CN107311399A - A kind of Full-automatic purification device for chemical experiment waste liquid - Google Patents
A kind of Full-automatic purification device for chemical experiment waste liquid Download PDFInfo
- Publication number
- CN107311399A CN107311399A CN201710655690.8A CN201710655690A CN107311399A CN 107311399 A CN107311399 A CN 107311399A CN 201710655690 A CN201710655690 A CN 201710655690A CN 107311399 A CN107311399 A CN 107311399A
- Authority
- CN
- China
- Prior art keywords
- container
- purification
- waste liquid
- organic matter
- full
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F9/00—Multistage treatment of water, waste water or sewage
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/001—Processes for the treatment of water whereby the filtration technique is of importance
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/28—Treatment of water, waste water, or sewage by sorption
- C02F1/283—Treatment of water, waste water, or sewage by sorption using coal, charred products, or inorganic mixtures containing them
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/52—Treatment of water, waste water, or sewage by flocculation or precipitation of suspended impurities
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F1/00—Treatment of water, waste water, or sewage
- C02F1/66—Treatment of water, waste water, or sewage by neutralisation; pH adjustment
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2101/00—Nature of the contaminant
- C02F2101/30—Organic compounds
- C02F2101/34—Organic compounds containing oxygen
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F3/00—Biological treatment of water, waste water, or sewage
- C02F3/02—Aerobic processes
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F3/00—Biological treatment of water, waste water, or sewage
- C02F3/28—Anaerobic digestion processes
-
- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F3/00—Biological treatment of water, waste water, or sewage
- C02F3/34—Biological treatment of water, waste water, or sewage characterised by the microorganisms used
Abstract
The invention discloses a kind of Full-automatic purification device for chemical experiment waste liquid, belong to chemical experiment device field, it adds second processing container and organic matter decomposition container on the basis of basic inorganic matter liquid waste treating apparatus, for the organic matter in decomposing wasting liquid；The first process container and peroxide decomposition container are added on aforementioned base again, peroxide is produced for preventing and eliminating ether；It is additionally provided with the driver elements such as the vibrator being electrically connected with the controller, color sensor and PH sensors；It is also provided with a kind of new-type purification mechanism.The present invention has three kinds of mode of operations, carries out purified treatment for ether, organic matter and inorganic matter respectively so that processing work is more strict and meticulous, can further lift the beneficial effect of chemical experiment waste liquid purified treatment；And treatment and purification process can realize full-automation, improve purification efficiency；It is practical in addition, purification mechanism clean-up effect therein is superior, moreover it is possible to save space.
Description
Technical field
The present invention relates to chemical experiment device field, a kind of Full-automatic purification device for chemical experiment waste liquid is specifically related to.
Background technology
With the continuous improvement of environmental management scientific degree, requirement to environmental monitoring also more and more higher.Environmental monitoring
Monitoring field is constantly widened, the ability of environmental management service is risen to.
The waste liquid environmental pollution produced in chemical experiment is serious, and organic pollution, inorganic pollution can not only pollute weight
Resource is wanted, residue can also influence experimenter's healthy.Emission test waste liquid, if not being acted upon directly polluting ring
Border, endangers the health of people, and its consequence is extremely serious.Therefore, related personnel must be with the sense of responsibility of height, section serious and conscientious
Learn attitude and consciously take correct measure, experimental waste liquid is handled, reach the discharge standard of country's permission, with reduction pair
The pollution of environment, protects ecological environment.For cleaning laboratory, the safety and reliability of chemical experiment, chemical experiment are improved
Liquid waste processing must make rational planning for, and be disposed waste liquid by way of appropriate.Because the composition in waste liquid often changes, choose
Single, traditional effluent purifying processing mode can not exclude the deleterious characteristics of waste liquid completely.
Ether has been also easy to produce volatile peroxide in processing procedure, it is most likely that can occur explosion accident, Jin Erwei
Coerce the safety of related personnel and equipment.But, current existing chemical experiment waste liquid purifier is only divided into organic matter and nothing
Machine thing, is not provided with the processing mechanism for ether.In addition, in existing chemical experiment waste liquid purifier use triple purifications more
Device carrys out purifying waste filtrate, and it includes three box containers that activated carbon is housed, and occupies larger space, it is necessary to make improvements.
