CN107354770A - A kind of plant dyeing method and device based on safflower - Google Patents
A kind of plant dyeing method and device based on safflower Download PDFInfo
- Publication number
- CN107354770A CN107354770A CN201710605221.5A CN201710605221A CN107354770A CN 107354770 A CN107354770 A CN 107354770A CN 201710605221 A CN201710605221 A CN 201710605221A CN 107354770 A CN107354770 A CN 107354770A
- Authority
- CN
- China
- Prior art keywords
- dyeing
- dye liquor
- puddler
- cloth
- plant
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000004043 dyeing Methods 0.000 title claims abstract description 77
- 241000196324 Embryophyta Species 0.000 title claims abstract description 32
- 235000003255 Carthamus tinctorius Nutrition 0.000 title claims abstract description 15
- 244000020518 Carthamus tinctorius Species 0.000 title claims abstract description 15
- 238000000034 method Methods 0.000 title claims abstract description 12
- 239000004744 fabric Substances 0.000 claims abstract description 30
- 238000000605 extraction Methods 0.000 claims abstract description 18
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 16
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 claims abstract description 5
- 229920001661 Chitosan Polymers 0.000 claims abstract description 5
- 229920002472 Starch Polymers 0.000 claims abstract description 5
- 239000001913 cellulose Substances 0.000 claims abstract description 5
- 229920002678 cellulose Polymers 0.000 claims abstract description 5
- 235000010413 sodium alginate Nutrition 0.000 claims abstract description 5
- 239000000661 sodium alginate Substances 0.000 claims abstract description 5
- 229940005550 sodium alginate Drugs 0.000 claims abstract description 5
- 239000008107 starch Substances 0.000 claims abstract description 5
- 235000019698 starch Nutrition 0.000 claims abstract description 5
- 239000000975 dye Substances 0.000 claims description 63
- 238000003756 stirring Methods 0.000 claims description 21
- 238000010438 heat treatment Methods 0.000 claims description 18
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 8
- 238000003825 pressing Methods 0.000 claims description 6
- 238000005352 clarification Methods 0.000 claims description 5
- 238000007599 discharging Methods 0.000 claims description 5
- 238000005253 cladding Methods 0.000 claims description 4
- 239000012153 distilled water Substances 0.000 claims description 3
- 238000001914 filtration Methods 0.000 claims description 3
- 230000002895 hyperchromatic effect Effects 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 3
- 230000001681 protective effect Effects 0.000 claims description 3
- 239000004615 ingredient Substances 0.000 claims 1
- 239000000049 pigment Substances 0.000 abstract description 11
- 230000009286 beneficial effect Effects 0.000 abstract description 2
- 230000007227 biological adhesion Effects 0.000 abstract description 2
- 239000003795 chemical substances by application Substances 0.000 abstract description 2
- 230000000694 effects Effects 0.000 description 5
- 239000000463 material Substances 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 241000209094 Oryza Species 0.000 description 2
- 235000007164 Oryza sativa Nutrition 0.000 description 2
- 238000005119 centrifugation Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 235000011389 fruit/vegetable juice Nutrition 0.000 description 2
- 238000001556 precipitation Methods 0.000 description 2
- 235000009566 rice Nutrition 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 235000013311 vegetables Nutrition 0.000 description 2
- WLYGSPLCNKYESI-RSUQVHIMSA-N Carthamin Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1[C@@]1(O)C(O)=C(C(=O)\C=C\C=2C=CC(O)=CC=2)C(=O)C(\C=C\2C([C@](O)([C@H]3[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O3)O)C(O)=C(C(=O)\C=C\C=3C=CC(O)=CC=3)C/2=O)=O)=C1O WLYGSPLCNKYESI-RSUQVHIMSA-N 0.000 description 1
- DYQVDISPPLTLLR-HJQYTNQXSA-N Carthamin Natural products CC[C@H]1O[C@H]([C@H](O)[C@@H](O)[C@@H]1O)[C@]2(O)C(=C(C=C/3C(=O)C(=C(O)[C@](O)([C@@H]4O[C@H](CO)[C@@H](O)[C@H](O)[C@H]4O)C3=O)C(=O)C=Cc5ccc(O)cc5)C(=O)C(=C2O)C(=O)C=Cc6ccc(O)cc6)O DYQVDISPPLTLLR-HJQYTNQXSA-N 0.000 description 1
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 1
- 206010020751 Hypersensitivity Diseases 0.000 description 1
- 241001074085 Scophthalmus aquosus Species 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 208000026935 allergic disease Diseases 0.000 description 1
- 230000007815 allergy Effects 0.000 description 1
- 239000000987 azo dye Substances 0.000 description 1
- 230000004888 barrier function Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 230000000711 cancerogenic effect Effects 0.000 description 1
- 231100000315 carcinogenic Toxicity 0.000 description 1
- 235000013339 cereals Nutrition 0.000 description 1
- 229910052804 chromium Inorganic materials 0.000 description 1
