CN107313252A - A kind of cowboy's antibacterial stiffening agent and preparation method thereof - Google Patents
A kind of cowboy's antibacterial stiffening agent and preparation method thereof Download PDFInfo
- Publication number
- CN107313252A CN107313252A CN201710628375.6A CN201710628375A CN107313252A CN 107313252 A CN107313252 A CN 107313252A CN 201710628375 A CN201710628375 A CN 201710628375A CN 107313252 A CN107313252 A CN 107313252A
- Authority
- CN
- China
- Prior art keywords
- antibacterial
- parts
- cowboy
- stiffening agent
- dispersant
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 230000000844 anti-bacterial effect Effects 0.000 title claims abstract description 45
- 239000003351 stiffener Substances 0.000 title claims abstract description 30
- 238000002360 preparation method Methods 0.000 title claims description 6
- 239000002270 dispersing agent Substances 0.000 claims abstract description 16
- 239000000178 monomer Substances 0.000 claims abstract description 15
- 239000003999 initiator Substances 0.000 claims abstract description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 12
- 239000003054 catalyst Substances 0.000 claims abstract description 11
- 239000003945 anionic surfactant Substances 0.000 claims abstract description 9
- 239000003795 chemical substances by application Substances 0.000 claims description 9
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 4
- XTXRWKRVRITETP-UHFFFAOYSA-N Vinyl acetate Chemical compound CC(=O)OC=C XTXRWKRVRITETP-UHFFFAOYSA-N 0.000 claims description 2
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 2
- 125000005395 methacrylic acid group Chemical group 0.000 claims description 2
- 229910000402 monopotassium phosphate Inorganic materials 0.000 claims description 2
- 235000019796 monopotassium phosphate Nutrition 0.000 claims description 2
- 229910000403 monosodium phosphate Inorganic materials 0.000 claims description 2
- 235000019799 monosodium phosphate Nutrition 0.000 claims description 2
- PJNZPQUBCPKICU-UHFFFAOYSA-N phosphoric acid;potassium Chemical compound [K].OP(O)(O)=O PJNZPQUBCPKICU-UHFFFAOYSA-N 0.000 claims description 2
- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 claims description 2
- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 claims description 2
- 239000011780 sodium chloride Substances 0.000 claims description 2
- 235000002639 sodium chloride Nutrition 0.000 claims description 2
- AJPJDKMHJJGVTQ-UHFFFAOYSA-M sodium dihydrogen phosphate Chemical compound [Na+].OP(O)([O-])=O AJPJDKMHJJGVTQ-UHFFFAOYSA-M 0.000 claims description 2
- FQENQNTWSFEDLI-UHFFFAOYSA-J sodium diphosphate Chemical compound [Na+].[Na+].[Na+].[Na+].[O-]P([O-])(=O)OP([O-])([O-])=O FQENQNTWSFEDLI-UHFFFAOYSA-J 0.000 claims description 2
- GCLGEJMYGQKIIW-UHFFFAOYSA-H sodium hexametaphosphate Chemical compound [Na]OP1(=O)OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])OP(=O)(O[Na])O1 GCLGEJMYGQKIIW-UHFFFAOYSA-H 0.000 claims description 2
- 229940048086 sodium pyrophosphate Drugs 0.000 claims description 2
- 235000019818 tetrasodium diphosphate Nutrition 0.000 claims description 2
- 239000001577 tetrasodium phosphonato phosphate Substances 0.000 claims description 2
- 229940117958 vinyl acetate Drugs 0.000 claims description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims 1
- 229920000388 Polyphosphate Polymers 0.000 claims 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims 1
- 238000006555 catalytic reaction Methods 0.000 claims 1
- 239000000460 chlorine Substances 0.000 claims 1
- 229910052801 chlorine Inorganic materials 0.000 claims 1
- 125000001309 chloro group Chemical group Cl* 0.000 claims 1
- 150000004702 methyl esters Chemical class 0.000 claims 1
- 150000004714 phosphonium salts Chemical group 0.000 claims 1
- 239000001205 polyphosphate Substances 0.000 claims 1
- 235000011176 polyphosphates Nutrition 0.000 claims 1
- 239000011591 potassium Substances 0.000 claims 1
- 229910052700 potassium Inorganic materials 0.000 claims 1
- 235000007686 potassium Nutrition 0.000 claims 1
- 239000011734 sodium Substances 0.000 claims 1
- 229910052708 sodium Inorganic materials 0.000 claims 1
- 239000004744 fabric Substances 0.000 abstract description 7
- 238000005406 washing Methods 0.000 abstract description 4
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical group [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 description 2
- 125000000129 anionic group Chemical group 0.000 description 2
- 230000003213 activating effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000003115 biocidal effect Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- -1 phosphonium salt group Ester Chemical class 0.000 description 1
