CN107372600A - 光驱动型纳米抗菌剂及其制备方法 - Google Patents
光驱动型纳米抗菌剂及其制备方法 Download PDFInfo
- Publication number
- CN107372600A CN107372600A CN201710679953.9A CN201710679953A CN107372600A CN 107372600 A CN107372600 A CN 107372600A CN 201710679953 A CN201710679953 A CN 201710679953A CN 107372600 A CN107372600 A CN 107372600A
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- Prior art keywords
- antibacterial agent
- nano antibacterial
- solution
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- 239000003242 anti bacterial agent Substances 0.000 title claims abstract description 44
- 230000003287 optical effect Effects 0.000 title claims abstract description 14
- 238000002360 preparation method Methods 0.000 title claims abstract description 14
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 claims abstract description 59
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims abstract description 42
- 239000000243 solution Substances 0.000 claims abstract description 36
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 claims abstract description 24
- 239000007788 liquid Substances 0.000 claims abstract description 17
- 239000007787 solid Substances 0.000 claims abstract description 16
- 229910021642 ultra pure water Inorganic materials 0.000 claims abstract description 16
- 239000012498 ultrapure water Substances 0.000 claims abstract description 16
- 239000007864 aqueous solution Substances 0.000 claims abstract description 11
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Natural products OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims abstract description 9
- 241000588724 Escherichia coli Species 0.000 claims abstract description 8
- 238000005406 washing Methods 0.000 claims abstract description 8
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 7
- 229910021389 graphene Inorganic materials 0.000 claims abstract description 7
- 239000002096 quantum dot Substances 0.000 claims abstract description 7
- 239000000126 substance Substances 0.000 claims abstract description 5
- XOOUIPVCVHRTMJ-UHFFFAOYSA-L zinc stearate Chemical compound [Zn+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O XOOUIPVCVHRTMJ-UHFFFAOYSA-L 0.000 claims abstract description 5
- 241000894006 Bacteria Species 0.000 claims description 15
- 238000006243 chemical reaction Methods 0.000 claims description 12
- 238000007792 addition Methods 0.000 claims description 9
- 238000012545 processing Methods 0.000 claims description 9
- 235000015165 citric acid Nutrition 0.000 claims description 7
- 238000005286 illumination Methods 0.000 claims description 7
- 238000010992 reflux Methods 0.000 claims description 7
- 238000003756 stirring Methods 0.000 claims description 7
- 238000012546 transfer Methods 0.000 claims description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 6
- 241000222122 Candida albicans Species 0.000 claims description 4
- 241000191967 Staphylococcus aureus Species 0.000 claims description 4
- 229940095731 candida albicans Drugs 0.000 claims description 4
- 230000005284 excitation Effects 0.000 claims description 4
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 claims description 3
- 230000035484 reaction time Effects 0.000 claims description 3
- 241000894007 species Species 0.000 claims description 3
- 206010059866 Drug resistance Diseases 0.000 abstract description 3
- 230000000844 anti-bacterial effect Effects 0.000 abstract description 3
- 230000007613 environmental effect Effects 0.000 abstract description 2
- PXRKCOCTEMYUEG-UHFFFAOYSA-N 5-aminoisoindole-1,3-dione Chemical compound NC1=CC=C2C(=O)NC(=O)C2=C1 PXRKCOCTEMYUEG-UHFFFAOYSA-N 0.000 abstract 1
