moulding material through a nozzle into a closed mould; Apparatus therefor
    • B29C45/17Component parts, details or accessories; Auxiliary operations
    • B29C45/76Measuring, controlling or regulating
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29CSHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C45/00Injection moulding, i.e. forcing the required volume of moulding material through a nozzle into a closed mould; Apparatus therefor
    • B29C45/17Component parts, details or accessories; Auxiliary operations
    • B29C45/76Measuring, controlling or regulating
    • B29C45/77Measuring, controlling or regulating of velocity or pressure of moulding material
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29CSHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C45/00Injection moulding, i.e. forcing the required volume of moulding material through a nozzle into a closed mould; Apparatus therefor
    • B29C45/17Component parts, details or accessories; Auxiliary operations
    • B29C45/76Measuring, controlling or regulating
    • B29C45/78Measuring, controlling or regulating of temperature
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29CSHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C2945/00Indexing scheme relating to injection moulding, i.e. forcing the required volume of moulding material through a nozzle into a closed mould
    • B29C2945/76Measuring, controlling or regulating
    • B29C2945/76494Controlled parameter
    • B29C2945/76498Pressure
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B29WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
    • B29CSHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
    • B29C2945/00Indexing scheme relating to injection moulding, i.e. forcing the required volume of moulding material through a nozzle into a closed mould
    • B29C2945/76Measuring, controlling or regulating
    • B29C2945/76494Controlled parameter
    • B29C2945/76531Temperature
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2201/00Properties
    • C08L2201/08Stabilised against heat, light or radiation or oxydation
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/03Polymer mixtures characterised by other features containing three or more polymers in a blend
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/14Polymer mixtures characterised by other features containing polymeric additives characterised by shape
    • C08L2205/16Fibres; Fibrils

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  • Engineering & Computer Science (AREA)
  • Manufacturing & Machinery (AREA)
  • Mechanical Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Reinforced Plastic Materials (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Injection Moulding Of Plastics Or The Like (AREA)

Abstract

The present invention relates to a kind of preparation method of enhanced environment-friendlyinsulation insulation material, the enhanced environment-friendlyinsulation insulation material is made up of the component of following parts by weight:6 10 parts of 80 120 parts of 6 resins of HRB, 20 40 parts of alkali-free glass fibre silk, 8 12 parts of polypropylene fibre, 46 parts of solubilizer, 16 24 parts of nano-stephanoporate silicon dioxide, 5 15 parts of dimethicone and antioxidant.The advantage of the invention is that:By the preparation method of the enhanced environment-friendlyinsulation insulation material of the present invention, the insulating materials mechanical strength prepared is high, heat-resist, has good resistance to sparking energy, is a kind of environment-friendlyinsulation insulation material of excellent combination property.

