CN107274326A - Detection and supervision message management system framework and the method for programming - Google Patents

Detection and supervision message management system framework and the method for programming Download PDF

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CN107274326A
CN107274326A CN201710645811.0A CN201710645811A CN107274326A CN 107274326 A CN107274326 A CN 107274326A CN 201710645811 A CN201710645811 A CN 201710645811A CN 107274326 A CN107274326 A CN 107274326A
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information
code
management system
product
equipment
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李振国
李大治
郑子栋
李思思
郭毅
周继春
高艺歌
柳桃
胡萌萌
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Abstract

The present invention relates to conducting food, medicine, cosmetics, health products, veterinary drug, agricultural chemicals, chemical fertilizer, when the information management system framework of the analysis testing laboratory (analysis testing agency) of chemical reagent and environmental protection tests sample and programming, propose the package solution of succinct and standardization an information management system framework and programming, the key element of this package solution is the standardization and the standardization of information data structure of physics (hardware) environment architecture for the information management system for analyzing testing agency and supervision and administration organization, it is a physical structure and the effective solution of programming that can apply to the information management system that government supervision and analysis testing agency initial data are traced to the source.

Description

Detection and supervision message management system framework and the method for programming
Technical field
The present invention relates to conducting food, medicine, cosmetics, health products, veterinary drug, agricultural chemicals, chemical fertilizer, chemical reagent and environmental protection When detecting information management system framework and the programming of the analysis testing laboratory (analysis testing agency) of sample, one is proposed Succinct and standardization information management system framework and the package solution of programming, this package solution Key element is the standard of physics (hardware) environment architecture for the information management system for analyzing testing agency and supervision and administration organization Change the standardization with information data structure.The number of analysis testing agency can be effectively improved using this package solution The ability traced to the source according to shared and increase analysis detection initial data, and make detection information and the supervision and management portion of analysis testing agency The supervision message fusion of door is with sharing, and it is directly supervision and management service to make analysis detecting data, while also making analysis testing agency Initial data be directly under the real-time monitoring of supervisory and management department, prevent analyze testing agency data fabrication.This letter It is real that breath management system framework and information data structure standardized solution can be widely suitable for Food Safety Analysis detection Test room, medicine, cosmetics, veterinary drug, agricultural chemicals, Fertilizer Analysis testing laboratory, Environmental Monitoring Laboratory, land resources detection, change A variety of research laboratories and government administration to analyze, be detected as main activities such as chemical product, environmental protection testing laboratory Superintendent office is in the information management system framework and programming of the supervision and management for analyzing testing laboratory, being one can answer Information management system (the Administrative and traced to the source for government supervision and analysis testing agency initial data Laboratory Information Management System, A&LIMS) physical structure and programming effective solution Certainly scheme.
Background technology
The technical merit and popularity for analyzing detection are the important indicators of a national science and technology level.Current China's economic High speed development state is still within, in each economic field, has strong demand to analysis detection.Yet with China's analysis The level of detection technique is uneven, and popularity is poor, largely governs the balanced development of China's economic, even It is the bottleneck problem for fettering economic development in some fields.For this problem, the central government is being increased to state-run analysis detection While laboratory is invested, the dynamics that guiding social funds establish third-party analysis testing laboratory is also increased.In this back of the body The third party laboratory of different scales is set up one after another under scape, especially in environmental monitoring and food safety monitoring field, is come from The third party laboratory of non-governmental capital investment occurs one after another as emerged rapidly in large numbersBamboo shoots after a spring rain, but also occurs in that some problems simultaneously.
Between in the past few decades, the analysis testing laboratory of China is mainly National Laboratory for main body, third party point Analysis testing laboratory almost seldom occurs.In the case where current third party analyzes the situation that testing laboratory largely arises at the historic moment, quickly The third party laboratory of development there are problems that a series of due to lacking good supervision, according to literature search, be summed up Mainly there is the following aspects:(1) legal consciousness of analysis testing agency has much room for improvement;(2) analysis testing agency is not set up The supervisory system of Sincere Service;(3) inspection examining report, the original record of analysis testing agency are lack of standardization;(4) detection machine is analyzed Specification is owed in checkout facility environmental condition and the testing equipment management of structure;(5) examination criteria management is not in place, and standard alternation procedure is done Reason is not in time;(6) internal check of analysis testing agency lacks depth, management review and become a mere formality;(7) in analysis testing agency Portion's supervision work does not play due effect;(8) the deficient validity is verified during the testing equipment of analysis testing agency;(9) sample QC reason also needs further specification;(10) analysis testing agency fails effectively to be placed in the message tube of laboratory supervisory and management department Under reason, cause the public letter degree for analyzing testing laboratory universal not high, especially in enterprises and non-public third party It is especially prominent the problem of social public credibility in laboratory;(11) the test in laboratory data of analysis testing agency fail to supervise for government Superintend and direct department directly to use, be still to continue to use the method that collect statistics report to pass between government supervision department and analysis testing agency Testing result is sent, etc..
In terms of the problem of existing from these, the factor of generation comes from many aspects, and effective solution is nothing but Come from the supervision and internal management of outside.Outside supervision be functional government departments should foreign developed country elder generation Enter experience, and be in for China's analysis testing laboratory's under-capitalization, overall technology low SI, the total quality of practitioner Present situation to be hoisted, takes the effective method geared to actual circumstances to strengthen the supervision to third party laboratory.And in analysis detection The inside of mechanism, then need the further inside self-discipline management for strengthening laboratory, overcome by effective management system on State the problems of presence.And by means of under the fast-developing and widely available overall situation of current information network technology, designing structure Build good analysis testing laboratory's information management system and its information management system with the supervision of government is organic Blend together, by analyze testing laboratory experimental activity and resulting initial data be placed in government supervision it Under, the detection data obtained can be called directly by regulator, government supervision mechanism utilizes and analyzes testing agency Detection data can effectively lift the technical merit of supervision, and this is clearly the effective of the social public credibility of lifting analysis testing agency Means.
Current is the approval procedure to lab analysis detectability to the mode that analysis testing agency is managed.At present Basic foundation to laboratory certification is that the whole world is generally acknowledged《The General Requirement of testing and calibration laboratories ability》Standard, its is newest Version be in May, 2015 issue, ISO/IEC17025:2005-5-15-《The general of testing and calibration laboratories ability will Ask》Standard, abbreviation ISO/IEC17025.《The General Requirement of testing and calibration laboratories ability》The essence of standard is to propose to recognize The basic skills of setting analysis testing laboratory real work ability, this is also to analyze the behavior method that testing laboratory must comply with Then.Analysis testing laboratory is being followed according in law of honor operation as defined in ISO/IEC17025, by means of LIMS It is very important means that (Laboratory Information Management System), which carries out comprehensive management, current It is that can analysis testing laboratory by country or International Laboratory certification the situation that informationization technology has been popularized comprehensively under Important content.
There are many commercial LIMS softwares to be applied to different analysis testing laboratories at present, play important Effect, wherein it is all very outstanding LIMS products to be no lack of a lot, but wherein there is also it is unsatisfactory the problem of, for example: (1) activity and analysis detecting data of analyzing testing laboratory effectively can not be placed in laboratory supervisory and management department in real time Under supervision;(2) analysis testing agency can not be with government's regulation department pair to examining the data structure of the information gathering of product Both the information data structure of supervised entities' collection and the information data structure of supervision product are consistent, or even in the supervision of government Also generally fail to accomplish the information data structure two by the information data structure of supervised entities and supervision product inside administrative department Person is consistent, and this is not only the definition for reducing information management, adds the complexity of information management system programming, Also difficulty is added to realizing that information data is shared.(3) information management of some commercially available preferable analysis testing laboratories at present The information of system (LIMS products) such as LIMS products of the very expensive import of some prices and analysis testing equipment (instrument) is led to News and management are concentrated mainly on large-scale analysis and detecting instrument, and large-scale analysis and detecting instrument is referred to as some are expensive " network edition work station " class LIMS products or the LIMS products etc. that are changed by this kind of product, not only can to oneself Analytical instrument product is controlled and information exchange management, same alanysis detector that can also be with extremely a small amount of other brands Device is controlled to be managed with information exchange, but have ignored numerous to those in analysis testing laboratory with analyzing detection knot The information exchange management that really closely related basic type equipment and Conventional compact are equipped, and these bases, using frequently small Exactly component analysis detects original number to the information (collection and memory of equipment operation information) of the running status of type experimental assembly According to important component, be just difficult to without them referred to as analysis testing laboratory initial data trace to the source because these count According to being the key factor that is directly connected to analysis detecting data authenticity and correctness.Product also much also titled with LIMS, Substantially do not possess and control and information exchange function are adopted to analysis testing equipment, some so-called initial data are substantially built upon people The level of work typing, has simply done some phases for belonging to management system in the testing process of product and signing and issuing for report in examination & verification Software is answered, its core is still the interactive information management of file category information, this software architecture sheet with OA (office automation) Matter is different without what, such as the pure files classes letter such as financial software, storehouse accounting management software, human resource information management software The interactive information management of breath is the same, in the software architecture system for inherently belonging to OA of software architecture.Therefore above-mentioned two class LIMS products can only small part or the initial data that does not possess laboratory trace to the source ability;(4) due to lacking technological layer Comprehensive Designing, also can not just realize high-level information standardization design, result in numerous analysis testing agencies and supervision is managed The information management software that reason mechanism is designed using different software mechanism, the poor compatibility of different information management softwares each other, Its result implements supervision to information sharing and effectively and produces obstacle;(5) basic reason for producing above mentioned problem is under at this stage The Essential Environment and basic hardware condition difference of numerous analysis testing laboratory of China are very big, and analyze the number of testing equipment The level of wordization control is uneven, and the overwhelming majority belongs to low-level state.And an analysis testing laboratory well Information management system is in addition to needing to be adapted to the supervision and management of Industry system specification, and very big dependence is own analysis detection The hardware condition and digitlization application level of laboratory internal, the information gathering that for example environmental Kuznets Curves are equipped and record (temperature, The numerical value of humidity, the wind speed of purge outlet, dust particle, indoor negative pressure, intensity of illumination etc.) and control information collection with Record the digitlization of (blower fan, compressor, heater, humidifier, UPS uninterrupted power sources, electric current, frequency, run time etc.) etc. Controlling extent.Analyze information management system (LIMS) and intendant of the Digital Control to laboratory of testing laboratory's hardware Effective supervision of the structure to laboratory behavior in analysis testing agency produces conclusive effect.
The present invention be patent application 201610438244.7,201620585833.3,201620585835.2, 201620600747.5 technology continues, and the design method that basic equipment analyzes testing laboratory has been stated in patent application, these Patent application is actually to disclose a kind of analysis detection basic equipment laboratory building mould that can be produced in batches in factory Block, customer can buy these basic equipment analysis testing laboratory's building blocks produced in factory just can be according to oneself The need for quickly build out required analysis testing laboratory.Because basic equipment analysis testing laboratory's building block is Uniting, the building block of unified production, the basic equipment (basis needed in environmental Kuznets Curves equipment, analysis detection therein Equipment, such as refrigeration equipment, heating equipment, constant temperature equipment, microculture equipment, microbial protection equipment) it can facilitate The design of digital control system being standardized, therefore by these basic equipments analysis testing laboratory's building block combine The hardware environment of various analysis testing laboratories will have uniformity largely, thus construct relative normalized Laboratory hardware environment.This standardization, digitized analysis testing laboratory hardware environment are clearly advantageous to data structure LIMS programmings after standardized designs, therefore the present invention is the continuation invention associated with above-mentioned patent application.
Inventors believe that, the information management system of an excellent analysis testing agency should be DCS (collecting and distributing control systems Unite Distributed Control System) combination with OA (office automation Office Automation).At present With the progress of science and technology, society is being rapidly introduced into the intelligent stage.For current existing technology, for dividing The DCS technologies of testing laboratory are analysed either in the arithmetic speed of chip or are all tended on the framework of substrate program module Maturation, can meet technical need of the present analysis testing laboratory to DCS completely.Simple OA technologies also compare into It is ripe, but the DCS in analysis testing laboratory's field of information management lacks corresponding hardware and software framework with OA combination, The programming personnel of the technical staff being especially the absence of in the object and professional domain of the direct management and control of DCS and DCS and OA build jointly The hardware physical structure for the LIMS that DCS and OA is organically combined.
The present invention be on the basis of analysis that above-mentioned patent application is stated detection basic equipment laboratory building module, It is addressed further under analyzing the hardware and software framework of the information management system of testing agency, specification analysis testing laboratory's information data Structure composition, make its generalization, standardization, and should also take into account with Chinese administrative organizations at different levels to analysis testing laboratory The technical supervision technical management means constantly put into effect of management and specification match, provided to analysis testing agency and regulator One is conducive to building the information management hardware and software framework that both supervisory organ's information management and laboratory calibration are blended The solution of design.
The content of the invention
The first technology essential factor of the present invention is to be analyzed at one in testing agency, will analyze the Global Information pipe of testing agency Reason system is divided into two parts, a part be laboratory information system (laboratory information system, LIS), its basic function is to be absorbed in each analysis detection business section office in analysis testing agency, administration and logistics management section office Work management information, coordination, supervise and examine check the information of each business section office in each analysis testing agency, run phase with testing agency The information of pass, data and analysis detecting data collect, collected, and the thus large data center of component analysis testing agency, The information management system can gather by supervision counterpart or examine the company information of product counterpart, product information, product satellite The information management system of supervisory organ can also be transplanted to after the information of position;Another part is Laboratory Operation System (laboratory Operation system, LOS), its basic function is that each is independent real in absorbed analysis testing agency Test the management of the digitizing equipment in space (or referred to as laboratory room) and the initial data related to analysis detection operation Collection and test data sheet.So-called independent experiment space is defined as what is only managed with a set of Laboratory Operation System (LOS) Physical space, this physical space can be a room, or an analysis detection basic equipment laboratory building module, also may be used Be multiple rooms or multiple analyses detection basic equipment laboratory building module.
The second technology essential factor of the present invention is that laboratory information system (LIS) is by information management system, analysis detection machine Structure information processing centre database, sampling (supervision) personnel motion trail satellite positioning information management system, product satellite fix Information management system, client terminal A and satellite positioning information receiving/emitter are collectively constituted, as shown in Figure 1.In this hair Technical characterstic in bright described laboratory information system (LIS) is the increase in sampling (supervision) personnel motion trail satellite fix Information management system and product global position system.The product refer to food, medicine, health products, cosmetics, veterinary drug, agricultural chemicals, Chemical fertilizer and environment supervise taken detection sample etc..(abbreviation satellite fix is filled the satellite positioning information receiving/emitter Put) refer to utilize GPS (global navigation satellite system) or Big Dipper global navigation satellite system, using by control chip (embedded main control chip, for controlling other hardware and running corresponding embedded software), worldwide navigation positioning system (GPS) Or Beidou satellite navigation and positioning system locating module (GPS or Beidou satellite navigation position data collecting can be achieved), GPRS module (data communication can be achieved, for software program in general wireless packet service system General Packet Radio System With the information communication between satellite positioning information management system), humiture induction module (humiture data acquisition) for it is main into Divide the miniature electric geo-location mark of constituted software and hardware system, be affixed in the packaging of product, it is real with the present invention One of dispatching from the factory to the product stream between consumer in product of the product satellite positioning information management system tested in the information system of room Logical link flows through implementation satellite navigation locating and tracking information gathering to product.Particularly (especially cold chain is needed to transport food Defeated chilled food), medicine (biological agent for especially needing cold chain), can effectively obtain these products circulation The geo-location and humiture information of link, and Database Systems are written into, form complete products in circulation message sense.Management Personnel can very easily laboratory information system (LIS) client terminal A tracking and supervising products circulation situation, be ensure Products in circulation link quality, prevents the effective means of fake products.Satellite navigation and location system locating module is matched in sample Collection or enforcer of administration, can effectively understand the movement track of sample collection and administrative law enforcement at work, have very much The scheduling layout with front staff and the management of corresponding accident beneficial to back-stage management personnel.Personnel's satellite fix can Realized with the satellite positioning functions simply using mobile phone, but drawback, which is mobile phone, belongs to personal objects, is directly positioned with mobile phone It is accused of exposing individual privacy, and lacks in information management system corresponding management system.Determined using the satellite navigation of work Position system locating module, is operationally worn, the non-working time is placed on Administrative Area, does not influence individual privacy, and valency Lattice will be less than the price of mobile phone far away.Another feature of laboratory information system (LIS) is by network and extraneous letter Breath communication, thus be that very important, basic way is the excellent fire wall skill of selection safely with extraneous network communication system Art ensures the safety of itself.The application of information network security technology in the present invention is the usual way in professional domain, this Invention book is just repeated no more.
The difficulty that satellite positioning information receiving/emitter faces at present is power issue, because being used as product thing The locating and tracking of link is flowed, satellite positioning information receiving/emitter is to need to consume the electricity provided by rechargeable battery Can, and the electric energy guarantee of rechargeable battery has the time limit.Solution is to make satellite positioning information receiving/transmitting dress The chip and electronic device of low-power consumption are selected when putting as far as possible and the chargeable of high power capacity is selected as far as possible under volume license Battery.Believe the progress with the Low-power Technology of electronic chip and the high density high-energy technology of rechargeable battery, satellite The volume of position information receiving/emitter can be less and less, battery cruising ability can increasingly be grown, price can be more and more lower, with Meet the product orientation tracking of more inner wrapping lower longer time.Instantly solution be satellite positioning information is received first/ Emitter is applied to the product stream locating and tracking of larger packaging even vehicle or whole counter, the middle bag of such as product Freezing and refrigeration transport case of dress, the van cooler of cold chain transportation, vaccine, strain and biological agent etc..With present chip and electricity Pool technology, the cruising time for meeting two weeks is the technology generally used, therefore is that can meet most products in circulation The locating and tracking of link.Satellite positioning information receiving/emitter is not expendable consumed product, after product transports destination to It can reclaim, therefore not only can provide means for administrative supervision mechanism, can also be as the production of product, wholesale enterprise in production The track and localization of the product field of circulation is used, and thus so supervision is combined with production can just construct product in intermediate links Quality assurance net.Satellite positioning module for sampling with supervisor can use the product solution electric energy of charger baby class to ask Topic.
There are one-dimension code, Quick Response Code and RFID (electronic tag) technology in the geolocation application field of product at present GPS location function is realized to product indirectly.One-dimension code, Quick Response Code must read data message, RFID by means of scanning machine Data message must be read by means of ETC card reader (RFID reader).They pass through the data message of reading Network transmission is to central information management system.Because the geographical position of scanning machine or ETC card reader is managed in central information Identified in system, so after can just reading these in the terminal of central information management system by scanning machine or ETC scannings The product for posting one-dimension code, Quick Response Code or electronic tag geographical location information.Due to using by reading one-dimension code, two dimension Code or electronic tag are come geographical position cloth in advance that the premise that obtains the geo-localisation information of product is scanning machine or ETC card reader Office, so the mode of this acquisition product geographical location information can be referred to as " passive product orientation " pattern by us.Passively The shortcoming of product orientation pattern is just to turn into what product orientation was tracked for the region without layout scanning machine or ETC card reader Blind spot, this is clearly that cannot ensure the supervision to track after product export.But one-dimension code and the advantage of Quick Response Code and RFID are Cheap, the price of especially one-dimension code and Quick Response Code is the price of paper, almost nil.The present invention recommend product orientation with Satellite positioning information receiving/emitter that track field is used belongs to " active product orientation " pattern, there's almost no product and determines Position dead angle, so can almost realize tracking all standing of the product in intermediate links.But a disadvantage is that the supply of price, electric energy is current It cannot also be used for as electronic tag and one-dimension code, Quick Response Code on the minimum package of product, and may be only available for product In or the packaging of FCL on.And be combined Quick Response Code with satellite positioning information receiving/emitter proposed by the present invention, will It is a perfect product orientation tracking scheme.Quick Response Code (also including one-dimension code, first-elected Quick Response Code) is namely attached to product All packagings on, then satellite positioning information receiving/emitter will be increased on the packing case of product, and in product satellite fix Also the information management content of Quick Response Code is increased in information management system, it is possible to by " active " and " passive " two kinds of product orientation work( It can organically combine.Therefore the technology essential factor of " product satellite positioning information management system " described in the present inventor is to contain Quick Response Code Information management manages the double technique that two technologies are combined together with satellite positioning information.
