CN107356555A - A kind of device based near infrared spectrum detection flower characters - Google Patents

A kind of device based near infrared spectrum detection flower characters Download PDF

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Publication number
CN107356555A
CN107356555A CN201710511032.1A CN201710511032A CN107356555A CN 107356555 A CN107356555 A CN 107356555A CN 201710511032 A CN201710511032 A CN 201710511032A CN 107356555 A CN107356555 A CN 107356555A
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CN
China
Prior art keywords
near infrared
turntable
beam splitter
infrared spectrum
detection
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710511032.1A
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Chinese (zh)
Inventor
李光煌
罗辉
杜丽娟
陈阳
朱鹏惠
李万建
陈亮亮
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Shenzhen Saiyi Technology Development Co Ltd
Original Assignee
Shenzhen Saiyi Technology Development Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Publication date
Application filed by Shenzhen Saiyi Technology Development Co Ltd filed Critical Shenzhen Saiyi Technology Development Co Ltd
Priority to CN201710511032.1A priority Critical patent/CN107356555A/en
Publication of CN107356555A publication Critical patent/CN107356555A/en
Pending legal-status Critical Current

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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/17Systems in which incident light is modified in accordance with the properties of the material investigated
    • G01N21/25Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
    • G01N21/31Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry
    • G01N21/35Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light
    • G01N21/359Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using infrared light using near infrared light
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/01Arrangements or apparatus for facilitating the optical investigation
    • GPHYSICS
    • G08SIGNALLING
    • G08CTRANSMISSION SYSTEMS FOR MEASURED VALUES, CONTROL OR SIMILAR SIGNALS
    • G08C17/00Arrangements for transmitting signals characterised by the use of a wireless electrical link
    • G08C17/02Arrangements for transmitting signals characterised by the use of a wireless electrical link using a radio link

Abstract

The present invention provides a kind of device based near infrared spectrum detection flower characters, including housing, IR light sources, beam splitter, detector, microprocessor, turntable, wireless transport module, supply unit are provided with the housing, the hull outside is provided with touch display screen, it is placed with specimen cup on the turntable, be provided with that loose-leaf is connected with housing above the turntable renovates.The IR light sources launch near infrared light after beam splitter, and obtained interference light is detected by the detector through specimen cup, and the axis for the interference light that the beam splitter obtains passes through specimen cup, and with detector axis on a horizontal line.The present invention can quick nondestructive detection flour quality, and draw the content of the talcum powder and benzoyl peroxide that influence flower characters, have without complicated pre-treatment, testing cost is low, automatic detection, fast detection speed the advantages of.