- 239000011651 chromium Substances 0.000 description 1
- 238000002788 crimping Methods 0.000 description 1
- 230000006837 decompression Effects 0.000 description 1
- 238000009792 diffusion process Methods 0.000 description 1
- 230000009977 dual effect Effects 0.000 description 1
- 230000003100 immobilizing effect Effects 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 1
- 229910052753 mercury Inorganic materials 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 239000003643 water by type Substances 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/34—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B61/00—Dyes of natural origin prepared from natural sources, e.g. vegetable sources
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0096—Purification; Precipitation; Filtration
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
- D06B1/00—Applying liquids, gases or vapours onto textile materials to effect treatment, e.g. washing, dyeing, bleaching, sizing or impregnating
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
- D06B23/00—Component parts, details, or accessories of apparatus or machines, specially adapted for the treating of textile materials, not restricted to a particular kind of apparatus, provided for in groups D06B1/00 - D06B21/00
- D06B23/20—Arrangements of apparatus for treating processing-liquids, -gases or -vapours, e.g. purification, filtration or distillation
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
- D06B23/00—Component parts, details, or accessories of apparatus or machines, specially adapted for the treating of textile materials, not restricted to a particular kind of apparatus, provided for in groups D06B1/00 - D06B21/00
- D06B23/20—Arrangements of apparatus for treating processing-liquids, -gases or -vapours, e.g. purification, filtration or distillation
- D06B23/205—Arrangements of apparatus for treating processing-liquids, -gases or -vapours, e.g. purification, filtration or distillation for adding or mixing constituents of the treating material
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
- D06B23/00—Component parts, details, or accessories of apparatus or machines, specially adapted for the treating of textile materials, not restricted to a particular kind of apparatus, provided for in groups D06B1/00 - D06B21/00
- D06B23/20—Arrangements of apparatus for treating processing-liquids, -gases or -vapours, e.g. purification, filtration or distillation
- D06B23/22—Arrangements of apparatus for treating processing-liquids, -gases or -vapours, e.g. purification, filtration or distillation for heating
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
- D06P1/651—Compounds without nitrogen
- D06P1/65106—Oxygen-containing compounds
- D06P1/65118—Compounds containing hydroxyl groups
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Coloring (AREA)
Abstract
A kind of plant dyeing method and device based on safflower, the pigment in safflower is solidified using starch, cellulose, separated, locked, the viscosity of solution is improved as biological adhesion agent using sodium alginate, chitosan, the hydrophilic radical for forming macromolecular further peels off pigment molecular, finally pigment is extracted by centrifuge as extractant using ethanol, dye liquor is formed, process is environment friendly and pollution-free and realizes dyeing course by dyeing pot.The beneficial effects of the invention are as follows the color fastness of cloth after the efficiency, pigment extraction performance and dyeing that greatly improve dyeing.
Description
Technical field
The present invention relates to dyeing and equipment technology field, and in particular to a kind of plant dyeing method based on safflower and
Device.
Background technology
Now with greatly improving for people's living standard, cloth, which dyes, mostly uses chemical dye, but chemical dye
Major part is that synthesis is extracted from oil, and this portioned product is to decomposite more than 20 kinds in production to have carcinogenic or cause allergy
Forbidding azo dyes and under certain condition also it is dissociable go out the huge sum of money harmful to human body and environment such as lead, chromium, pick, brill and mercury
Belong to ion.Thus we are dyed using vegetable colour as far as possible, and vegetable colour derives from plant world, with plant
It is raw, died also with plant very environmentally friendly, healthy.Existing plant dyeing also according to traditional pigment due to extracting dyer
Not only dyeing time is long, color fastness is low but also it is very big and existing to contaminate the later very heavy worker's workload of cloth for skill
Dip-dye mode cloth mutually folds, and folds vestige and clearly drastically influence Color, how to improve the skill of plant dyeing
The object of the horizontal always those skilled in the art research of art.