The content of the invention
1. the technical problem to be solved passes through
The technical problem to be solved in the present invention is to provide a kind of Full-automatic purification device for chemical experiment waste liquid, and it has three
Mode of operation is planted, purified treatment is carried out for ether, organic matter and inorganic matter respectively so that processing work is more strict and meticulous, can
Further lift the beneficial effect of chemical experiment waste liquid purified treatment；And treatment and purification process can realize full-automation, improve
Purification efficiency；It is practical in addition, purification mechanism clean-up effect therein is superior, moreover it is possible to save space.2. technical scheme
To solve the above problems, the present invention is adopted the following technical scheme that：
A kind of Full-automatic purification device for chemical experiment waste liquid, including controller, alembic and driver element,
The alembic includes waste liquid inlet channel, feed tube, the first process container for being built-in with sodium or iron filings, is built-in with
The second processing container of anaerobism active bacteria all living creatures's thing liquid, the 3rd process container for being built-in with precipitating reagent, peroxide decomposition container,
Organic matter decomposition container, filter, purification mechanism, cut-back tank and discharging tube, the waste liquid inlet channel connect the defeated of feed tube
Enter end, first process container, second processing container and the 3rd process container are connected with the output end of feed tube respectively；It is described
First process container output end is equipped with starch-kalium iodide test paper, and the first process container output end connects peroxide decomposition respectively
The input of container and second processing container, and the peroxide decomposition container output end and second processing container input company
Connect；The organic matter decomposition container connects the output end of second processing container and the input of the 3rd process container respectively；It is described
3rd process container, filter, purification mechanism and cut-back tank are sequentially connected, and output end and the discharging tube of the cut-back tank connect
Connect；Connected between each utensil by connecting tube, being also equipped with filter residue on the filter collects pipe；
The driver element includes the electric valve located at feed tube output end and three process container junctions, located at connection
Pipe, discharging tube and filter residue collect the magnetic valve on pipe, the compression pump in connecting tube located at input less than output end, are located at
The vibrator of peroxide breaks down container bottom, the agitator in the 3rd process container and cut-back tank, be located at starch-
The color sensor of potassium iodide starch paper, the PH sensors in the 3rd process container, color sensor and the PH sensor
The input of controller is connected, the electric valve, magnetic valve, compression pump, vibrator and agitator connect the output end of controller；
The controller includes three kinds of control models, i.e. ether effluent purifying pattern, organic matter purification pattern and inorganic matter is net
Under change pattern, the inorganic matter purification pattern, only waste liquid inlet channel, feed tube, the 3rd process container, filter, clearing machine
Structure, cut-back tank, discharging tube, filter residue collect pipe and connecting tube participates in running；Under organic matter purification pattern, mould is purified in inorganic matter
Second processing container is added on the basis of formula and organic matter decomposition container participates in running；Under ether effluent purifying pattern, organic
The first process container is added on the basis of thing purification pattern and peroxide decomposition container participates in running.
Specifically, the purification mechanism includes clarifier and the spiral purification pipe around clarifier, and purification pipe lower end
Woven hose provided with insertion clarifier bottom, clarifier upper end side is provided with the opening connected for connecting tube, net to connect
Change device and cut-back tank；Center is provided with along purification pipe spiral in the full activated carbon of filling, the purification pipe in the clarifier
Annular catch is uniformly arranged with fixing axle, the fixing axle, the connected mode between the catch and fixing axle is the company of slip
Connect, catch periphery, which is fixed between annular filter paper, the catch, fills full activated carbon, and the purification infratubal port is provided with sealing
Plug；Three parts are uniformly divided into from top to bottom in the purification pipe, and it is sequentially filled completely big mesoporous activated carbon, transition mesoporous activated carbon and micro-
Mesoporous activated carbon.
More specifically, the radius of the big mesoporous activated carbon is 25000nm, the radius of the transition mesoporous activated carbon is
1000nm, the radius of the microporous activated carbon is 150nm.
Specifically, the peroxide decomposition container is built with the copperas solution that concentration is 5%, the organic matter point
Solution container content has aerobic active bacteria all living creatures thing liquid.
Specifically, in the 3rd process container when PH reactions are adjusted, the material of addition is nertralizer；Carrying out
When generating the reaction of precipitation, the material of addition is precipitating reagent.
