CN107348502A - A kind of method for separating natural phospholipid class material in capsicum - Google Patents
A kind of method for separating natural phospholipid class material in capsicum Download PDFInfo
- Publication number
- CN107348502A CN107348502A CN201710413047.4A CN201710413047A CN107348502A CN 107348502 A CN107348502 A CN 107348502A CN 201710413047 A CN201710413047 A CN 201710413047A CN 107348502 A CN107348502 A CN 107348502A
- Authority
- CN
- China
- Prior art keywords
- capsicum
- class material
- natural phospholipid
- hexane
- extract
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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- 240000008574 Capsicum frutescens Species 0.000 title claims abstract description 34
- 235000002566 Capsicum Nutrition 0.000 title claims abstract description 31
- 239000001390 capsicum minimum Substances 0.000 title claims abstract description 28
- 239000000463 material Substances 0.000 title claims abstract description 23
- 238000000034 method Methods 0.000 title claims abstract description 23
- 229940042880 natural phospholipid Drugs 0.000 title claims abstract description 22
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 claims abstract description 45
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 17
- 229940116257 pepper extract Drugs 0.000 claims abstract description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 13
- 238000000605 extraction Methods 0.000 claims abstract description 11
- 238000001914 filtration Methods 0.000 claims abstract description 5
- 238000001035 drying Methods 0.000 claims description 10
- 239000000843 powder Substances 0.000 claims description 8
- 229940007061 capsicum extract Drugs 0.000 claims description 7
- 239000001943 capsicum frutescens fruit extract Substances 0.000 claims description 7
- 239000007788 liquid Substances 0.000 claims description 7
- 239000002904 solvent Substances 0.000 claims description 7
- 238000001514 detection method Methods 0.000 claims description 6
- 238000003756 stirring Methods 0.000 claims description 6
- 238000010438 heat treatment Methods 0.000 claims description 5
- 238000005070 sampling Methods 0.000 claims description 5
- 239000007787 solid Substances 0.000 claims description 3
- 238000012805 post-processing Methods 0.000 claims description 2
- 239000000243 solution Substances 0.000 abstract description 10
- 239000000284 extract Substances 0.000 abstract description 6
- 238000012545 processing Methods 0.000 abstract description 6
- VYIRVAXUEZSDNC-TXDLOWMYSA-N (3R,3'S,5'R)-3,3'-dihydroxy-beta-kappa-caroten-6'-one Chemical compound C([C@H](O)CC=1C)C(C)(C)C=1/C=C/C(/C)=C/C=C/C(/C)=C/C=C/C=C(C)C=CC=C(C)C=CC(=O)[C@]1(C)C[C@@H](O)CC1(C)C VYIRVAXUEZSDNC-TXDLOWMYSA-N 0.000 abstract description 3
- VYIRVAXUEZSDNC-LOFNIBRQSA-N Capsanthyn Natural products CC(=C/C=C/C=C(C)/C=C/C=C(C)/C=C/C1=C(C)CC(O)CC1(C)C)C=CC=C(/C)C=CC(=O)C2(C)CC(O)CC2(C)C VYIRVAXUEZSDNC-LOFNIBRQSA-N 0.000 abstract description 3
- 239000006002 Pepper Substances 0.000 abstract description 3
- 241000722363 Piper Species 0.000 abstract description 3
- 235000016761 Piper aduncum Nutrition 0.000 abstract description 3
- 235000017804 Piper guineense Nutrition 0.000 abstract description 3
- 235000008184 Piper nigrum Nutrition 0.000 abstract description 3
- WRANYHFEXGNSND-LOFNIBRQSA-N capsanthin Natural products CC(=C/C=C/C=C(C)/C=C/C=C(C)/C=C/C1=C(C)CC(O)CC1(C)C)C=CC=C(/C)C=CC(=O)C2(C)CCC(O)C2(C)C WRANYHFEXGNSND-LOFNIBRQSA-N 0.000 abstract description 3
- 235000018889 capsanthin Nutrition 0.000 abstract description 3
- 235000012658 paprika extract Nutrition 0.000 abstract description 3
- 239000001688 paprika extract Substances 0.000 abstract description 3
- 239000007864 aqueous solution Substances 0.000 abstract description 2
- 238000001816 cooling Methods 0.000 abstract description 2
- 239000000126 substance Substances 0.000 description 3
- 241000208293 Capsicum Species 0.000 description 2
- 235000013305 food Nutrition 0.000 description 2
- 150000003904 phospholipids Chemical class 0.000 description 2
- 208000024827 Alzheimer disease Diseases 0.000 description 1
- 235000008534 Capsicum annuum var annuum Nutrition 0.000 description 1
- 240000008384 Capsicum annuum var. annuum Species 0.000 description 1
- 208000024172 Cardiovascular disease Diseases 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- 206010039966 Senile dementia Diseases 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 230000017531 blood circulation Effects 0.000 description 1
- 210000004958 brain cell Anatomy 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 239000001722 capsicum frutescens oleoresin Substances 0.000 description 1
- 229940050948 capsicum oleoresin Drugs 0.000 description 1
- 210000004027 cell Anatomy 0.000 description 1