Description

A kind of device based near infrared spectrum detection flower characters
Technical field
It is more particularly to a kind of based near infrared spectrum detection flower characters the present invention relates to flower characters detection technique field Device.
Background technology
With the continuous enhancing of china's overall national strength, the increasingly raising of living standards of the people, the health and quality of food are asked Topic also enjoys the concern of people.Flour can be used for making boiled dumpling, noodles, steamed bun as one of Main Foods raw material in the world Etc. Flour product.Various famous with color based on Flour product is made with boiling, this whiteness to flour requires higher, simultaneously Most consumers are also to judge flour quality quality according to color and luster perception.Wheat flour and its products are pure whiter, finer and smoother, consumer More favor, many flour mills cater to consumer demand for sales volume, and bleaching agent for flour is widely used to increase Add the whiteness of flour, benzoyl peroxide (BPO) is exactly a kind of bleaching agent for flour being often used.BPO has very strong oxidation Property, it faster can aoxidize the lutein in flour, the yellow in flour is disappeared, so as to play whitening effect.It is but excessive Ground addition BPO can destroy the intrinsic nutritional ingredient of some in flour, such as carrotene, vitamin A, vitamin B, vitamin E, This kind of flour is eaten for a long time, the shortage of vitamin can be caused, so as to cause some diseases, such as angular stomatitis, neuritis, seriously very The infringement of central nervous system cumulative bad, liver failure etc. can extremely be caused.In March, 2011, the Ministry of Public Health of China issue newest bulletin: Forbade to add brightening agent into flour from 1 day May in 2011.But in fierce market competition and chase the factors such as more high profit Driving under, the small-sized flour enterprises of China Partial are still using BPO as bleaching agent for flour.
Long-term consumption can cause people uncomfortable or even carcinogenic containing the flour for being harmful to or being excessively added agent.Part face Powder enterprise adds a large amount of talcum powder (Mg into flour to speculate3[Si4O10](OH)2), to increase the weight of flour, 50kg flour most adds the talcum powder more than 10kg, has seriously endangered the health of people.
Near infrared spectrum (Near Infrared Spectroscopy, NIR) analytical technology is the swift and violent height of a development New technology, it is to utilize optical characteristics of the chemical substance near infrared spectrum, quickly determines one kind or more in certain sample The physics determination techniques of kind chemical composition content and characteristic.It is to utilize absorption, scattering, reflection and transmission of the laboratory sample to light Etc. a kind of method that characteristic determines sample interior composition.Near-infrared spectral analysis technology is as a kind of " green " Non-Destructive Testing skill Art, it have the advantages that it is quick, lossless, pollution-free, in multiple fields such as agricultural, food industry, petrochemical industry and pharmaceutical engineerings Middle near infrared detection turns into a kind of very effective quick determination method for substituting chemical analysis detection, and is widely used in agriculture In crop and its quantitative of byproduct, qualitative analysis, play an important role.
The content of the invention
It is an object of the invention to provide a kind of device based near infrared spectrum detection flower characters, near infrared light is utilized Spectrum detection flour sample, obtains sample near infrared light spectral curve, the gained curve of spectrum is handled, finally draws mistake in sample The content of BP and talcum powder.
The present invention provides a kind of device based near infrared spectrum detection flower characters, an including housing, in the housing It is provided with IR light sources, beam splitter, detector, microprocessor, turntable, wireless transport module, supply unit, the hull outside It is provided with touch display screen.
Further, specimen cup is placed with the turntable, the specimen cup is made of quartz material.
Further, be provided with that loose-leaf is connected with housing above the turntable renovates.
The IR light sources are high-energy air air cooling NIR light source.
The beam splitter is with quartz and CaF2For material, polychromatic light is changed into interference light.
The detector is high sensitivity PbS detectors.
The microprocessor digital intelligent control, automatic gain selection, controls turntable, carries out spectroscopic data processing.
The turntable is used to place specimen cup, and rotation process can be carried out in detection, is easy to carry out heterogeneous sample Detection.
The wireless transport module wireless connection cloud storage platform, intelligent terminal, carry out data transmission.
The touch display screen is controlled to the near-infrared detection apparatus detection process, and shows described detection As a result.
The supply unit provides required electric energy for the near-infrared detection apparatus.
The IR light sources launch near infrared light after beam splitter, and obtained interference light is detected through specimen cup by detector To arrive, the axis for the interference light that the beam splitter obtains passes through specimen cup, and with detector axis on a horizontal line.
When using the near-infrared detection apparatus, the flour sample of required detection is fitted into specimen cup, by specimen cup It is positioned on turntable, open detection power supply is detected, and turntable starts to rotate, IR light sources transmitting near infrared light, through beam splitting Device obtains interference light, and the interference light is irradiated on the specimen cup on turntable, after the energy of sample Absorption Characteristics wave number, hair The interference light that raw intensity changes is detected by the detector, and the spectral signal detected is transferred to microprocessor and carries out Fu by detector In leaf transformation, so as to obtain atlas of near infrared spectra, the atlas of near infrared spectra of the detection is deposited by wireless transport module and cloud The near infrared spectrum of flour in storage platform is compared, and draws the quality quality of institute's test sample product, and result is included described In touch display screen.
The beneficial effects of the present invention are:The present invention provides a kind of device based near infrared spectrum detection flower characters, Pass through the setting of IR light sources, beam splitter, detector, microprocessor, turntable, wireless transport module, supply unit, quick nondestructive Detection flour quality, and draw the content of the talcum powder and benzoyl peroxide that influence flower characters, have without multiple Miscellaneous pre-treatment, testing cost are low, automatic detection, fast detection speed the advantages of.
Brief description of the drawings