- 235000011164 potassium chloride Nutrition 0.000 description 1
- 239000001103 potassium chloride Substances 0.000 description 1
- 235000019832 sodium triphosphate Nutrition 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/244—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus
- D06M13/282—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus with compounds containing phosphorus
- D06M13/313—Unsaturated compounds containing phosphorus atoms, e.g. vinylphosphonium compounds
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/07—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with halogens; with halogen acids or salts thereof; with oxides or oxyacids of halogens or salts thereof
- D06M11/11—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with halogens; with halogen acids or salts thereof; with oxides or oxyacids of halogens or salts thereof with halogen acids or salts thereof
- D06M11/13—Ammonium halides or halides of elements of Groups 1 or 11 of the Periodic Table
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/68—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with phosphorus or compounds thereof, e.g. with chlorophosphonic acid or salts thereof
- D06M11/70—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with phosphorus or compounds thereof, e.g. with chlorophosphonic acid or salts thereof with oxides of phosphorus; with hypophosphorous, phosphorous or phosphoric acids or their salts
- D06M11/71—Salts of phosphoric acids
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/68—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with phosphorus or compounds thereof, e.g. with chlorophosphonic acid or salts thereof
- D06M11/72—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with phosphorus or compounds thereof, e.g. with chlorophosphonic acid or salts thereof with metaphosphoric acids or their salts; with polyphosphoric acids or their salts; with perphosphoric acids or their salts
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M16/00—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Biochemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Microbiology (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
Abstract
The present invention provides a kind of cowboy's antibacterial stiffening agent, it is characterised in that include the component of following parts by weight：Monomer containing antibacterial group：15 ~ 25 parts；Anion surfactant：1 ~ 2.5 part；Initiator：0.01 ~ 0.1 part；Catalyst：0.01 ~ 0.1 part；Water：25 ~ 35 parts；Dispersant：1 ~ 4 part；Buffer：0.5 ~ 2 part.A kind of cowboy's antibacterial stiffening agent of the present invention has the antibacterial action of function admirable, and denim fabric is after the arrangement of the stiffening agent, and stiffness is significantly improved, and washing fastness is good, glossiness, and unfading etc. is significantly improved.
Description
Technical field
The present invention relates to a kind of cowboy's antibacterial stiffening agent and preparation method thereof.
Background technology
Cloth hard finishing agent is that a kind of particularly important Fabric Style is arranged, and it is widely used in the Final finishing of drapery
In technique, the research both at home and abroad to a series of this finishing agent is very deep, and the kind of stiffening agent also has as many as hundreds of.But
For various cloth hard finishing agents, high, the serious living environment that have impact on people of its chemical composition.The effect of its stiffening agent simultaneously
It is single, it is impossible to meet requirement of the product in antibiosis.
The content of the invention
To solve above-mentioned problem, it is an object of the invention to provide a kind of cowboy's antibacterial stiffening agent.The cowboy
Antibacterial stiffening agent has the antibacterial action of function admirable, and denim fabric is after the arrangement of the stiffening agent, and stiffness is significantly improved, and
Washing fastness is good, glossiness, and unfading etc. is significantly improved.
To reach above-mentioned purpose, the technical scheme is that：
A kind of cowboy's antibacterial stiffening agent, includes the component of following parts by weight：Monomer containing antibacterial group：15 ~ 25 parts；It is cloudy from
Sub- surfactant：1 ~ 2.5 part；Initiator：0.01 ~ 0.1 part；Catalyst：0.01 ~ 0.1 part；Water：25 ~ 35 parts；Dispersant：1~
4 parts；Buffer：0.5 ~ 2 part.
Further, the component of following parts by weight is included：Monomer containing antibacterial group：15 ~ 20 parts；Anionic surface
Activating agent：1.5 ~ 2.5 parts；Initiator：0.01 ~ 0.05 part；Catalyst：0.01 ~ 0.05 part；Water：25 ~ 30 parts；Dispersant：1~2
Part；Buffer：1 ~ 2 part.