- 210000000170 cell membrane Anatomy 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 230000036039 immunity Effects 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 210000005036 nerve Anatomy 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 230000004936 stimulating effect Effects 0.000 description 1
- 238000005728 strengthening Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Botany (AREA)
- Mycology (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Medicines Containing Plant Substances (AREA)
- Seasonings (AREA)
- Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
Abstract
The invention discloses a kind of method for separating natural phospholipid class material in capsicum, comprise the following steps：Extracted first with n-hexane and ethanol, be separated by filtration capsanthin, extract solution is concentrated, obtain preliminary pepper extract；Then add water to be diluted into pepper extract, add n-hexane, carry out further extraction and separate；During cooling, natural phospholipid class material sinks, between upper strata n-hexane and lower floor's water, upper strata hexane solution is evaporated and is concentrated to give pepper extract, the aqueous solution containing natural phospholipid class material of lower floor is dried, and obtains natural phospholipid class material, it is applied to health products trade, a direction is provided for capsicum deep processing, increases peasant income to greatest extent, reduces the risk of pepper planting.
Description
Technical field
The present invention relates to food processing technology field, more particularly to a kind of side for separating natural phospholipid class material in capsicum
Method.
Background technology
Phosphatide is the lipoid substance containing phosphatide, is the main component for forming cell membrane, is the basic substance of life.Phosphorus
Fat improves blood circulation, prevention of cardiovascular disease has many effects, and phosphatide can accelerate nerve to strengthening body immunity
The speed of information transmission between cell and brain cell, strengthen memory, senile dementia can be prevented.Therefore, phosphatide is in health care conduct
Industry application space is extremely extensive.
And the plantation of capsicum large area in recent years, cause capsicum price to go way down, it is often more important that China some areas
Capsicum there is no processing approach at all, can only be consumed by catering industry, catering industry consumption again be a long-term process.Therefore
Capsicum deep processing seems more and more urgent, and under this environmental condition, phosphatide is extracted from capsicum, is applied to health care conduct
Industry, a direction is provided for capsicum deep processing, peasant income can be increased to greatest extent, reduce the risk of pepper planting.
The content of the invention
In order to solve the above technical problems, the invention provides it is a kind of separate capsicum in natural phospholipid class material method, with
Reach the purpose for the market added value for improving capsicum.
To reach above-mentioned purpose, technical scheme is as follows：
A kind of method for separating natural phospholipid class material in capsicum, comprises the following steps：
(1) by capsicum remove seed, crush, cross 40 eye mesh screens, extracting screen underflow chilli powder, Extraction solvent is being added just into chilli powder
Hexane and ethanol, post processing extraction solvent consumption are 1-10 times of chilli powder quality, are heated to 30-60 DEG C and stir, are stood, and are stood
Extract solution is filtered with fast grade filter paper afterwards；
(2) the extraction solution after filtering is concentrated on a rotary evaporator, sampling detection capsicum extraction in concentration process
Total volatile matter of liquid, when total volatile matter of capsicum extract is reduced to below 1.00%, stops concentration, obtain pepper extract
One；
(3) water of 2 times of quality is added into pepper extract one, the n-hexane of 4 times of quality, 30 are stirred in closed container
Minute, maintained the temperature in whipping process within the scope of 30-50 DEG C, stirring stops heating after terminating, and closed container is placed in cold
In storehouse, 12-24 hours are stood, dwell temperature is -5 DEG C to -15 DEG C；
(4) stand after terminating, separate upper liquid and subnatant, upper liquid are concentrated on a rotary evaporator, it is concentrated
Total volatile matter of sampling detection capsicum extract, when total volatile matter is reduced to below 1.00%, stops concentration, obtains peppery in journey
Green pepper extract two, lower floor dries in an oven, when drying to lower floor's thing is semi-solid always, stops drying, the thing now obtained
Matter is natural phospholipid class material.