3. beneficial effect
(1) chemical experiment waste liquid purifier provided by the present invention has three kinds of mode of operations, respectively for only containing nothing
The waste liquid of machine thing, the waste liquid containing organic matter and the waste liquid containing ether, to adapt to the spy that chemical experiment waste liquid composition often changes
Point.Refinement analyzing and processing chemical experiment waste liquid, makees further classification to waste liquid, and rationally handled so that processing work is more
To be strict and meticulous, the beneficial effect of chemical experiment waste liquid processing discharge can be further lifted.
(2) purification mechanism in chemical experiment waste liquid purifier provided by the present invention includes clarifier and spiral ring
Around the purification pipe of clarifier, first purified pipe is acted on waste liquid to be clean by an adsorption cleaning, then purified device is by secondary
Adsorption cleaning is acted on, and its action effect is enough up to standard；Compared to triple clarifiers, purification mechanism provided by the present invention also has
Space-saving advantage.
(3) it is provided by the present invention purification pipe in be uniformly divided into three parts from top to bottom, be sequentially filled completely big mesoporous activated carbon,
Full activated carbon is filled in transition mesoporous activated carbon and microporous activated carbon, clarifier.The activated carbon of three kinds of different sizes is gradable to useless
Liquid is adsorbed so that it is applied to the application of various impurity absorptions, so as to improve clean-up effect；Moreover, purified Guan Jing
Waste liquid after change enters from clarifier lower end, from the outflow of clarifier upper end, and has carried out once preferable adsorption cleaning to waste liquid,
Further strengthen absorption purifying effect.It follows that the clean-up effect of purification mechanism provided by the present invention is superior.
(4) because purification pipe provided by the present invention is helical form, the activated carbon of its internal filling, which exists, is difficult to what is changed
Problem, to solve this problem, the present invention is provided with the fixing axle along purification pipe spiral at its inside center, and in fixing axle
It is even to be arranged with annular catch, connected mode between the catch and fixing axle to be slidably connected, activated carbon be filled in catch it
Between.When changing activated carbon, purification pipe lower end port is opened, using the Gravitative Loads of catch, it is moved downward along fixing axle, point
Section releases activated carbon；Then purification pipe lower end port is blocked, from purification pipe upper end port filling activated carbon, a part is often filled
A catch is just worn in fixing axle, until end-of-fill.It is difficult to obtain the problem of replacing it follows that above-mentioned activated carbon is present
Good solution.
(5) catch periphery is fixed with annular filter paper in purification pipe provided by the present invention, can further filter waste liquid, promote
Effluent purifying, lifts clean-up effect.
(6) present invention is handled the organic matter in waste liquid using active bacteria all living creatures thing liquid, it is resolved into inorganic matter,
Then the purification of inorganic matter is carried out.In the decomposable process of organic matter, preliminary exposition is first carried out using the active flora of anaerobism,
Deep decomposition is carried out using aerobic active bacteria again so that organic matter is decomposed completely as far as possible, simple inorganic matter is generated, after being easy to
Continuous processing.
(7) present invention is directed to ether, first adds sodium or iron filings, can prevent from forming peroxide；It is first sharp before being decomposed
It is detected with starch-kalium iodide test paper, if aobvious blueness, illustrates there is peroxide generation, utilize copperas solution
Decomposed after removing peroxide.It can ensure that the threat for avoiding peroxide, it is ensured that the security during subsequent operation.
(8) whether detection starch-kalium iodide test paper is also included in chemical experiment waste liquid purifier provided by the present invention
Show the color sensor of blueness, detect the pH value of waste liquid in the 3rd process container PH sensors whether up to standard.Controller according to
The difference of testing result opens corresponding magnetic valve, realizes Automated condtrol, improves the automatic degree of device, and device is realized in promotion
It is full-automatic, be conducive to improve purification efficiency.
The present invention has three kinds of mode of operations, carries out purified treatment for ether, organic matter and inorganic matter respectively so that processing
Work is more strict and meticulous, can further lift the beneficial effect of chemical experiment waste liquid purified treatment；And treatment and purification process can
Full-automation is realized, purification efficiency is improved；It is practical in addition, purification mechanism clean-up effect therein is superior, moreover it is possible to save space
Property is strong.
Brief description of the drawings
Fig. 1 is structure schematic diagram of the invention；
Fig. 2 is the structural representation of purification mechanism；
Fig. 3 is the internal structure schematic diagram of purification pipe 9；
Fig. 4 is the Section A-A figure in Fig. 3.