Description

A kind of preparation method of enhanced environment-friendlyinsulation insulation material
Technical field
The present invention relates to insulating materials technical field, more particularly to a kind of preparation method of enhanced environment-friendlyinsulation insulation material.
Background technology
Polyester due to its excellent molding processibility, electrical insulating property and heat resistance be widely used in electronics, electrical equipment and The industries such as household electrical appliances.In recent years, with highest attention of the society to environmental problem, the environmentally friendly poly terephthalic acid in polyester Butanediol ester(PBT)It is widely used in insulating material field.Electric field is often referred to high temperature, hyperbaric environment, and common Because mechanical strength, heat resistance and dielectric properties are not good enough electrical breakdown easily occurs in above-mentioned environment for PBT material.
The content of the invention
The technical problem to be solved in the present invention is to provide it is a kind of disclosure satisfy that high temperature, hyperbaric environment requirement it is enhanced The preparation method of environment-friendlyinsulation insulation material.
In order to solve the above technical problems, the technical scheme is that:A kind of preparation side of enhanced environment-friendlyinsulation insulation material Method, its innovative point are:The preparation method comprises the following steps:
(1)Each raw material for standby is accurately weighed by weight ratio:HRB-6 resin 80-120 parts, alkali-free glass fibre silk 20-40 Part, polypropylene fibre 8-12 parts, solubilizer 4-6 parts, nano-stephanoporate silicon dioxide 16-24 parts, dimethicone 5-15 parts and anti- Oxygen agent 6-10 parts;
(2)HRB-6 resins, solubilizer, nano-stephanoporate silicon dioxide and antioxidant are sequentially added in banbury, with 100 turns/ Min rotating speed is stirred 20min, and banbury then is warming up into 190 DEG C, and nothing is sequentially added from loading hopper while stirring Alkali containing glass fibre silk, polypropylene fibre and dimethicone, 10~20min of banburying, compound is set all to mix, after cooling down Discharging, and cut into fine grained chippings;
(3)By step(2)The injection machine injection molding of the fine grained chippings of middle preparation, Shooting Technique condition are:One 190 DEG C of area's temperature, Two 220 DEG C of area's temperature, three 220 DEG C of area's temperature, four 220 DEG C of area's temperature, five 200 DEG C of area's temperature, injection pressure 10MPa, during pressurize Between 5min.
The advantage of the invention is that:By the preparation method of the enhanced environment-friendlyinsulation insulation material of the present invention, the insulation prepared Mechanics of materials intensity is high, heat-resist, has good resistance to sparking energy, is a kind of environmentally friendly insulation material of excellent combination property Material.
Embodiment
The following examples can make professional and technical personnel that the present invention be more fully understood, but therefore not send out this It is bright to be limited among described scope of embodiments.
Embodiment 1
The preparation method of the enhanced environment-friendlyinsulation insulation material of the present embodiment, the preparation method comprise the following steps:
(1)Each raw material for standby is accurately weighed by weight ratio:80 parts of HRB-6 resins, 20 parts of alkali-free glass fibre silk, polypropylene 6 parts of 8 parts of fiber, 4 parts of solubilizer, 16 parts of nano-stephanoporate silicon dioxide, 5 parts of dimethicone and antioxidant;
(2)HRB-6 resins, solubilizer, nano-stephanoporate silicon dioxide and antioxidant are sequentially added in banbury, with 100 turns/ Min rotating speed is stirred 20min, and banbury then is warming up into 190 DEG C, and nothing is sequentially added from loading hopper while stirring Alkali containing glass fibre silk, polypropylene fibre and dimethicone, banburying 10min, compound is all mixed, go out after cooling down Material, and cut into fine grained chippings;
(3)By step(2)The injection machine injection molding of the fine grained chippings of middle preparation, Shooting Technique condition are:One 190 DEG C of area's temperature, Two 220 DEG C of area's temperature, three 220 DEG C of area's temperature, four 220 DEG C of area's temperature, five 200 DEG C of area's temperature, injection pressure 10MPa, during pressurize Between 5min.
Embodiment 2
The preparation method of the enhanced environment-friendlyinsulation insulation material of the present embodiment, the preparation method comprise the following steps:
(1)Each raw material for standby is accurately weighed by weight ratio:120 parts of HRB-6 resins, 40 parts of alkali-free glass fibre silk, poly- third 10 parts of 12 parts of alkene fiber, 6 parts of solubilizer, 24 parts of nano-stephanoporate silicon dioxide, 15 parts of dimethicone and antioxidant;
(2)HRB-6 resins, solubilizer, nano-stephanoporate silicon dioxide and antioxidant are sequentially added in banbury, with 100 turns/ Min rotating speed is stirred 20min, and banbury then is warming up into 190 DEG C, and nothing is sequentially added from loading hopper while stirring Alkali containing glass fibre silk, polypropylene fibre and dimethicone, banburying 20min, compound is all mixed, go out after cooling down Material, and cut into fine grained chippings;
(3)By step(2)The injection machine injection molding of the fine grained chippings of middle preparation, Shooting Technique condition are:One 190 DEG C of area's temperature, Two 220 DEG C of area's temperature, three 220 DEG C of area's temperature, four 220 DEG C of area's temperature, five 200 DEG C of area's temperature, injection pressure 10MPa, during pressurize Between 5min.
Embodiment 3
The preparation method of the enhanced environment-friendlyinsulation insulation material of the present embodiment, the preparation method comprise the following steps:
(1)Each raw material for standby is accurately weighed by weight ratio:100 parts of HRB-6 resins, 30 parts of alkali-free glass fibre silk, poly- third 8 parts of 10 parts of alkene fiber, 5 parts of solubilizer, 20 parts of nano-stephanoporate silicon dioxide, 10 parts of dimethicone and antioxidant;
(2)HRB-6 resins, solubilizer, nano-stephanoporate silicon dioxide and antioxidant are sequentially added in banbury, with 100 turns/ Min rotating speed is stirred 20min, and banbury then is warming up into 190 DEG C, and nothing is sequentially added from loading hopper while stirring Alkali containing glass fibre silk, polypropylene fibre and dimethicone, banburying 15min, compound is all mixed, go out after cooling down Material, and cut into fine grained chippings;
(3)By step(2)The injection machine injection molding of the fine grained chippings of middle preparation, Shooting Technique condition are:One 190 DEG C of area's temperature, Two 220 DEG C of area's temperature, three 220 DEG C of area's temperature, four 220 DEG C of area's temperature, five 200 DEG C of area's temperature, injection pressure 10MPa, during pressurize Between 5min.
The general principle and principal character and advantages of the present invention of the present invention has been shown and described above.The skill of the industry For art personnel it should be appreciated that the present invention is not limited to the above embodiments, described in above-described embodiment and specification is explanation The principle of the present invention, without departing from the spirit and scope of the present invention, various changes and modifications of the present invention are possible, these Changes and improvements all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appended claims and Its equivalent thereof.

