CN107362763A - Taper reactor produces the device of 2,4 D sylvite - Google Patents
Taper reactor produces the device of 2,4 D sylvite Download PDFInfo
- Publication number
- CN107362763A CN107362763A CN201710684150.2A CN201710684150A CN107362763A CN 107362763 A CN107362763 A CN 107362763A CN 201710684150 A CN201710684150 A CN 201710684150A CN 107362763 A CN107362763 A CN 107362763A
- Authority
- CN
- China
- Prior art keywords
- partition
- agitating shaft
- interface channel
- cavity
- offer
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J4/00—Feed or outlet devices; Feed or outlet control devices
- B01J4/001—Feed or outlet devices as such, e.g. feeding tubes
- B01J4/002—Nozzle-type elements
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/41—Preparation of salts of carboxylic acids
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2204/00—Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices
- B01J2204/002—Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices the feeding side being of particular interest
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Mixers Of The Rotary Stirring Type (AREA)
Abstract
The invention discloses taper reactor production 2, the device of 4 D sylvite, taper reactor body including hollow structure, the inside of body is welded with first partition and second partition successively along its short transverse, first partition is located at the surface of second partition, the inside of second partition offers cylindrical cavity along its length, side of the cavity away from first partition offers the spray orifice connected with cavity inside, the connecting pipe connected with cavity inside is installed at the top of first partition, the inside of body is provided with the agitating shaft with first partition and second partition pivot bush unit, agitating shaft stretches into axis direction array of the one end of cavity along agitating shaft and offers inlet opening.The present invention is simple in construction, easy to operate, and effectively the raw material inside reactor is sufficiently mixed, and improves the preparation efficiency of product, convenient that reactor inside is cleared up, and prevents product adhesion in the madial wall of reactor.
Description
Technical field
The present invention relates to reactor technical field, more particularly to the device of taper reactor production 2,4-D sylvite.
Background technology
2,4-D sylvite are 2,4- drop important intermediates, wherein monoxone directly with 2, the 4- Dichlorophenols potassium in alkalescence
Under the conditions of reaction obtain 2,4-D sylvite, i.e. available 2,4-D after the acidifying of 2,4-D sylvite.It is sticky larger due to salt, commonly
Reactor and mixing plant stirring intensity it is not high so that production 2,4-D sylvite reaction speed it is slow, influence the lifting of production capacity,
Simultaneous reactions kettle internal cleaning is inconvenient, and the madial wall of especially reactor is easily adhered product, needs a kind of taper anti-for this
Answer the device of kettle production 2,4-D sylvite.
The content of the invention
The invention aims to solve shortcoming present in prior art, and the taper reactor proposed produces 2,4-
The device of D sylvite.
To achieve these goals, present invention employs following technical scheme：
Taper reactor produces the device of 2,4-D sylvite, includes the taper reactor body of hollow structure, the inside of the body
First partition and second partition are welded with successively along its short transverse, and the first partition is located at the surface of second partition, institute
The inside for stating second partition offers cylindrical cavity along its length, and side of the cavity away from first partition offers
The spray orifice connected with cavity inside, is provided with the connecting pipe connected with cavity inside at the top of the first partition, described
The inside of body is provided with the agitating shaft with first partition and second partition pivot bush unit, and the agitating shaft stretches into one end edge of cavity
The axis direction array of agitating shaft offers inlet opening, and the inside of the agitating shaft offers what is be coaxially disposed along its axis direction
First interface channel, one end that the agitating shaft stretches into second partition bottom are vertically welded with connecting rod, the connecting rod it is interior
Portion offers the second interface channel connected with the first interface channel, and the one end of the connecting rod away from agitating shaft is welded with and the
The cleaning rabbling mechanism of two interface channels connection, the side of the body are provided with the admission line connected with cavity inside, institute
The opposite side for stating body is provided with the inlet channel connected with cavity inside.