Wherein, at 1- waste liquids inlet channel, 2- feed tubes, the process containers of 3- first, 4- peroxide decomposition containers, 5- second
Container is managed, 6- organic matter decomposition containers, the process containers of 7- the 3rd, 8- filters, 9- purifications are managed, 10- clarifiers, 11- woven hoses,
12- cut-back tanks, 13- discharging tubes, 14- connecting tubes, 15- filter residues collect pipe, 16- electric valves, 17- starch-kalium iodide test paper,
18- magnetic valves, 19- compression pumps, 20- color sensors, 21- vibrators, 22- agitators, 23-PH sensors, 24- fixing axles,
25- catch, 26- annular filter paper, 27- sealing plugs.
Embodiment
The present invention is further detailed explanation with reference to the accompanying drawings and examples.
Embodiment
A kind of Full-automatic purification device for chemical experiment waste liquid as shown in Figure 1, including controller, alembic and driving are single
Member,
The alembic includes waste liquid inlet channel 1, feed tube 2, the first process container 3 for being built-in with sodium or iron filings, interior
The second processing container 5 for being equipped with anaerobism active bacteria all living creatures's thing liquid, the 3rd process container 7 for being built-in with precipitating reagent, peroxide point
Solve container 4, organic matter decomposition container 6, filter 8, purification mechanism, cut-back tank 12 and discharging tube 13, the waste liquid inlet channel 1
Connect feed tube 2 input, first process container 3, the process container 7 of second processing container 5 and the 3rd respectively with feed liquor
The output end connection of pipe 2；The output end of first process container 3 is equipped with starch-kalium iodide test paper 17, and the first process container 3 is defeated
Go out the input that end connects peroxide decomposition container 4 and second processing container 5 respectively, and the peroxide decomposition container 4
Output end is connected with the input of second processing container 5；The organic matter decomposition container 6 connects the defeated of second processing container 5 respectively
Go out the input of end and the 3rd process container 7；3rd process container 7, filter 8, purification mechanism and cut-back tank 12 according to
Secondary connection, the output end of the cut-back tank 12 is connected with discharging tube 13；Connected between each utensil by connecting tube 14, institute
State and filter residue is also equipped with filter 8 collects pipe 15；
The driver element includes the electric valve 16 located at the output end of feed tube 2 and three process container junctions, is located at
Connecting tube 14, discharging tube 13 and filter residue collect the magnetic valve 18 on pipe 15, in the connecting tube 14 located at input less than output end
Compression pump 19, the vibrator 21 located at the bottom of peroxide decomposition container 4, located at the 3rd process container 7 and cut-back tank 12
Interior agitator 22, is located at the color sensor 20 of starch-kalium iodide test paper 17, the PH in the 3rd process container 7
Sensor 23, the color sensor 20 and PH sensors 23 connect the input of controller, the electric valve 16, magnetic valve
18th, compression pump 19, vibrator 21 and agitator 22 connect the output end of controller；
The controller includes three kinds of control models, i.e. ether effluent purifying pattern, organic matter purification pattern and inorganic matter is net
Under change pattern, the inorganic matter purification pattern, only waste liquid inlet channel 1, feed tube 2, the 3rd process container 7, filter 8, net
Change mechanism, cut-back tank 12, discharging tube 13, filter residue and collect pipe 15 and the participation running of connecting tube 14；Under organic matter purification pattern,
Second processing container 5 is added on the basis of inorganic matter purification pattern and organic matter decomposition container 6 participates in running；Ether effluent purifying
Under pattern, the first process container 3 is added on the basis of organic matter purification pattern and peroxide decomposition container 4 participates in fortune
Make.
Specifically, shown as shown in Figure 2, Figure 3 and Figure 4, the purification mechanism includes clarifier 10 and spirally around clarifier
10 purification pipe 9, and woven hose 11 of purification pipe 9 lower end provided with insertion clarifier 10 bottom, the upper end side of clarifier 10
Provided with the opening connected for connecting tube 14, to connect clarifier 10 and cut-back tank 12；The full activity of filling in the clarifier 10
Center is provided with the fixing axle 24 along the purification spiral of pipe 9, the fixing axle 24 and is uniformly arranged with ring in charcoal, the purification pipe 9
Shape catch 25, the connected mode between the catch 25 and fixing axle 24 is is slidably connected, and the periphery of catch 25 is fixed with annular filter
Full activated carbon is filled between paper 26, the catch 25, the lower port of purification pipe 9 is provided with sealing plug 27；It is described purification pipe 9 in from
Top to bottm is uniformly divided into three parts, and it is sequentially filled completely big mesoporous activated carbon, transition mesoporous activated carbon and microporous activated carbon.
