CN107366827A - A kind of vacuum insulation vessel palladium oxide absorber - Google Patents

A kind of vacuum insulation vessel palladium oxide absorber Download PDF

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Publication number
CN107366827A
CN107366827A CN201710541564.XA CN201710541564A CN107366827A CN 107366827 A CN107366827 A CN 107366827A CN 201710541564 A CN201710541564 A CN 201710541564A CN 107366827 A CN107366827 A CN 107366827A
Authority
CN
China
Prior art keywords
palladium oxide
cover plate
explosion
groove
filter paper
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
CN201710541564.XA
Other languages
Chinese (zh)
Inventor
谢少卿
杨鹏
毛海涛
彭彬
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
JIANGXI OXYGEN PLANT CO Ltd
Original Assignee
JIANGXI OXYGEN PLANT CO Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by JIANGXI OXYGEN PLANT CO Ltd filed Critical JIANGXI OXYGEN PLANT CO Ltd
Priority to CN201710541564.XA priority Critical patent/CN107366827A/en
Publication of CN107366827A publication Critical patent/CN107366827A/en
Withdrawn legal-status Critical Current

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Classifications

    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C1/00Pressure vessels, e.g. gas cylinder, gas tank, replaceable cartridge
    • F17C1/12Pressure vessels, e.g. gas cylinder, gas tank, replaceable cartridge with provision for thermal insulation
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C13/00Details of vessels or of the filling or discharging of vessels
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C13/00Details of vessels or of the filling or discharging of vessels
    • F17C13/002Details of vessels or of the filling or discharging of vessels for vessels under pressure
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F17STORING OR DISTRIBUTING GASES OR LIQUIDS
    • F17CVESSELS FOR CONTAINING OR STORING COMPRESSED, LIQUEFIED OR SOLIDIFIED GASES; FIXED-CAPACITY GAS-HOLDERS; FILLING VESSELS WITH, OR DISCHARGING FROM VESSELS, COMPRESSED, LIQUEFIED, OR SOLIDIFIED GASES
    • F17C2203/00Vessel construction, in particular walls or details thereof
    • F17C2203/03Thermal insulations
    • F17C2203/0391Thermal insulations by vacuum

Abstract

A kind of vacuum insulation vessel palladium oxide absorber, including the explosion-proof seat being arranged on storage tank shell, the explosion-proof seat upper end is provided with cover plate, packing ring is provided between cover plate and explosion-proof seat, the cover plate lower surface is provided with groove, is provided with filter paper bag in groove, filter paper bag outer layer covers have stainless steel cloth, the groove lower end is provided with sieve plate, and the sieve plate is fixed on cover plate lower surface through screw.The present invention have it is simple in construction, easily manufactured, be easily installed, recoverable the characteristics of, ensure that the service life of storage tank laminated vacuum, while improve competitiveness of the type product in market.