The content of the invention
It is an object of the invention to provide a kind of plant dyeing method and device based on safflower, to solve above-mentioned background skill
The problem of being proposed in art.
To achieve the above object, the present invention provides following technical scheme：
A kind of plant dyeing method based on safflower comprises the following steps：
First, the safflower mixing starch after crushing, cellulose, sodium alginate, chitosan are formed into dyestuff, each composition in dyestuff
Weight proportion is 30: 1: 1: 1: 1, and then dyestuff is put into the ethanol solution that concentration is 25% and carries out the 1st extraction；
2nd, the solution by the first extraction is filtered；
The 3rd, ethanol solution that solution after filtering is put into 25% carries out the 2nd extraction, and the dye liquor after extraction passes through centrifugation
Machine obtains clarification dye liquor；
4th, clarification dye liquor is matched into distilled water according to weight ratio, 1 to 50, is placed in thermostat water bath and is heated to 80 DEG C, 2h
Filtered afterwards on vavuum pump, then the centrifuging and taking upper strata dye liquor on sedimentator.
5th, the dye liquor that step 4 obtains is put into plant dyeing device and is put into 4g/L citric acid simultaneously, it is to be dyed
Cloth it is cylindrical cladding plant dyeing device in puddler, puddler be arranged on agitating shaft on, stirring axis center be provided with
Heating rod, for heating rod to dye liquor heating and temperature control between 55-65 degree, cloth immerged time in plant dyeing device is 24
Hour, obtain through hyperchromatic cloth.
Safflower is the main component of haematochrome in current plant dyeing, and existing extraction process is：Roric safflower is plucked
Hui Hou, through " treadle-operated tilt hammer for hulling rice is smash " into after slurry, clear water is added to impregnate.In neutral conditions, uranidin dissolves, and is twisted with cloth bag and goes uranidin (i.e. yellow
Juice), so, remaining major part has been haematochrome in residual flower.And then with acid such as the sour grain turned sour or rice washing waters
Juice rinses, and further removes the uranidin of residual, you can obtain the residual flower cake containing haematochrome.The side of this extraction carthamin
Method complex process, color fastness is relatively low in dyeing course.The present invention is consolidated using starch, cellulose to the pigment in safflower
Change, separate, locking, improving the viscosity of solution as biological adhesion agent using sodium alginate, chitosan, forming the parent of macromolecular
Pigment molecular is further peeled off by water base group, is finally extracted pigment by centrifuge as extractant using ethanol, is formed
Dye liquor, process are environment friendly and pollution-free.Further increase the precipitation effect of pigment by heating as further technological means, and it is true
The decompression of empty pump filters, and not only increases the extraction rate of dye liquor, and can prevent that pigment is secondary in rapid extraction process
Precipitation, increase dye liquor yield.As the puddler in the cylindrical cladding plant dyeing device of further technological means material
Form circular dip-dye structure and avoid the occurrence of pleat trace, folding line, greatly improve the uniformity of dyeing, and in stirring axis center
Provided with heating rod, for heating rod to dye liquor heating and temperature control between 55-65 degree, this center mode of heating causes dye liquor temperature
Center highest, surrounding is minimum, and dye liquor spreads from center to surrounding with temperature change, and dye liquor is in diffusion process by cloth bag
Wrap up in so that cloth is improved Color by dip-dye power from inside to outside.