The 3rd technology essential factor of the present invention is Laboratory Operation System (laboratory Operation system, LOS) It is by digital (data) collection and equipment management system, experiment information database and experimental implementation management system, equipment control Terminal B, experimental implementation terminal C and incidental active equipment are collectively constituted, as shown in Figure 2.As seen from the figure, laboratory operation System (LOS) can be defined as " the front-end information data processing list in a minimum space region in analysis testing agency Member ".In fig. 2, active equipment refers to the equipment and sensor unit for needing to consume power supply at work.Digital (data) collection It is the status information and data message for gathering active equipment, terminal B manages active equipment by equipment management system, and to it Associative operation is carried out, experimental implementation terminal C carries out instruction interaction by experimental implementation management system and active equipment, and then operates Equipment.Analysis detection testing crew can pass through the equipment management terminal B in Laboratory Operation System (LOS) or operation terminal C Read the status information of active equipment, and in good time with active equipment interactive instruction, complete experiment information processing, for example, manipulate active Operation information, record test data and the Test Information of active equipment are equipped, recorded, experimental analysis report, record experiment is formed Consumptive material and primary evaluation is carried out to test operation, etc..The active equipment refers to that environmental Kuznets Curves equipment is (including air-conditioning system, net Change air-conditioning system, detection of particulates system, ventilating system, illuminator, harmful gas detection system, anti-explosion fire fire-fighting system Deng), intelligentized power outlet and distribution box (cabinet), various conventional analytical instruments (including various photometers and optics, spectral class Equipment, chromatogram class equipment, mass spectrum kind equipment, Electrochemical Detection class equipment, dissolution and disintegration tester, balance and assay balance class dress Standby, incubator class is equipped, sterilizes class equipment, heating and dried class equipment, Biohazard Safety Equipment and superclean bench class are equipped, various Refrigeration equipment, centrifugation vibration class are equipped, crushed and emulsification homogenate class equipment, ultrasound class equipment, autoclave sterilization equipment, pumping of supplying gas Equipment, etc.) various environmental Kuznets Curves equipment, the ups powers analyzed detection auxiliary equipments and instrument, be detected inspection product deposit position (group containing silicon photocell generates electricity and wind power generation management system), recording camera class equipment (for example analyze by image automatic identification Equipment) etc., this is actually a typical one-level DCS system.
The 4th technology essential factor of the present invention is that a laboratory information system (LIS) operates system with several independent laboratories The overall information system hardware physical structure for the analysis testing agency that system (LOS) is collectively formed is as shown in Figure 3.This is actually Be built jointly with multiple LOS by core of a LIS can effectively realize that analysis testing agency initial data is traced to the source LIMS, the present inventor is referred to as LIS+LOS frameworks, has significant two-stage DCS special in this framework Levy.In this system architecture, according to the concrete function system of required access, A, B, C three basic forms of it client terminal are defined, Client terminal A Terminal Types belong to the hardware physical structure of laboratory information system (LIS), for providing the user and integrated information The man-machine information interaction of management system;B Terminal Types are the systems for the hardware physical structure for being under the jurisdiction of Laboratory Operation System (LOS) Man machine operation interface, direct management equipment;C Terminal Types are the hardware physical structures for belonging to Laboratory Operation System (LOS), are used for Provide the user the man-machine information interaction with experimental implementation management system.Actually C terminals together constitute analysis inspection with B terminals Survey in-house one minimum front-end information data processing unit.Thus avoid and crowd is directly managed by Center For Information Management The complexity of management program required for more active equipment, is conducive to analyzing the information management inside testing agency, is also beneficial to The information interchange outside testing agency is analyzed, this is actually a kind of modular information management hardware physical structure in front end, The information management of front end can be carried out as needed it is modular supporting, it is changeable, very convenient information management system with The docking of user's request, the quantities of docking is small, is advantageous for being greatly lowered the cost of information system, is conducive to cheap popularization Using.
In the information management system of this analysis testing agency, the analysis testing agency of laboratory information system (LIS) It is public that information processing centre database recommends the Orcale databases of Oracle, the Sql databases of Microsoft, IBM The database of the dBase databases price of department costly, but the database of Laboratory Operation System (LOS) is recommended Database this kind of free or cheap mysql, if having sufficient funds certainly or having higher privacy requirements, is used The database of the prices such as Orcale, Sql, dBase costly is also extraordinary selection.Can be between database and database The synchronization of relevant information data is carried out by background program, the uniformity of information is kept.External mechanism can be by predefined Interface, which is realized, authorizes accessing database data.
On the basis of the hardware physical structure for the laboratory information system (LIS) that Fig. 1 is stated, increase product satellite Position information management system and laboratory monitoring management system, and just construct doing for supervision and administration organization according to OA software architecture Public automated information management system (monitoring management and office automation CM-OA Control Manage and Office Automation) as shown in Figure 4.The 5th technology essential factor of the present invention is in CM-OA (the Office Information pipes of supervision and administration organization Reason) framework on embed product satellite positioning information management system and laboratory supervision message management system, analyze testing agency Laboratory supervision message management system be to be realized under the management by internet permission to being equipped with the technology of the present invention The database intrusion supervision of the analysis testing laboratory for the laboratory information system (LIS) that key element 1 is stated, can be with direct reading The technical data of the correlation analysis detection activity in the saved laboratory in laboratory information system (LIS) database, also It can further invade experimental implementation system (LOS), read the technical data of ongoing correlation analysis detection activity, and by This reaches the real-time technique supervision and management in the laboratory to analyzing testing agency.Product global position system therein is by connecing The satellite positioning information come by the satellite positioning information receiving entrained by supervised product itself/emitter transmission is realized to production The geographical position of product intermediate links and humiture information exercise supervision management.The present inventor is by this in the normal of supervision and administration organization Product satellite positioning information management system and the management of laboratory supervision message have been embedded on rule Office Information management system framework The information management system of the new supervision and administration organization of system is referred to as CM-OA (Control Manage and Office Automation monitoring managements and office automation) system.
The conventional OA softwares of supervision and administration organization are installed actually on laboratory information system of the present invention (LIS) It is exactly that can be widely used in the CM-OA of supervision and administration organization to embed laboratory supervision message management system again.Why say Product satellite positioning information management system and laboratory prison are embedded on the office information management framework of conventional supervision and administration organization Superintend and direct information management system and allow for current supervision and administration organization and all using the OA systems of oneself, so only needing to product Satellite positioning information management system and laboratory supervision message management system are embedded into the original OA systems of supervision and administration organization New CM-OA systems can be just changed into bright body.
Not only supervision and management can be realized in this CM-OA system according to the existing information management mode of supervisory organ OA (Office Automation), the administrative staff of administrative supervision management organization can be in this information management system Line supervision has detection activity and initial data and the examining report in the laboratory of the analysis testing agency in region, Ke Yijian under its command Superintend and direct products in circulation state and humiture state of the product for the manufacturing enterprise having under its command in region from dispatching from the factory wholesale enterprise.Need The concept of " having under its command in region " is highlighted in the brighter statement being above, because the supervision and management machine of China at present The supervision region of structure be according to task of supervision number and it is heavy carry out supervision responsibility division.The supervision of such as food security Responsibility is person directly responsible with regard to the clear and definite regulation people's governments at the county level.The water quality supervision of such as rivers and lakes is just clearly advised again The management organization of these fixed rivers and lakes is person directly responsible etc..Based on the theory of supervision " having under its command in region ", in above-mentioned CM-OA System in the quantity of supervised entities be not just very huge, therefore the supervisor of administrative supervision mechanism directly takes part in experiment The work that the supervision of room and products in circulation can be achieved on, is not a concept, is a kind of technology prison that can effectively implement Control means.Because the credibility of current Chinese society is being built, so the administrative staff of administrative supervision mechanism directly take part in tool The behavioural norm that the supervision and management of body supervises counterpart to constraint can play most direct effect, be that current structure China is whole The link that social credit system is subjected to.The information management system of the analysis testing agency of foregoing LIS+LOS physical structures It may be directly applied to production and the wholesale domains of product.The supervision counterpart of production and wholesale domains is using this system Afterwards, it is possible to directly with the CM-OA information butt joints of supervisory organ and shared, while CM-OA product satellite positioning information management The correlation technique of system is also very beneficial for supervising supervision and management of the counterpart to oneself product.
The 6th technology essential factor of the present invention is Laboratory Operation System (the LOS)+laboratory information stated by the present invention The information management system of the analysis testing agency of system (LIS)+product satellite positioning information management system is with containing laboratory prison Superintend and direct what information management system was connected with the information management system (CM-OA) of the supervisory organ of product satellite positioning information management system Internet architecture, as shown in Figure 5.The information management system for analyzing testing agency is passed through into internet and country, province and district city, county The supervision and administration organization of the analysis testing laboratory of level Four government is connected, as a letter that mutually can be exchanged and supervise in real time Breath system, belongs to the network architecture of Browser/Server (browser and server) pattern, this belongs to Client/ with some The LIMS products of Server (server/customer end) framework are different, and this is the main flow direction of current LIMS production developments.This In the supervision and administration organization of described analysis testing laboratory refer to CNCA, country in State-level Quality supervision and test quarantine general bureau, state food pharmaceuticals administration general bureau, State Administration for Industry & Commerce, national health and family planning The related State Council such as the committee, Department of Commerce, the Ministry of Agriculture, Ministry of Land and Resources, National Industrial and informationization portion, national environmental protection portion What the government organs of subordinate and its affiliated or these officials of government organs specified can represent being administered to itself for State-level The analysis testing agency in field has the supervisory organ of analysis testing laboratory of the supervision authority of office;Provincial aspect refers to should be with above-mentioned state The supervisory and management department of Government Analytical testing laboratory provincial, prefecture-level, at county level in a government office of family's aspect, for example, save Level, quality supervision and test Quarantine Bureau prefecture-level, at county level, food and medicine Surveillance Authority, State Bureau for Industrial and Commercial Administration, health and plan life Educate the committee, Department of Commerce (office), Department of Agriculture (office), Department of Land Resources (office), National Industrial and the information-based Room (office), environmental protection Portion (office) etc. and its subordinate's or its specify analysis testing laboratory supervision and administration organization.In view of governments at all levels of current China The architecture of supervision and administration organization to analyzing testing laboratory is not formed clearly also, for analysis testing laboratory's political affairs Mansion mechanism does not set up effective supervision system also, but has had really to analysis test experience actually in every field Exercise the department of the authority of office of technical supervision management, such as quality and metrological supervision field, food and medicine, cosmetics, health products in room Supervision field, environmental protection detection supervision field, the agricultural chemicals of agricultural planting cultivation, veterinary drug, chemical fertilizer detection supervision field, customs's matter The all substantial analysis that also should be to association area of government's regulation mechanism in amount detection quarantine field, health and epidemic prevention field etc. Testing laboratory's later exercises supervision responsibility, the supervisory organ of analysis testing laboratory of the signified government of the present invention also supervises comprising these Management organization.
Administrative supervision management organization and the analysis of the present invention in the network architecture of Browser/Server patterns are detected The information system of mechanism, as previously described can be by between real-time performance supervisory organ, between supervisory organ and testing agency, inspection The information exchange surveyed between mechanism, can be by the way that in laboratory information system (LIS) open interface, supervisory organ enters the present invention Analysis testing agency laboratory information system (LIS) central database access, relevant information can be had access to, be can also pass into Each Laboratory Operation System (LOS) in analysis testing agency has access to the ongoing sound related to analysis detection activity The related initial data such as the test data sheet that video data is detected to the operational factor of active equipment and ongoing analysis Information.It suffices to say that, the analysis detection information management system under LIS+LOS physical structures proposed by the invention will significantly The difficulty that degree reduction laboratory supervisory organ is managed the real-time oversight for analyzing testing laboratory, lifting is to analysis testing laboratory The quality for supervision that internal original experimentation is recorded and initial data is traced to the source.
Why current numerous LIMS (LIMS) product receives outside real-time oversight in laboratory With to internal original experimentation record and initial data trace to the source on there is many defects not in place, in that lack institute's table of the present invention The hardware physical structure of the LIM+LOS stated information management system.The hardware physical structure technology stated according to the present invention will Element, the program architecture of information management system can just design more scientific reasonable, more succinct capable and experienced, with more scalability and by force Big vitality, therefore the hardware physical structure of good information management system is the visitor for ensureing information management system function admirable See material base.
Based on the technology essential factor three of the present invention, the 7th technology essential factor of the invention is in Laboratory Operation System (LOS) institute Cable communication, fiber optic communications (data/address bus) and channel radio can be used between the active equipment and Laboratory Operation System of administration News, wireless communication mode and wireless and wired (data/address bus) mashed up communication mode are recommended in the case where condition is permitted Or wired (data/address bus) communication mode.Wireless digital transmission mechanics of communication is mainly using those short distances low cost without line number Word transmission mode, such as ZigBee, bluetooth, infrared ray, WiFi, UWB, RFID, NFC.Recommend in the present invention preferred wireless Communication data transmission mode and the mashed up data-transmission mode of Wireless-wire, wireless mode first choice ZigBee, WiFi.
Based on the technology essential factor three of the present invention, during the 8th technology essential factor of the invention is Laboratory Operation System (LOS) Digital collection and equipment management system need periodically to be believed with the active equipment in Laboratory Operation System compass of competency In the program for ceasing interaction, increase periodic clock alignment link, by digital collection and equipment management system according to oneself when Active equipment of the clock frequency into domain sends active equipment in clock alignment signal, domain and carries out response adjustment, makes this communication cycle Information gathering and instruction send according to clock alignment signal fiducial time order progress.Inventor thinks laboratory operation When the digital collection and equipment management system of system are communicated with the active equipment in Laboratory Operation System compass of competency, it can use Pattern or bus (wired) communication mode of wireless telecommunications.But the communication of meeting existence information is nonsynchronous existing in information communication As this for analyzing the information exchange of testing equipment to causing very big puzzlement.In digital collection and equipment management system to region Interior active equipment is carried out in cyclical information interacting activity, and clock alignment link is increased in the initial phase of each communication cycle It can be effectively prevented from because information is asynchronous caused by clock is asynchronous, it is ensured that the information exchange activity of active equipment is normally transported OK.
Based on the technology essential factor three of the present invention, the 9th technology essential factor of the invention is the present inventor in above-mentioned active equipment Especially emphasize intelligent power socket and intelligent power distribution cabinet (case) as in the region administered with Laboratory Operation System (LOS) The supply port of active equipment.This point is in highly important status in the technical program.Because in general, supplying Supplier of the socket and power distribution cabinet (case) of power supply as just power supply.And in the practice of analysis detection, to some equipments The collection of related information about power, can be often to constitute the important information part that initial data is traced to the source.These are simply tried Equipment is tested such as electric furnace, centrifuge, crushing and emulsification refiner, Turning motion instrument, minitype high voltage autoclave, its electrical equipment control An only simple power switch is possible to, lacks numerical control system, or even have numerical control system to also tend to Lack communication interface, this phenomenon is still universal at present to be present in numerous cheap low sides analysis testing equipment.Although one A little low side rigs for testing are with the renewal of technology, and digitized design has been widely adopted, but still has substantial amounts of, and price is low The honest and clean equipment for lacking Digital Control, is still generally welcome by client and is widely used in being difficult in laboratory, short-term Eliminate.Design of digital and low price experimental assembly and the letter of information management system with communication interface are more even carried out Breath communication is also to be inconvenient to what is popularized.Because designing the communication interface part of a digital equipment and information system in many occasions Developer can ask for higher development cost, and those produce the small producer of the cheap active equipment in laboratory, do not possess out generally Send out the technology and economic capability of digital communication interface.Also band is bought without more funds in some small-sized analysis testing laboratories There is the Conventional compact experimental assembly that the price of information system communication interface is higher.Therefore by with to it is active equipment operationally Electricity (voltage and current) information gathering and run time is recorded and can be by bus with communication interface Or the intelligent electric supply socket and intelligent distributing box of information exchange are wirelessly realized with Laboratory Operation System (LOS) (case) realizes the information to the operational factor (electricity and run time) of these active equipments of cheap small-size laboratory It is acquired so that these operation informations for lacking the cheap testing equipment of communication interface can also turn into laboratory initial data The important component traced to the source.
Based on the technology essential factor three of the present invention, the tenth technology essential factor of the invention is to carry out experiment to analysis testing agency Equipment is carried out in the room of laboratory to place the planning of station and assign uniqueness code identification to the station of each placement equipment, Here the room stated falls within the room in physical significance, and its basic definition is the region quilt of only a set of LOS administrations Referred to as laboratory room.In conventional site management, rough field division is usually carried out, some are on a place Many equipments are placed, also some are to equip usually to be placed on other places, take out of to be placed on the station of operation when in use.This Plant way and be all unfavorable for place and the information system management of equipment.As long as inventor proposes to be located in analysis detection operation room Experimental assembly must carry out unified site planning, and be assigned to place uniqueness code identification, and the letter for placing place will be equipped Code is ceased as the part of equipment information code.Table 1 below lists the expression side of the uniqueness coding of equipment place information The example of method, is merely illustrative the feasibility of technology essential factor, is in no way limiting of here.
Equipment position carries out uniqueness coding in the laboratory room and room of 1 pair of analysis testing agency of table, use Coding method is combinational code
Byte Code digit The meaning sum digit of byte
A 000 Code // 3 in laboratory room are represented in research and application mechanism
B 000 Code // 3 of the position of station are represented in the room of laboratory in research and application mechanism
C 000 Location code // 3 under station (mainly store supporting with material, the byte are stored for 000) without material
Based on the technology essential factor three of the present invention, the 11st technology essential factor of the invention is to the dress in analysis testing agency Standby, the equipment that can especially have influence on analysis testing result carries out uniqueness code identification, and the code identification includes active The information of the station uniqueness coding of equipment.These equipments include environmental Kuznets Curves and equip (including air-conditioning system, purification air-conditioning system System, detection of particulates system, ventilating system, illuminator, harmful gas detection system, anti-explosion fire fire-fighting system etc.), it is intelligent Power outlet and distribution box, various conventional analytical instruments (including various photometers and optical equipment, chromatograph, electrochemistry inspection Survey instrument, dissolution and disintegration tester, balance, incubator, heating and drying equipment, Biohazard Safety Equipment, superclean bench, various refrigeration dress Standby, centrifugation vibration class is equipped, crushed and emulsification homogenate class equipment, ultrasound class equipment, autoclave sterilization equipment, pumping equipment of supplying gas) Various analysis detection auxiliary equipments are equipped with instrument, the environmental Kuznets Curves equipment for being detected inspection product deposit position, ups power, shooting Deng.To these equipment carry out uniqueness code identifications after, can facilitate the information registering of experimental assembly, facilitate data acquisition, The information exchange of Laboratory Operation System (LOS) and equipment.