Fig. 1 is the structural representation of device of the present invention based near infrared spectrum detection flower characters;
Fig. 2 is device Cleaning Principle schematic diagram of the present invention based near infrared spectrum detection flower characters.
Label declaration in figure:
1 --- housing 11 --- is renovated
2 --- IR light sources 3 --- beam splitters
4 --- turntable 41 --- specimen cups
5 --- detector 6 --- microprocessors
7 --- wireless transport module 8 --- touch display screens
Embodiment
In order that the purpose of the present invention, technical scheme are clearer, below in conjunction with the accompanying drawings and embodiment, the present invention is carried out Detailed description.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, it is not used to limit this hair It is bright.
The present invention provides a kind of device based near infrared spectrum detection flower characters, as shown in figure 1, including a housing 1, IR light sources 2, beam splitter 3, turntable 4, detector 5, microprocessor 6, wireless transport module 7, power supply are provided with the housing Device, the outside of housing 1 are provided with touch display screen 8, and the top of turntable 4 is provided with loose-leaf and is connected with housing 1 Renovate 11.
The housing 1 is made of opaque material so that detection process is in dark environment.
IR light sources 2 are specially high-energy air air cooling NIR light source, launch the wave-number range of near infrared light for 12500~ 4000cm-1, required detection light source is provided for the near-infrared detection apparatus.
Beam splitter 3 is with quartz and CaF2For material, the polychromatic light for being sent IR light sources 2 by Michelson's interferometer principle It is changed into interference light.
Turntable 4 is used to place specimen cup 41, and the specimen cup 41 is made of quartz, the sample of required detection is put into In specimen cup 41, the specimen cup 41 equipped with testing sample is placed on turntable 4, detection process transfer by least cover cup bottom Dynamic turntable 4, is easy to the detection to heterogeneous sample.
Detector 5 is high sensitivity PbS photodetectors.The interference light obtained by beam splitter 3 is radiated on turntable 4 it Spectrum after being changed afterwards is detected by detector 5.
Microprocessor 6 receives the spectral signal that detector 5 transmits, and carries out Fourier transformation processing, obtains the detection of sample Atlas of near infrared spectra.In addition, microprocessor 6 controls with digital intelligent, automatic gain selects, and controls the function of turntable.
The wireless connection cloud storage platform of wireless transport module 7, it is stored with meeting national mark in the cloud storage platform It is mixed with the atlas of near infrared spectra of accurate flour, flour in the atlas of near infrared spectra of different content talcum powder, flour added with not With the atlas of near infrared spectra of content benzoyl peroxide, wireless transport module 7 carries out data transmission, and microprocessor 6 will be handled To detection atlas of near infrared spectra be compared with the spectrogram in cloud storage platform, qualitatively analysis detection sample whether contain Talcum powder and benzoyl peroxide, using talcum powder and benzoyl peroxide first in the near infrared spectrum and flour of least square method foundation The regression model of acyl content carries out quantitative analysis, and will compare obtained result including in the touch display screen 8.In addition, institute State wireless transport module 7 also can wireless connection intelligent terminal, testing result is shown by the APP matched in intelligent terminal Show, count and data analysis.
Supply unit provides required electric energy for the near-infrared detection apparatus.
As shown in Fig. 2 the IR light sources 2 are arranged in a linear with beam splitter 3, the beam splitter 3 is with the turntable 4 in straight Line arranges, and the IR light sources 2 are in linearly linearly 90 ° of angles with beam splitter 3 and the turntable 4 with the institute of beam splitter 3;Institute State turntable 4 to be arranged in a linear with detector 5, and beam splitter 3 and detector 5 are located at the both sides of turntable 4, and beam splitter 3 Optical axis, the center of specimen cup 41 placed on turntable 4 and the optical axis of detector 5 be in same horizontal line.It is described The connecting detection device 5 of microprocessor 6, the wireless transport module 7 are electrically connected microprocessor 6, and the touch display screen 8 is electrically connected microprocessor Device 6.
When needing detection, first by electric power starting, the detection means is preheated, then by the sample of required detection It is put into specimen cup 41, the amount of sample at least covers brimmer bottom, and specimen cup 41 is placed on turntable 4, and covers described 11 are renovated, open detection switch, is detected, IR light sources 2 send near infrared light, and entering line light source by beam splitter 3 handles to obtain Interference light, the interference light are radiated on the detection sample in specimen cup 41, the energy of the detection sample energy Absorption Characteristics wave number Measure, corresponding change occurs for the interference pattern intensity curve obtained by detector 5, and the spectrogram detected is transferred into microprocessor 6 carry out Fourier transformation processing, obtain the detection atlas of near infrared spectra of sample, the wireless connection cloud storage of wireless transport module 7 is put down Platform, wireless transport module 7 carry out data transmission, and microprocessor 6 puts down the detection atlas of near infrared spectra that processing obtains with cloud storage Spectrogram in platform is compared, and qualitatively whether analysis detection sample contains talcum powder and benzoyl peroxide, using minimum The regression model of talcum powder and Determination of benzoyl peroxide in wheat carries out quantitative analysis near infrared spectrum and flour that square law is established, And obtained result will be compared including in the touch display screen 8.In addition, the wireless transport module 7 also can wireless connection intelligence Can terminal, testing result is shown by the APP matched in intelligent terminal, counted and data analysis.Obtain final inspection Result is surveyed, whole detection is completed.
To sum up, by the design of the detection means and the support based on cloud storage platform big data, simplify to flour The detection of quality, accomplish lossless, containing without the talcum powder and benzoyl peroxide that may contain in pretreatment, quick detection flour Amount, system architecture is simple, easily operated, realizes automatic detection substantially, has a good application prospect.
Above is the preferable implementation to the present invention is illustrated, but the invention is not limited to the implementation Example, those skilled in the art can also make a variety of equivalent variations on the premise of without prejudice to spirit of the invention or replace Change, these equivalent deformations or replacement are all contained in the application claim limited range.

