CN107286678A - A kind of resin compounded plastic cement and preparation method thereof - Google Patents
A kind of resin compounded plastic cement and preparation method thereof Download PDFInfo
- Publication number
- CN107286678A CN107286678A CN201710667875.0A CN201710667875A CN107286678A CN 107286678 A CN107286678 A CN 107286678A CN 201710667875 A CN201710667875 A CN 201710667875A CN 107286678 A CN107286678 A CN 107286678A
- Authority
- CN
- China
- Prior art keywords
- oil
- plastic cement
- added
- preparation
- minutes
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L93/00—Compositions of natural resins; Compositions of derivatives thereof
- C08L93/02—Shellac
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L91/00—Compositions of oils, fats or waxes; Compositions of derivatives thereof
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L91/00—Compositions of oils, fats or waxes; Compositions of derivatives thereof
- C08L91/005—Drying oils
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2237—Oxides; Hydroxides of metals of titanium
- C08K2003/2241—Titanium dioxide
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/02—Flame or fire retardant/resistant
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
- C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
A kind of resin compounded plastic cement and preparation method thereof, is made up of the raw material components of following number：Linseed oil 30 50, tung oil 5 10, gum dammar 8 16, rosin glyceride 18 28, orange oil 10 16, turpentine oil 30 45, shellac 30 45, natural plant mill base 8 12, macromolecule filming material 8 10, auxiliary agent 68, deionized water are some, a kind of resin compounded plastic cement that the present invention is provided and preparation method thereof, preparation method is simple, it is easily operated, obtained resin compounded plastic cement intensity is high, anti-bacterial and anti-fouling excellent performance, good flame resistance, manufacturing cost is low, with good market prospects.
Description
Technical field
The present invention relates to plastic cement technical field, and in particular to a kind of resin compounded plastic cement and preparation method thereof.
Background technology
Plastic cement application is indispensable portion in household electrical appliances, automobile, mobile phone, PC, medicine equipment, electric lighting widely
Part.China's economy realizes steady and stabilized growth in recent years, and the industry such as household electrical appliances, automobile, mobile phone, PC, medicine equipment is benefited from
Good external environment condition also achieves fast development, and the development of downstream industry has further pulled on the demand to plastic cement, but and
Foreign Advanced Lerel is compared, and China's synthetic resin industry still suffers from certain gap, and some domestic high-end product quantity can not be met
The market demand, quality also has much room for improvement and improved.The performance deficiency that current plastic cement is present show wearability, ageing-resistant, oil resistant,
, it is necessary to constantly improve in terms of high temperature resistant, intensity, chemical stability, bending strength, croop property.Improved approach has pair
The improvement of raw material, technique, is also exactly to be improved by adding filler, the performance of filler improves plastic cement to a certain extent
Performance, so research filler modified technique it is critically important.
The content of the invention
The technical problem to be solved in the present invention is to provide a kind of resin compounded plastic cement and preparation method thereof.
The present invention is achieved through the following technical solutions：
A kind of resin compounded plastic cement, is made up of the raw material components of following number：Linseed oil 30-50, tung oil 5-10, gum dammar
8-16, rosin glyceride 18-28, orange oil 10-16, turpentine oil 30-45, shellac 30-45, natural plant mill base 8-12, height
Molecular film-forming material 8-10, auxiliary agent 6-8, deionized water are some.
The auxiliary agent is made up of the raw material of following weight：Magnesium stearate 0.2-0.3, di-n-octyl sebacate 0.2-0.3, ethylene
Double oleamide 0.4-0.6, OPE 0.3-0.5, tall oil 0.3-0.4, graphene oxide 0.3-0.5, lanolin
Alcohol APEO 0.2-0.3, nano titanium oxide 2-3, polyamide wax micropowder 0.2-0.3, urethane acrylate 0.3-
0.5th, allyl glycidyl ether 0.2-0.3, toluene di-isocyanate(TDI) 0.1-0.2, phosphoesterase 30 .2-0.3, tripropylene glycol
Diacrylate 13-16；Preparation method is：Urethane acrylate, allyl glycidyl ether are added to two contractings 3 the third two
In alcohol diacrylate, 50-55 DEG C is heated to, is stirred 20-30 minutes, the double oil of magnesium stearate, di-n-octyl sebacate, ethylene are added
Sour acid amides, OPE, tall oil, graphene oxide, lanolin alcohol APEO, nano titanium oxide, polyamide
Wax micro mist, phosphate, are continuously heating to 70-80 DEG C after stirring, stirring reaction 30-40 minutes, are cooled to 35-40 DEG C, then
Other residual components are added, stirring reaction 50-60 minutes is produced.
The preparation method of described resin compounded plastic cement, it is characterised in that comprise the following steps：
(1) linseed oil, tung oil, gum dammar, rosin glyceride, orange oil, turpentine oil are added in deionized water, filled
Divide and stir, be heated to 75-85 DEG C, obtain slurry；
(2) shellac, natural plant mill base, macromolecule filming material are mixed, then makes it to its hot-air for blowing 75-85 DEG C
Seethe, then the slurry that vaporific (1) step is obtained is sprayed into the powder seethed, make after the two is sufficiently mixed, keeping temperature is
75-85 DEG C, continue to seethe 40-50 minutes；
(3) mixed material for obtaining (2) step is dried, and is added in high-speed kneading machine, is added other residual components, then rise
Temperature is to 120-130 DEG C, and insulation is mediated 15-20 minutes, then grinds to form 10-50 μm of particle, produces this product.