Preferably, the cleaning rabbling mechanism includes fixing the parallel along body madial wall length direction of welding with connecting rod
The strip fixed plate of setting, side movable sleeve of the fixed plate away from connecting rod are connected to strip scraper plate, and the scraper plate leans on
The side of nearly fixed plate offers strip chute, offers what is connected with the second interface channel inside one end of the fixed plate
3rd interface channel, the one end of the interface channel away from connecting rod offers to be led to the strip transition connected inside chute
Road, one end of the scraper plate offer the 4th interface channel, and the 4th interface channel offers close to one end of transition passage
With the inlet opening connected inside transition passage, the described one end of 4th interface channel away from inlet opening, which is vertically offered along scraper plate, to be grown
The accommodating chamber that direction is set is spent, length direction of the one end of the scraper plate away from fixed plate along scraper plate equidistantly offers and accommodating chamber
The spray hole of connection.
Preferably, a side-lower of the second partition is provided with the discharge duct connected with body interior, the exhaust
One end that pipeline stretches out body is connected with admission line, and air pump is provided with the discharge duct.
Preferably, feed pipe and loading hopper are installed, the bottom of the body is provided with row at the top of the body
Pipe material.
Preferably, the stirring vane being fixedly connected with agitating shaft is installed at the top of the first partition.
Preferably, one end of the agitating shaft stretching bodies top is provided with motor.
Beneficial effects of the present invention：
Pass through the body of setting, first partition, second partition, agitating shaft, cavity, spray orifice, admission line, inlet channel, connection
Pipeline, inlet opening, the first interface channel, connecting rod, cleaning rabbling mechanism, the second interface channel, fixed plate, scraper plate, the 3rd connect
Connect road, transition passage, the 4th interface channel, inlet opening, accommodating chamber and spray hole, raw material from the feed pipe of bodies top and
Loading hopper enters the top of first partition, then proceeds by stirring by the stirring vane on agitating shaft, on discharge duct
Air pump the gas of body interior is transported to the pressure for the inside of cavity, increasing cavity inside from admission line, made with facilitating
Mixed raw material carries out being allowed to be mixed with the raw material of the bottom of second partition at spray from spray orifice, after another convenient mixing
Raw material from the inlet opening on agitating shaft along the first interface channel, the second interface channel, the 3rd interface channel, transition passage, enter
Water hole and the 4th interface channel are finally entered inside accommodating chamber and sprayed from spray hole, using above-mentioned same equally when cleaning
The mode of sample is carried out, and the design structure is simple, easy to operate, and effectively the raw material inside reactor is sufficiently mixed, carried
The preparation efficiency of high product, it is convenient that reactor inside is cleared up, prevent product adhesion in the madial wall of reactor.
Brief description of the drawings
Fig. 1 is the structural representation for the device that taper reactor proposed by the present invention produces 2,4-D sylvite；
Fig. 2 is the structural representation for the device cleaning rabbling mechanism that taper reactor proposed by the present invention produces 2,4-D sylvite.
In figure：1 body, 2 first partitions, 3 second partitions, 4 agitating shafts, 5 cavitys, 6 spray orifices, 7 admission lines, 8 water inlet pipes
Road, 9 connecting pipes, 10 inlet openings, 11 first interface channels, 12 connecting rods, 13 cleaning rabbling mechanisms, 14 second interface channels,
15 fixed plates, 16 scraper plates, 17 the 3rd interface channels, 18 transition passages, 19 the 4th interface channels, 20 inlet openings, 21 accommodating chambers, 22
Spray hole.
Embodiment
Below in conjunction with the accompanying drawing in the embodiment of the present invention, the technical scheme in the embodiment of the present invention is carried out clear, complete
Site preparation describes, it is clear that described embodiment is only part of the embodiment of the present invention, rather than whole embodiments.