In such scheme, the volume ratio of n-hexane and ethanol is 6 in the step (1)：4.
In such scheme, the water bath heating temperature of Rotary Evaporators is 60 DEG C in the step (2) and step (4), vacuum
Spend between -0.04Mpa to -0.06Mpa.
In such scheme, the temperature of the water added in the step (3) is 35-50 DEG C, and the temperature of n-hexane is 30-45
℃。
In such scheme, drying temperature is 105 DEG C to 110 DEG C in the step (4).
Pass through above-mentioned technical proposal, the method provided by the invention for separating natural phospholipid class material in capsicum is first with just
Hexane and ethanol are extracted, and are separated by filtration capsanthin, and extract solution is concentrated, and obtain preliminary pepper extract；Then
Into pepper extract plus water is diluted, and adds n-hexane, carries out further extraction separation；During cooling, natural phospholipid class
Material sinks, and between upper strata n-hexane and lower floor's water, upper strata hexane solution is evaporated and is concentrated to give capsicum extraction
Thing, the aqueous solution containing natural phospholipid class material of lower floor are dried, and obtain natural phospholipid class material.
Obtained phospholipid substance can be applied to using this method by health products trade, the by-product during separating phospholipids
Thing can be used as capsanthin, capsicum oleoresin to sell, and a direction is provided for capsicum deep processing, increase peasant to greatest extent and receive
Benefit, reduce the risk of pepper planting.
Embodiment
The technical scheme in the embodiment of the present invention will be clearly and completely described below.
The invention provides a kind of method for separating natural phospholipid class material in capsicum, specific embodiment are as follows：
(1) by 2000 grams of capsicum remove seed, stalk, then crushed with high speed disintegrator, the chilli powder after crushing crosses 40 mesh
Screen cloth, one 10 liters of stainless steel cask with cover is taken, 1000 grams of chilli powders are added into bucket, continuously add double solvents, it is (compound
Solvent is n-hexane and ethanol, n-hexane：Ethanol volume ratio is 6：4), double solvents addition is 5000 milliliters, is heated to 45
DEG C and stir, stood, extract solution filtered with fast grade filter paper after standing.
(2) the extraction solution after filtering is concentrated on a rotary evaporator, and water bath heating temperature is 60 degrees Celsius, vacuum
Spend between -0.04Mpa to -0.06Mpa, total volatile matter of sampling detection capsicum extract, works as extract solution in concentration process
Total volatile matter when being reduced to less than 1.00%, stop concentration, obtain pepper extract one.
(3) water of 2 times of quality is added into pepper extract one, the temperature of water is 35 DEG C, the n-hexane of 4 times of quality, just
The temperature of hexane is 30 DEG C, is stirred 30 minutes in closed container, 35 DEG C is maintained the temperature in whipping process, stirring stops after terminating
Only heat, by closed container as in freezer, stand 24 hours, dwell temperature is -5 DEG C.
(4) stand after terminating, separate upper liquid and subnatant, upper liquid are concentrated on a rotary evaporator, water-bath adds
Hot temperature is 60 DEG C, and vacuum is between -0.04Mpa to -0.06Mpa, and detection capsicum extract always waves in concentration process
Stimulating food, when total volatile matter of extract solution is reduced to below 1.00%, stops concentration, obtain pepper extract two, lower floor is drying
Dried in case, drying temperature is 105-110 DEG C, when drying to lower floor's thing is semi-solid always, stops drying, the thing now obtained
Matter is natural phospholipid class material.
The foregoing description of the disclosed embodiments, professional and technical personnel in the field are enable to realize or using the present invention.