The beneficial effects of the present invention are：A kind of resin compounded plastic cement proposed by the present invention, preparation method is simple, it is easy to grasp
Make, obtained resin compounded plastic cement intensity is high, anti-bacterial and anti-fouling excellent performance, good flame resistance, manufacturing cost is low, with good city
Field prospect.
Embodiment
Embodiment:A kind of resin compounded plastic cement, is made up of the raw material components of following number：Linseed oil 30-50, tung oil 5-10,
Gum dammar 8-16, rosin glyceride 18-28, orange oil 10-16, turpentine oil 30-45, shellac 30-45, natural plant mill base
8-12, macromolecule filming material 8-10, auxiliary agent 6-8, deionized water are some.
The auxiliary agent is made up of the raw material of following weight：Magnesium stearate 0.2-0.3, di-n-octyl sebacate 0.2-0.3, ethylene
Double oleamide 0.4-0.6, OPE 0.3-0.5, tall oil 0.3-0.4, graphene oxide 0.3-0.5, lanolin
Alcohol APEO 0.2-0.3, nano titanium oxide 2-3, polyamide wax micropowder 0.2-0.3, urethane acrylate 0.3-
0.5th, allyl glycidyl ether 0.2-0.3, toluene di-isocyanate(TDI) 0.1-0.2, phosphoesterase 30 .2-0.3, tripropylene glycol
Diacrylate 13-16；Preparation method is：Urethane acrylate, allyl glycidyl ether are added to two contractings 3 the third two
In alcohol diacrylate, 50-55 DEG C is heated to, is stirred 20-30 minutes, the double oil of magnesium stearate, di-n-octyl sebacate, ethylene are added
Sour acid amides, OPE, tall oil, graphene oxide, lanolin alcohol APEO, nano titanium oxide, polyamide
Wax micro mist, phosphate, are continuously heating to 70-80 DEG C after stirring, stirring reaction 30-40 minutes, are cooled to 35-40 DEG C, then
Other residual components are added, stirring reaction 50-60 minutes is produced.
The preparation method of described resin compounded plastic cement, it is characterised in that comprise the following steps：
(1) linseed oil, tung oil, gum dammar, rosin glyceride, orange oil, turpentine oil are added in deionized water, filled
Divide and stir, be heated to 75-85 DEG C, obtain slurry；
(2) shellac, natural plant mill base, macromolecule filming material are mixed, then makes it to its hot-air for blowing 75-85 DEG C
Seethe, then the slurry that vaporific (1) step is obtained is sprayed into the powder seethed, make after the two is sufficiently mixed, keeping temperature is
75-85 DEG C, continue to seethe 40-50 minutes；
(3) mixed material for obtaining (2) step is dried, and is added in high-speed kneading machine, is added other residual components, then rise
Temperature is to 120-130 DEG C, and insulation is mediated 15-20 minutes, then grinds to form 10-50 μm of particle, produces this product.
Described above is only the preferred application implementation mode of the present invention, it is noted that for the common skill of the art
For art personnel, without departing from the technical principles of the invention, some improvement can also be made.
Claims (2)
1. a kind of resin compounded plastic cement, it is characterised in that：It is made up of the raw material components of following number：Linseed oil 30-50, tung oil 5-
10th, gum dammar 8-16, rosin glyceride 18-28, orange oil 10-16, turpentine oil 30-45, shellac 30-45, natural plant
Mill base 8-12, macromolecule filming material 8-10, auxiliary agent 6-8, deionized water are some.
The auxiliary agent is made up of the raw material of following weight：The double oil of magnesium stearate 0.2-0.3, di-n-octyl sebacate 0.2-0.3, ethylene
Sour acid amides 0.4-0.6, OPE 0.3-0.5, tall oil 0.3-0.4, graphene oxide 0.3-0.5, lanolin alcohol gather
Oxygen vinethene 0.2-0.3, nano titanium oxide 2-3, polyamide wax micropowder 0.2-0.3, urethane acrylate 0.3-0.5, alkene
Propyl glycidyl ether 0.2-0.3, toluene di-isocyanate(TDI) 0.1-0.2, phosphoesterase 30 .2-0.3, the propylene of tripropylene glycol two
Acid esters 13-16；Preparation method is：Urethane acrylate, allyl glycidyl ether are added to tripropylene glycol dipropyl
In olefin(e) acid ester, 50-55 DEG C is heated to, is stirred 20-30 minutes, the double oleic acid acyls of magnesium stearate, di-n-octyl sebacate, ethylene are added
Amine, OPE, tall oil, graphene oxide, lanolin alcohol APEO, nano titanium oxide, polyamide wax are micro-
Powder, phosphate, are continuously heating to 70-80 DEG C, stirring reaction 30-40 minutes is cooled to 35-40 DEG C, added after stirring
Other residual components, stirring reaction 50-60 minutes, are produced.