Claims (1)

  1. A kind of 1. preparation method of enhanced environment-friendlyinsulation insulation material, it is characterised in that:The preparation method comprises the following steps:
    (1)Each raw material for standby is accurately weighed by weight ratio:HRB-6 resin 80-120 parts, alkali-free glass fibre silk 20-40 Part, polypropylene fibre 8-12 parts, solubilizer 4-6 parts, nano-stephanoporate silicon dioxide 16-24 parts, dimethicone 5-15 parts and anti- Oxygen agent 6-10 parts;
    (2)HRB-6 resins, solubilizer, nano-stephanoporate silicon dioxide and antioxidant are sequentially added in banbury, with 100 turns/ Min rotating speed is stirred 20min, and banbury then is warming up into 190 DEG C, and nothing is sequentially added from loading hopper while stirring Alkali containing glass fibre silk, polypropylene fibre and dimethicone, 10~20min of banburying, compound is set all to mix, after cooling down Discharging, and cut into fine grained chippings;
    (3)By step(2)The injection machine injection molding of the fine grained chippings of middle preparation, Shooting Technique condition are:One 190 DEG C of area's temperature, Two 220 DEG C of area's temperature, three 220 DEG C of area's temperature, four 220 DEG C of area's temperature, five 200 DEG C of area's temperature, injection pressure 10MPa, during pressurize Between 5min.
CN201710823444.9A 2017-09-13 2017-09-13 A kind of preparation method of enhanced environment-friendlyinsulation insulation material Pending CN107383925A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201710823444.9A CN107383925A (en) 2017-09-13 2017-09-13 A kind of preparation method of enhanced environment-friendlyinsulation insulation material

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Application Number Priority Date Filing Date Title
CN201710823444.9A CN107383925A (en) 2017-09-13 2017-09-13 A kind of preparation method of enhanced environment-friendlyinsulation insulation material

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112466663A (en) * 2020-11-09 2021-03-09 太仓优盛电子有限公司 High-temperature dipping treatment process of transformer

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103589122A (en) * 2013-10-15 2014-02-19 昆山市奋发绝缘材料有限公司 Reinforced environment-friendly insulation material and preparation method thereof
CN105272182A (en) * 2015-10-30 2016-01-27 太仓市天合新材料科技有限公司 Multifunctional insulating material

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103589122A (en) * 2013-10-15 2014-02-19 昆山市奋发绝缘材料有限公司 Reinforced environment-friendly insulation material and preparation method thereof
CN105272182A (en) * 2015-10-30 2016-01-27 太仓市天合新材料科技有限公司 Multifunctional insulating material

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112466663A (en) * 2020-11-09 2021-03-09 太仓优盛电子有限公司 High-temperature dipping treatment process of transformer

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Application publication date: 20171124