The information data structure of uniqueness code identification is equipped in addition to equipping the information of itself, should also include equipment Place place, the relevant information such as metering state, service mode, busy-idle condition of equipment.The present inventor recommends one kind and included The expression of the equipment uniqueness coding of place information is exemplified below shown in table 2, and table 2 below is only citing, is not limited System.
The analysis test experience equipment of table 2 carries out uniqueness coding, and the coding method used is combinational code
Byte Code digit The meaning sum digit of byte
A 0000 Sequence code/4 are equipped to represent (sequential coding during equipment typing information system)
B 0000000000 Equip name code // 10 and represent (coding rule of equipment sees below embodiment ## statement)
C 0000 Auxiliary information storage address code // 4 are equipped to represent
D 000 Room code/3 of analysis testing agency where equipment
E 000 Particular location code/3 in the room of analysis testing agency where equipment
F 0 Equip busy and identify/1,0=is not busy, and 1=hurries
G 0 Equipment repair status indicator/1,0=is normal, 1=maintenances
H 0 Equipment metering mark/1,0=meterings are normal, and 1=meterings are abnormal
In the citing of table 2, A byte informations are the serial number of equipment typing analysis testing agency information management system, B Byte information represents the specific name of equipment, and the classification present invention of equipment does not recommend sorting technique specifically, can be by client certainly Oneself is classified according to the convention in professional domain.But in order to which the present invention is expanded on further in experimental assembly full information uniqueness The technical characterstic of coding, the present inventor recommends using 5 grades (major class, subclass, secondary subclass, class, secondary class) every grade of 2 bit digitals subdivision Sorting technique, on this point, the present inventor will illustrate in the following embodiments.
Based on the technology essential factor three of the present invention, the 12nd technology essential factor of the invention is to having in Laboratory Operation System The management mode of the parameter setting of source equipment is that the equipment parameter setting link in process of the test takes tabular to equip parameter The pattern for setting data carries out the setting of equipment parameter, and each equips a kind of the logical of digital equipment of parameter setting form correspondence Interrogate agreement.It is Digital Control and the basis with communication interface that the design of equipment parameter setting form, which is built upon equipment, On, that is to say, that equipment parameter setting form correspond to a kind of communication interface identical Digital Control equipment, only in this way, institute Supplemental characteristic in the equipment parameter table of design could use compiling and anti-volume on the basis of the communications protocol by interface The operation of the equipment parameter setting table edited under Laboratory Operation System (LOS) and equipment is realized instruction interaction by translator program, Parameter in equipment parameter setting table can instruct equipment to run, and the electric parameter of equipment operation can also be in laboratory operation system Shown in the document of system (LOS).Therefore equipment parameter setting table is with very strong with Laboratory Operation System (LOS) Specific aim, its specific aim is to rely on the communications protocol of equipment, and only communications protocol identical equipment could share an equipment Parameter setting table.Equipment parameter setting table need the accumulation of an equipment used with the buying of analysis testing agency be one by The process of accumulation is walked, with more, control ability of the Laboratory Operation System (LOS) to equipment of equipment parameter setting table accumulation Also it is stronger, it will also become more and more clever.
As previously described in analysis detection practice, the equipment required for also having some experiments does not possess digital control circuit And communication interface.Solution for this kind of equipment is that the power supply of these equipments is used into the foregoing intelligence electricity of the present invention Supply socket (power distribution cabinet), the electric energy and run time that intelligent power socket can operationally be consumed to these equipments is carried out Monitoring record.Therefore (matched somebody with somebody using intelligent power socket, it is necessary to design a mark if necessary to this kind of equipment in experimentation Electric cabinet) equipment special parameter setting form, with meet experiment original record demand.
Based on the technology essential factor three of the present invention, the 13rd technology essential factor of the invention is Laboratory Operation System (LOS) institute Active equipment in the domain of area under one's jurisdiction must carry out information registering to the equipment management system in Laboratory Operation System (LOS) (to be recognized Know).Information registering is exactly that equipment management system can set up communication connection with equipment, so as to information exchange.Register (cognition) by Two part constitute, one be the equipment newly used equipment parameter setting table experiment management system (LOS) carry out equipment ginseng Number setting table registration, another is when active be equipped in after energization starts is sent out to the experiment management system (LOS) administered immediately Go out " revival is informed " information, and thus start the information exchange of equipment and experiment management system.
Equipment required for one analysis testing agency can be placed on different test site in use, according to this Invention is defined as independent experiment space advance data processor to the theory of Laboratory Operation System (LOS), so if one It is first using a certain equipment in individual independent experiment space, it is necessary to first in the laboratory operation in this independent experiment space System (LOS) carries out the registration of the equipment, in order to the cognitive this dress of the Laboratory Operation System (LOS) in the independent experiment space It is standby.For being equipped first using a certain, it is necessary to which program professional is for this equipment in an analysis testing agency Communications protocol and equipment parameter characteristic design the equipment parameter setting form for this equipment, and in analysis testing agency Register and preserve in the database of laboratory information system (LIS), each Laboratory Operation System (LOS) is being used in order to subordinate Before call registration to use.Another meaning of equipment registration is setting " revival is informed " program in the communication interface program of equipment Link, the active equipment required for analysis detection is tested once powers up startup, will setting to Laboratory Operation System (LOS) Standby management system sends signal, informs the working condition of oneself, if can receive instruction, the instruction of what form received. During analysis detection, when testing crew recalls pre-designed " active equipment electric parameter setting " form, fill in point The operational factor of this kind equipment required in analysis detection experiment, the equipment management system of Laboratory Operation System (LOS) is by phase Related control information is sent to the equipment, and the equipment receives after instruction, it is possible to run according to new parameter.Facility registration (cognition) Two kinds of registration contents realize that analysis detection testing crew can be by Laboratory Operation System (LOS) in analyte detection process The important step that active rig for testing required for man-machine interface or/and C (operation) terminal-pair of B terminals is controlled.
One citing of the expression for active (electrical equipment) equipment electrical control parameter setting table that table 3 is showed, here During being merely illustrative test data sheet in the present invention, specific rig for testing parameter can be passed through in C terminals Set the feasibility of table setting.There can also be the pattern of a variety of forms in practice, but as long as being to adhere to the pattern using form The technology category of the present invention is belonged to come the technical operation for the electrical control parameter setting for completing active equipment.Therefore table 3 is only It is citing, is in no way limiting of.
The citing of the electrical control parameter table design of table 3 active (electrical equipment) equipment
The parameter setting of the temperature programming of electric oven (roasting) case illustrated using the electrical control parameter list of the equipment of table 3, such as Shown in table 4 below.The sets requirement of electric dry oven temperature programming is using a digital electric dry oven with temperature programming performance, it is assumed that After test requirements document baking oven is opened, rise to 40 DEG C by room temperature with 2 DEG C/min heating rate first, maintain 10min, then with 5 DEG C/min heating rate rises to 60 DEG C, maintains 20min, then rises to 80 by room temperature with 1 DEG C/min heating rate DEG C, 30min is maintained, then 120 DEG C are risen to 4 DEG C/min heating rate, 40min is maintained.As can be seen here, electric dry oven program The parameter of heating is that the temperature value, heating of each stage slope, each stage reached by each stage is held time and heated up The equipment operational factors of time beginning this four can just summarize substantially (be only a kind of citing of temperature programming here, not generation Table is whole, therefore is also in no way limiting of).There is this rule, we can design a simple clearly form, allow experimenter The equipment management system in relevant device operational factor, Laboratory Operation System (LOS) is filled in as needed according to form typing Information, the recognizable instruction stream of translation forming apparatus, sends to equipment, allows equipment execute instruction.Such Laboratory Operation System (LOS) the operation note complete documentation of equipment can be got off, a part of information that can be reported as experimental record is experiment The favourable proof of authenticity.
The citing of the electric dry oven temperature programming parameter setting of table 4 is (it is assumed that " analysis inspection of this required electric dry oven according to table 2 Survey rig for testing uniqueness coding " be encoded to 0110-0202020100-10111-003-13-0-0-0)
Based on the technology essential factor three of the present invention, the 14th technology essential factor of the invention is to examination in Laboratory Operation System The management for testing record is, by experimentation links tabular data inputting, to complete experimentation track record, and first choice is pushed away The tabular recording mode of the form of a thing one is recommended, and each form possesses uniqueness serial number volume in each test data sheet Code, identification means are provided for the editor of laboratory report.The experimental record of analysis test experience process is laboratory informationization management More insoluble problem, because under current technical conditions, analysis testing laboratory can not possibly fully achieve automation, The record of people is necessary in each experiment link.But during experimental record, how to reduce human error, it is ensured that record The accuracy and integrality of data are the main points and difficult point of LIMS.The present inventor is according to oneself long-term reality Room working experience is tested, proposes, in the program frame design of the present invention, tabular Data Enter to be taken to Initial experiments record Method, simplifies and standardized experiment personal information typing, reduces typing mistake.Specific way is the operation link in active equipment The preparation link of (above having illustrated), solution, balance weigh link, experiment determination data (result) and record this four basic examinations Test in link and use the tabular recording mode of the form of a thing one, the first place of each form should be the order of form in test Numbering or other marks, but the mark should be unique in this test data sheet.Of course pass through certain reality Trample with after work summary, it is also feasible that thing more than two pieces, which is converged into a form to complete experimental record, but in this hair The frame design of bright designed information management system or the initial stage of operation, the method for the table of a thing one is the method shun the complicated and tackle the simple. Illustrated before equipment parameter setting table, before expression to the electrical control parameter list of equipment carried out table State, table 5 below, 6,7,8 are that link is prepared to solution, link, the Table Design of the record link of experiment determination data is weighed Expression is for example, but be in no way limiting of.
The citing for the testing record sheet design that the solution of table 5 is prepared
The citing for the testing record sheet design that table 6 is weighed
The experiment determination data record form citing of table 7
A B C D * *
The numbering of this form Testing result title As a result 1 As a result 2 ...... As a result n
......
......
......
Using above-mentioned these four test data sheet forms of table 3,5,6,7, the logging mode of the form of a thing one is adhered to, it is possible to complete Into the original experimentation record of a variety of analysis detection experiments.Experimental implementation management system in Laboratory Operation System (LOS) Under editor, arranged with these four forms according to the order of experiment process, just constitute a kind of analysis detection experiment of tabular Original experimentation is recorded, and such original experimentation record is not only clear, be conducive to detecting the COMPREHENSIVE CALCULATINGs of data and data analysis and Detection the original of data trace to the source, be also very beneficial for error correction inquiry, while be also prevent test data fraud the precautionary measures and The strength evidence of test data authenticity.
Based on the technology essential factor three of the present invention, the 15th technology essential factor of the invention is to there is the analytical instrument class of work station The testing result of equipment takes work station output file to take passages and regard work station testing result output file as attachment management Pattern.Some have carry work station analytical instrument class equipment can complete independently information gathering and information processing, exported Analysis testing result belongs to file category information.Recommend for processing the present inventor of this alanysis detection information by detection therein Data extract is had the original of the analysis testing result of work station output into the experiment determination data record sheet of above-mentioned table 7 Beginning file is managed as the attached sheet of report.Certainly, if the analysis testing equipment with work station can be to the present invention Laboratory Operation System (LOS) open interface communications protocol, then just can by it is this kind of equipment output testing result data believe Breath directly transcription is in the original experimentation record of the Laboratory Operation System (LOS) of the present invention, and this will be better information management Pattern.From the point of view of the information management angle that initial data is traced to the source, the information management of both analysis testing results can reach Why the purpose that initial data is traced to the source, specially illustrate this problem, is because many expensive big type analysis inspections of current China The source for surveying equipment is that outer analysis testing equipment giant supplier of state provides, and these international vendors are for various economic and politics The reasons why, it is communication interface agreement not to be opened to domestic LIMS.And the most analysis inspection of China Surveying laboratory can not meet under the situation of work requirements in current domestic analysis and detecting instrument, it has to use point of a large amount of imports Analyse testing equipment.In view of current this present situation, forces us to have to not open from analysis testing equipment interface communication protocol In the case of look for the solution that initial data is traced to the source, above-mentioned simple solution is exactly one of those.
Based on the technology essential factor three of the present invention, the 16th technology essential factor of the invention is to being related in detection and analysis operating process And to the electrical operation parameter information of associated equipment recorded, and be used as the attached report supporting with analysis examining report It is true and reliable that the analysis detection that evidence analysis examining report is relied on is operated.Inventors believe that, analysis detection initial data The accurate definition traced to the source should come from two aspects, one is the source of analysis detecting data is in detail and true, the second is Analysis testing staff is provided the proof of the behavior authenticity in inspection product examine flow gauge.We are said in analysis detection process of the test Allow the operation of laboratory technician mistake occur, but never allow the behavior of laboratory technician to play tricks.Will be same with analysis testing process operation The active equipment electrical operation parameter information that step is produced is recorded, and record is preserved automatically by Laboratory Operation System (LOS) Automatic editor, therefore the record of active equipment electrical operation parameter information is in inspection product examine to analysis testing staff as requested The maximally effective objective proof of behavior authenticity in operating process is surveyed, while being also the objective technique money of testing result correctness Material.The trip information of the active equipment of generation synchronous with analysis testing process is subjected to record editor, and as analysis inspection The attached report of announcement is observed and predicted, " shadow address " that is referred to as examining report that this attached report can be vivid.By shadow address It is synchronous with analysis report and laboratory technician's experimental record that laboratory information system is submitted to by Laboratory Operation System (LOS) (LIS) audit, and achieve preservation, this is the strong evidence to analysis detection result of the test public credibility.Therefore by " shadow address " The important information traced to the source as analysis detection initial data, is the important creation that the present inventor starts thinking.
Record required for " shadow address " described here is to analyze that analysis detection can be had influence in detection process of the test Relevant device running state information as a result, such as environmental Kuznets Curves equipment (including the inspection of air-conditioning system, air cleaning and conditioning system, particulate Examining system, ventilating system, illuminator, harmful gas detection system, anti-explosion fire fire-fighting system etc.), intelligentized power supply insert Seat and distribution box, various conventional analytical instruments (including various photometers and optical equipment, chromatograph, Electrochemical detector, dissolution Shaken with disintegration tester, balance, incubator, heating and drying equipment, Biohazard Safety Equipment, superclean bench, various refrigeration equipments, centrifugation Swing class equipment, crush and emulsification homogenate class equipment, ultrasonic class equipment, autoclave sterilization equipment, pumping equipment of supplying gas) various analysis inspections Survey auxiliary equipment and instrument, the environmental Kuznets Curves equipment for being detected inspection product deposit position, ups power, shooting equipment etc..
Based on the technology essential factor three of the present invention, the 17th technology essential factor of the invention is in C terminal landing laboratory operations When system (LOS) and entrance experimental implementation interface, the interface of computer screen is divided into two parts, a part is used to show The concrete operation step (SOP, the S.O.P. of analysis detection experiment) of analysis detection experiment, a part, which is used to analyze, to be examined Test the original data record tested in operating process.Such C terminal interfaces design is very beneficial for the experiment behaviour of analysis detection Make, be a typical characteristics for realizing with no paper test data sheet.
The information management system and the information of supervisory organ for the analysis testing agency stated by the present invention that Fig. 5 is shown The network architecture diagram of the Browser/Server patterns of management system, interconnection is passed through by the information management system for analyzing testing agency Net is connected with the supervision and administration organization of country, province and district city, the analysis testing laboratory of level Four government of county, can be real as one When the information network system that mutually exchanges and supervise.In the network architecture of this Browser/Server pattern, supervisory organ Between, between supervisory organ and testing agency, the information exchange between testing agency can be by laboratory information system (LIS) open interface, supervisory organ enters the central database of the analysis testing agency laboratory information system (LIS) of the present invention Access, relevant information can be had access to, each Laboratory Operation System (LOS) that can also pass into analysis testing agency is had access to The ongoing audio frequency and video data related to analysis detection activity and the operational factor of active equipment and ongoing point Analyse the related primary data information (pdi) such as test data sheet of detection.Current numerous LIMS (LIMS) product it So receive outside real-time oversight in laboratory and exist on tracing to the source internal original experimentation record and initial data it is many less than The defect of position, in that lack the hardware physical environment of the information management system with two-stage DCS features that the present invention states with And the thus technical characteristic for the technology of the present invention key element three to 17 that hardware environment can be produced.
On the basis of the technology of the present invention key element one to 17, the technology essential factor below the present inventor proposed in chapters and sections can To range the normalized by definition category of information management system information data structure, one is only defined comprehensively, general information Data structure, can just construct functional, extension facility, the information management system of information sharing.
At present governments at all levels of China to food, medicine, health products, cosmetics, veterinary drug, agricultural chemicals, chemical fertilizer, chemical reagent with And more strict supervision and management system is carried out in the multiple fields such as environment.Supervision and management point administrative supervision and technology for detection supervision Two plates.One of basic duty of public analysis testing laboratory in analysis testing laboratory of the present invention is exactly to match somebody with somebody Close administrative supervision management organization and carry out technology for detection supervision;In the quality analysis testing laboratory of the enterprise itself of enterprises, Its responsibility is also the technology for detection supervision to itself product quality;Government supervision mechanism is also required to set up to non-government investment Tripartite's analysis testing laboratory's purchase analysis and detection technology is the supervision and management service of government.Government is in each professional domain simultaneously Inside it is also required to implement supervisory duty to the public or third-party analysis testing agency in field.So either public analysis detection Mechanism, or third-party analysis testing agency, or enterprise itself analysis testing agency, all suffer from be supervision with it is supervised Two aspects are constrained.For ease of supervising with being supervised this two-way information interchange, the present inventor emphasizes to analyze testing agency Information management system should be unified and compatible with the information data structure of the supervision message management system of government, form standardization Information data structure.
The definition of information data structure that the present invention is stated is:Under the information unit (content) that minimum can not be split most The integrated combination of the small element information unit that can not be split, further increased definition is the minimum information unit that can not be split Line item position (order), further definition is that the minimum information unit that can not be split can use letter in information data structure 2 grades, the other information segmentation of the more stages such as 3 grades that breath code is represented.So-called element information unit refers to those in statistical analysis The minimum information unit of positive role can be produced, some information for not possessing positive effect carry out unlimited fractionation and are not belonging to this Invent the technology category pursued.
18th technology essential factor of the invention is to analyze the information management system and corresponding administrative supervision and management machine of testing agency The information management system of structure gather inspection product counterpart and supervision counterpart information and counterpart inspection product and product information when, The integrated information data structure of the minimum information unit related to supervision and management should be unified and compatible, and it is in information data structure In item position position or order should be consistent, and it is possible thereby to form the information data structure of standardization.With point of food security Analysis detection is illustrated with supervision, and so-called " corresponding " refers to that the administrative supervision management organization for analyzing testing agency and food of food is mutual Accordingly, the situation in the field such as agricultural chemicals, veterinary drug, medicine, health products, cosmetics is also such.It is so-called that " information data structure should unite One with compatibility " " unified and compatible " refer to that information data structure is consistent, or the pattern arranged each other and can pass through Both information datas afterwards are identified in the related subprogram of information management system can unify or can be compatible each other.Example Such as in the information gathering of foods supervision counterpart and inspection product counterpart, the name information data item of business entity is detected in analysis The 3rd can be come in the information system of mechanism and administrative supervision management organization, this is referred to as " information data structure is consistent ", Can also one make number one, one comes the 3rd, but two information systems are coordinated, and passes through recognition subroutine Step, can recognize this information data of the name of the business entity of other side, and this is referred to as " unified or compatible ".