In the present embodiment, the radius of the big mesoporous activated carbon is 25000nm, and the radius of the transition mesoporous activated carbon is
1000nm, the radius of the microporous activated carbon is 150nm.
Specifically, the peroxide decomposition container 4 is built with the copperas solution that concentration is 5%, the organic matter
Decomposition container 6 is built with aerobic active bacteria all living creatures thing liquid.
Specifically, in the 3rd process container 7 when PH reactions are adjusted, the material of addition is nertralizer；Entering
During the reaction of row generation precipitation, the material of addition is precipitating reagent.
The application content of above-mentioned Full-automatic purification device for chemical experiment waste liquid includes：
1. only contain organic/inorganic substance in experimental waste liquid
(1) slowly waste liquid is poured into from waste liquid inlet channel 1, and selects inorganic matter purification pattern, controller control opens the
Three process containers 7 and the electric valve 16 of the junction of feed tube 2, waste liquid enter the 3rd process container 7, and waste liquid is toppled over after end,
Load onto the supply tank being electrically connected with the controller in the top of waste liquid inlet channel 1；
(2) start PH sensors 23 and PH detections are carried out to waste liquid, if pH value is slowly added to standard not in the range of 6~9
The nertralizer got ready, until up to standard；Controller control adds ready precipitating reagent, stands a period of time；Adding nertralizer
The agitator 22 in the 3rd process container 7 is all started during with precipitating reagent；
(3) it is to be precipitated completely after, open the magnetic valve 18 in connecting tube 14 between the 3rd process container 7 and filter 8, sink
Shallow lake mixed liquor enters filter 8；
(4) magnetic valve 18 between filter 8 and purification mechanism in connecting tube 14 is opened, filtrate passes through the cocurrent of filter 8
Enter purification mechanism, sediment, which is stayed in filter 8, (to be opened filter residue and collect magnetic valve 18 on pipe 15, you can take sediment
Go out)；
(5) filtrate enters from purification pipe 9 upper end, by the adsorption cleaning of three amount of activated charcoals, from the defeated of purification pipe 9 lower end
Liquid pipe enters clarifier 10, opens the magnetic valve 18 in connecting tube 14 between purification mechanism and cut-back tank 12, with input liquid
Body increases, and filtrate is gradually increasing and in uphill process by second adsorption catharsis, is then overflow from clarifier 10 upper end
Connecting tube 14 is flowed into, and flows to cut-back tank 12；After cleaning the phase, supply tank is opened, clear water is accessed at waste liquid inlet channel 1,
Clear water is flowed through along waste liquid to be sequentially passed through and (relevant apparatus is carried out simply cleaning in passing), eventually arrives at clarifier, and and filtrate
Entering cut-back tank 12 together, (remaining in the water in clarifier 10 can be arranged by the way of water service pipe is set in the bottom of clarifier 10
Go out), start the agitator 22 in cut-back tank 12, make clear water and waste liquid filtrate well mixed, and successfully dilute filtrate；
(6) magnetic valve 18 on discharging tube 13 is opened, the waste liquid filtrate after dilution is discharged.
2. contain organic matter in experimental waste liquid
(1) slowly waste liquid is poured into from waste liquid inlet channel 1, and selects organic matter purification pattern, controller control opens the
Two process containers 5 and the electric valve 16 of the junction of feed tube 2, waste liquid enter second processing container 5, and waste liquid is toppled over after end,
Load onto the supply tank being electrically connected with the controller in the top of waste liquid inlet channel 1；
(2) the active flora of the anaerobism in second processing container 5 carries out preliminary exposition to organic matter；
(3) after preliminary exposition terminates, open between second processing container 5 and organic matter decomposition container 6 in connecting tube 14
Magnetic valve 18, waste liquid enters organic matter decomposition container 6, and aerobic active flora therein carries out deep decomposition to organic matter；
(4) decompose after terminating, open the electromagnetism in connecting tube 14 between organic matter decomposition container 6 and the 3rd process container 7
Valve 18, waste liquid enters the 3rd process container 7, afterwards as above-mentioned inorganic matter purification pattern is run.