A kind of plant dyeing device, including frame and dyeing pot, the centre position of the dyeing pot outer surface are arranged with
Two support shafts, the support shaft and the support arm of frame both sides are rotatablely connected, wherein a support shaft is connected with housing motor
Connect；Stirring motor is provided with the dyeing pot, stirring motor is fixedly connected with the left inside side wall of dyeing pot, connected on stirring motor
There is agitating shaft, agitating shaft is horizontally disposed with, and agitating shaft circumferencial direction is evenly arranged the puddler of more than three, outside puddler top
360 degree of week is wound with cloth, and the pressing plate for being bonded puddler top is provided with the outside of cloth, by located at stirring between pressing plate and puddler
Mix the circular arc spring leaf crimping on bar；Lifter is fixed with the dyeing pot madial wall, the lifter is in arc-shaped；
Dye liquor charging aperture is provided with the top of described dyeing pot, dye liquor charging aperture is provided with the first valve；Dyeing pot bottom goes out provided with dye liquor
Material mouth, dye liquor discharging opening are provided with the second valve；Described stirring axis center is provided with heating rod.This kind of plant dyeing apparatus passes through
Two motors realize dyeing pot and the dual rotation of agitating shaft, not only dye liquor can be rotated, and cloth can be rotated,
Reach the technical purpose fully contaminated, pass through the circular arc spring leaf on puddler between another aspect pressing plate and puddler
Cloth is crimped, avoids cloth damage from also solving the technical barrier that cloth can not wind dyeing always.On dyeing pot madial wall
Lifter structure is the thin slice of a laminated structure in fact, is poured over as the rotation of dyeing pot raises up dye liquor on cloth
Prevent the pigementation in dye liquor.
Protective cover is provided with outside the stirring motor, improves the safe effect of equipment.It is additionally provided with below the frame universal
Wheel.
The agitating shaft right-hand member and dyeing pot sidewall rotation connection.The dyeing pot bottom outside wall is provided with balancing weight,
So that the position that dyeing pot stops every time immobilizing.
The beneficial effects of the invention are as follows cloth after the efficiency, pigment extraction performance and dyeing that greatly improve dyeing
Color fastness.
Brief description of the drawings
Fig. 1 is the structural representation of dyeing pot in the present invention；
Fig. 2 is dyeing pot internal structure in the present invention.
Embodiment
Below in conjunction with the accompanying drawing in the embodiment of the present invention, the technical scheme in the embodiment of the present invention is carried out clear, complete
Site preparation describes, it is clear that described embodiment is only part of the embodiment of the present invention, rather than whole embodiments.It is based on
Embodiment in the present invention, those of ordinary skill in the art are obtained every other under the premise of creative work is not made
Embodiment, belong to the scope of protection of the invention.
Fig. 1 and Fig. 2 are referred to, a kind of plant dyeing method based on safflower comprises the following steps：
First, the safflower mixing starch after crushing, cellulose, sodium alginate, chitosan are formed into dyestuff, each composition in dyestuff
Weight proportion is 30: 1: 1: 1: 1, and then dyestuff is put into the ethanol solution that concentration is 25% and carries out the 1st extraction；
2nd, the solution by the first extraction is filtered；
The 3rd, ethanol solution that solution after filtering is put into 25% carries out the 2nd extraction, and the dye liquor after extraction passes through centrifugation
Machine obtains clarification dye liquor；
4th, clarification dye liquor is matched into distilled water according to weight ratio, 1 to 50, is placed in thermostat water bath and is heated to 80 DEG C, 2h
Filtered afterwards on vavuum pump, then the centrifuging and taking upper strata dye liquor on sedimentator.
5th, the dye liquor that step 4 obtains is put into plant dyeing device and is put into 4g/L citric acid simultaneously, it is to be dyed
Cloth it is cylindrical cladding plant dyeing device in puddler, puddler be arranged on agitating shaft on, stirring axis center be provided with
Heating rod, for heating rod to dye liquor heating and temperature control between 55-65 degree, cloth immerged time in plant dyeing device is 24
Hour, obtain through hyperchromatic cloth.
Above-mentioned plant dyeing device, including frame 1 and dyeing pot 7, the centre position of the outer surface of dyeing pot 7 are arranged with two
Root support shaft 4, support shaft 4 and the support arm of the both sides of frame 1 are rotatablely connected, wherein a support shaft is connected with housing motor 3,
Stirring motor 5 is provided with dyeing pot 7, stirring motor 5 is fixedly connected with the left inside side wall of dyeing pot 7.It is connected with stirring motor 5
Agitating shaft 12, the right-hand member of agitating shaft 12 are rotatablely connected with the side wall of dyeing pot 7, and agitating shaft 12 is horizontally disposed, the circumferencial direction of agitating shaft 12
The puddler 11 of more than three is evenly arranged, 360 degree of 11 top periphery of puddler is wound with cloth 16, and the outside of cloth 16 is provided with
The pressing plate 17 on puddler top is bonded, is pressed between pressing plate 17 and puddler 11 by the circular arc spring leaf 18 on puddler
Connect, avoid producing damage to cloth.In order to reach heating Color, the center of agitating shaft 12 is provided with heating rod.Outside stirring motor 5
Portion is provided with protective cover 6.