Reference picture 1-2, taper reactor produce the device of 2,4-D sylvite, include the taper reactor body of hollow structure
1, the inside of body 1 is welded with first partition 2 and second partition 3 successively along its short transverse, and first partition 2 is located at second partition
3 surface, the inside of second partition 3 offer cylindrical cavity 5 along its length, cavity 5 away from first partition 2 one
Side offers the spray orifice 6 connected with the inside of cavity 5, and the top of first partition 2 is provided with the connecting pipe connected with the inside of cavity 5
9, the inside of body 1 is provided with the agitating shaft 4 with first partition 2 and the pivot bush unit of second partition 3, and agitating shaft 4 stretches into cavity 5
Axis direction array of the one end along agitating shaft 4 offers inlet opening 10, and the inside of agitating shaft 4 offers coaxially along its axis direction
The first interface channel 11 set, one end that agitating shaft 4 stretches into the bottom of second partition 3 is vertically welded with connecting rod 12, connecting rod
12 inside offers the second interface channel 14 connected with the first interface channel 11, the one end of connecting rod 12 away from agitating shaft 4
The cleaning rabbling mechanism 13 connected with the second interface channel 14 is welded with, the side of body 1 is provided with what is connected with the inside of cavity 5
Admission line 7, the opposite side of body 1 are provided with the inlet channel 8 connected with the inside of cavity 5.
Cleaning rabbling mechanism 13 includes fixing be arrangeding in parallel along the madial wall length direction of body 1 for welding with connecting rod 12
Strip fixed plate 15, side movable sleeve of the fixed plate 15 away from connecting rod 12 are connected to strip scraper plate 16, and scraper plate 16 is close to solid
The side of fixed board 15 offers strip chute, and connected with the second interface channel 14 is offered inside one end of fixed plate 15
Three interface channels 17, the one end of interface channel 14 away from connecting rod 12 offer the strip transition passage with being connected inside chute
18, one end of scraper plate 16 offers the 4th interface channel 19, and the 4th interface channel 19 offers close to one end of transition passage 18
The inlet opening 20 connected with the inside of transition passage 18, the 4th one end of interface channel 19 away from inlet opening 20 vertically offer edge and scraped
The accommodating chamber 21 that the length direction of plate 16 is set, length direction of the one end of scraper plate 16 away from fixed plate 15 along scraper plate 16 equidistantly open up
There is the spray hole 22 connected with accommodating chamber 21.
One side-lower of second partition 3 is provided with the discharge duct connected with the inside of body 1, and discharge duct stretches out body 1
One end connected with admission line 7, air pump is installed, the top of body 1 is provided with feed pipe and charging is leaked on discharge duct
Bucket, the bottom of body 1 are provided with drainage line, and the top of first partition 2 is provided with the paddle being fixedly connected with agitating shaft 4
Piece, one end that agitating shaft 4 stretches out the top of body 1 are provided with motor.
Operation principle：Raw material enters the top of first partition 2 from the feed pipe and loading hopper at the top of body 1, then
Stirring is proceeded by by the stirring vane on agitating shaft 4, and the air pump on discharge duct is by the gas inside body 1 from air inlet pipe
Road 7 is transported to the inside of cavity 5, is increased the pressure inside cavity 5, mixed raw material is sprayed at spray orifice 6 to facilitate
Place is allowed to be mixed with the raw material of the bottom of second partition 3, another to facilitate mixed raw material from the inlet opening on agitating shaft 4
10 connect along the first interface channel 11, the second interface channel 14, the 3rd interface channel 17, transition passage 18, inlet opening 20 and the 4th
Connect road 19 to finally enter the inside of accommodating chamber 21 and spray from spray hole 22, equally utilize above-mentioned same side when cleaning
Formula is carried out, and the design structure is simple, easy to operate, and effectively the raw material inside reactor is sufficiently mixed, and improves product
Preparation efficiency, it is convenient that reactor inside is cleared up, prevent product adhesion in the madial wall of reactor.