Claims (8)

  1. A kind of 1. device based near infrared spectrum detection flower characters, it is characterised in that:Including housing, set in the housing There are IR light sources, beam splitter, detector, microprocessor, turntable, wireless transport module, supply unit, the hull outside is set There is touch display screen, specimen cup is placed with the turntable, be provided with loose-leaf above the turntable is connected with housing Renovate;
    The IR light sources are arranged in a linear with beam splitter, and the beam splitter is arranged in a linear with the turntable, the IR light sources It is in linearly linearly 90 ° of angles with beam splitter and the turntable with beam splitter institute;The turntable is with detector in straight Line arranges, and beam splitter and detector are located at the both sides of turntable, and the sample placed on the optical axis of beam splitter, turntable The center of cup and the optical axis of detector are in same horizontal line;The microprocessor connecting detection device, it is described to be wirelessly transferred Module is electrically connected microprocessor, and the touch display screen is electrically connected microprocessor.
  2. A kind of 2. device based near infrared spectrum detection flower characters according to claim 1, it is characterised in that:It is described Specimen cup is made of quartz material.
  3. A kind of 3. device based near infrared spectrum detection flower characters according to claim 1, it is characterised in that:It is described IR light sources are high-energy air air cooling NIR light source.
  4. A kind of 4. device based near infrared spectrum detection flower characters according to claim 1, it is characterised in that:It is described Beam splitter is with quartz and CaF2For material.
  5. A kind of 5. device based near infrared spectrum detection flower characters according to claim 1, it is characterised in that:It is described Detector is PbS detectors.
  6. A kind of 6. device based near infrared spectrum detection flower characters according to claim 1, it is characterised in that:It is described Wireless transport module wireless connection cloud storage platform, intelligent terminal, carry out data transmission.
  7. 7. it is according to claim 6 it is a kind of based near infrared spectrum detection flower characters device wireless transport module without The cloud storage platform of line connection, it is characterised in that:The flour on meeting national standard is stored with the cloud storage platform It is mixed with atlas of near infrared spectra, flour in the atlas of near infrared spectra of different content talcum powder, flour and is added with different content peroxide Change the atlas of near infrared spectra of benzoyl.
  8. A kind of 8. device based near infrared spectrum detection flower characters according to claim 1, it is characterised in that:It is described Wireless transport module carries out data transmission, and the microprocessor will handle obtained detection atlas of near infrared spectra and cloud storage platform In spectrogram be compared, qualitatively analysis detection sample whether contain talcum powder and benzoyl peroxide, using a most young waiter in a wineshop or an inn The regression model of talcum powder and Determination of benzoyl peroxide in wheat carries out quantitative analysis near infrared spectrum and flour that multiplication is established, and Obtained result will be compared including in the touch display screen.
CN201710511032.1A 2017-06-29 2017-06-29 A kind of device based near infrared spectrum detection flower characters Pending CN107356555A (en)