By the information of the information management system of the supervision and administration organization of government and the information management system of analysis testing agency Data structure is unified and standardized, and is beneficial to two-sided information exchange, it is to avoid information management is chaotic, be conducive to data message Share, be conducive to the ZOOM analysis to information and statistical analysis.
The 19th technology essential factor of the present invention is the information management system and administrative supervision supervisor in analysis testing agency The information management system of structure will be sent when to censorship people and inspection product information and to supervision counterpart and the collection of its product information Inspection people information, inspection product information, supervision counterpart information, the product information of supervision counterpart are merged into (kind) information data knot In structure.
For example in food safety supervision and Food Safety Analysis detection field, food supervisory and management department is to food production The expression of information definition needed for the comprehensive supervision of enterprise is as shown in table 8 below.Content shown in table 8 is only citing, absolutely It is unrestricted.
Information definition of the food safety supervision administrative department of table 8 to supervision counterpart's collection (numerical value uses decimal representation)
Recommend information registration and the information gathering of supervision and administration organization of the Food Safety Analysis testing agency to submitted sample As shown in table 9 below using the expression of identical information definition typing, table 9 is only to illustrate, and is in no way limiting of.
(numerical value uses the decimal system to information definition of the Food Safety Analysis testing agency of table 9 to the information gathering of submitted sample Represent)
T data messages further illustrates in upper table:The definition of the detection qualitative classification of product/sample is that supervision is relative People need to need in sample=01 of censorship, production process when declaring product to supervisory organ detection sample=02, because Sample=03 of various reason sample owner active censorships, supervisory organ for supervision demand sampling observation sample=04, need into Sample=06 of port detection is needed when sample=05 of row quick detection, product import overseas, needs to check the sample of detection =07, need sample=08 of coordination detection, testing agency to carry out sample=09, supervisory organ that technological service is detected to penalize Sample=10 not, analysis testing agency are in nonproductive place since it is desired that sample=11 gathered.
It can see in above- mentioned information gathered data structure, some information datas and non-minimum indivisible information list Member, can continue segmentation, for example these data item of data item C, G, I, O, P, R, V, W, AB, AD, AH, AI and it is non-minimum not Divisible information unit, therefore be indicated with message code.Message code plays correlation in information management program, also It is to say that, by this message code, information management program can easily jump to the caching of (guide) associated by message code Or storage region, in the associated caching of message code or storage region, these information are inseparable into minimum by secondary splitting The information unit cut.Such as detection project of a product/sample of AD information datas and detection data, in associated storage Each detection project and corresponding detection data can be divided into region.And AE information datas just belong to minimum can not The information data of segmentation because no matter the project of product/sample detection how many, as long as there is unqualified a, principle On do not allow for let pass (No pass do not pass through).As can be seen here, the signified minimum indivisible information data of inventor be can With the need for according to information management and convenient and design, 2 grades of segmentations, the segmentation side of even 3 grades or more ranks can be taken Formula carries out minimal information data segmentation, and the purpose is to the convenience of information management, it would be desirable to directly be easy to the information of observation analysis to enter Row information data combination be placed in 1 grade, by and do not need byte read information combination use information code representative, 2 grades, 3 Thinner information segmentation is carried out under level even more multi-level environment again in information associate to these message codes, up to can be with Accomplish the minimum indivisible degree of information data.The sole purpose so done exactly classified relevant information, by it The pattern of relation use information data structure each other express, so facilitate setting for information management program framework Meter and programming and the facility of compiling, and the program architecture being consequently formed is strong, program is quick, interface clearly trusted computer Cease management system.
Based on this, the 20th technology essential factor of the invention is the association mould of the use information code in information data structure Formula, 2 grades, 3 grades, 4 grades, 5 grades, 6 grades are carried out to information and the other information of more stages is carefully divided and cut, and are consequently formed multi-level letter Cease data structure pattern.This is very clear and convenient letter for the expression of the huge information data structure of information data structure Cease data structure edit methods.
The table of comparisons 8,9 is visible, and the information of 4 has been lacked in table 9.The typing project for above-mentioned table 8,9 why occur is poor Different the reason for is that supervision authority is limited.In quality supervision and control of the China for food, the items in food table 8 are just should be recognized that Information, the production of food and distributors should also declare to food supervision and administration organization or during accepting oversight to prison Superintend and direct the content that above-mentioned table O-R projects are submitted by mechanism.But in the mechanism register information of food inspection, enterprise's O-R projects it is interior Hold and belong to the security information of enterprise, will not be to its outside all food supervision and administration organizations including analysis testing agency Other people reveal.The table of comparisons 8 and 9 is visible, although the content of information integration is different, information data structure is identical, The order of representation of the item of information used is consistent, here it is administrative supervision management organization is with analyzing testing agency to supervision phase To people, supervise counterpart product, send and (take out) inspection object and send and (take out) inspection product information gathering information data structure one Cause property, can close the standard of information data structure of the referred to as administrative supervision management organization with analysis testing agency in art Change or standardize.
It is emphasized that the above-mentioned table 8-9 of inventor information data structure is only citing, it is in no way limiting of, because row Political affairs supervision and administration organization and analysis testing agency can be according to the contents of oneself action and usage of trade design information typing Designed and Data Enter sequence with lising, diversified forms are had in real operation.But the technology of the technology of the present invention key element When core is that administrative supervision mechanism and analysis testing agency gather to the information data for supervising counterpart, both information data knots Structure should merge in (kind) information data structure.Especially in current China's field of food safety, by food security The information management system of supervisory organ and the supervision counterpart in the information management system of food analysis mechanism and inspection product pair As both information data structures are consistent and standardization, this will have to the integrated information processing of analysis monitoring food security with analysis There is important positive effect.
This important positive effect further can sufficiently be shown in following statistical analysis.For example with Exemplified by the detection of food and the supervision of food, it is assumed that FDA mechanisms are carried out to the food enterprises in affiliated supervision and management region can Sampling Detection, sampling Detection is undertaken by having qualified food analysis mechanism, and percentage is only used only to analysis testing result The analysis method of ratio, then can be easily when only carrying out food quality analysis using the detection data of food analysis mechanism Obtain the statistical data analysis of table 10 below
The simple statistical analysis project (16 that table 10 can be carried out according to the testing result of inspection product register information and inspection product Class)
If food supervision and administration organization merged to the information of food supervision and management object, still only with simple hundred Divide and compare analysis method, it is possible to be as shown in table 11 below using the analysis detecting data acquisition statistical analysis content of 26.
Table 11 needs the content (26) that register information can be analyzed conveniently with reference to foods supervision
Professional in information management software field can be clearly seen that by above-mentioned citing, when supervisory organ and inspection When the information data structure of survey mechanism is consistent, the facility of the programming and programming of the simple formula to realizing above-mentioned percentage Property be also it will be apparent that simple formula programming with programming in this way, for entering row information using increasingly complex formula Statistical analysis also can be such.The uniformity design of same information data structure is also obvious to information sharing.This reality It is exactly a kind of standardization behavior of information data structure design on border, the standardization behavior of this information data structure design can be with The citing of reference table 9,10 is by extensive expanded application in food, medicine, health products, cosmetics, veterinary drug, agricultural chemicals, chemical fertilizer, chemistry Reagent, environmental protection detect the scope of sample, and this comes for the information management in professional domain and programming and programming personnel Say, be referred to the elaboration and citing of the present invention to realize the related content of table 8,9 and table 10,11, and reference is pushed away successively Extensively, current China product (product in the field of information management of administrative supervisory organ and analysis testing agency can effectively be solved Kind) or/and the classification of sample (inspection product) compare mix, be easy to the information from the supervision of the angle design of top layer and testing agency Data structure.
The 21st technology essential factor of the present invention is to analyze the information management system and administrative supervision mechanism of testing agency Information management system should manage the title of the title of the product for supervising counterpart or kind, sample or inspection product according to administrative supervision The product classification or the product classification of retrieval or national standard or ministry standard or professional standard for the authoritative file that mechanism is promulgated Title or the name of product classification of trade classification convention be referred to as the " mark of product in information system or kind, sample or inspection product Quasi- title ", and for " title " in information system assign a uniqueness code, this code can be it is digital, Letter or word, but should regular follow.The present inventor recommend first according to the 1-5 levels under the decimal system, every grade Use the sorting code number rule of 2-3 digits to be encoded for " title " of specific product, and exist as the product or sample The unique product for analyzing the information management system of testing agency and the information management system of administrative supervision mechanism is identified.Can also The code coding of the similar specific product carried out using other systems or letter, but the regular property followed must be adhered to and unique The principle of property, and belong to the category that the technology key element is stated.
Based on above-mentioned 21 technology essential factor, the 22nd technology essential factor of the invention is due to professional etiquette, the difference of standard The different information managements that there is authoritative product classification pattern and different " title ", testing agency is analyzed occur The information management system of system and administrative supervision mechanism should design correlation retrieval and specification subroutine, solve different classifications and not With the information exchange inquiry between " title " in information management system and exchange substitution problem.
Based on above-mentioned 21 technology essential factor, the 23rd technology essential factor of the invention is by every grade double-digit point of Pyatyi The classification gauge that rule-like is encoded as " title " of all kind/articles/inspection product/sample in information management system of the present invention Then.So-called 1-5 grades can be referred to as 1 grade, 2 grades, 3 grades, 4 grades, 5 grades of meaning, can also be referred to as meaning class, subclass, secondary class, kind, secondary kind, also press The difference between 1-5 grades is represented according to the different method such as A, B, C, D, E or I, II, III, IV, V.Every grade of (according to the decimal system) 2-3 Digit represents, i.e. 001-999 or 01-99, it is recommended to use 01-99 can meet most of exhaustive division demand, such as following table Shown in 12.By taking 01-99 as an example, so there can be 01-01-01-01-01~99-99-99- if Pyatyi all uses maximum 99-99 classification, can meet the product (kind) of analysis detection object and/or the classification of sample (inspection product) completely.
The present inventor first elects the decimal system (byte for including all use numeric representations of present specification), can also actually make With binary system, octal system, hexadecimal statement, because these are for the personnel in the computer major field of information management system For may more facilitate.But it is just uncomfortable for the personnel in Non-computer Majors field.Due to for product Sorting code number should be understood first by the client technical staff of Non-computer Majors (overwhelming majority be) according to the specialty of oneself and Demand carries out sorting code number, and the thus correlation (association) of each clear and definite information unit, and computer is given by this coding After the program staff of specialty, the programming personnel of computer major can just be understood according to the coding of client information management object each Information unit interrelated and unique identification as a certain kind information unit set will be encoded.This hair in view of the situation A person of good sense first elects the decimal system as intermediary's work of representation manners unit incidence relation between client and the programming personnel of computer major Tool is feasible, and is very unused for most of client if represented using other systems, or even needs one The process of individual academic program.Based on this, the present inventor recommends to be used as technology between client and programming information personnel using the decimal system The mathematical tool of exchange, but the mathematical tool of other systems in the technology category stated of the present invention using falling within the present invention Technology category.
1-5 levels, every grade of digit of use 2 under the decimal system of table 12 carry out the signal table of product classification coding
The foundation of the uniqueness code coding rule of the specific product of title under being classified with food is expanded on further The 21st and 23 technology essential factors of the present invention.The authoritative food inspection classification of administrative supervision management organization of current China Method has six kinds, and this six kinds of food classification all have authority, it is difficult to negate which kind of food classification in information system, therefore just There must be the classification of authoritative food all to include in information management system by this six kinds, and according to the 1-5 under the above-mentioned decimal system Food standard name encoding during coding rule of the class per the digit of class 2 is classified to every kind of food assigns its uniqueness marking code. This six kinds authoritative food classification and codings are that (1) state food pharmaceuticals administration general bureau (CFDA) all issued every year in recent years Cloth《Food safety supervision is inspected by random samples and Risk Monitoring detailed rules for the implementation》's《Food security inspects food kind, inspection project in the works by random samples And detection method》Directory name carry out sorting code number;(2)GB2760《Food additives use standard》Annex E " food point The directory name of class system " carries out sorting code number;(3)GB2761《Mycotoxin is limited the quantity in food》Appendix A " food classification (title) illustrates " carry out sorting code number;(4)GB2762《Pollutants in food is limited the quantity》Appendix A " food classification (title) is said It is bright " carry out sorting code number;(5)GB2763《Pesticide MRL》Appendix A " food classification and measurement site " Carry out sorting code number, (6) permits the classification of classified catalogue title to carry out sorting code number according to the food production of CFDA systems;
The present inventor recommends the information management system in the administrative supervision management organization in foods supervision field and point of food Analyse the message tube of the information management system of testing agency and the product quality analysis testing laboratory of the food enterprises itself The classification of above-mentioned six kinds of food should be all embodied in reason system in information management system, and set up corresponding data cube computation and Corresponding database.When the relevant information of typing food, operating personnel should select to use first in information management system The Data Enter of product is carried out after which kind of food classification mode again.The authoritative status that above-mentioned six kinds of food is classified further is divided Analysis, the present inventor recommends the information management system in the administrative supervision management organization in foods supervision field and the analysis detection of food In the information management system of mechanism, it should which the food classification mode of preferred (1) and (6) is encoded.
Current China food is various in style, and various new food names emerge in an endless stream, and the food name that in the market occurs is simultaneously It is all not consistent with the food name that the classification of above-mentioned six kinds of food is included, therefore in the administrative supervision pipe in foods supervision field The information management system and the food enterprises itself of the information management system of reason mechanism and the analysis testing agency of food In the information management system of product quality analysis testing laboratory, the food name that should also occur on design and use with above-mentioned point Standard food title cross reference, the function of artificial control sorted generalization used in class, that is to say, that when in information management system In system during one brand-new food name of typing, it should artificial that this new food name classification collocation is had been saved in into information In the standard food name class of above-mentioned six kinds of food classification in management system.Such as standard food title have " preserved fruit " this Food, but product/sample ID at hand is " honey preserved plum processed ", it is clear that it should use the method for manual sort will " honey system words Plum " is concluded into the food classification of " preserved fruit ".
More specifically way is to set up a delicatessen food title in information management system to compare with criteria for classification title Table.When being different from the delicatessen food title of food criteria for classification food name to information management system typing one first, by New food name is carried out classification classification by the personnel with professional experiences according to the classification of above-mentioned six kinds of food.Thereafter when defeated again When entering this food name, information management system will automatic identification, retrieve the food name it is corresponding standard food name Claim, it is possible to readily have access to the data related to the food, such as examination criteria in information management system retrieval, detect SOP Etc. relevant information etc..This is a kind of approaches to IM for allowing information management system to possess learning ability, when typing is a certain amount of After new food noun, then the Similar Problems of typing will automatic identification again.Using the pattern of the criteria for classification title table of comparisons, Inquiry/retrieval the subprogram that is mutually related between each table can be designed, a specific kind is solved in different classifications pattern Exchange sex chromosome mosaicism.The interchangeability between different classifications is solved, can be the correlation techniques such as the standard related to specific kind text The sorted generalization and statistics of part information are analyzed.
The present inventor detects sample to medicine, health products, cosmetics, veterinary drug, agricultural chemicals, chemical fertilizer products and environmental protection Provide/adopt according to the regulator file of current China's administrative supervision administrative department, national standard, professional standard, employer's organization The classification mode taken, according to above-mentioned " 1-5 levels, every grade of digit of use 2 under the decimal system carry out product classification coding rule " to food Product, medicine, health products, veterinary drug, agricultural chemicals, chemical fertilizer, etc. the uniqueness sorting code number of product further lift in the following embodiments Example explanation, in the hope of elaboration in further detail.
In the field of information management of analysis detection, an important information management content be exactly analyzed detection product with Analyze the information data management between the standard of detection.This issue handling is good, will design the information management of high level The framework of system and succinct relative program is write out, the information management system so designed there will be healthy and strong life Power and easily extension upgrading.
Sample is detected in food, medicine, cosmetics, health products, veterinary drug, agricultural chemicals, chemical fertilizer, chemical reagent and environmental protection It is usually to be detected that for example national standard, portion issue mark with reference to the test stone that government or employer's organization promulgate when carrying out analysis detection Accurate, professional standard etc..In these examination criterias, crucial part is detection project, the control limit of institute's detection project, sample Product pre-treating method and the content for this four parts of detection method taken.For different inspection product, complex analysis Detection content is sample (inspection product) pre-treating method of sample (inspection product) before detection.In order to adapt to different sample detection and letter Change standard content, there are many standards in same standard while defining a variety of detection methods, this variety of detection method is same When can correspond to several samples detection pre-treating method.Such standard compliation pattern result in the complexity of examination criteria reading Property.Especially for numerous basic units and for those just enter the primary analysis detection laboratory technician analyzed in detection field, detection The complexity of standard adds the difficulty read and understood to examination criteria, while the also information management to analysis testing laboratory System proposes higher technical requirements.
For the ease of illustrating, the present inventor is by taking most complicated food security standard relatively as an example, the detailed elaboration present invention The technical scheme that information data of the people between the analyzed detection product of processing and the standard of analysis detection is proposed when managing.
In China, the complexity of the analysis examination criteria of current food in promulgation and editor to be higher than far away medicine, The complexity of other class products such as cosmetics, veterinary drug, agricultural chemicals, chemical fertilizer, environmentally friendly sample.The current food security standard of China is divided into four Individual basic pattern, the food safety detection establishing criteria that (1) country promulgates;(2) the food safety detection method that country promulgates Standard;(3) the state food safety quick detection method standard just promulgated recently, this is the standard that central portion office rank is promulgated, We can still be regarded as the standard of country level, referred to as " national standard ";(4) each provincial government promulgates food safety detection method Food safety detection standard used in standard or the enterprise put on record in supervision department of provincial government, we can be commonly referred to as " Square food security quick determination method standard, referred to as " terrestrial reference ".
One of the characteristics of these standard compliation modes is that standard contains detection project, detection project control limit, inspection product Pre-treating method, detection method.The two of feature are the food safety detection establishing criteria and country's promulgation promulgated in country It is much to employ the edit mode that a standard applies mechanically a standard in the edit mode of food safety detection method standard, That is some detection project of some product is completed, it is necessary to which one can be completed with reference to more than one standard The detection project of specific product.By the north it is most common be also most popular hawthorn roll exemplified by, hawthorn roll food classification on return Belong to candied food.The detection establishing criteria of candied food has GB/T10782-2006《Preserved fruit general rule》, and preserved fruit is defended Raw standard be by《Preserved fruit general rule》GB/T10782-2006 is guided out GB14884-2003《Preserved fruit sanitary standard》, in GB14884 The hygiene for defining preserved fruit is according to GB/T4789.24-2003《Food hygiene hygiene inspection-candy, cake, preserved fruit inspection Test》.In above-mentioned standard, GB/T10782-2006 extends GB14884-2003, and GB14884-2003 extends GB/ T4789.24-2003, it is possible to 1 grade of standard (GB/T10782-2006) that they are referred to as to be mutually associated, 2 grades of standards (GB14884-2003), 3 grades of standards (GB/T4789.24-2003).It is to concentrate to promulgate also in some detection establishing criterias, example Such as GB2760 concentrates the detection project and control limit for having promulgated food additives, and GB2761, which is concentrated, has promulgated fungi poison in food The detection project and control limit of element, GB2762 concentrate the detection project and control limit for having promulgated pollutants in food, GB2763 concentrates the detection project and control limit for having promulgated maximum persticide residue in food, etc..Food security Product checking The maximum feature of establishing criteria is that most of they do not provide specific detection method, it is necessary to can be complete by extension standard Into whole analysis detection projects of a specific inspection product.These extension standards are often multistage.Such as in hawthorn roll lead content Measure need to extend grade III Standard, the detection of pathogenic bacteria Escherichia coli needs to extend to level Four standard.