Description

A kind of vacuum insulation vessel palladium oxide absorber
Technical field
The present invention relates to a kind of vacuum insulation vessel palladium oxide absorber.
Background technology
Normal temperature adsorbent equipment used in the high vacuum multiple layer heat insulation low-temperature (low temperature) vessel of existing manufacture production uses palladium oxide Wrapping is fixed on the structure design of outer container inwall, and the adsorbent equipment of this structure design mainly has the disadvantage that:
1st, palladium oxide adsorbent equipment is mainly made up of filter paper, filter screen, stainless steel horizontal stripe, the palladium oxide that stainless steel horizontal stripe will bandage Outer container inwall is fixed on, stainless steel horizontal stripe welds with outer container.For low temperature tank car during adverse circumstances situation, this fixes dress The danger to come off is equipped with, causes adsorbent adsorption capacity to lose.
2nd, this device must install before inner pressurd vessel and outer container set courage, so cause palladium oxide in absorption vacuum interlayer Before interior gas, moisture, gas in air are first adsorbed, is completed when low-temperature (low temperature) vessel manufactures, the adsorption capacity of palladium oxide It is very poor.
The content of the invention
Its purpose of the invention, which is that, provides a kind of vacuum insulation vessel palladium oxide absorber, solves low temperature tank car and exists During adverse circumstances situation, this fixing device has the danger to come off, cause adsorbent adsorption capacity lose the problem of, have knot Structure is simple, it is easily manufactured, be easily installed, recoverable the characteristics of.
Adopt the technical scheme that to achieve the above object, a kind of vacuum insulation vessel palladium oxide absorber, including The explosion-proof seat being arranged on storage tank shell, the explosion-proof seat upper end are provided with lid
Plate, is provided with packing ring between cover plate and explosion-proof seat, the cover plate lower surface is provided with groove, filter paper bag is provided with groove, filters Paper bag outer layer covers have stainless steel cloth, and the groove lower end is provided with sieve plate, and the sieve plate is fixed on cover plate lower surface through screw On.
Beneficial effect
The present invention has advantages below compared with prior art.
(1) compare and be fixed palladium oxide with two flat bar cross welding, this structural stability is stronger, preferably ensures The absorption property of palladium oxide;
(2) compare and encase palladium oxide with filter paper and be put into interlayer, this structure provides effective type of feed and economic filling Amount, preferably ensure that layer vacuum;
(3) compare and be weldingly fixed on the inside of outside head, this structure is easy to dismount, can recycle palladium oxide, cost-effective;
(4) palladium oxide is placed in the perforate on end socket that compares, and this structure can reduce leak source, preferably ensure that layer vacuum;
(5) compare and place palladium oxide before courage is covered, this structure can carry out placing palladium oxide when heating vacuumizes in tank body, avoid Palladium oxide is too early to be put into mezzanine space and makes moist, and preferably ensure that layer vacuum.
Brief description of the drawings
Below in conjunction with accompanying drawing, the invention will be further described.
Fig. 1 is schematic structural view of the invention.
Embodiment
The present apparatus includes the explosion-proof seat 7 being arranged on storage tank shell 8, as shown in figure 1, the upper end of explosion-proof seat 7 is provided with lid Plate 1, is provided with packing ring 6 between cover plate 1 and explosion-proof seat 7, the lower surface of cover plate 1 is provided with groove 9, filter paper bag is provided with groove 9 5, filter paper bag outer layer covers have stainless steel cloth 4, and the lower end of groove 9 is provided with sieve plate 3, and the sieve plate 3 is fixed on lid through screw 2 On the lower surface of plate 1.
Palladium oxide of the filter paper bag 5 built with high-temperature activation.
Palladium oxide can add after tank body interlayer dehydrogenation displacement in the present invention, it is understood that the content of hydrogen is very in air It is low, but carbon steel in vacuum interlayer and stainless steel plate and sheathing paper adsorption more hydrogen, particularly these materials The hydrogen adsorbed after heating will be discharged largely, and palladium oxide is put in if now, and palladium oxide will adsorb very More hydrogen, during use so afterwards, its suction hydrogen effect will have a greatly reduced quality.
As shown in figure 1, the installation of palladium oxide is carried out according to the following steps, the first step, appropriate palladium oxide threading filter paper The filter paper bag of making;Second step, with stainless (steel) wire filter paper bag is wrapped up, the 3rd step, the palladium oxide wrapped is put into lid In groove on plate lower surface, the 4th step, side pressure upper sieve plate installs housing screw under groove.Treat that nitrogen displacement helium leak test is qualified Afterwards, it is possible to the cover plate for having installed palladium oxide is attached on explosion-proof seat tank body is carried out to vacuumize operation, due to being done using above-mentioned Method, in the case where meeting identical suction hydrogen effect, palladium oxide can at least halve placement.
Storage tank recyclable palladium oxide for having filled half when reprocessing for 5 years, the as everybody knows vacuum of high vacuum multilayer low-temperature (low temperature) vessel Life-span is 5 years, that is to say, that after general 5 years, tank body interlayer will vacuumize again, now with a mistaken ideas many people think that, five Year after only at will mend take out vacuum can that, actually such effect is very poor, and 5 years vacuum are returned for overview Herein below should at least be included by repairing:
A. rise again, that is to say, that the temperature of inner pressurd vessel will return to normal temperature during tank body interlayer vacuum-pumping.
B. interlayer nitrogen displacement, that is to say, that nitrogen displacement several times is carried out during interlayer vacuum-pumping, because the past five Using in interlayer for year leaks into many inert gases(Other non-inert gas leaked into interlayer air are inhaled by molecular sieve It is attached), and vavuum pump only by way of nitrogen displacement, sweeps along inert gas to the pumping speed very little of these inert gases Release,
C. molecular sieve is changed, by the use of 5 years, a part of molecular sieve may fail because absorbing water excessive, and another part may It is shattered.
D. seal washer is changed, the seal washer time has been grown can aging.
E. palladium oxide is changed, the hydrogen now adsorbed in the material in interlayer is also put almost, oxygen when reapposing Changing the dosage of palladium can halve again, the palladium oxide of recovery can dry activate after reuse.