3. contain ether in experimental waste liquid
(1) slowly waste liquid is poured into from waste liquid inlet channel 1, and selects ether effluent purifying pattern, controller control opens the
One process container 3 and the electric valve 16 of the junction of feed tube 2, waste liquid enter the first process container 3, and waste liquid is toppled over after end,
Load onto the supply tank being electrically connected with the controller in the top of waste liquid inlet channel 1；
Sodium or iron filings in (2) first process containers 3 can prevent the formation of peroxide, and waste liquid flows through starch-kalium iodide
Test paper, starts color sensor 20, if test paper does not show blueness, controller opens the connecting tube 14 towards second processing container 5
On magnetic valve 18；If test paper is aobvious blue (indicating peroxide generation), the company towards peroxide decomposition container 4 is opened
Magnetic valve 18 in adapter 14, waste liquid enters in peroxide decomposition container 4, Vibration on Start-up device 21, peroxide decomposition container 4
Copperas solution peroxide is decomposed, remove peroxide, turn off vibrator 21 and open peroxide point
Magnetic valve 18 and compression pump 19 in connecting tube 14 between container 4 and second processing container 5 are solved, waste liquid flows to second processing container
5；
(3) waste liquid enters second processing container 5, afterwards as above-mentioned organic matter purification pattern is run.
Those of ordinary skill in the art it should be appreciated that the embodiment of the above be intended merely to explanation the present invention,
And be not used as limitation of the invention, as long as in the spirit of the present invention, the change to embodiment described above
Change, modification will all fall in scope of the presently claimed invention.
Claims (5)
1. a kind of Full-automatic purification device for chemical experiment waste liquid, it is characterised in that single including controller, alembic and driving
Member,
The alembic include waste liquid inlet channel (1), feed tube (2), the first process container (3) for being built-in with sodium or iron filings,
Second processing container (5), the 3rd process container (7) for being built-in with precipitating reagent, the peroxide for being built-in with anaerobism active bacteria all living creatures's thing liquid
Compound decomposition container (4), organic matter decomposition container (6), filter (8), purification mechanism, cut-back tank (12) and discharging tube
(13), the input of waste liquid inlet channel (1) the connection feed tube (2), first process container (3), second processing container
(5) it is connected with output end of the 3rd process container (7) respectively with feed tube (2)；First process container (3) output end is equipped with
Starch-kalium iodide test paper (17), the first process container (3) output end is connected at peroxide decomposition container (4) and second respectively
The input of container (5) is managed, and peroxide decomposition container (4) output end is connected with second processing container (5) input；
The organic matter decomposition container (6) connects the input of the output end and the 3rd process container (7) of second processing container (5) respectively
End；3rd process container (7), filter (8), purification mechanism and cut-back tank (12) are sequentially connected, the cut-back tank
(12) output end is connected with discharging tube (13)；Connected between each utensil by connecting tube (14), on the filter (8)
It is also equipped with filter residue and collects pipe (15)；
The driver element includes the electric valve (16) located at feed tube (2) output end and three process container junctions, is located at
Connecting tube (14), discharging tube (13) and filter residue collect the magnetic valve (18) on pipe (15), and the company of output end is less than located at input
The compression pump (19) taken on (14), the vibrator (21) located at peroxide decomposition container (4) bottom holds located at the 3rd processing
Agitator (22) in device (7) and cut-back tank (12), is located at the color sensor of starch-kalium iodide test paper (17)
(20), the PH sensors (23) in the 3rd process container (7), the color sensor (20) and PH sensors (23) connection
The input of controller, the electric valve (16), magnetic valve (18), compression pump (19), vibrator (21) and agitator (22) are even
Connect the output end of controller；
The controller includes three kinds of control models, i.e. ether effluent purifying pattern, organic matter purification pattern and inorganic matter purification mould
Under formula, the inorganic matter purification pattern, only waste liquid inlet channel (1), feed tube (2), the 3rd process container (7), filter
(8), purification mechanism, cut-back tank (12), discharging tube (13), filter residue collect pipe (15) and connecting tube (14) participates in running；It is organic
Under thing purification pattern, second processing container (5) and organic matter decomposition container (6) are added on the basis of inorganic matter purification pattern
Participate in running；Under ether effluent purifying pattern, the first process container (3) and peroxide are added on the basis of organic matter purification pattern
Compound decomposition container (4) participates in running.