Further, the component of following parts by weight is included：Monomer containing antibacterial group：16 parts；Anionic surface is lived
Property agent：2 parts；Initiator：0.03 part；Catalyst：0.04 part；Water：26 parts；Dispersant：1.2 part；Buffer：1.6 part.
Further, the monomer containing antibacterial group is the sour first of the acrylic or methacrylic containing quaternary phosphonium salt group
Ester or the fine monomer of vinylacetate or propylene.
Further, the dispersant is that the dispersant is sodium tripolyphosphate, calgon and sodium pyrophosphate.
Further, the buffer is that the buffer is potassium chloride, sodium chloride, sodium dihydrogen phosphate, potassium dihydrogen phosphate
In one or more.
A kind of preparation method of cowboy's antibacterial stiffening agent, is made cowboy's antibacterial hard by each component ultrasonic mixing in proportion
Very agent.
The beneficial effects of the present invention are：
A kind of cowboy's antibacterial stiffening agent of the present invention has the antibacterial action of function admirable, and denim fabric is through the stiffening agent
After arrangement, stiffness is significantly improved, and washing fastness is good, glossiness, and unfading etc. is significantly improved.
Embodiment
Embodiment 1
A kind of cowboy's antibacterial stiffening agent, includes the component of following parts by weight：Monomer containing antibacterial group：15 parts；Anion
Surfactant：2 parts；Initiator：0.06 part；Catalyst：0.1 part；Water：25 parts；Dispersant：2 parts；Buffer：0.5 part.
Embodiment 2
A kind of cowboy's antibacterial stiffening agent, includes the component of following parts by weight：Monomer containing antibacterial group：20 parts；Anion
Surfactant：2.5 part；Initiator：0.01 part；Catalyst：0.02 part；Water：30 parts；Dispersant：4 parts；Buffer：1 part.
Embodiment 3
A kind of cowboy's antibacterial stiffening agent, includes the component of following parts by weight：Monomer containing antibacterial group：16 parts；Anion
Surfactant：2 parts；Initiator：0.03 part；Catalyst：0.04 part；Water：26 parts；Dispersant：1.2 part；Buffer：1.6 part.
Embodiment 4
A kind of cowboy's antibacterial stiffening agent, includes the component of following parts by weight：Monomer containing antibacterial group：25 parts；Anion
Surfactant：1 part；Initiator：0.1 part；Catalyst：0.05 part；Water：32 parts；Dispersant：2 parts；Buffer：1.5 part.
Embodiment 5
A kind of cowboy's antibacterial stiffening agent, includes the component of following parts by weight：Monomer containing antibacterial group：18 parts；Anion
Surfactant：1 part；Initiator：0.05 part；Catalyst：0.01 part；Water：35 parts；Dispersant：1 part；Buffer：2 parts.
A kind of preparation method of cowboy's antibacterial stiffening agent, is made cowboy's antibacterial hard by each component ultrasonic mixing in proportion
Very agent.
A kind of cowboy's antibacterial stiffening agent of the present invention has the antibacterial action of function admirable, and denim fabric is stiffening through this
After the arrangement of agent, stiffness is significantly improved, and washing fastness is good, glossiness, and unfading etc. is significantly improved.
It should be noted that the above embodiments are merely illustrative of the technical solutions of the present invention and it is unrestricted.Although with reference to compared with
The present invention is described in detail good embodiment, it will be understood by those within the art that, can be to the technology of invention
Scheme is modified or equivalent substitution, and without departing from the scope of technical solution of the present invention, it all should cover the power in the present invention
In sharp claimed range.
Claims (7)
1. a kind of cowboy's antibacterial stiffening agent, it is characterised in that include the component of following parts by weight：List containing antibacterial group
Body：15 ~ 25 parts；Anion surfactant：1 ~ 2.5 part；Initiator：0.01 ~ 0.1 part；Catalyst：0.01 ~ 0.1 part；Water：25
~ 35 parts；Dispersant：1 ~ 4 part；Buffer：0.5 ~ 2 part.