In order to further improve Color, lifter 8 is fixed with the madial wall of dyeing pot 7, lifter 8 is in circular arc
Shape.The top of dyeing pot 7 is provided with dye liquor charging aperture 10, and dye liquor charging aperture 10 is provided with the first valve 9；The bottom of dyeing pot 7 is provided with dye
Liquid discharging opening 14, dye liquor discharging opening 14 are provided with the disengaging of the second valve 15 control dye liquor.The bottom outside wall of dyeing pot 7 is provided with
Balancing weight 13, frame lower section are additionally provided with universal wheel 2.
The present invention the course of work be：Dye liquor, citric acid are added at feed inlet and outlet 10, close the first valve 9, housing
Motor 3, which works, causes dyeing pot 7 to be rotated around support shaft 4, while stirring motor 5 drives puddler 11 to rotate to inside dyeing pot 7
Dye liquor be stirred effect, the steering of housing motor 3 and stirring motor 5 is set herein on the contrary, further increasing dye liquor pair
The Color of cloth；When dyeing pot 7 rotates, lifter 8 drives the dye liquor in part dyeing pot 7 to rise, so as to enter to dye liquor
Row disturbance, the mixed effect of dye liquor is further expanded, improves Color；After dyeing terminates, go out under the effect of balancing weight 13
Material mouth 14 can be easy to discharge down.
It is obvious to a person skilled in the art that the invention is not restricted to the details of above-mentioned one exemplary embodiment, Er Qie
In the case of without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, embodiment all should be regarded as exemplary, and be nonrestrictive, the scope of the present invention is by appended power
Profit requires rather than described above limits, it is intended that all in the implication and scope of the equivalency of claim by falling
Change is included in the present invention.Any reference in claim should not be considered as to the involved claim of limitation.
Moreover, it will be appreciated that although the present specification is described in terms of embodiments, not each embodiment is only wrapped
Containing an independent technical scheme, this narrating mode of specification is only that those skilled in the art should for clarity
Using specification as an entirety, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
It is appreciated that other embodiment.
Claims (6)
1. a kind of plant dyeing method based on safflower comprises the following steps：
First, the safflower mixing starch after crushing, cellulose, sodium alginate, chitosan are formed into dyestuff, each Ingredients Weight in dyestuff
Match as 30: 1: 1: 1: 1, then dyestuff is put into the ethanol solution that concentration is 25% and carries out the 1st extraction；
2nd, the solution by the first extraction is filtered；
The 3rd, ethanol solution that solution after filtering is put into 25% carries out the 2nd extraction, and the dye liquor after extraction is obtained by centrifuge
Dye liquor must be clarified；
4th, clarification dye liquor is matched into distilled water according to weight ratio, 1 to 50, is placed in thermostat water bath and is heated to 80 DEG C, after 2h
Filtered on vavuum pump, then the centrifuging and taking upper strata dye liquor on sedimentator.
5th, the dye liquor that step 4 obtains is put into plant dyeing device and is put into 4g/L citric acid simultaneously, cloth to be dyed
Expect the puddler in cylindrical cladding plant dyeing device, puddler is arranged on agitating shaft, and stirring axis center is provided with heating
Rod, for heating rod to dye liquor heating and temperature control between 55-65 degree, cloth immerged time in plant dyeing device is 24 small
When, obtain through hyperchromatic cloth.
2. a kind of plant dyeing device according to claim 1, including frame and dyeing pot, it is characterised in that the dye
The centre position of color tank outer surface is arranged with two support shafts, and the support shaft and the support arm of frame both sides are rotatablely connected,
Wherein a support shaft is connected with housing motor；A left side for stirring motor, stirring motor and dyeing pot is provided with the dyeing pot
Madial wall is fixedly connected, and agitating shaft is connected with stirring motor, and agitating shaft is horizontally disposed with, and agitating shaft circumferencial direction has been evenly arranged
The puddler of more than three, 360 degree of puddler top periphery are wound with cloth, and the pressure on fitting puddler top is provided with the outside of cloth
Plate, crimped between pressing plate and puddler by the circular arc spring leaf on puddler；It is fixed on the dyeing pot madial wall
Provided with lifter, the lifter is in arc-shaped；Dye liquor charging aperture is provided with the top of described dyeing pot, dye liquor charging aperture is provided with
First valve；Dyeing pot bottom is provided with dye liquor discharging opening, and dye liquor discharging opening is provided with the second valve；Described stirring axis center is set
There is heating rod.