The foregoing is only a preferred embodiment of the present invention, but protection scope of the present invention be not limited thereto,
Any one skilled in the art the invention discloses technical scope in, technique according to the invention scheme and its
Inventive concept is subject to equivalent substitution or change, should all be included within the scope of the present invention.
Claims (6)
1. taper reactor produces the device of 2,4-D sylvite, include the taper reactor body of hollow structure（1）, its feature exists
In：The body（1）Inside be welded with first partition successively along its short transverse（2）And second partition（3）, described first every
Plate（2）Positioned at second partition（3）Surface, the second partition（3）Inside offer cylindrical empty along its length
Chamber（5）, the cavity（5）Away from first partition（2）Side offer and cavity（5）The spray orifice of inside connection（6）, described
One dividing plate（2）Top be provided with and cavity（5）The connecting pipe of inside connection（9）, the body（1）Inside be provided with
First partition（2）And second partition（3）The agitating shaft of pivot bush unit（4）, the agitating shaft（4）Stretch into cavity（5）One end edge
Agitating shaft（4）Axis direction array offer inlet opening（10）, the agitating shaft（4）Inside offered along its axis direction
The first interface channel being coaxially disposed（11）, the agitating shaft（4）Stretch into second partition（3）One end of bottom is vertically welded with company
Extension bar（12）, the connecting rod（12）Inside offer and the first interface channel（11）Second interface channel of connection（14）,
The connecting rod（12）Away from agitating shaft（4）One end be welded with and the second interface channel（14）The cleaning rabbling mechanism of connection
（13）, the body（1）Side be provided with and cavity（5）The admission line of inside connection（7）, the body（1）It is another
Side is provided with and cavity（5）The inlet channel of inside connection（8）.
2. the device of taper reactor production 2,4-D sylvite according to claim 1, it is characterised in that the cleaning is stirred
Mix mechanism（13）Including with connecting rod（12）Fixed welding along body（1）The strip that madial wall length direction be arranged in parallel is consolidated
Fixed board（15）, the fixed plate（15）Away from connecting rod（12）Side movable sleeve be connected to strip scraper plate（16）, the scraper plate
（16）Close to fixed plate（15）Side offer strip chute, the fixed plate（15）One end inside offer with second
Interface channel（14）3rd interface channel of connection（17）, the interface channel（14）Away from connecting rod（12）One end offer
With the strip transition passage connected inside chute（18）, the scraper plate（16）One end offer the 4th interface channel（19）,
4th interface channel（19）Close to transition passage（18）One end offer and transition passage（18）The water inlet of inside connection
Hole（20）, the 4th interface channel（19）Away from inlet opening（20）One end vertically offer along scraper plate（16）Length direction is set
The accommodating chamber put（21）, the scraper plate（16）Away from fixed plate（15）One end along scraper plate（16）Length direction equidistantly offer
With accommodating chamber（21）The spray hole of connection（22）.
3. the device of taper reactor according to claim 1 production 2,4-D sylvite, it is characterised in that described second every
Plate（3）A side-lower be provided with and body（1）The discharge duct of inside connection, the discharge duct stretch out body（1）One
End and admission line（7）Connect, air pump is installed on the discharge duct.
4. the device of taper reactor production 2,4-D sylvite according to claim 1, it is characterised in that the body（1）
Top feed pipe and loading hopper, the body are installed（1）Bottom drainage line is installed.
5. the device of taper reactor according to claim 1 production 2,4-D sylvite, it is characterised in that described first every
Plate（2）Top be provided with and agitating shaft（4）The stirring vane being fixedly connected.