The detection method standard of state food safety there are many what classification was promulgated, and the standard of such as GB5009 series contains The Physico-chemical tests method of 260 food safety detections;The standard of GB4789 series contains 41 food microbiological examinations Method;The standard of GB1886 series contains the detection method of 296 food additives;The standard of GB5413 series contains 28 The detection method of Related Component in individual infant food and dairy products;GB18932 series standards have contained related substances in 28 honey Specific detection method;GB31604 series standards have contained the specific detection of related substances in 45 food contact materials and product Method;GB14883 series standards contain the specific detection method of radioactive substance in 10 food, etc..State food safety One of detection method standard maximum feature be exactly these detection methods standard for a specific monitoring object, Often occur as the extension standard of the detection establishing criteria of monitoring object, such as the Escherichia coli inspection of above-mentioned hawthorn roll Survey, it is necessary to which extending to level Four standard-GB4789.3 can complete.
The food safety detection method mark promulgated due to the food safety detection establishing criteria promulgated with reference to country and country Standard is detected, can not effectively meet current China's food on time and operating efficiency in the detection work of the line of basic unit one Food Safety Analysis Detection task to be processed is needed under the severe situation of safety, so in the line food safety supervision law enforcement of basic unit one In the urgent need to the quick determination method of food security in work.Under this strong demand, some food securities in the last few years Quick determination method it is recommended out.These numerous food safety detection methods are much built upon new analysis detection On the basis of, because its Technical comparing is new, lack the inspection of time, so the food-safe quick determination method of supervision department Legal sanction takes the careful attitude of comparison.Until CFDA on May 16th, 2017 (state food pharmaceuticals administration general bureau) First batch of six food security quick determination methods are just disclosed in the form of CFDA is announced, this is the state that the Chinese government promulgates first The food security quick determination method of family's rank.This six quick determination methods are read, its feature has:(1) detection method is belonged to The standard of class, but specify that (for example this six standards clearly detect that object is to monitoring object, aquatic products, breeding water, paddy Thing processed goods and grain milling processed goods, chilli powder and thick chilli sauce, meat and meat products (dining food), the flesh of fish, shrimp, crab meat etc. The animal muscle tissues such as aquatic products, pork, beef), and applicable scope is relatively wide (namely detects object according to above-mentioned five Level product classification, the category level of product is higher), apply also for non-food stuff class detection object (for example:Breeding water).This with In current food security national standard detection method, an only small part specify that monitoring object scope, and most of method class standard does not have There is clearly detection object range to have significantly feature.(2) it is to estimate to develop the color to compare or precipitate to sentence as last testing result Calmly, this and the non-fast state food safety detection standard for examining class are used as product using specific a data or data area is No qualified result judgement has very big difference.Since being range estimation result of determination, this is just the report in information management system Automatic result judgement bring technical difficulty, analyzed with existing routine techniques, otherwise the range estimation of manual typing testing staff As a result, or using image automatic identification analytical equipment in the hardware device of system.(3) it is qualitative detection;(4) do not have Extension other standards can constitute the phenomenon of a complete detection method before and after appearance standard needs, but also without because It is that national standard examines the appearance of standard and negates the non-fast inspection national standard of the identical monitoring object of same detection project soon.(5) bulletin and Do not represent that the qualitative judgement result of this quick detection also needs to further check by other countries' standard in standard, this explanation The food security fast qualitative judgement detection announced in the first batch is can be as final legal detection method, this imply that having more Many national standard food security quick determination method standards promulgate appearance successively.This five essential characteristics have meant that state food peace Full fast qualitative judges that examination criteria will be independently of a voluntarily standards system outside other countries' food safety detection standard, its In topmost feature be " fast qualitative judgement ".
Start to promulgate in October, 2015 is new《The law of food safety》Article 29 regulation " to special local food, There is no national food safety standard, administrative department of public health of the people's governments of provinces and autonomous regions and municipalities can formulate and announce food Place of safety standard, reports to the State Council administrative department of public health to put on record ... "." country encourages the food enterprises to Article 30 regulation Formulate and be strict in the company standard of national food safety standard or provincial standard, be applicable in this enterprise, and report province, it is autonomous region, straight Linchpin municipal people's government administrative department of public health puts on record ".This two legal provisions specify that being used for outside state food safety standard The legal status of the standard of food safety monitoring, therefore just derived from field Nei You state of the current China in food-safe detection The phenomenon that family's standard, national quick detection standard, provincial standard, four kinds of examination criterias of company standard coexist." enterprise mentioned here Industry standard " must surmount the scope of " enterprise itself " in actual motion, because numerous testing agencies must not in detection Do not repeat " company standard " that product is relied on.Especially in the provincial standard promulgated without national standard, local provincial government When being referred to detection, the detection foundation whether " company standard " that must take correlation is passed through as food security.According to this The information that inventor contacts and recognized is visible, and the local food security standard or food safety of enterprises standard occurred at present is big absolutely The mark for belonging to quick determination method that majority occurs both for existing state food safety standard detection of complex, cycle length It is accurate.Therefore the characteristics of also just generally having identical with six food security quick detection standards that above-mentioned CFDA is promulgated recently.
Which type of technical measures to manage these four food security standards using, be Food Safety Analysis testing laboratory The skill of information management technique.What can be used for reference has the pattern of two kinds of standard managements, and (1) is managed according to the classification of standard, For example respectively will according to class standard, method class standard, soon inspection class standard, place or enterprise put on record standard carry out Classification Management, and Set up correlation inquiry each other.When there is Detection task, query criteria, Ran Hougen are first gone according to detected product (sample) The SOP (Standard Operating Procedure S.O.P.s) of this monitoring task is designed according to standard.This is At present using most information management modes to standard management, especially for the detection possessed compared with horn of plenty laboratory experience For personnel, direct reading Standard texts, then according to Detection task, write out the very strong concrete analysis detection experiment of specific aim SOP, not only can be very good complete analysis Detection task, while be also one analysis testing staff show self-ability tool Body surface shows.(2) another is, when seeing the analysis object for needing to detect, can just to be facilitated by the title of detected product Inquire and the associated examination criteria and their SOP of detection object.This method to standard management be particularly suitable for through Test the primary analysis testing staff of deficiency.In the case where the SOP editted is instructed, even departing from experienced analysis and detection technology The on-the-spot guidance of personnel, primary analysis testing staff is also the ground preferably completion analysis Detection task that can read according to the copy.
The present inventor selects first in design analysis testing laboratory's information management system framework and program solution Be that (2) are planted to the management method of standard.The reasons why selection is that it is comprehensive that current China's analysis testing laboratory is in needs The state of popularization, the especially popularization for analyzing testing laboratory to basic unit, in addition to laboratory hardware, management software, base The one universal facing challenges in line analysis testing laboratory of layer are the line analysis testing agency famine educational background height of basic unit one and experiment The veteran analysis testing staff in room.And one of abundant technology evaluation criterion of analysis testing staff of a laboratory experience This analysis and detection technology personnel reading, understanding standard and the ability that SOP is quickly write out according to standard are exactly seen, this Ability is to need the long-time in laboratory to temper to turn out what is come.If so can be by a small amount of laboratory experience The SOP of prior each analysis detection project that various detection objects are write out according to standard of abundant analysis testing staff, and SOP is associated with standard, detected name of product in the information management system in laboratory, so in analysis test experience In the information management system of room, Detection task just can quickly be inquired by the name of product for inquiring about detected object SOP and associated examination criteria.The educational background of a line analysis testing staff obviously can be just greatly lowered in the SOP for having specification Required with laboratory experience, for those educational backgrounds are relatively low, primary that is lacking experience analyzes testing staff, by simple skill As long as the conscientious operation sequence according to SOP after art training, rigorous operation, it is possible to preferably complete analysis Detection task, this shows Having energetically meaning in the scarcity of the line analysis testing staff of basic unit one so is solved to comprehensive popularization in analysis testing laboratory. The initial data for being also very beneficial for laboratory simultaneously is traced to the source.
In order to reach this design object, the present inventor just must design a skill according to the general character for analyzing examination criteria Art rule instructs the analysis and detection technology personnel according to the rule of agreement, and the relation further according to standard and monitoring object writes out phase The SOP of pass.Because without certain treaty rule, different analysis detection testing crews can write according to the experience and custom of oneself The SOP of different specification is write out, program staff's design program architecture of information management system is thus highly detrimental to and writes tool The program of body.
The 24th technology essential factor of the present invention is to analyzing the analyzing detecting method included in examination criteria as required The object (kind) of detection carries out single piece of information unit and sorts out editor, and to the information unit edited according to detection project, quilt Control limit, a kind of pre-treating method of sample (inspection product), a kind of order of detection method of sample (inspection product) of detection project Information data structure design is carried out, and to the integrated information data of the information unit for containing Product checking full information after design Structure assign uniqueness coding so that formed one it is regular, contain foregoing four substances and be detected Some detection project of sample (inspection product), detection project control limit data, a certain pre-treating method, a certain detection side The uniqueness code (coding) of the data splitting information of method.Specific way is according to detection object (inspection to analysis examination criteria Product) product assortment, examination criteria, the specific detection project in examination criteria, the detection as defined in examination criteria A kind of pre-treating method of object (inspection product) is detected specified in purpose control limit, examination criteria, specified in examination criteria A kind of order of detection method of detection object (inspection product) enters edlin, and is consequently formed the specific detection of detection object (inspection product) A kind of specific analysis detection operating procedure of project, synchronously detects each above-mentioned letter of operating procedure to the analysis edited The uniqueness coding that interest statement member is standardized, the set of these uniqueness coding just constitutes analysis detection operating procedure Uniqueness code,The code of analysis detection operating procedure is actually the information list for a detection operating method for detecting object The integrated unique identification of member, this unique identification just characterizes the complete of this analyzing detecting method of detection object/kind Information data structure.Information expressed by this analyzing detecting method full information data structure can go out single analysis with direct correlation The S.O.P. (SOP Standard Operating Procedure) of experiment is detected, therefore this is also that a kind of use is believed The SOP of analysis examination criteria method represented by breath data structure is edited.Because this SOP is edited coding schedule can be used to reach It is to be very beneficial for the information management to analyzing detecting method, and thus derived as the mark of its uniqueness having Beneficial to many advantages of analysis detection operation.For example be conducive to the framework of system in the information management system of analysis testing agency The succinct and program operation of design and polling routine is quick and with good scalability;, can for analysis testing staff Concluded, edited out with multiple examination criterias that the rule for following this uniqueness coding is involved in a specific kind The operating method (SOP) of capable and experienced clear specific detection experiment, the SOP so edited out can be readily with examination criteria Change carries out the revision of piece of relevant information;Such SOP and examination criteria mapping are good, are conducive to operating personnel in experiment Preceding reference standard and specific Detection task make up SOP deficiency, and bring many benefits for testing inspection.The present inventor will The message code of this data encoding structures for containing analyzing detecting method information is also referred to as " analysis examination criteria method SOP codes (below this specification can abbreviation SOP coding) ".
The 25th technology essential factor extended by the 24th technology essential factor of the present invention is to be saved in SOP codes with China Draw the information unit that structuring food prods safety standard based on code distinguishes and distinguish four kinds of above-mentioned standards systems in level administrative region. Wherein provide the dibit in 00=state food safety standards, 99=state foods safely and fast qualitative detection standard, table 13 below The food security company standard that digital code is used in the local food security standard for distinguishing provincial promulgation and the province region, this It is the code that front two in six digits according to china administration zoning code represents provincial administrative division.By the ground of provincial promulgation Food security company standard in square food security standard and the province region draws code using provincial administrative region and is subject to area Other reason is to be based on《The law of food safety》Article 29 regulation " ... after food-safe national standard is formulated, the place Standard is abrogated at once " regulation because in the local food security standard of provincial promulgation and the province region food security enterprise Industry standard be respectively provided with " Interim Standard " and transprovincially domain using needing the government's regulation mechanism " approval " or " standby of province's domain rank The food security standard that could be used after case ".
Table 13:Food security company standard difference code table in the local food security standard in different province domains and the province region
The present inventor lists a kind of full information data code (the analysis examination criteria method of analyzing detecting method with table 14 SOP codes) expression.In following citing, represented, pressed again in specific programming using the numeral under the decimal system Used ten's digit is compiled using other encoding laws the need for according to programming.Table 14 is only to illustrate It is bright, it is in no way limiting of.
The food analysis full information code coding of 17 information units under the decimal system of table 14, the coding method of use For combinational code.
I information datas in upper table are the codes of the detection limit data of detection project, by detection project control limit Data embodied in food analysis full information code as information data, be easy for laboratory calibration system Unite to analyzing the facility that examining report book result is edited automatically.Due to the data and the disunity of data unit of detection project, So use information associated codes are to corresponding buffer area or database.
Often there is such case in the edit pattern for the food security standard that current China performs:Such as food preserved fruit Hawthorn roll total sugar content, the detection of lead limit, the food safety detection method of the detection of staphylococcus aureus limit.First have to Read national standard GB/T10782-2006《Preserved fruit general rule》With《Preserved fruit haw products》GB/T31318-2014, the two standards are honey Give a farewell dinner two parallel primary standards required for food safety detection;Then reading GB14884-2003 is reviewed《Preserved fruit health mark It is accurate》, this standard belongs to secondary standard in the detection of candied food;The detection of regulation lead limit is pressed in GB14884-2003 According to GB5009-12-2010 regulation detection, so GB5009-12-2010 belongs to grade III Standard.In GB14884-2003 also Pathogenic bacteria detection is defined with reference to GB/T-4789.24-2003《Food microbiological examination-candy, cake, preserved fruit are examined》Inspection Survey, so GB/T-4789.24-2003 falls within grade III Standard;Golden yellow grape is defined in GB/T-4789.24-2003 Coccus detects that then GB/T-4789.10-2010 belongs to level Four standard according to GB/T-4789.10-2010.
One-level in table 14, two grades, three-level, the implication of level Four each mean that spreading out for standard stretches number of times.The level Four in table 15 Standard is spread out the upper limit stretched and stretched to spread out, but be not excluded for having spread out 5 grades of stretching and 6 grades of standards even more more spread out the phenomenons stretched, this be because It is still within for present food security standard in constantly revision process.In the revision of food security standard, it is possible to meeting The phenomenon that the local or a small number of standards of this influence of existing standard change is borrowed in using the standard newly put into effect, such standard Revision amount relative simplicity.But the present inventor be not intended to this standard spread out the standard of stretching phenomenon excessively continue extension, this The complexity that standard can be caused to read, is highly detrimental to experimental implementation, it is desirable to appropriate regulatory bodies in the rectification of standard Standard is reduced as far as possible to spread out the phenomenon of the standard of stretching, makes standard simple and clear, is easy to read and is understood and perform operation.
There is the technical staff in the SOP coding rules of this citing of table 14, analysis detection specialty can be according to above-mentioned rule Then, classification is carried out to the examination criteria required for detection object and compiles the SOP for being conducive to analysis detection test operation and tax Give the coding of the SOP uniqueness.What the program architecture design of information management and program technique of compiling personnel can encode according to SOP Information data structure and coding uniqueness design information management system good framework and easily inquire about, modification program. The content that so information management system not only can quickly inquire about SOP according to the demand of user also may be used for testing crew reading So that when new change occurs in analysis examination criteria, local modification can be carried out to some information data byte of SOP codes, The change of Standard Edition can be shown with some data structure table in SOP codes and avoided because the change of standard is believed standard The confusion of management is ceased, information management system is reached optimal degree to the efficiency of management for analyzing examination criteria.
In the data item for having food classification during above-mentioned SOP is encoded, this is critically important information unit in SOP codings.Information The A items of unit illustrate the code of food classification, and wherein 1=is promulgated every year according to CFDA《Food security is inspected by random samples in the works Food kind, inspection project and detection method》Catalogue classified;2=GB2760《Food additives use standard》It is attached Record E " food categorizing system " catalogue is classified;3=GB2761《Mycotoxin is limited the quantity in food》Appendix A " food classification (title) illustrates " classified;4=GB2762《Pollutants in food is limited the quantity》Appendix A " food classification (title) illustrates " enter Row classification;5=GB2763《Pesticide MRL》Appendix A " food classification and measurement site " carry out classification volume Code;6=permits the classification of classified catalogue to carry out sorting code number according to the food production of CFDA systems;The B items of information unit are exactly The sorting code number of 5 grades every grade 2 digits under the decimal system of food classification;The content of other has handed over clear in table 14.
There are many analysis testing agencies to work out some analysis detection operations for some specific detection methods at present SOP, this kind of SOP are that have the SOP for being adapted to multiple detection kinds for what a class or a kind of analyzing detecting method were write, can be with Simply it is referred to as that " general character SOP ", this is good, with above-mentioned the stated SOP of the present invention and not colliding, and can be this The SOP of project offers reference.The SOP of the above-mentioned statement of this project is the specific examination criteria for detecting object (kind) that places one's entire reliance upon Formed by SOP edit rule, it has been mainly characterized by varietal check, and the general character SOP, Ke Yijian of multiple kinds are not applied to Singly it is referred to as " individual character SOP "." the characteristics of general character SOP ", is used for some veteran analysis testing staff, especially The analysis testing laboratory of information management system is the absence of, general character SOP is widely used.
And the present invention state " individual character SOP " many-sided advantage is also apparent in information management, wherein most prominent Advantage have two aspects, one is for analysis detection original experimentation record information management succinct design is provided, It is easy to initial data to trace to the source (statements of the related Sections of the tabular design recorded referring to previous experiments).It is excellent that another is protruded The rule that point carries out SOP codings according to analysis examination criteria can easily instruct professional and technical personnel to go to write new according to standard SOP, and thus progressively accumulate and construct with the SOP databases that strictly associate of analysis examination criteria, and retrieval has access to Convenient, this will considerably reduce the educational background and skill requirement to analyzing testing staff, and especially those are engaged in analysis detection Orientation test person can just tax one's brains less the step-by-step operation read according to the copy, and thus improve operating efficiency, reduce mistake, this Point is particularly important for setting up in the analysis testing laboratory (mechanism) of the line of basic unit one.Because in current situations, lacking Be not only line analysis testing laboratory of basic unit one hardware and software management, the talent of line analysis testing laboratory of basic unit one Scarcity is also suitable distinct issues.Educational background and laboratory experience requirement in the case of routine to analysis testing staff compare Height, and in the case where analysis detection SOP is clearly instructed, it is possible to it is greatly lowered and analysis testing staff educational background and experience is wanted Ask, complicated analysis detection practice is changed into the skilled work post of programming operations, its advantage is obvious.
According to the SOP coding rules to medicine, cosmetics, health food, veterinary drug, agricultural chemicals, chemical fertilizer, environmental protection tests sample The SOP of analyzing detecting method edit, the SOP relative to food safety detection standard edits more fairly simple because In their analyzing detecting method standard, the derivatives phenomenon of standard set standard is more relatively easy, can directly use The method for the SOP coding rules statement that the present invention is stated, carries out SOP with reference to specific analysis examination criteria and edits, and assign only The SOP codes of one property.On this point, it will be further illustrated in the following embodiments.
The present inventor will select the specific food kind food standard related to its further in following embodiments Analysis and detection technology personnel in the editor and coding method of citing, further explaination and displaying SOP, this professional domain can join " individual character SOP " editors and coding are carried out to specific analysis object according to specific embodiment.