3. plant dyeing device according to claim 2, it is characterised in that be provided with protective cover outside the stirring motor.
4. plant dyeing device according to claim 2, it is characterised in that the agitating shaft right-hand member turns with dyeing pot sidewall
Dynamic connection.
5. plant dyeing device according to claim 2, it is characterised in that the dyeing pot bottom outside wall, which is provided with, matches somebody with somebody
Pouring weight.
6. plant dyeing device according to claim 2, it is characterised in that be additionally provided with universal wheel below the frame.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710605221.5A CN107354770A (en) | 2017-07-11 | 2017-07-11 | A kind of plant dyeing method and device based on safflower |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710605221.5A CN107354770A (en) | 2017-07-11 | 2017-07-11 | A kind of plant dyeing method and device based on safflower |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107354770A true CN107354770A (en) | 2017-11-17 |
Family
ID=60285359
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710605221.5A Pending CN107354770A (en) | 2017-07-11 | 2017-07-11 | A kind of plant dyeing method and device based on safflower |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107354770A (en) |
Citations (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1152646A (en) * | 1995-11-10 | 1997-06-25 | Ykk株式会社 | Dyeing arrangement |
| CN203021779U (en) * | 2012-12-08 | 2013-06-26 | 江阴骏华纺织科技有限公司 | Drum structure |
| CN103741505A (en) * | 2013-12-20 | 2014-04-23 | 大连创达技术交易市场有限公司 | Silk dyeing process adopting gardenia yellow vegetable dye |
| CN104762834A (en) * | 2015-03-25 | 2015-07-08 | 苏州威尔德工贸有限公司 | Process for dyeing silk fabric by using tuber fern wood dye |
| CN105113289A (en) * | 2015-09-16 | 2015-12-02 | 张家港天隆针织服饰织造有限公司 | Preparing method for balsamine dyed cloth |
| CN106087473A (en) * | 2016-07-11 | 2016-11-09 | 山东如意科技集团有限公司 | A kind of digit printing dyestuff |
| CN107268299A (en) * | 2017-07-11 | 2017-10-20 | 金柯楠 | A kind of plant dyeing method and device based on rat-tail leaf |
| CN107287937A (en) * | 2017-07-11 | 2017-10-24 | 金柯楠 | A kind of plant dyeing method and device based on cork tree |
| CN107287938A (en) * | 2017-07-11 | 2017-10-24 | 金柯楠 | A kind of plant dyeing method and device based on dye yam |
| CN107287936A (en) * | 2017-07-11 | 2017-10-24 | 何小平 | A kind of plant dyeing method and device based on leaf of Chinese ilex |
| CN107313268A (en) * | 2017-07-11 | 2017-11-03 | 金柯楠 | A kind of plant dyeing method and device based on purple perilla |
| CN107354769A (en) * | 2017-07-11 | 2017-11-17 | 何小平 | A kind of plant dyeing method and device based on Chinese tallowtree leaf |
| CN107419558A (en) * | 2017-07-11 | 2017-12-01 | 何小平 | A kind of plant dyeing method and device based on sophora flower |
| CN107476083A (en) * | 2017-07-11 | 2017-12-15 | 金柯楠 | A kind of plant dyeing method and device based on mulberry leaf |
| CN107476082A (en) * | 2017-07-11 | 2017-12-15 | 何小平 | A kind of plant dyeing method and device based on Asian puccoon |
-
2017
- 2017-07-11 CN CN201710605221.5A patent/CN107354770A/en active Pending
Patent Citations (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1152646A (en) * | 1995-11-10 | 1997-06-25 | Ykk株式会社 | Dyeing arrangement |
| CN203021779U (en) * | 2012-12-08 | 2013-06-26 | 江阴骏华纺织科技有限公司 | Drum structure |
| CN103741505A (en) * | 2013-12-20 | 2014-04-23 | 大连创达技术交易市场有限公司 | Silk dyeing process adopting gardenia yellow vegetable dye |
| CN104762834A (en) * | 2015-03-25 | 2015-07-08 | 苏州威尔德工贸有限公司 | Process for dyeing silk fabric by using tuber fern wood dye |