2. a kind of Full-automatic purification device for chemical experiment waste liquid according to claim 1, it is characterised in that the clearing machine
Structure includes clarifier (10) and spirally surround the purification pipe (9) of clarifier (10), and purification pipe (9) lower end is provided with insertion purification
The woven hose (11) of device (10) bottom, clarifier (10) the upper end side is provided with the opening for connecting tube (14) connection, with even
Logical clarifier (10) and cut-back tank (12)；The full activated carbon of filling, the interior center of the purification pipe (9) in the clarifier (12)
Provided with the fixing axle (24) along purification pipe (9) spiral, annular catch (25), the gear are uniformly arranged with the fixing axle (24)
Connected mode between piece (25) and fixing axle (24) is is slidably connected, and catch (25) periphery is fixed with annular filter paper (26), institute
The full activated carbon of filling between catch (25) is stated, purification pipe (9) lower port is provided with sealing plug (27)；In the purification pipe (9)
Three parts are uniformly divided into from top to bottom, and it is sequentially filled completely big mesoporous activated carbon, transition mesoporous activated carbon and microporous activated carbon.
3. a kind of Full-automatic purification device for chemical experiment waste liquid according to claim 2, it is characterised in that the macropore is lived
Property charcoal radius be 25000nm, the radius of the transition mesoporous activated carbon is 1000nm, and the radius of the microporous activated carbon is
150nm。
4. a kind of Full-automatic purification device for chemical experiment waste liquid according to claim 1, it is characterised in that the peroxidating
Thing decomposition container (4) is built with the copperas solution that concentration is 5%, and the organic matter decomposition container (6) is built with aerobic work
Property flora biological fluids.
5. a kind of Full-automatic purification device for chemical experiment waste liquid according to claim 1, it is characterised in that at the described 3rd
In reason container (7) when PH reactions are adjusted, the material of addition is nertralizer；When carrying out the reaction of generation precipitation, addition
Material be precipitating reagent.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710655690.8A CN107311399B (en) | 2017-08-03 | 2017-08-03 | Full-automatic purification device for chemical experiment waste liquid |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710655690.8A CN107311399B (en) | 2017-08-03 | 2017-08-03 | Full-automatic purification device for chemical experiment waste liquid |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN107311399A true CN107311399A (en) | 2017-11-03 |
| CN107311399B CN107311399B (en) | 2020-11-06 |
Family
ID=60170063
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710655690.8A Active CN107311399B (en) | 2017-08-03 | 2017-08-03 | Full-automatic purification device for chemical experiment waste liquid |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107311399B (en) |
Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20060016763A1 (en) * | 2004-07-20 | 2006-01-26 | Kerfoot William B | Superoxidant poiser for groundwater and soil treatment with in-situ oxidation-reduction and acidity-basicity adjustment |
| CN102381946A (en) * | 2011-08-09 | 2012-03-21 | 天津市化学试剂研究所 | Preparation method of ether eluent |
| CN103570189A (en) * | 2013-10-15 | 2014-02-12 | 大连北方成套教学设备有限公司 | Full-automatic purification device for chemical experiment waste liquid |
| CN105271561A (en) * | 2014-06-21 | 2016-01-27 | 广东石油化工学院 | Chemical experiment waste liquid processing system |
| CN205061799U (en) * | 2015-09-12 | 2016-03-02 | 王伟珍 | Sewage multilevel processing device |
| DE102014112240A1 (en) * | 2014-08-26 | 2016-03-03 | Ava-Co2 Schweiz Ag | Process for the treatment of process water |
| CN205222900U (en) * | 2015-12-14 | 2016-05-11 | 山东凯盛新材料有限公司 | 2 - chloroethyl propyl ether effluent treatment plant |
| CN105800834A (en) * | 2016-05-10 | 2016-07-27 | 姚旺东 | Chemical laboratory liquid waste treatment device |
| CN106866387A (en) * | 2015-12-11 | 2017-06-20 | 国药集团化学试剂有限公司 | A kind of store method for suppressing hydrogen peroxide generation in high-purity ether |
-
2017
- 2017-08-03 CN CN201710655690.8A patent/CN107311399B/en active Active
Patent Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20060016763A1 (en) * | 2004-07-20 | 2006-01-26 | Kerfoot William B | Superoxidant poiser for groundwater and soil treatment with in-situ oxidation-reduction and acidity-basicity adjustment |