Claims (2)

1. a kind of vacuum insulation vessel palladium oxide absorber, including the explosion-proof seat (7) being arranged on storage tank shell (8), it is special Sign is that explosion-proof seat (7) upper end is provided with cover plate (1), and packing ring (6), the lid are provided between cover plate (1) and explosion-proof seat (7) Plate (1) lower surface is provided with groove (9), is provided with filter paper bag (5) in groove (9), filter paper bag (5) outer layer covers have stainless steel cloth (4), groove (9) lower end is provided with sieve plate (3), and the sieve plate (3) is fixed on cover plate (1) lower surface through screw (2).
A kind of 2. vacuum insulation vessel palladium oxide absorber according to claim 1, it is characterised in that the filter paper (5) built with the palladium oxide of high-temperature activation.
CN201710541564.XA 2017-07-05 2017-07-05 A kind of vacuum insulation vessel palladium oxide absorber Withdrawn CN107366827A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201710541564.XA CN107366827A (en) 2017-07-05 2017-07-05 A kind of vacuum insulation vessel palladium oxide absorber

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201710541564.XA CN107366827A (en) 2017-07-05 2017-07-05 A kind of vacuum insulation vessel palladium oxide absorber

Publications (1)

Publication Number Publication Date
CN107366827A true CN107366827A (en) 2017-11-21

Family

ID=60305105

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201710541564.XA Withdrawn CN107366827A (en) 2017-07-05 2017-07-05 A kind of vacuum insulation vessel palladium oxide absorber

Country Status (1)

Country Link
CN (1) CN107366827A (en)

Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CH420233A (en) * 1959-08-31 1966-09-15 Union Carbide Corp Process for removing traces of hydrogen gas present in an evacuated space
US4394929A (en) * 1981-04-10 1983-07-26 Union Carbide Corporation Cryogenic liquid storage container having an improved access conduit
CN103453312A (en) * 2013-09-11 2013-12-18 张家港韩中深冷科技有限公司 External silver zeolite adsorption plant for low-temperature tank
CN104214511A (en) * 2014-08-20 2014-12-17 安徽金鼎锅炉股份有限公司 Marine natural gas storage tank provided with explosion protection device
CN104500972A (en) * 2014-12-15 2015-04-08 南车长江车辆有限公司 Low-temperature adsorbing agent device for cryogenic pressure container and production process of low-temperature adsorbing agent device
CN104676238A (en) * 2013-11-27 2015-06-03 张家港中集圣达因低温装备有限公司 High-vacuum insulation low-temperature vessel
CN205079049U (en) * 2015-10-23 2016-03-09 陕西汽车集团有限责任公司 LNG gas cylinder normal atmospheric temperature adsorbent storage device
CN206229369U (en) * 2016-12-05 2017-06-09 潍坊新力超导磁电科技有限公司 A kind of adsorbent equipment for vacuum environment
CN207065065U (en) * 2017-07-05 2018-03-02 江西制氧机有限公司 A kind of vacuum insulation vessel palladium oxide adsorbent equipment

Patent Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CH420233A (en) * 1959-08-31 1966-09-15 Union Carbide Corp Process for removing traces of hydrogen gas present in an evacuated space
US4394929A (en) * 1981-04-10 1983-07-26 Union Carbide Corporation Cryogenic liquid storage container having an improved access conduit
CN103453312A (en) * 2013-09-11 2013-12-18 张家港韩中深冷科技有限公司 External silver zeolite adsorption plant for low-temperature tank
CN104676238A (en) * 2013-11-27 2015-06-03 张家港中集圣达因低温装备有限公司 High-vacuum insulation low-temperature vessel
CN104214511A (en) * 2014-08-20 2014-12-17 安徽金鼎锅炉股份有限公司 Marine natural gas storage tank provided with explosion protection device
CN104500972A (en) * 2014-12-15 2015-04-08 南车长江车辆有限公司 Low-temperature adsorbing agent device for cryogenic pressure container and production process of low-temperature adsorbing agent device
CN205079049U (en) * 2015-10-23 2016-03-09 陕西汽车集团有限责任公司 LNG gas cylinder normal atmospheric temperature adsorbent storage device
CN206229369U (en) * 2016-12-05 2017-06-09 潍坊新力超导磁电科技有限公司 A kind of adsorbent equipment for vacuum environment
CN207065065U (en) * 2017-07-05 2018-03-02 江西制氧机有限公司 A kind of vacuum insulation vessel palladium oxide adsorbent equipment

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Application publication date: 20171121