The 26th technology essential factor of the present invention is the material information data structure for defining unique identification, recording laboratory The whole life cycle that consumptive material (including expendable material, equipment accessory, or abbreviation material) disappears from procurement request to material Change procedure.The quantity register information data item under least unit entry and least unit used in material is wherein included, The least unit of material is " gram " (g) for solid, is " milliliter " (ml) for liquid, can also extend to milligram (mg), milliliter (ml), this is for some expensive materials such as reference substance, standard items, standard reagent, smaller metering list Position is conducive to the management of more fine test consumable and material.Specific citing is as shown in Table 15.
Under above-mentioned " least unit " theory, the solid reagent of chemical reagent recommends to use g and/or mg for registration unit (valuable and standard reagent and reference substance, standard items can use mg to be registration unit), liquid reagent recommend using ml and/or Ul is registration unit (valuable and trace reagent and reference substance, standard items can use ul to be registration unit), minimum registration unit Under the quantity of material refer to that according to g or ml be the quantity that calculates of unit.Such as CH3CH2OH, purchase one case is commercially available CH3CH2OH, specification is 500ml/ bottles, or 20 bottles/case, and this is the unit and quantity typically registered, if according to least unit ml Registration, then should accelerate for 10000 record.Such as NaCl again, buys one case commercially available NaCl, and specification is 500g/ bottles, or 20 Bottle/case, this is the unit and quantity typically registered, if according to least unit g register, should accelerate for 10000 note Record.Non-chemical reagent can be according to minimum package unit of the service condition using the material such as individual, branch, bag, box, volume, block, bottle.Dress The unit registration of standby accessory amount of appellation according to used in consumption and maintenance, such as individual, branch, bag, box, volume, block, bottle.Note Meaning is not negated conventional registration content, for example, changed this point it is emphasized that increase above- mentioned information data content in typing information Ml/ bottles, bottle/case, bag/case, branch/bag of length of schooling agent etc..Quantity under this material information increase least unit and least unit The information content advantage be calculate experiment consumption when, it is not necessary to conversion process directly invokes the quantity of material under least unit Adjusted, simplify the complexity of the accounting program of test consumable consumption, be conducive to the computerized information of supplies consumption information Management, because such programming programming is more simple and operation is quick.
The 27th technology essential factor of the present invention is material goods yard information data structure of the definition with unique identification, note Recording laboratory consumptive material (comprising expendable material, equipment accessory, can also include office, logistics etc. directly not related to experiment Material and consumptive material, or abbreviation material) the change in location information of the whole life cycle of disappearance from procurement request to material.
Test consumable (following or abbreviation is generally all set up inside analysis testing agency:Material) total storehouse, Point material storehouse of different technologies detection section office can also be set up, but the material for having received, the management of material is just lost The order in store management has been gone, has caused the confusion of " material terminal management ", this is the generally existing of existing analysis testing agency As.Chaotic in order to avoid the material terminal management of test consumable, the present inventor takes the concept for avoiding total storehouse or point storehouse, will Analyze the places of all storage materials in testing agency, it is unified to carry out goods yard planning, and assign uniqueness coding, including can With the place of " total storehouse " " point storehouse " that is considered as analyzing inside testing agency, this uniqueness coding can clearly identify material Physical location information, be conducive to the architecture design of information management system to be programmed with retrieval and inquisition.
Goods yard referred herein is relative concept.For example in a rack-layer of a smaller cupboard, many placed Ampoule equipped with standard items or reference substance or control substance of plant drug, is that will place these standards under being managed in common warehouse goods yard The shelf of product or reference substance or control substance of plant drug are managed as a goods yard, and in the inventive solutions, recommending will Goods yard further refine to each and the standard items or reference substance or control substance of plant drug of each lot number are carried out as a goods yard Management, and uniqueness code identification is carried out in information management system to each goods yard., can using this material management method So that in addition to total storehouse, point storehouse, the handling of goods and materials end of the test site detected in analysis can be according to field condition pair Material carries out goods yard planning and assigns uniqueness code identification, realizes the fine-grained management of material end.Perhaps someone can consider After big goods yard numbering, the effect that each goods is carried out to numbering and above-mentioned situation in goods yard is the same.But The present inventor do not think so, from the theory of information management for, goods yard is the information for belonging to goods yard, and goods on goods yard Code belong to the information of goods, the different information of two attribute is mixed, the confusion of information management is easily caused, this It is Programming and the program composition for being highly detrimental to information management.Therefore material in the total storehouse for analyzing testing agency is stored Goods yard according to analysis testing laboratory room (or separate space) and single variety planned, and to goods yard progress uniqueness Code identification is one of technical characteristic of material information management in the present invention, wherein total storehouse of analysis testing agency can be with broad sense Definition be all storehouses, storehouse such as office facility, the storehouse of manufacturing enterprise, test consumable can using the definition of broad sense as All materials, for example, can cover office appliance, daily necessities etc..Concept according to fine goods yard carries out goods yard planning can be with Material terminal management confusion phenomena is effectively prevented from, is conducive to the fine-grained management of material.
With reference to two technology essential factors of the present invention the 26th, 27, inventor is recommended under the decimal system of table 15 The coding rule of test consumable (material) full information data structure, what this rule was shown is that a material is entirely being tested The uniqueness code identification of quantity under Life cycle information and the material least unit in flow.The method of table 15 is only It is to illustrate that the technical scheme of inventor can effectively be implemented, be in no way limiting of.
Citing (the generation in table 15 of the coding rule of test consumable (material) full information data structure under the decimal system of table 15 Representation can be represented directly with numeral, can also be represented with code, the information such as time, quantity.Code means the letter Breath each content of item can use code to carry out link queries), table 15 is only to illustrate, and is in no way limiting of.
B information are the classification of test consumable in table 15, and invention is for analysis testing laboratory, so experiment consumptive material Classification recommend with chemical reagent be categorized as main frame carry out classification statement, be classification of this present inventor to test consumable The coding rule for recommending following two classification mode, the 1-5 levels (class) under the decimal system, every grade (class) to be classified using 2 digits.
The first test consumable classification mode is the classification mould that catalogue is managed according to the chemical reagent of China's establishment in 1981 Formula:8500 plurality of reagents are divided into ten major classes, divide the chemical classification method of some subclass below every class again.This ten classes sorting technique For:(first kind) inorganic analysis reagent (inorganic analyticl reagents) is used for the inorganic chemistry of chemical analysis Product, such as metal, non-metal simple-substance, the reagent such as oxide, alkali, acid, salt;(Equations of The Second Kind) organic analytical reagents (organic Analyticl reagents) it is used for the organic chemicals of chemical analysis, such as hydrocarbon, aldehyde, ketone, ether and its derivative reagent;(the Three classes) specical regent (specific reagents) determines in inorganic analysis, discrete, enriched element when special some Organic reagent, such as precipitating reagent, developer, intercalating agent.This kind of reagent sensitivity is high, and selectivity is strong;(the 4th class) standard reagent (primary standards) is mainly used in demarcating the concentration of standard liquid.The characteristics of this kind of reagent is that purity is high, and impurity is few, Stability is good, and chemical composition is constant;(the 5th class) standard substance (standard substance) is used for chemical analysis, instrument point The chemical standard product compared during analysis, or the chemicals for calibration instrument;(the 6th class) indicator and test paper indicators And test papers) it is used to indicate titration end-point in titrimetry, or for examining the examination of some presence in gas or solution Agent.The paper slip of dipped indicator or reagent solution is test paper;(the 7th class) reagent for instrumental analysis (instrumental Analytical reagents) it is used for the reagent of Instrumental Analysis;(the 8th class) biochemical reagents (biochemical reagents) Reagent for life science;(the 9th class) high purity material (high purity material), as some special need Material (such as electronics industry raw material, monocrystalline, optical fiber) and some trace analysis reagents that will be industrial.Its purity is general 4 More than individual " 9 " (99.9%), Control of Impurities hundred a ten thousandths even ppb grades;(the tenth class) liquid crystal (liquid crystal) Liquid crystal is the abbreviation of liquid crystal, the feature of the liquid such as its existing mobility, surface tension, has optical anisotropy, double again The feature of the solid crystals such as refraction.There are other sorting techniques to the classification of chemical reagent, such as in Chemistry In China in 1981 Reagent association provides ammonium reagent purposes and discipline classification, and reagent is divided into the chemical reagent classification side of eight major classes and some subclass Method.
Second of test consumable classification mode is classification mode of the Chinese Chemical Society to chemical reagent:Wherein (first kind) leads to With reagent, 8 subclass such as lower point of general inorganic reagent, general organic reagent, teaching reagent;(Equations of The Second Kind) high purity reagent;(the 3rd Class) analytical reagent, 11 subclass such as lower point of benchmark and standard reagent, inorganic analysis sensitive reagents, organic analysis special reagent; (the 4th class) Instrumental Analysis special agent, lower point of chromatorgaphy reagent, NMR reagent, ultraviolet and infrared spectrum reagent etc. 7 Subclass;(the 5th class) organic synthesis research reagent, lower point of basic organic reaction reagent, Protecting gene reagent, phase transfer catalysis (PTC) The subclass of agent etc. 8;(the 6th class) reagent for clinical diagnosis, lower point of general reagent, biochemical investigation are with reagent, radioimmunoassay reagent Deng 7 subclass;(the 7th class) biochemical reagents, under 13 subclass such as mitogenetic alkaloids, amino acid and its derivative;(the 8th class) novel foundation Material and fine chemicals.
The classification mode of two kinds of test consumables of above-mentioned recommendation is only citing, is in no way limiting of, can be according to the row of oneself The other test consumable classification modes of industry custom selection, it should be noted that some following factor.(A) analysis should be followed as far as possible The classification common-sense rule to material in professional domain is detected, is classified according to the convention in professional domain or custom.If There is material (being primarily referred to as tentative consumable material) criteria for classification that analysis regulator of testing laboratory or employer's organization propose Specification should just be used as far as possible.(B) emphasis in Classification of materials is the classification to chemical reagent.(C) should be by chemical reagent Other test consumables that classifying to include specially are classified, such as face label, scraper plate, hairbrush.(D) will should easily it be lost Analysis detection is individually classified with glassware.(E) for office appliance, logistics support articles for use, equipment repair spare part and consumption Material etc. and the expendable material of analysis detection indirect association, also should individually classify in the information data structure of Classification of materials.
The AE data item of material information data structure embodies two fundamental types in table 15, and a type is material From in outside, a type is that material comes from inside, such as oneself prepare, many experiment reagents be all before experiment by Laboratory technician is prepared according to the demand of oneself.Such as 10% CH3CH2OH solution is exactly with 10% absolute ethyl alcohol and 90% Water mixed preparing form.The data structure of AE is the important means for effectively overcoming test consumable end managerial confusion.Cause Many standard liquids are configured usually to may require that in analysis detection practice, such as many indicator, titrand, mark Benchmark mother liquor of directrix curve solution etc..These solution are often made with commercially available experiment reagent and oneself prepared in laboratory , and often prepare first use repeatedly, and typically will not also be included in the total storehouse or point store management of analysis testing agency Item, to this management often feel simply helpless allowing unrestrained freedom state.This is managed not only bad for the end of material, Also the initial data for being highly detrimental to analysis detection is traced to the source.The AE items that the table 15 of the present invention is illustrated are by the management to such material Stated by a simple data item, be to be very beneficial for tracing back to the use management from reagent preparation and initial data Source.
The goods yard code of material is to determine that T represents room residing for material by T and U of the material full information data code of table 15 Between code, U represents material goods yard (can be a position of cupboard, shelf, drawer etc.) residing in room.Material Least unit is one material unit form of structure in information management system, and each form is as an address, and storage is a kind of The unit of material, such as unit of weight:Ton, kilogram, gram, milligram etc., volume unit:Kilolitre, liter, milliliter, microlitre etc..In information In data structure, the unit of material is represented with the code of material unit storage address, is to transfer the facility used.
From upper table 15, the sub-item of test consumable (material) full information data structure is a lot.It is right for a long time Test consumable fine-grained management is always the problem of numerous analysis testing agencies feel headache.For some easy-consumed goods of low value kinds, Either user or manager are intended to take simple thick lines to manage, because so meet that the mankind have tends to be lazy Lazy person's character.But for some valuable, hypertoxic, mentals, inflammable and explosive class material, if not taking fine-grained management may Serious legal consequence occurs.It is thickness two lines pipe in the traditional method carried over without the computer information management epoch Reason, and be self-evident the drawbacks of the waste of manpower inefficiency of two lines management appearance.Come into computer now The epoch of auxiliary informationization management, that people have been intended to is convenient, stably, extension easily, save labour, simple material information management system System.And an outstanding material information management program is to need to become more meticulous to the information data structure of test consumable (material) Ground is rationally designed, and writes out rational information management subprogram based on this.The material information data structure of table 15 is exactly In order to reach this purpose, for example, the handling of goods and materials Data Structure Design in table 15 is applied in Drug Administration, it is especially right In the strict control of smart (spiritual medication) numb (Anesthesia medicine) similar drug, it is possible to readily accomplish the supervision that becomes more meticulous, because In the material information data structure of table 15, to the applicant of links, approver, recipient, receive people and all devise accordingly Information data.And for general material, some data item are clearly that some are cumbersome, it can not gather upon execution, It is zero equivalent to the data item, but therefore its information data structure does not change.In detail with consistent material information number According to structure, the programming to material information management is clearly very favorable, and its related subprogram write also can be terse, tool There are stronger vitality and scalability, resulting information comprehensive analysis, it will make management work more step to a new level. In information-based highly developed today, the importance of information data structure reasonable in design can be peeped out typically by table 16.Computer One of difference between the information management and traditional before information management of network technology highly developed today is that letter What breath was gathered becomes more meticulous, while it appear that some are cumbersome, but the processing of the information data in later stage will be convenient for management in the future There is provided and greatly facilitate, it is just so-called once to bother, it is convenient permanent.It can just have a taste of this point from the citing of table 16 below.
Table 16 adjusts information unit-" the test consumable core for having direct relation in material full information code with test consumable Calculate message code "
Table 16 is the test consumable data structure according to table 15, will wherein be conducive to analysis detection in or after to experiment consume The relevant information data unit that material is adjusted.If purchasing the whole material life cycle withered away until material in material request All it is to be managed according to the material life cycle full information data structure of above-mentioned table 16 in information management system, then in analysis Directly it can just be entered during detection experiment process using the contiguous items in the full information data of the material of above-mentioned table 16 The accounting of consumptive material consumption is tested in row experiment process, because its data structure is more succinct than table 15, then what relevant information was managed sets Meter and programming also can be and then succinct, and focus of the testing crew when considering test consumable problem also can be succinct, and " experiment consumes table 16 Stone calculates message code " just embody this point.
The 28th technology essential factor of the present invention is that sequence number of the material in information management system is arranged using order successively Row coding, material disappearance after sequence number upgrade automatically and when material is called using storehouse " first in first out, it is laggard after Go out " retrieval recall pattern.The sequence number of material is one of important information element of material unique identification, in material sequence number Mark under, easily the identical material of the correlative information such as manufacturer, product batch number can be distinguished. In table 15,16, the sequence number of material employs 6 codes under the decimal system, and the number of code digit can be according to involved The quantity of material determines, but how sequence number is edited, it is necessary to take seriously, if processing is bad, is unfavorable for information management frame The design of frame structure, and easily produce the confusion of handling of goods and materials information.The present inventor is proposed in material typing information management system When sequence number should be using order arranging and encoding successively, when the material of typing in information management system is using finishing, should Sequence code of the information of material in information management system typing will disappear automatically, and material sequence code followed by is by automatic Shanxi Level, while the automatic transfer history of the information of the material is stored and preserves the maximum time for being no more than 24 months by information management system When information management system be purged again.
For example, if the material under 001100 sequence code is consumed and is over, this material for corresponding to 001100 will Disappeared from the material library of the information management system of analysis testing agency, while the material that original material sequence code is 001101 is certainly Dynamic to be promoted as 001100, by that analogy, sequence code is more than the sequence code promotion that all subtracts 1 one by one of 001101 material.In material library The material information of middle disappearance, which is stored in as historical summary in the historical summary database of information management system, to be preserved to no more than Disappeared again from information system after the time of 24 months.The benefit of so design material sequence code is the sequence code of material without void Number, maximum material sequence code illustrates the material of the physical presence in the material library of the information management system of analysis testing agency Batch size.The mode of this order successively to the information management system typing material sequence code of analysis testing agency is highly beneficial In operator to the information management system typing material of analysis testing agency and and more thoughts need not be spent to consider materials Sequence code encoded question.Material sequence code is different from the production batch code of material, and both differences are the lifes of material Production batch code is that the producer (manufacturer or makers-up) of material assigns, and material sequence code is by analyzing testing agency Information management system material library typing material operator (experimenter or warehouseman etc.) successively order arrangement assign 's.Have after this typing of order successively material pattern, it is possible to which the convenient principle design according to storehouse analyzes testing agency Information management system material recall the subprogram of (or have access to or retrieve).So-called " storehouse " be exactly " first in first out, it is laggard after Go out " recall pattern.Information management system according to the principle design analysis testing agency of storehouse recalls the subprogram of material Advantage is in time can to take out old stock to use.Such as same reagent has first bought a collection of, has bought a collection of again thereafter, has pressed Subprogram is recalled according to stack mechanism design material retrieval, it is possible to first recommend what early stage purchased to experimenter according to serial number Reagent, early stage buying reagent be finished with the information management system of post analysis testing agency recall again the reagent of later procurement with For using.In addition, it is determined that on the basis of the basic subroutine that material storehouse is recalled, should also give experimenter's refusal and use Advanced right first, this has been to confer to the right of experimenter oneself selective reagent, selection of this right in Self-made reagent In be important.Because experimenter prepares personal reagent using commercial reagent, laboratory technician should be generally advocated according to feelings How much condition uses how many accurate formulation, does not advocate once to prepare much being used for late comer.But the reagent for needing to demarcate The comparatively laborious reagent with preparation, it is necessary to special messenger such as various standard reagents, titrand, the standard solution of high concentration Used after preparation, demarcation for long-term and many person-time.Even such case, the testing crew after also allowing is to formulated Good Self-made reagent produces distrust, it is allowed to which later testing crew has the right that refusal is used, and this is beneficial to be avoided need not The test error wanted.So in the information management system of analysis testing agency, design material recalls thing in the way of storehouse Testing crew should be increased during the subprogram of material and refuse advanced subfunction first.The sequence code of material is designed as 6 by this citing Bit digital, can analyze the typing of 0-999900 batch materials the information management system of testing agency.For big type analysis detection machine Structure, when the material batch in needing typing to analyze the information management system of testing agency is more, can take the circumstances into consideration increase material sequence The digit of row number, therefore the coding of the material sequence number in the program frame design of the information management system of analysis testing agency The information management system client that should increase in subprogram allows to analyze testing agency increaseds or decreases material serial number digit Selection subfunction, to facilitate the client of information management system of analysis testing agency to set suitable thing according to the situation of oneself Expect serial number space.There is typing to analyze the sequence number of the information management system material of testing agency, it is possible to avoid material Other information it is identical when same material analysis testing agency information management system in duplication of name, it is ensured that record Enter to analyze the uniqueness of the material code of each batch of the information management system of testing agency.
The 29th technology essential factor of the present invention is to make the ratio of the theoretical consumption of test consumable and actual consumption amount For the important performance assessment criteria of examination analysis detection experiment preciseness.