| CN102381946A (en) * | 2011-08-09 | 2012-03-21 | 天津市化学试剂研究所 | Preparation method of ether eluent |
| CN103570189A (en) * | 2013-10-15 | 2014-02-12 | 大连北方成套教学设备有限公司 | Full-automatic purification device for chemical experiment waste liquid |
| CN105271561A (en) * | 2014-06-21 | 2016-01-27 | 广东石油化工学院 | Chemical experiment waste liquid processing system |
| DE102014112240A1 (en) * | 2014-08-26 | 2016-03-03 | Ava-Co2 Schweiz Ag | Process for the treatment of process water |
| CN205061799U (en) * | 2015-09-12 | 2016-03-02 | 王伟珍 | Sewage multilevel processing device |
| CN106866387A (en) * | 2015-12-11 | 2017-06-20 | 国药集团化学试剂有限公司 | A kind of store method for suppressing hydrogen peroxide generation in high-purity ether |
| CN205222900U (en) * | 2015-12-14 | 2016-05-11 | 山东凯盛新材料有限公司 | 2 - chloroethyl propyl ether effluent treatment plant |
| CN105800834A (en) * | 2016-05-10 | 2016-07-27 | 姚旺东 | Chemical laboratory liquid waste treatment device |
Also Published As
| Publication number | Publication date |
|---|---|
| CN107311399B (en) | 2020-11-06 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN206204026U (en) | A kind of new and effective heavy-metal waste water treatment device | |
| CN210287029U (en) | Waste water treatment device for production workshop | |
| CN108709774A (en) | A kind of sampler of multi-stag treatment tank sampling | |
| CN107555672A (en) | A kind of back yard industry sewage treatment equipment | |
| CN106698867A (en) | Textile wastewater treatment system<0} | |
| CN102432121A (en) | Device for separately storing and treating chemical experiment wastewater | |
| CN206228989U (en) | Full automatic high efficiency settling vessel | |
| CN205442895U (en) | Heavy metal waste water treatment equipment | |
| CN210683412U (en) | Sewage treatment plant that intelligence adds medicine | |
| CN107311399A (en) | A kind of Full-automatic purification device for chemical experiment waste liquid | |
| CN104003559A (en) | Integrated water purifying device capable of strengthening pretreatment | |
| CN207159018U (en) | A kind of integrated equipment for eutrophied water treatment | |
| CN215559458U (en) | High-efficient purification treatment system of industrial waste water | |
| CN211035489U (en) | Chemical waste liquid classification recovery processing device | |
| CN209940676U (en) | Water purification device for environmental protection | |
| CN212050968U (en) | Tank wagon cleaning wastewater treatment system | |
| CN208766003U (en) | A kind of multistage sampler for the treatment of tank sampling | |
| CN202542970U (en) | Novel purifying disposer for optically catalyzing and degrading organic wastewater and acid-base waster liquid | |
| CN104229947B (en) | Use wastewater treatment equipment and the method for polynary coal ferrum carbon | |
| CN209052510U (en) | Sewage treatment high-efficient purification equipment | |
| CN2892849Y (en) | Multifunction efficient sewage processing equipment | |
| CN207998515U (en) | A kind of industrial waste water disposal device | |
| CN205398397U (en) | Integrated sewage treatment device | |
| CN111018074A (en) | Treatment method and treatment device for laboratory waste liquid | |
| CN206428099U (en) | Acid-washing waste acid purification recovery device |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| CB03 | Change of inventor or designer information |
Inventor after: Wang Lei Inventor after: Yan Jiaying Inventor after: Liu Qinqin Inventor after: Wang Jianing Inventor before: Wang Jianing |
|
| CB03 | Change of inventor or designer information | ||
| TA01 | Transfer of patent application right |
Effective date of registration: 20200917 Address after: No.329, West Zone, Xiangguang Economic Development Zone, Yanggu County, Liaocheng City, Shandong Province Applicant after: Shandong Hechuang Environmental Protection Technology Co.,Ltd. Address before: 252000 Hunan West Road in Shandong province Liaocheng city Dongchangfu District No. 15 Applicant before: Wang Jianing |
|
| TA01 | Transfer of patent application right | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20210420 Address after: 5 / F, office building, Liaocheng Industrial Technology Research Institute, No.88, Huanghe Road, high tech Zone, Liaocheng City, Shandong Province, 252000 Patentee after: Liaocheng Industry Research Testing Technology Co.,Ltd. Address before: No.329, West Zone, Xiangguang Economic Development Zone, Yanggu County, Liaocheng City, Shandong Province Patentee before: Shandong Hechuang Environmental Protection Technology Co.,Ltd. |
|
| TR01 | Transfer of patent right |