- 238000001035 drying Methods 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 239000000725 suspension Substances 0.000 description 9
- 230000001954 sterilising effect Effects 0.000 description 6
- 238000004659 sterilization and disinfection Methods 0.000 description 6
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 3
- 229940088710 antibiotic agent Drugs 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 239000011701 zinc Substances 0.000 description 3
- 229910052725 zinc Inorganic materials 0.000 description 3
- RSWGJHLUYNHPMX-UHFFFAOYSA-N 1,4a-dimethyl-7-propan-2-yl-2,3,4,4b,5,6,10,10a-octahydrophenanthrene-1-carboxylic acid Chemical compound C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 description 2
- 208000035143 Bacterial infection Diseases 0.000 description 2
- 230000000845 anti-microbial effect Effects 0.000 description 2
- 230000002421 anti-septic effect Effects 0.000 description 2
- 208000022362 bacterial infectious disease Diseases 0.000 description 2
- 230000003115 biocidal effect Effects 0.000 description 2
- 239000003814 drug Substances 0.000 description 2
- 229940079593 drug Drugs 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 231100000252 nontoxic Toxicity 0.000 description 2
- 230000003000 nontoxic effect Effects 0.000 description 2
- DCXXMTOCNZCJGO-UHFFFAOYSA-N tristearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(OC(=O)CCCCCCCCCCCCCCCCC)COC(=O)CCCCCCCCCCCCCCCCC DCXXMTOCNZCJGO-UHFFFAOYSA-N 0.000 description 2
- 241000192125 Firmicutes Species 0.000 description 1
- 230000001580 bacterial effect Effects 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 210000002429 large intestine Anatomy 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 239000003595 mist Substances 0.000 description 1
- 239000002086 nanomaterial Substances 0.000 description 1
- 230000033116 oxidation-reduction process Effects 0.000 description 1
- 238000011056 performance test Methods 0.000 description 1
- 108090000623 proteins and genes Proteins 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N titanium dioxide Inorganic materials O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/16—Heavy metals; Compounds thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/02—Saturated carboxylic acids or thio analogues thereof; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
- A61L9/00—Disinfection, sterilisation or deodorisation of air
- A61L9/16—Disinfection, sterilisation or deodorisation of air using physical phenomena
- A61L9/18—Radiation
- A61L9/20—Ultraviolet radiation
- A61L9/205—Ultraviolet radiation using a photocatalyst or photosensitiser
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y40/00—Manufacture or treatment of nanostructures
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- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Nanotechnology (AREA)
- General Health & Medical Sciences (AREA)
- Dentistry (AREA)
- Plant Pathology (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Agronomy & Crop Science (AREA)
- Crystallography & Structural Chemistry (AREA)
- Inorganic Chemistry (AREA)
- General Physics & Mathematics (AREA)
- Condensed Matter Physics & Semiconductors (AREA)
- Physics & Mathematics (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- Manufacturing & Machinery (AREA)
- Epidemiology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Animal Behavior & Ethology (AREA)
- Composite Materials (AREA)
- Materials Engineering (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Medicines Containing Material From Animals Or Micro-Organisms (AREA)
Abstract
Description
Claims (6)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201710679953.9A CN107372600B (zh) | 2017-08-10 | 2017-08-10 | 光驱动型纳米抗菌剂及其制备方法 |