Technology essential factor 29 needs to illustrate by the example of experiment.For example with graphite furnace atomic absorption spectrometry The SOP of " the pressure dispelling tank resolution method " of the sample pre-treatments that method is detected to the lead in food is as follows:【Pressure dispelling tank disappears Solution】Weigh 1g~2g samples and (be accurate to 0.001g, dry sample, fatty high sample < 1g, fresh sample < 2g or pressing force are cleared up Tank operation instructions weigh sample) in polytetrafluoroethylene (PTFE) inner canister, plus nitric acid (commercially available nitric acid) 2mL~4mL soaked overnights.Added again Hydrogen oxide (commercially available 30% hydrogen peroxide) 2mL~3mL (1/3 of total amount no more than tank volume).Inner cap is covered, is screwed stainless Steel sleeve, is put into thermostatic drying chamber, and 120 DEG C~140 DEG C holding 3h~4h naturally cool to room temperature in case, will disappeared with dropper Change liquid to wash or filter in (depending on the salinity of sample after digestion) 10mL~25mL volumetric flasks, repeatedly washed on a small quantity with water Tank, washing lotion is incorporated in volumetric flask and is settled to scale, mixes standby;Make reagent blank simultaneously.
Before this in experiment of processing, if it is desired to the quantity of the sample of analysis is 1 part, according to while doing blank control With the parallel basic demand for doing two parts, then needing the experiment consumptive material of consumption has:(1) nitric acid (2ml-4ml) × 4=8ml-16ml, Wherein nitric acid is commercially available top pure grade nitric acid, can be brought directly to consumption calculations;(2) hydrogen peroxide (2ml-3ml) × 4=8ml- 12ml, wherein hydrogen peroxide can also be brought directly to consumption calculations for commercially available 30% hydrogen peroxide;If necessary to the sample of analysis Product are 10 parts, then the nitric acid needed be (2ml-4ml) × 22=44ml-88ml, it is necessary to hydrogen peroxide be (2ml-3ml) × 22 =44ml-66ml (according to the two parts of calculating of blank sample and every part of sample configured in parallel).Assuming that handling experiment before this is carried out Laboratory room reagent rack on, we save nitric acid in the B terminals in the room (room advance data processor) 2300ml, hydrogen peroxide 1879ml (being all to be recorded into goods yard according to the least unit of material respectively) material storage information, then B The computerized information experimental system of terminal according to the SOP of above-mentioned experiment and can need the number of sample (inspection product) detected, The theoretical consumption of the consumed nitric acid of this analysis detection experiment and hydrogen peroxide is easily calculated, can also very easily The amount of the consumed nitric acid of this experiment and hydrogen peroxide is deducted from the nitric acid of on-hand inventory and the total amount of hydrogen peroxide, most Theoretical quantity in stock is obtained eventually.But in the practice of the analysis detection experiment of reality, any one analysis detection laboratory technician will do Theoretical consumption to 100% is difficult.Such as accidentally spilling some reagents in test operation, it can all cause actually to disappear The error of consumption and theoretical consumption.Solution is very simple, is exactly (to claim in the Work Process Management link of analysis detection Be workflow work flow) working link checked the consumptive material scene of carrying out of laboratory technician of the increase after off-test, and will Consumptive material quantity after checking is entered into Laboratory Operation System (LOS) by C terminals, then in LOS and laboratory information system (LIS) accounting arrangement is carried out to the material in whole analysis detecting system (LIS+LOS) in, the consumption of this experiment is calculated, Again make an inventory the stock of the material being consumed.
The theoretical consumption and reality of test consumable will be automatically carried out according to the designed subprogram of this management philosophy Border consumption ratio Analysis computing (theoretical consumption is that molecule/actual consumption amount is denominator).This simple ratio Analysis knot If fruit is used in as routine evaluations data in the management of analysis detection practice, it will with energetically meaning.One is Can as evaluation analysis testing staff work Stringency important evaluation indicators, the second is test run cost can be used as Evaluation index, the third is the magnitude of recruitment of test consumable can be obtained quickly, accurately index is provided for rationally buying.More than Simply enumerating these three advantages just can obviously see, one so simple ratio Analysis is just real by analysis detection Fine-grained management lifting of the room one from people to thing is tested to the management level of a higher level.
The 30th technology essential factor of the present invention is the supervision and administration organization in exclusive industry and the letter for analyzing testing agency Cease what management system should be big to usage amount in industry, the file higher to the Regulatory requirements of file and form carry out personalized Classification, and form the standard form database of the stronger file of specificity and form, so in use just can root According to needing to recall stronger specific aim from file and form standard form database and normative preferable file and form mark Quasi-mode plate, can so reduce the mistake using file and Table edit, improve office efficiency.
What such as CFDA (State Food and Drug Administration) was promulgated《Food security sampling observation food kind, inspection in the works Test project and the method for inspection》Food security inspection sampling observation it is single, wherein 4 " the safe sampling inspection sampling of state food is single " of annex It is that portion needs a form that inspector scene is filled in, it is more complicated, fill in very cumbersome.If nevertheless, Carefully compareed from the angle of technology《Food security inspects food kind, inspection project and the method for inspection in the works by random samples》The skill stated Art requirement, what existing this form of annex 4 can not be rigorous meets the technical requirements that file is stated.For example《Food security Inspect food kind, inspection project and the method for inspection in the works by random samples》There are " sampling observation amount ", " sampling observation position ", " every in many kinds The sampling observation number at one position ", " mixing the sample of sampling observation ", " sample needs to detect and back up the number rechecked " etc..When every When the sampling observation number at one position is equal with the number that sample needs detection and backup to recheck, the relatively good processing of problem, but such as It is really unequal, then need on sampling observation list clearly by " the sampling observation number at each position " and " detection of sample needs and backup The number of reinspection " is recorded respectively, and should indicate the temperature, humidity, cleaning of unpack packing handler and place and place Degree etc. and the influential respective record of sample quality.But column relevant in annex 4 only has " sampling place ", " sampling When Sample storage condition ", " sample packaging " " sample mode " fill in column, this obviously can not meet《Food security Inspect food kind, inspection project and the method for inspection in the works by random samples》The technical requirements stated, because this form can not embody sample The related contents such as sampling position, number, the fractionation situation of product in detail.It is assumed that testing result is unqualified, product counterpart is inspected by random samples Proposition is because changing in the quality that sampling observation link result in product, if now inspected by random samples according still further to the verification demanded strict technology Links, it finds that due to form can not fully meet the technical requirements of file defined and occur that responsibility is unclear can not Investigate and cause supervision and by supervision between dispute, this be obviously unfavorable for law enforcement authority.Therefore, in strict accordance with《Food security Inspect food kind, inspection project and the method for inspection in the works by random samples》The technical requirements stated, are edited out each for food classification The annex 4 " the safe sampling inspection sampling of state food is single " of food specificity is planted, is that present food security sampling observation work is compeled to be essential The problem of solving.And simplest method is by the strong standard form typing food safety supervision mechanism of annex four of specificity Database, reproduces field according to the situation of specific food, finds out and be stored in specificity in file/form standard form database Annex 4, and the column in form is filled in automatically using the relevant information of other in database is had been saved in, it is clear that it is to have Beneficial to the preciseness and operating efficiency of supervision and management.Actually CFDA and various regions FDA information management system have been set up letter Management system is ceased, and is had been realized in using the single situation of the information data Auto-writing sampling observation preserved, such as medicine Sampling observation is single, as long as the authentication code for the medicine that typing is inspected by random samples, single manufacturing enterprise, the legal person that just will automatically inspect sample by random samples of sampling observation Column of the related information Auto-writing such as representative, address to correlation.Technology essential factor that the present inventor proposes herein with Do not conflict, and be propose more refine, the standardisation requirements of more rigorous and high-specificity and unified standard.
The standardization issue of the examining report book of testing agency is also analyzed, in face of different detection samples and detection project And the batch size of product is examined, the report form of examining report book has ever-changing.In practice usually because examining report book Form and sequential write it is nonstandard and check and audit link be retired in the laboratory technician's hand drafted rewrite, especially that A little primary laboratory technicians, are usually criticized because of the lack of standardization of report writing.Therefore framework individual character in testing agency is being analyzed Change and the analysis examining report book template of specificity by force is also very necessary.
Similar situation can also be enumerated a lot, therefore the supervision and administration organization in exclusive industry and analysis testing agency Information management system should be big to usage amount in industry, the file higher to the Regulatory requirements of file and form are carried out The classification of property, and formed the standard form database of the stronger file of specificity and form be information management standardization not The link that can be lacked, although many information management systems have had many models to use for reference, the present inventor will This technology essential factor is proposed again, and is used as analysis testing laboratory's information management system framework and programming package solution Technology essential factor in scheme is the ring that whole technical solution can not be lacked.
The 31st technology essential factor of the present invention is supervision and administration organization and analysis testing agency in exclusive industry The key data information cited by table 18 below is contained in the data list structure of the database of information management system.The main number It is believed that breath refers to the data message of the database related to technical characteristic of the present invention.The data of some conventional databases Information is common due to belonging to database such as conventional human resource management, store management, handling of goods and materials, standard instrument template Common denominator data information, be similarly the requisite information for the database of information management framework that the present invention is stated, for this kind of The data message of database is just no longer set forth in following main information table and suffered.The tables of data of cited database in table 18 Information can according to specialty difference accept or reject.For example in agriculture field should using veterinary drug, agricultural chemicals, chemical fertilizer information as It is main, the relevant content of relevant food is avoided the need in environmental monitoring, etc..
Key data in the data list structure of the database of the information management system of the analysis of table 18 detection and supervisory organ Information
Review to the present invention.Above inventor comprehensively elaborates " detection and supervision message management system framework and journey The full content of the method for sequence design ", overall to look back to get up to may be summarized to be two aspects, the is the skill of the present invention on one side Art key element is divided into two parts, and (1) proposes the physical structure of the information management system of two-stage DCS features;(2) this is depended on The design of the information unit of physical structure and the planning of information data structure, it is proposed that analysis testing agency and supervision and administration organization The unification and standardization issue of information data structure.Second aspect is the advantage that the technology of the present invention is brought, and can be concluded Into it is following some, (1) using the present invention technical supervision mechanism information management system can effectively to analyze testing agency Behavior carry out real-time oversight;(2) initial data in laboratory can be traced to the source and put into effect;(3) 2 points based on more than Advantage can extend further out many benefits, and (3-1) can be by substandard product closure in manufacturing enterprise or circulation enterprise Analysis detection;(3-2) using the technology of the present invention analysis testing agency can with factum to public display from Oneself it is rigorous with it is fair, quickly draw high and itself obtain social from public credibility;(3-3) can be effectively by present by governmental input High-level public analysis testing laboratory from " sampling observation " work that is swamped with it is busy in free and then turn to low level Analysis testing agency technical supervision and technical training, the strong political affairs of picked troops of public analysis testing agency can be effectively realized; The accumulation of (3-4) with analysis detection SOP in systems is perfect, can effectively lift the basic unit in analysis detection First Line The working level of testing laboratory is analyzed, work difficulty is reduced, the deficient awkward office of basic unit analysis testing laboratory personnel is solved Face;The higher big data of confidence level that (3-5) provides detection detection by analysis to government organs and the public;(3- 6) be conducive to attracting the construction of non-government fund input third-party analysis testing laboratory and promote manufacturing enterprise, institute of circulation enterprise The analysis testing laboratory for itself high level built, and thus quickly build with the public analysis test experience of governmental investment Room is that technological core analyzes inspection by China of wing lattice of third-party analysis testing laboratory and own analysis testing laboratory of enterprise Survey the grid architecture in laboratory, and the thus significantly product quality of lifting China and technological progress.
Brief description of the drawings
The system architecture diagram of Fig. 1 analysis testing agency's generalized information management systems (LIMS)
The system architecture diagram of Fig. 2 analyses testing agency's internal independence space (LIS)
Fig. 3 by LIMS+LIS build analysis testing agency information management system system architecture diagram
The system architecture block diagram of Fig. 4 supervision and administration organizations information management system (CM-OA)
Fig. 5 analyzes testing agency's information management system and the system tray under supervisory organ's information management system internet environment Composition
Embodiment
Uniqueness sorting code number presently in connection with product, the SOP under analysis detection full information code regulation edit and SOP only The editor of one property marking code and the embodiment citing of coding method, are described in further detail the technology contents of the present invention, it is clear that implement Example is only in no way limiting of for explanation.
The classification of the product of embodiment one is the important means that standardization is realized in specification information management.But the classification of product Inventors believe that should be with reference to China authoritative file or standard or professional etiquette, and according to five classes per class two as far as possible now Several cryptoprinciples assigns the coding of uniqueness to the product of different field.The present inventor in the present embodiment to food, medicine, The product in nine fields such as cosmetics, veterinary drug, agricultural chemicals, chemical fertilizer, environmentally friendly sampling, chemical reagent, equipment is according to five classes of the invention It is exemplified below per the double-digit cryptoprinciple of class.By length is limited, citing below can only carry out schematic example, specialty Technical staff in field can voluntarily complete whole product uniqueness sorting code numbers according to following schematic example.
1st, six kinds of uniqueness sorting code numbers citing of food
1-1 is promulgated with reference to state food pharmaceuticals administration general bureau《Food safety supervision is inspected by random samples and Risk Monitoring is implemented Detailed rules and regulations》's《Food security inspects food kind, inspection project and detection method in the works by random samples》Classified 5 grades every grade of catalogue The food kind uniqueness coding citing of 2 digits is shown in Table 19.
Table 19
1-2 is with reference to GB2760《Food additives use standard》Annex E " food categorizing system " catalogue classified 5 grades every grade 2 digits food kind uniqueness coding citing be shown in Table 20
Table 20
1-3 is with reference to GB2761《Mycotoxin is limited the quantity in food》Appendix A " food classification (title) illustrates " classified 5 grades every grade 2 digits food kind uniqueness coding citing between table 21.This classification is relatively simple, lacks edible agricultural production The classification of product, therefore without the classification of the flesh of fish, pork etc., lack the classification of meat and meat products, the also classification without aquatic products.
Table 21
1-4 is with reference to GB2762《Pollutants in food is limited the quantity》Appendix A " food classification (title) illustrates " classified 5 The food kind uniqueness coding citing of every grade of 2 digits of level, is shown in Table 21.
Table 21
1-5 is with reference to GB2763《Pesticide MRL》Appendix A " food classification and measurement site " carry out The food kind uniqueness coding citing of 5 grades every grade 2 digits of classification, is shown in Table 22.The standard is due to laying particular emphasis on the agriculture in food Medicine inspection is looked into, therefore substantially former plant is in the majority, and the mainly subdivision of vegetables and fruit adds without cereal processed goods and grain milling The classification of work product, similar classification is that the finished product of grain in cereal is classified, and the classification without thick chilli sauce, meat products.
Table 22
1-6 is divided with reference to the classification for the food production license classified catalogue that state food pharmaceuticals administration general bureau promulgates The food kind uniqueness coding citing of 5 grades every grade 2 digits of class, is shown in Table 23.Lack the classification of edible agricultural product in this classification, Classification such as not oppressing, pork, etc..
Table 23
2nd, two kinds of uniqueness sorting code numbers citing of medicine.The current drug standards of China have standards of pharmacopoeia, ministry standard (new Medicine) two a variety of basic standards.Standards of pharmacopoeia has the sequence of Latin title, the stroke of medicine name and the sequence of Chinese phonetic alphabet title, English Literary fame claims four types that sort.According to the common practice of the query and search of current information management system, the present inventor recommends difference The kind of medicine is classified according to the sequence of the Chinese phonetic alphabet of Chinese Pharmacopoeia medicine name and according to the template that is ordered as of stroke And carry out medicine kind (product) uniqueness sorting code number.
5 grades every grade 2 digits that 2-1 is classified according to the sequence template of the medicine trade name Chinese phonetic alphabet of Chinese Pharmacopoeia The coding citing of medicine kind uniqueness, is shown in Table 24.
Table 24
The medicine kind for 5 grades every grade 2 digits that 2-2 is classified according to the catalog classification sequence template of Chinese Pharmacopoeia is unique Property coding citing, be shown in Table 25.
Table 25
2-3,5 grades every grade 2 digits classified according to the sorting code number template of Chinese Medical Packing Materials standard Medical Packing Materials product Uniqueness coding is planted, 26 are shown in Table.
Table 26
3rd, the specific product uniqueness classified according to the cosmetic product of GB/T18670-2002 cosmetics classification modes Coding citing, is shown in Table 27.
Table 27
4th, 5 classified with reference to the Chinese Chinese phonetic alphabet retrieval of Chinese veterinary drug pharmacopeia and the sorting technique of pharmacopeia for template The veterinary drug kind uniqueness coding of every grade of 2 digits of level.The classification recommended with reference to veterinary drug pharmacopeia carries out the classification of basic veterinary drug database.Beast Medicine pharmacopeia point one (chemicals), text has Chinese Chinese phonetic alphabet retrieval and English inspection using Chinese stroke retrieval, the end of writing Rope;Two (herbal medicine and plant medicines, plant extracts), point medicinal material and medicine materical crude slice, vegetable fat and extract, prescribed preparation and Single preparation, text has Chinese Chinese phonetic alphabet retrieval and Latin retrieval using Chinese stroke retrieval, the end of writing;Three are for animals Biological products, text is classified according to biological products classification, and the end of writing has Chinese Chinese phonetic alphabet retrieval and English retrieval. According to the common practice of the query and search of current information management system in the input mode using the Chinese phonetic alphabet, the present inventor recommends Respectively according to Chinese veterinary drug pharmacopeia nomenclature of drug the Chinese phonetic alphabet sequence and according to stroke be ordered as product of the template to medicine Plant and classified and carried out medicine kind (product) uniqueness sorting code number.
5 grades every grade 2 digits that 4-1 is classified according to the sequence template of the nomenclature of drug Chinese phonetic alphabet of Chinese veterinary drug pharmacopeia Medicine kind uniqueness coding citing, be shown in Table 28.
Table 28
The medicine kind for 5 grades every grade 2 digits that 4-2 is classified according to the catalog classification sequence template of Chinese veterinary drug pharmacopeia Uniqueness coding citing, is shown in Table 29.
Table 29
5th, two kinds of uniqueness sorting code numbers citing of agricultural chemicals:Pesticidal preparations are according to GB/T19378-2003《Formulations of pesticide name Claim and code》, agricultural chemicals national standard and pesticide industry standard and Chinese phonetic alphabet principle of classification carry out two kinds of product uniqueness point Class is encoded.
5-1 assigns uniqueness code according to the classification mode of formulations of pesticide title and code table to the agricultural chemicals of each kind Classifying rules signal table 30.
Table 30
The classification mode that 5-2 is retrieved according to the formulations of pesticide title Chinese phonetic alphabet assigns uniqueness to the agricultural chemicals of each kind The classifying rules signal table 31 of code.
Table 31
6th, the chemical fertilizer product for 5 grades every grade 2 digits classified with reference to the sorting code number template that Ministry of Agriculture's chemical fertilizer is registered Plant uniqueness coding citing and be shown in Table 32.
Table 32
7th, the uniqueness sorting code number citing of environmentally friendly sample is shown in Table 33.
Table 33
8th, the uniqueness sorting code number using chemical reagent as the test consumable of representative and unclassified stores is illustrated
The Classification of materials that 8-1 serves as theme according to the chemical reagent operation catalogue of China's establishment in 1981 is classified for template 5 grades every grade 2 digits chemical reagent kind uniqueness coding citing be shown in Table 34.
Table 34
The change for 5 grades every grade 2 digits that 8-2 is classified according to Chinese Chemical Society to the classification mode of chemical reagent for template Learn varieties of reagent uniqueness coding and be shown in Table 35.