2. the preparation method of resin compounded plastic cement according to claim 1, it is characterised in that comprise the following steps：
(1) linseed oil, tung oil, gum dammar, rosin glyceride, orange oil, turpentine oil are added in deionized water, fully stirred
Mix uniform, be heated to 75-85 DEG C, obtain slurry；
(2) shellac, natural plant mill base, macromolecule filming material are mixed, then it is turned over to its hot-air for blowing 75-85 DEG C
Rise, then the slurry that vaporific (1) step is obtained is sprayed into the powder seethed, make after the two is sufficiently mixed, keeping temperature is 75-
85 DEG C, continue to seethe 40-50 minutes；
(3) mixed material for obtaining (2) step is dried, and is added in high-speed kneading machine, is added other residual components, then be warming up to
120-130 DEG C, insulation is mediated 15-20 minutes, then grinds to form 10-50 μm of particle, produces this product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710667875.0A CN107286678A (en) | 2017-08-07 | 2017-08-07 | A kind of resin compounded plastic cement and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710667875.0A CN107286678A (en) | 2017-08-07 | 2017-08-07 | A kind of resin compounded plastic cement and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107286678A true CN107286678A (en) | 2017-10-24 |
Family
ID=60104489
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710667875.0A Pending CN107286678A (en) | 2017-08-07 | 2017-08-07 | A kind of resin compounded plastic cement and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107286678A (en) |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1318574A (en) * | 2001-05-28 | 2001-10-24 | 方忠熙 | Modified natural resin |
| CN102634072A (en) * | 2012-04-20 | 2012-08-15 | 桂中宇 | Degradable thermoplastic rubber membrane using agricultural plant resources as main material and preparation method of degradable thermoplastic rubber membrane |
| CN104987565A (en) * | 2015-06-13 | 2015-10-21 | 合肥和安机械制造有限公司 | High-compression-resistance soil composite resin hose |
-
2017
- 2017-08-07 CN CN201710667875.0A patent/CN107286678A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1318574A (en) * | 2001-05-28 | 2001-10-24 | 方忠熙 | Modified natural resin |
| CN102634072A (en) * | 2012-04-20 | 2012-08-15 | 桂中宇 | Degradable thermoplastic rubber membrane using agricultural plant resources as main material and preparation method of degradable thermoplastic rubber membrane |
| CN104987565A (en) * | 2015-06-13 | 2015-10-21 | 合肥和安机械制造有限公司 | High-compression-resistance soil composite resin hose |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN104211995A (en) | Anticorrosive plastic filler and preparation method thereof | |
| CN104592742A (en) | Special filler for modified light calcium carbonate plastic and preparation method for special filler | |
| CN103917597A (en) | Resin composition for optical semiconductor sealing material | |
| CN104592551A (en) | Filler capable of enhancing low-temperature resistance of plastic and preparation method thereof | |
| CN108948795A (en) | Surface modification method of special flame-retardant heavy calcium carbonate for wires and cables | |
| CN104194309A (en) | Plastic filler with high wear resistance and preparation method of plastic filler | |
| CN104311961A (en) | Fiber enhanced nozzle | |
| CN104592720A (en) | Calcium carbonate filler capable of enhancing toughness of plastic and preparation method thereof | |
| CN106433067B (en) | A kind of formula and preparation method thereof of environment-friendly type PC/ABS alloy materials | |
| CN104194058A (en) | Flame-retardant plastic packing and preparation method thereof | |
| CN106065302A (en) | A kind of compunication power distribution cabinet installation fluid sealant | |
| CN104194057A (en) | Heat-resistant filler for plastics and preparation method of heat-resistant filler | |
| CN113912824A (en) | Modified epoxy acrylate prepolymer, photo-thermal dual-curing conductive adhesive and preparation method thereof | |
| CN107286678A (en) | A kind of resin compounded plastic cement and preparation method thereof | |
| CN104449025A (en) | Method for producing oil paint | |
| CN105906840A (en) | Filler for reinforcing low temperature resistance of plastic products and preparation method of filler | |
| CN109913080A (en) | A kind of novel solvent-free electrostatic conductive anticorrosion paint | |
| CN107474459A (en) | A kind of corrosion-resisting resin copolymer synthetic plastic filler and preparation method thereof | |
| CN105368251B (en) | A kind of extra-high voltage coatings and preparation method thereof | |
| CN105304255A (en) | Neodymium iron boron magnetic material with high magnetic energy and preparation method thereof | |
| CN104211990A (en) | Special filler for anti-agglomeration plastics, and preparation method thereof | |
| CN109880293A (en) | Toughened epoxy resin and preparation method thereof | |
| CN109777248A (en) | A kind of water-base epoxy anti-corrosion primer | |
| CN106752894A (en) | A kind of preparation method of self-lubricating polyamide acid imide enamelled wire paint | |
| CN106832353B (en) | A method of solving dust pollution when pearlescent pigment is coloured for ABS |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WD01 | Invention patent application deemed withdrawn after publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20171024 |