Applications Claiming Priority (1)
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CN201710679953.9A CN107372600B (zh) | 2017-08-10 | 2017-08-10 | 光驱动型纳米抗菌剂及其制备方法 |
Publications (2)
Publication Number | Publication Date |
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CN107372600A true CN107372600A (zh) | 2017-11-24 |
CN107372600B CN107372600B (zh) | 2019-12-17 |
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Family Applications (1)
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CN201710679953.9A Active CN107372600B (zh) | 2017-08-10 | 2017-08-10 | 光驱动型纳米抗菌剂及其制备方法 |
Country Status (1)
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CN (1) | CN107372600B (zh) |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109077062A (zh) * | 2018-08-09 | 2018-12-25 | 陕西科技大学 | 一种改性MMT/ZnO/GQDs纳米复合抗菌剂的制备方法 |
CN111213674A (zh) * | 2019-12-06 | 2020-06-02 | 鲁东大学 | 一种具有抑菌活性的化合物及其制备方法和应用 |
US10780115B2 (en) | 2018-08-09 | 2020-09-22 | Shaanxi University Of Science & Technology | Preparation of antimicrobial agent based on ZnO/GQD-PEI composites |
CN111961349A (zh) * | 2020-08-26 | 2020-11-20 | 南京林业大学 | 一种高强度、光致发光大豆蛋白膜及其制备方法 |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103706349A (zh) * | 2014-01-21 | 2014-04-09 | 中国计量学院 | 一种纳米ZnO微球/石墨烯光催化剂及其制备方法 |
CN106172494A (zh) * | 2016-08-29 | 2016-12-07 | 佛山市高明区尚润盈科技有限公司 | 一种多孔石墨烯载银抗菌复合材料及其制备方法 |
CN106359373A (zh) * | 2016-08-29 | 2017-02-01 | 佛山市高明区尚润盈科技有限公司 | 一种多孔石墨烯负载氧化锌抗菌复合材料及其制备方法 |
-
2017
- 2017-08-10 CN CN201710679953.9A patent/CN107372600B/zh active Active
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103706349A (zh) * | 2014-01-21 | 2014-04-09 | 中国计量学院 | 一种纳米ZnO微球/石墨烯光催化剂及其制备方法 |
CN106172494A (zh) * | 2016-08-29 | 2016-12-07 | 佛山市高明区尚润盈科技有限公司 | 一种多孔石墨烯载银抗菌复合材料及其制备方法 |
CN106359373A (zh) * | 2016-08-29 | 2017-02-01 | 佛山市高明区尚润盈科技有限公司 | 一种多孔石墨烯负载氧化锌抗菌复合材料及其制备方法 |
Non-Patent Citations (1)
Title |
---|
李碧桐,: ""柠檬酸热解法制备石墨烯量子点及其光学性能研究",", 《基础科学辑》 * |
Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109077062A (zh) * | 2018-08-09 | 2018-12-25 | 陕西科技大学 | 一种改性MMT/ZnO/GQDs纳米复合抗菌剂的制备方法 |
US10780115B2 (en) | 2018-08-09 | 2020-09-22 | Shaanxi University Of Science & Technology | Preparation of antimicrobial agent based on ZnO/GQD-PEI composites |
CN109077062B (zh) * | 2018-08-09 | 2021-05-18 | 陕西科技大学 | 一种改性MMT/ZnO/GQDs纳米复合抗菌剂的制备方法 |
CN111213674A (zh) * | 2019-12-06 | 2020-06-02 | 鲁东大学 | 一种具有抑菌活性的化合物及其制备方法和应用 |
CN111961349A (zh) * | 2020-08-26 | 2020-11-20 | 南京林业大学 | 一种高强度、光致发光大豆蛋白膜及其制备方法 |
CN111961349B (zh) * | 2020-08-26 | 2022-02-08 | 南京林业大学 | 一种高强度、光致发光大豆蛋白膜及其制备方法 |
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CN107372600B (zh) | 2019-12-17 |
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Effective date of registration: 20230828 Address after: 618000 Luoxin Road, Xiaohan Town, Guanghan City, Deyang City, Sichuan Province Patentee after: Sichuan Huayun Tianchen New Material Technology Co.,Ltd. Address before: 509 Kangrui Times Square, Keyuan Business Building, 39 Huarong Road, Gaofeng Community, Dalang Street, Longhua District, Shenzhen, Guangdong Province, 518000 Patentee before: Shenzhen lizhuan Technology Transfer Center Co.,Ltd. Effective date of registration: 20230828 Address after: 509 Kangrui Times Square, Keyuan Business Building, 39 Huarong Road, Gaofeng Community, Dalang Street, Longhua District, Shenzhen, Guangdong Province, 518000 Patentee after: Shenzhen lizhuan Technology Transfer Center Co.,Ltd. Address before: 710021 Shaanxi city of Xi'an province Weiyang University City Patentee before: SHAANXI University OF SCIENCE & TECHNOLOGY |
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