6. the device of taper reactor production 2,4-D sylvite according to claim 1, it is characterised in that the agitating shaft
（4）Stretch out body（1）The one end at top is provided with motor.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710684150.2A CN107362763B (en) | 2017-08-11 | 2017-08-11 | The device of taper reaction kettle production 2,4-D sylvite |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710684150.2A CN107362763B (en) | 2017-08-11 | 2017-08-11 | The device of taper reaction kettle production 2,4-D sylvite |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN107362763A true CN107362763A (en) | 2017-11-21 |
| CN107362763B CN107362763B (en) | 2019-06-04 |
Family
ID=60309353
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710684150.2A Active CN107362763B (en) | 2017-08-11 | 2017-08-11 | The device of taper reaction kettle production 2,4-D sylvite |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107362763B (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112058198A (en) * | 2020-08-18 | 2020-12-11 | 常熟市天工医药化工设备有限公司 | A reation kettle for pharmaceutical production |
| CN112970773A (en) * | 2021-02-26 | 2021-06-18 | 河北佩清科技有限公司 | Preparation method and device of efficient and environment-friendly maleic anhydride grafted polyguanidine disinfectant |
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| CN105251393A (en) * | 2015-10-31 | 2016-01-20 | 周俊良 | Material stirring machine |
| CN105289359A (en) * | 2015-10-31 | 2016-02-03 | 周俊良 | Stirring burdening machine |
| CN205084742U (en) * | 2015-11-06 | 2016-03-16 | 江苏常丰农化有限公司 | Device of toper reation kettle production 2, 4 -D potassium salt |
| CN205730975U (en) * | 2016-01-13 | 2016-11-30 | 泉州德科达机械制造有限公司 | A kind of New type agitation cylinder with pump function and automatic cleaning function |
| CN106621979A (en) * | 2017-02-08 | 2017-05-10 | 安徽鹰龙工业设计有限公司 | Stirring device for horizontally pushing liquid to flow |
| CN106732267A (en) * | 2016-12-19 | 2017-05-31 | 天津雪赢世纪专利技术有限公司 | A kind of Cosmetic Manufacture device |
-
2017
- 2017-08-11 CN CN201710684150.2A patent/CN107362763B/en active Active
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105251393A (en) * | 2015-10-31 | 2016-01-20 | 周俊良 | Material stirring machine |
| CN105289359A (en) * | 2015-10-31 | 2016-02-03 | 周俊良 | Stirring burdening machine |
| CN205084742U (en) * | 2015-11-06 | 2016-03-16 | 江苏常丰农化有限公司 | Device of toper reation kettle production 2, 4 -D potassium salt |
| CN205730975U (en) * | 2016-01-13 | 2016-11-30 | 泉州德科达机械制造有限公司 | A kind of New type agitation cylinder with pump function and automatic cleaning function |
| CN106732267A (en) * | 2016-12-19 | 2017-05-31 | 天津雪赢世纪专利技术有限公司 | A kind of Cosmetic Manufacture device |
| CN106621979A (en) * | 2017-02-08 | 2017-05-10 | 安徽鹰龙工业设计有限公司 | Stirring device for horizontally pushing liquid to flow |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112058198A (en) * | 2020-08-18 | 2020-12-11 | 常熟市天工医药化工设备有限公司 | A reation kettle for pharmaceutical production |
| CN112970773A (en) * | 2021-02-26 | 2021-06-18 | 河北佩清科技有限公司 | Preparation method and device of efficient and environment-friendly maleic anhydride grafted polyguanidine disinfectant |
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| Publication number | Publication date |
|---|---|
| CN107362763B (en) | 2019-06-04 |
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Effective date of registration: 20220818 Address after: No. 480, Jigu Road, Jilin Economic and Technological Development Zone, Jilin City, Jilin Province, 132000 (Room 307, Jilin Province Fine Chemical Entrepreneurship Incubation Park) Patentee after: Changfeng Chemical (Jilin) Co., Ltd. Address before: 224500 Coastal Industrial Park of Yancheng Coastal Economic Development Zone, Jiangsu Province Patentee before: JIANGSU CHANGFENG AGROCHEMICAL Co.,Ltd. |
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