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Application Number Priority Date Filing Date Title
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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108872143A (en) * 2018-05-22 2018-11-23 南京农业大学 A kind of wheat infection head blight level detection method based near infrared spectrum

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5258825A (en) * 1991-11-13 1993-11-02 Perten Instruments North America, Inc. Optical compositional analyzer apparatus and method for detection of ash in wheat and milled wheat products
CN201177600Y (en) * 2008-03-12 2009-01-07 李赫君 Portable near-infrared detector
CN102042968A (en) * 2010-11-24 2011-05-04 南京财经大学 Grain quality near infrared rapid detection wireless system
CN102879352A (en) * 2012-09-13 2013-01-16 江苏恒顺醋业股份有限公司 Acquisition device for near-infrared transmitted spectrum of vinegar and method for identifying vinegar origin
CN105044023A (en) * 2015-08-06 2015-11-11 黑龙江大学 Method for quickly detecting content of benzoyl peroxide in flour in nondestructive mode and application thereof
CN105527246A (en) * 2016-01-14 2016-04-27 昆明睿意铂科技股份有限公司 Portable near infrared spectrum detection system
CN105675537A (en) * 2015-12-31 2016-06-15 深圳市芭田生态工程股份有限公司 Spectrum detection system and wireless data connection adopted spectrum detector thereof

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5258825A (en) * 1991-11-13 1993-11-02 Perten Instruments North America, Inc. Optical compositional analyzer apparatus and method for detection of ash in wheat and milled wheat products
CN201177600Y (en) * 2008-03-12 2009-01-07 李赫君 Portable near-infrared detector
CN102042968A (en) * 2010-11-24 2011-05-04 南京财经大学 Grain quality near infrared rapid detection wireless system
CN102879352A (en) * 2012-09-13 2013-01-16 江苏恒顺醋业股份有限公司 Acquisition device for near-infrared transmitted spectrum of vinegar and method for identifying vinegar origin
CN105044023A (en) * 2015-08-06 2015-11-11 黑龙江大学 Method for quickly detecting content of benzoyl peroxide in flour in nondestructive mode and application thereof
CN105675537A (en) * 2015-12-31 2016-06-15 深圳市芭田生态工程股份有限公司 Spectrum detection system and wireless data connection adopted spectrum detector thereof
CN105527246A (en) * 2016-01-14 2016-04-27 昆明睿意铂科技股份有限公司 Portable near infrared spectrum detection system

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108872143A (en) * 2018-05-22 2018-11-23 南京农业大学 A kind of wheat infection head blight level detection method based near infrared spectrum

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Application publication date: 20171117