| CN105113289A (en) * | 2015-09-16 | 2015-12-02 | 张家港天隆针织服饰织造有限公司 | Preparing method for balsamine dyed cloth |
| CN106087473A (en) * | 2016-07-11 | 2016-11-09 | 山东如意科技集团有限公司 | A kind of digit printing dyestuff |
| CN107268299A (en) * | 2017-07-11 | 2017-10-20 | 金柯楠 | A kind of plant dyeing method and device based on rat-tail leaf |
| CN107287937A (en) * | 2017-07-11 | 2017-10-24 | 金柯楠 | A kind of plant dyeing method and device based on cork tree |
| CN107287938A (en) * | 2017-07-11 | 2017-10-24 | 金柯楠 | A kind of plant dyeing method and device based on dye yam |
| CN107287936A (en) * | 2017-07-11 | 2017-10-24 | 何小平 | A kind of plant dyeing method and device based on leaf of Chinese ilex |
| CN107313268A (en) * | 2017-07-11 | 2017-11-03 | 金柯楠 | A kind of plant dyeing method and device based on purple perilla |
| CN107354769A (en) * | 2017-07-11 | 2017-11-17 | 何小平 | A kind of plant dyeing method and device based on Chinese tallowtree leaf |
| CN107419558A (en) * | 2017-07-11 | 2017-12-01 | 何小平 | A kind of plant dyeing method and device based on sophora flower |
| CN107476083A (en) * | 2017-07-11 | 2017-12-15 | 金柯楠 | A kind of plant dyeing method and device based on mulberry leaf |
| CN107476082A (en) * | 2017-07-11 | 2017-12-15 | 何小平 | A kind of plant dyeing method and device based on Asian puccoon |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN107354769A (en) | A kind of plant dyeing method and device based on Chinese tallowtree leaf | |
| CN107419558A (en) | A kind of plant dyeing method and device based on sophora flower | |
| CN106281656A (en) | A kind of processing technique of almond oil | |
| CN107476083A (en) | A kind of plant dyeing method and device based on mulberry leaf | |
| CN107287937A (en) | A kind of plant dyeing method and device based on cork tree | |
| CN107476082A (en) | A kind of plant dyeing method and device based on Asian puccoon | |
| CN109628210A (en) | A kind of rapeseed oil processing method | |
| CN106866725A (en) | A kind of method for preparing the transparent concentrating soya lecithin of food grade | |
| CN105524789A (en) | Preparation method of sweet flower sparkling wine | |
| CN107287936A (en) | A kind of plant dyeing method and device based on leaf of Chinese ilex | |
| CN107268299A (en) | A kind of plant dyeing method and device based on rat-tail leaf | |
| CN107354770A (en) | A kind of plant dyeing method and device based on safflower | |
| CN106867816A (en) | A kind of dandelion Howthorn Wine and preparation method thereof | |
| CN107313268A (en) | A kind of plant dyeing method and device based on purple perilla | |
| CN107287938A (en) | A kind of plant dyeing method and device based on dye yam | |
| CN102337196B (en) | Haematococcus alcoholic drink and preparation method thereof | |
| CN104845734B (en) | The absorption decoloring method of one vegetable oil | |
| CN102816056B (en) | Method for extracting itaconic acid through extraction of itaconic acid fermentation solution | |
| CN108795648A (en) | A kind of manufacturing device of blueberry wine | |
| CN105861205B (en) | A kind of red beer of the fruit of glossy privet and preparation method thereof | |
| CN109536360A (en) | A kind of special filtering equipment of wine production | |
| CN105833844B (en) | A kind of preparation method of lotus leaf deacidification agent | |
| CN113150875B (en) | Low-chroma lacquer wax refining process | |
| CN208975278U (en) | A kind of Chinese medicine production peony seed oil filter device | |
| CN211384086U (en) | Polyurethane filter equipment |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20171117 |