2. cowboy's antibacterial stiffening agent according to claim 1, it is characterised in that include the component of following parts by weight：Contain
There is the monomer of antibacterial group：15 ~ 20 parts；Anion surfactant：1.5 ~ 2.5 parts；Initiator：0.01 ~ 0.05 part；Catalysis
Agent：0.01 ~ 0.05 part；Water：25 ~ 30 parts；Dispersant：1 ~ 2 part；Buffer：1 ~ 2 part.
3. cowboy's antibacterial stiffening agent according to claim 1, it is characterised in that include the component of following parts by weight：Contain
There is the monomer of antibacterial group：16 parts；Anion surfactant：2 parts；Initiator：0.03 part；Catalyst：0.04 part；Water：26
Part；Dispersant：1.2 part；Buffer：1.6 part.
4. cowboy's antibacterial stiffening agent according to claim 1, it is characterised in that the monomer containing antibacterial group be containing
There are the sour methyl esters of acrylic or methacrylic or vinylacetate or the fine monomer of propylene of quaternary phosphonium salt group.
5. cowboy's antibacterial stiffening agent according to claim 1, it is characterised in that the dispersant is that the dispersant is three
Polyphosphate sodium, calgon and sodium pyrophosphate.
6. cowboy's antibacterial stiffening agent according to claim 1, it is characterised in that the buffer is that the buffer is chlorine
Change the one or more in potassium, sodium chloride, sodium dihydrogen phosphate, potassium dihydrogen phosphate.
7. a kind of preparation method of cowboy's antibacterial stiffening agent as claimed in claim 1, it is characterised in that in proportion by each component
Cowboy's antibacterial stiffening agent is made in ultrasonic mixing.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710628375.6A CN107313252A (en) | 2017-07-28 | 2017-07-28 | A kind of cowboy's antibacterial stiffening agent and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710628375.6A CN107313252A (en) | 2017-07-28 | 2017-07-28 | A kind of cowboy's antibacterial stiffening agent and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107313252A true CN107313252A (en) | 2017-11-03 |
Family
ID=60169809
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710628375.6A Pending CN107313252A (en) | 2017-07-28 | 2017-07-28 | A kind of cowboy's antibacterial stiffening agent and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107313252A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108004773A (en) * | 2017-12-12 | 2018-05-08 | 苏州经贸职业技术学院 | A kind of stiffening agent and preparation method thereof |
| CN108589269A (en) * | 2018-04-28 | 2018-09-28 | 陈毅忠 | A kind of special stiffening agent of cotton fabric |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103524652A (en) * | 2013-09-30 | 2014-01-22 | 江南大学 | Quaternary ammonium salt group-containing halide amine polymer antibacterial agent, and preparation method and application thereof |
| CN105155269A (en) * | 2015-08-09 | 2015-12-16 | 浙江康德新材料有限公司 | Modified fabric finishing agent containing quaternary ammonium salt anti-bacterial agent monomer and preparation method of modified fabric finishing agent |
| CN105237668A (en) * | 2014-08-28 | 2016-01-13 | 江苏神涛环保科技有限公司 | Preparation method and application of novel high-molecular quaternary ammonium salt antibacterial finishing agent |
| CN106565912A (en) * | 2016-11-11 | 2017-04-19 | 广州大学 | Polyquaternium polymer emulsion antibacterial agent, preparation method thereof and application thereof |
| CN106638002A (en) * | 2016-11-10 | 2017-05-10 | 董晓 | Preparation method of non-ironing garment material fabric stiffening agent |
| CN107815871A (en) * | 2017-11-24 | 2018-03-20 | 东华大学 | A kind of preparation method of durable antibiotic fabric |
-
2017
- 2017-07-28 CN CN201710628375.6A patent/CN107313252A/en active Pending
Patent Citations (6)
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| CN103524652A (en) * | 2013-09-30 | 2014-01-22 | 江南大学 | Quaternary ammonium salt group-containing halide amine polymer antibacterial agent, and preparation method and application thereof |
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| CN106638002A (en) * | 2016-11-10 | 2017-05-10 | 董晓 | Preparation method of non-ironing garment material fabric stiffening agent |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108004773A (en) * | 2017-12-12 | 2018-05-08 | 苏州经贸职业技术学院 | A kind of stiffening agent and preparation method thereof |
| CN108589269A (en) * | 2018-04-28 | 2018-09-28 | 陈毅忠 | A kind of special stiffening agent of cotton fabric |
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| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
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| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20171103 |