A variety of modifications to these embodiments will be apparent for those skilled in the art, as defined herein
General Principle can be realized in other embodiments without departing from the spirit or scope of the present invention.Therefore, it is of the invention
The embodiments shown herein is not intended to be limited to, and is to fit to and principles disclosed herein and features of novelty phase one
The most wide scope caused.
Claims (5)
- A kind of 1. method for separating natural phospholipid class material in capsicum, it is characterised in that comprise the following steps：(1) by capsicum remove seed, crush, cross 40 eye mesh screens, extracting screen underflow chilli powder, Extraction solvent n-hexane is added into chilli powder And ethanol, post processing extraction solvent consumption are 1-10 times of chilli powder quality, are heated to 30-60 DEG C and stir, stood, are used after standing Fast grade filter paper filters to extract solution；(2) the extraction solution after filtering is concentrated on a rotary evaporator, sampling detection capsicum extract in concentration process Total volatile matter, when total volatile matter of capsicum extract is reduced to below 1.00%, stops concentration, obtain pepper extract one；(3) water of 2 times of quality is added into pepper extract one, the n-hexane of 4 times of quality, 30 points are stirred in closed container Clock, maintain the temperature within the scope of 30-50 DEG C in whipping process, stirring stops heating after terminating, and closed container is placed in into freezer In, 12-24 hours are stood, dwell temperature is -5 DEG C to -15 DEG C；(4) stand after terminating, separate upper liquid and subnatant, upper liquid are concentrated on a rotary evaporator, in concentration process Total volatile matter of sampling detection capsicum extract, when total volatile matter is reduced to below 1.00%, stops concentration, obtains capsicum and carry Thing two is taken, lower floor dries in an oven, when drying to lower floor's thing is semi-solid always, stops drying, the material now obtained is Natural phospholipid class material.
- A kind of 2. method for separating natural phospholipid class material in capsicum according to claim 1, it is characterised in that the step Suddenly the volume ratio of n-hexane and ethanol is 6 in (1)：4.
- A kind of 3. method for separating natural phospholipid class material in capsicum according to claim 1, it is characterised in that the step Suddenly the water bath heating temperature of Rotary Evaporators is 60 DEG C in (2) and step (4), vacuum for -0.04Mpa to -0.06Mpa it Between.
- A kind of 4. method for separating natural phospholipid class material in capsicum according to claim 1, it is characterised in that the step Suddenly the temperature of the water added in (3) is 35-50 DEG C, and the temperature of n-hexane is 30-45 DEG C.
- A kind of 5. method for separating natural phospholipid class material in capsicum according to claim 1, it is characterised in that the step Suddenly drying temperature is 105 DEG C to 110 DEG C in (4).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710413047.4A CN107348502A (en) | 2017-06-05 | 2017-06-05 | A kind of method for separating natural phospholipid class material in capsicum |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710413047.4A CN107348502A (en) | 2017-06-05 | 2017-06-05 | A kind of method for separating natural phospholipid class material in capsicum |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107348502A true CN107348502A (en) | 2017-11-17 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710413047.4A Pending CN107348502A (en) | 2017-06-05 | 2017-06-05 | A kind of method for separating natural phospholipid class material in capsicum |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107348502A (en) |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102041166A (en) * | 2011-01-20 | 2011-05-04 | 山东师范大学 | Method for extracting krill oil with high phosphatide content from Antarctic krills |
| CN102304147A (en) * | 2011-04-09 | 2012-01-04 | 吕维学 | Method for extracting phospholipid |
| CN102600294A (en) * | 2011-12-15 | 2012-07-25 | 武城县英潮经贸有限公司 | Novel process for extracting pepper phospholipid from pepper |
-
2017
- 2017-06-05 CN CN201710413047.4A patent/CN107348502A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102041166A (en) * | 2011-01-20 | 2011-05-04 | 山东师范大学 | Method for extracting krill oil with high phosphatide content from Antarctic krills |
| CN102304147A (en) * | 2011-04-09 | 2012-01-04 | 吕维学 | Method for extracting phospholipid |
| CN102600294A (en) * | 2011-12-15 | 2012-07-25 | 武城县英潮经贸有限公司 | Novel process for extracting pepper phospholipid from pepper |
Non-Patent Citations (1)
| Title |
|---|
| 车云波: "《功能食品加工技术》", 31 January 2013, 中国质检出版社、中国标准出版社 * |
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| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20171117 |