Table 35
9th, the equipment uniqueness sorting code number citing by representative of rig for testing is shown in Table 34.The present inventor fails to have found one The template of the rig for testing classification of fixed authority.In order to ensure the integrality of database, present inventors have proposed following experiment dress Standby uniqueness sorting code number, is exemplified below, only for reference.
Table 36
Embodiment two is introduced the analysis stated using the present invention and detects full information code regulation by taking food hawthorn roll as an example Under SOP edit and SOP uniqueness encode editor and coding method.Due to the food safety detection method of hawthorn roll is whole Editor and coding out need very big length, therefore the present inventor takes passages only can illustrate that editor and coding method are limited Partial content therein.If desired, the present inventor can continue to give citing supplement.
The first step:Confirm name of product, such as fruit product is not the title that information system has been included, a kind of production of selection Product classification mode, by new product name editor ownership under the title that information system has been included.
Second step:The code of the previous section of editor's analysis detection full information code:A=product classifications are selected (for example:Food Product 1=sampling observations detailed rules and regulations, 2=GB2760,3=GB2761,4=GB2762,5=GB2763,6=food registration classification);B=should Item category code;C=levels of the standard selection (00=state foods standard, other=provincial provincial standard);D=examines standard soon If (being not belonging to fast inspection standard, D=KJ000000, the expression of years is 0000, standard code is 00;If examining standard soon, As KJ201706 represent be 2017 promulgate the 06th standard.D are joined together with C, it is possible to which whether difference is country The fast inspection standard that the fast inspection standard promulgated or each province or enterprise oneself are promulgated, such as 00-KJ201706, which is meant that, belongs to country No. 06 fast inspection standard promulgated in 2017.Such as 61-KJ201606 represents No. 06 fast inspection that Shaanxi Province is promulgated for 2016 Standard.In same province, the numbering for the fast inspection standard promulgated by people's government at the provincial level is defined, and belongs to enterprise or testing agency certainly The fast inspection standard that oneself takes, it should being organized in standard after the numbering of the standard of provincial government's promulgation and leaving certain Open numbering again at space.The fast inspection standard that such as enterprise of Shaanxi Province puts on record oneself, can be compiled as 61-KJ201751, before 50 space encoders are left to ensure the standard code of enough provincial governments.
For example:The food Sort Code that food hawthorn roll=standard food title " preserved fruit " is write according to six kinds of food classification models It is as shown in the table:
Table 37:The A-D for the uniqueness code table that hawthorn roll (preserved fruit) is classified according to six kinds of food of non-fast inspection national standard detection The coding of position is as shown in the table
Table 37
Sequence number Classification model Food uniqueness code
1 State food inspects safely detailed rules for the implementation (2017 editions) by random samples 1-1701010000-00-KJ000000
2 GB2760《Food additives use standard》 2-0401020801-00-KJ000000
3 GB2761《Mycotoxin is limited the quantity in food》 3-0102050000-00-KJ000000
4 GB2762《Pollutants in food is limited the quantity》 4-0102050000-00-KJ000000
5 GB2763《Pesticide MRL》 5-2005000000-00-KJ000000
6 What CFDA was promulgated《Classified catalogue is permitted in food production》 6-1701010000-00-KJ000000
3rd step:All standards and extension standard under the product coding are searched (preferably by the technology people of professional domain Correlation is related to standard and is all integrated under the ProductName by member according to the title under product classification, is confirming A, B, C above Code after, all standard directories under the product code are according to 1,2,3,4 grades sequentially show.)
4th step:Build examination criteria and detection project sequence list it is as shown in the table [with food hawthorn roll (title= Preserved fruit) detection exemplified by].
The standard and detection project and detection method project order permutation table (food name of the detected product of table 38:Mountain Short, bristly hair or beard is rolled up)
Table 38
5th step:Write analysis detection full information code aft section code, and write SOP form citing, It see the table below 39:
Table 39
The Section 1 of (citing 1) hawthorn roll (standard food title=preserved fruit) detects " analyzing and detect complete for " examination by sensory organs " Message code " and SOP, see the table below 40:
Table 40
Section 3 detection " the method for moisture inspection-the first-directly do of (citing 2) hawthorn roll (standard food title=preserved fruit) " the analysis detection full information code " and SOP of dry method ", see the table below 41:
Table 41
" four methods of moisture inspection-the-karr is taken for the Section 3 detection of (citing 3) hawthorn roll (standard food title=preserved fruit) " the analysis detection full information code " and SOP of not method ", see the table below 42:
Table 42
Section 4 detection " the preserved fruit sanitary standard-Section 1-lead of (citing 4) hawthorn roll (standard food title=preserved fruit) " the analysis detection full information code " and SOP of content detection-graphite furnace atomic absorption spectrometry -1 ", see the table below 43:
Table 43
Section 4 detection " the preserved fruit sanitary standard-Section 2-copper of (citing 5) hawthorn roll (standard food title=preserved fruit) " the analysis detection full information code " and SOP of content detection-atomic absorption spectrography (AAS)-flame method -1 ", see the table below 44:
Table 44
" preserved fruit sanitary standard-Section 3-is total for the Section 4 detection of (citing 6) hawthorn roll (standard food title=preserved fruit) The-the first method of arsenic content detection inductively coupled plasma mass spectrometry-inductively coupled plasma mass spectrometry 1- Microwave Digestions " " analysis detection full information code " and SOP, see the table below 45:
Table 45
Section 4 detection " the preserved fruit sanitary standard-Section 5-food of (citing 7) hawthorn roll (standard food title=preserved fruit) Product health hygiene inspection-candy, cake, " the analysis detection full information generation of preserved fruit inspection-Section 1-total plate count detection-1 Code " and SOP, see the table below 46:
Table 46
6th step:The example above 1-7 and Liu are planted " analysis detection full information code " after food sorting code number merges (SOP codes) is as shown in following table 47:
Table 47:The part detection operation SOP of seven detection projects of food hawthorn roll code table
Coding key to detecting control limit data code:As seen from the above table, the I items of SOP codes are " detection control limits Degrees of data code ", in the example above, inventor is designed as " 00001-00007 ".This is in order to which the numeral for representing H is actual Upper is exactly " the link indications " of an information, can be that, according to programmer's self-defining, the operation with standard is not related, Address using the code of I as indications or buffering area etc. are placed on the purpose is to the Con trolling index for detecting this.
The SOP of above-mentioned hawthorn paper analysis detection citing is only the part that hawthorn paper analysis detects selectable SOP, It is many that the analysis of actually hawthorn roll detects that SOP also has, and the detection of such as lead just has 22 SOP, and the detection of copper has 12 SOP, total plate count detection SOP has 2 etc..Exactly because this complexity of examination criteria, just result in detection practice The complexity of reading standard and edit operation SOP.But after the above is made in order, it is possible to looked into by means of information management system The quick and convenient of retrieval is ask, complicated SOP being illustrated on the interface of computer in order is easily browsed for operator, and It is accurate in order easily to carry out testing preceding preparation, experimental implementation, complete experiment note according to the condition of own analysis testing laboratory The examining report of specification is analyzed and provided to record and experiment calculation.
In above-mentioned SOP codings, due to there is product classification uniqueness Code location, so even coding has occurred below The sequence of sequence, the pre-treatment of complete the same extension standard and detection project, the sequence of detection method are just the same, also will not There are duplicate SOP codings.Therefore above-mentioned coding is uniqueness, because can not possibly appear in complete one in a product The examination criteria of sample is supporting.
Embodiment three is situated between by taking a standard in the state food safety quick detection method standard that CFDA is newly promulgated as an example Introduce the volume that the SOP under the analysis detection full information code regulation stated using the present invention is edited and SOP uniqueness is encoded Collect and coding method.If desired, the present inventor can continue to give citing supplement.For the SOP of quick detection standard, due to Standard extension and more sample-pretreating methods are not present and in the absence of more detection methods, phase in the standard of quick detection To fairly simple, but along with the uniqueness point of food after above added with the standard code of the fast inspection standard of state food safety Class is encoded, and is not in the phenomenon that SOP codings hit face.There is a phenomenon it is noted that state food safety examines standard soon It is wide using variety protection, that is to say, that the code level being applicable in the rank of food uniqueness sorting code number is higher, such as KJ201706 suitable for pork, beef etc. animal muscle tissue Clenbuterol, Ractopamine and salbutamol it is quick Determine, be that pork, beef are divided into a classification in some food sorting techniques.
1st, by taking aquatic products as an example, to the quick detection colloidal gold immunity chromatography (KJ201701) of aquatic products Malachite Green Fast inspection SOP codings
First step criteria classification is as shown in following table 48.
The SOP of the quick detection colloidal gold immunity chromatography of second step aquatic products Malachite Green writes coding schedule, sees below Shown in table 49:
Table 49:
3rd being encoded to for step aquatic products sorting code number Table A-D see the table below 50:
Table 50
Sequence number Classification model The SOP uniqueness codes of the quick detection colloidal gold immunity chromatography of aquatic products Malachite Green
1 State food inspects safely detailed rules for the implementation (2017 editions) by random samples 1--00-KJ201701-3203000000-01-00-00-00-nnnnn-01-00-00-00-01-00-00-00-
2 GB2760《Food additives use standard》 2--00-KJ201701-0900000000-01-00-00-00-nnnnn-01-00-00-00-01-00-00-00
3 GB2761《Mycotoxin is limited the quantity in food》 3--00-KJ201701- without
4 GB2762《Pollutants in food is limited the quantity》 4--00-KJ201701-0901010000-01-00-00-00-nnnnn-01-00-00-00-01-00-00-00
5 GB2763《Pesticide MRL》 5--00-KJ201701-2707000000-01-00-00-00-nnnnn-01-00-00-00-01-00-00-00
6 What CFDA was promulgated《Classified catalogue is permitted in food production》 6--00-KJ201701- without
2nd, with the colloidal gold immunochromatographimethod quick determination method of Clenbuterol, Ractopamine and salbutamol in beef (method two) solid phase extraction SOP writes coding schedule.
The first step writes SOP according to standard and SOP related data section is encoded, and see the table below 51:
Second step completes beef muscle tissue sorting code number table-(method two) solid phase according to food uniqueness code coding and extracted The SOP full codings followed the example of, see the table below 52:
Coding key to detecting control limit data code:From citing above, the I items of SOP codes are " detections Control limit data code ", in the example above, inventor is designed as nnnnn, and this is to further indicate that the numeral of I " the link indications " of actually one information, can be that, according to programmer's self-defining, the operation with standard does not have Relation, an address or the buffering using the code of I as indications are placed on the purpose is to the Con trolling index for detecting this Area etc..Therefore represented with 00001-00007 to be represented with nnnnn with citing above in citing above, be exactly in order to from two Individual different angle illustrates where the real meaning of this data cell of the I items of SOP codes.

Claims (28)

1. detection and supervision message management system framework and the method for programming, it is characterised in that analyze testing agency at one It is interior, the Global Information management system design for analyzing testing agency is divided into two parts, a part is laboratory information system, Its basic function is to be absorbed in the instrumentation tubes that each analysis detection business section office in analysis testing agency, administration and logistics manage section office Manage information, coordinations, supervise and examine and check and each analyze the information of each business section office in testing agency, the letter related to testing agency operation Breath, data and analysis detecting data collect, collected, and the thus large data center of component analysis testing agency, laboratory Information system can be gathered can also be transplanted work after the company information of supervised entities, product information, product satellite positioning information For the information management system of supervisory organ;Another part is Laboratory Operation System, and its basic function is to be absorbed in analysis detection The management of the digitizing equipment in independent experiment space in mechanism in each physical significance and to analysis detection operation it is related Initial data collection and test data sheet, the independent experiment space in so-called physical significance is defined as only with a set of experiment The regional space of room operating system, can be a room or an analysis detection basic equipment laboratory building module or multiple Room or multiple analyses detection basic equipment laboratory building module,
The physical structure for the collecting and distributing controlling feature of two-stage that laboratory information system is collectively formed with several Laboratory Operation Systems Under analysis testing agency initial data trace to the source LIMS,
The office automation information management system of supervision and administration organization is on the basis of laboratory information system physical structure, to increase Plus product satellite positioning information management system and laboratory monitoring management system are collectively formed,
Message tube containing separate space Laboratory Operation System, the analysis testing agency of product satellite positioning information management system Reason system and the information of the supervisory organ containing laboratory supervision message management system and product satellite positioning information management system The connected Internet architecture of management system,
The information management system of testing agency and the information management system of corresponding administrative supervision and administration organization are analyzed in collection inspection product When the inspection product and product information of the information and counterpart of counterpart and supervision counterpart, the minimal information list related to supervision and management The integrated information data structure of member should be unified and compatible, and its item position position or order in information data structure should one Cause, and it is possible thereby to form the information data structure of standardization,
Analysis testing agency information management system and administrative supervision management organization information management system to censorship people with And when examining product information and supervision counterpart and its product information being gathered, by censorship people information, inspection product information, supervision counterpart Information, the product information of supervision counterpart are merged into one or a kind of information data structure,
The information management system of supervision and administration organization and analysis testing agency should be big to usage amount in industry, to the rule of file Plasticity requires higher file and the personalized classification of form progress, and forms the mark of the stronger file of specificity and form Quasi- template database,
The tables of data knot of the database of the information management system of supervision and administration organization and the information management system of analysis testing agency Sampling (supervision) personnel motion trail satellite positioning information database, product satellite positioning information database are contained in structure, is divided The active equipment communication interface of analysis testing agency is with equipping parameter setting table database, including censorship people information, inspection product information, prison Counterpart's information is superintended and directed, database that the product information of counterpart is merged together is supervised, includes least unit entry and most Quantity register information and test consumable deposit position code under subsection, test consumable storage temperature data, experiment consumption The test consumable inventory database of material term of validity data, include rig for testing placement location code, normal/maintenance code, meter Measure the rig for testing database of time limit code information, with reference to the promulgation of state food pharmaceuticals administration general bureau《Food security is supervised Superintend and direct sampling observation and Risk Monitoring detailed rules for the implementation》's《Food security inspects food kind, inspection project and detection method in the works by random samples》's The food kind uniqueness coded data storehouse for 5 grades every grade 2 digits that catalogue is classified, reference national standard GB2760《Food is added Agent uses standard》Annex E " food categorizing system " the food kind uniqueness of 5 grades every grade 2 digits classified of catalogue Coded data storehouse, reference national standard GB2761《Mycotoxin is limited the quantity in food》Appendix A " food classification (title) illustrates " carry out The food kind uniqueness coded data storehouse of 5 grades every grade 2 digits of classification, reference national standard GB2762《Pollutants in food is limited the quantity》 5 grades every grade 2 digits being classified of appendix A " food classification (title) illustrates " food kind uniqueness coded data storehouse, With reference to national standard GB2763《Pesticide MRL》Appendix A " food classification and measurement site " classified 5 The food kind uniqueness coded data storehouse of every grade of 2 digits of level, the food promulgated with reference to state food pharmaceuticals administration general bureau The food kind uniqueness coded data storehouse of classified 5 grades of every grade of 2 digits of production permit classified catalogue, food peace Full inspection is surveyed according to national standard database, food safety detection method national standard database, with reference to state food safety standard SOP databases edit and with uniqueness code, food security quick determination method national standard database, reference country Food security quick detection is standard compliant and there is the SOP databases of uniqueness code, each provincial government to promulgate food peace Full inspection surveys method standard database, the food safety detection method standard database that each province region state-owned enterprise industry is put on record, with reference to province Level government promulgates that the food safety detection method standard that food safety detection method standard and each province region state-owned enterprise industry are put on record is compiled Volume and with uniqueness code SOP databases, according to Chinese Pharmacopoeia medicine name the Chinese phonetic alphabet sequence template divided The medicine kind uniqueness coded data storehouse of 5 grades every grade 2 digits of class, the catalog classification sequence template progress according to Chinese Pharmacopoeia The medicine kind uniqueness coded data storehouse of 5 grades every grade 2 digits of classification, the sorting code number template according to Chinese Medical Packing Materials standard The Medical Packing Materials kind uniqueness coded data storehouse for 5 grades every grade 2 digits classified, according to national standard GB/T18670-2002 make up The cosmetics kind uniqueness coded data storehouse for 5 grades every grade 2 digits that product classification mode is classified, the Chinese veterinary drug pharmacopeia of reference The Chinese Chinese phonetic alphabet be retrieved as the veterinary drug kind uniqueness coded data storehouse for 5 grades every grade 2 digits that template is classified, reference National standard GB/T19378-2003《Formulations of pesticide title and code》And enter according to the classification mode of formulations of pesticide title and code table The pesticide species uniqueness coded data storehouse of 5 grades every grade 2 digits of row classification, reference national standard GB/T19378-2003《Pesticide agent Type title and code》And 5 grades every grade 2 digits being classified of classification mode retrieved according to the formulations of pesticide title Chinese phonetic alphabet Pesticide species uniqueness coded data storehouse, 5 grades classified with reference to the sorting code number template that Ministry of Agriculture chemical fertilizer is registered are often The fertilizer variety uniqueness coded data storehouse of 2 digits of level, the mark for the environment protectment protection (HJ/T) promulgated with reference to Environmental Protection Department The pattern of quasi- classification and sequence carries out the environmental protection sample kind uniqueness coding for 5 grades every grade 2 digits classified Database, 5 grades classified according to Chemistry In China reagent association offer in 1981 by reagent purposes and discipline classification for template The chemical reagent kind uniqueness coded data storehouse of every grade of 2 digits, the chemical reagent operation catalogue according to China's establishment in 1981 The Classification of materials served as theme is the chemical reagent kind uniqueness coded data storehouse for 5 grades every grade 2 digits that template is classified, divided Analysis examining report standard form database, issued historical analysis examining report book and it is matched have recorded it is active Equip " shadow address " database, the single classification editor standard form data of food safety supervision mechanism inspection product sampling observation of operational factor Storehouse, supervisory organ's fine and confiscation material registration management database, analysis testing agency this 37 letters of inspection product registration management database Cease database composition.
2. the method with supervision message management system framework and programming is detected according to claim 1, it is characterised in that experiment Room information system is by information management system, information processing centre of analysis testing agency database, sampling (supervision) personnel motion Track satellite positioning information management system, product satellite positioning information management system, client terminal A and satellite positioning information Receiving/emitter is collectively constituted.
3. the method with supervision message management system framework and programming is detected according to claim 1, it is characterised in that experiment Room operating system is by digital (data) collection and equipment management system, experiment information database and experimental implementation management system System, equipment management terminal B, experimental implementation terminal C and incidental active equipment are collectively constituted, and the active equipment is finger ring Border control equipment, including air-conditioning system, air cleaning and conditioning system, detection of particulates system, ventilating system, illuminator, pernicious gas Detecting system, anti-explosion fire fire-fighting system etc.), various conventional analytical instruments, including various photometers and optics, spectral class dress Standby, chromatogram class equipment, mass spectrum kind equipment, Electrochemical Detection class equipment, dissolution and disintegration tester, balance and assay balance class equipment, Incubator class equipment, sterilization class equipment, heating and dried class equipment, Biohazard Safety Equipment and superclean bench class equipment, various systems Cold charge is standby, centrifugation vibration class is equipped, crush and emulsification homogenate class equipment, ultrasound class equipment, autoclave sterilization equipment, pumping dress of supplying gas Standby, analysis detection auxiliary equipment and instrument, the environmental Kuznets Curves equipment for being detected inspection product deposit position, ups power are (containing silicon photocell Group generates electricity and wind power generation management system), recording camera class equipment.
4. the method with supervision message management system framework and programming is detected according to claim 1, it is characterised in that food The information management system of safety analysis testing agency is with the information management system of food security administrative supervision management organization to censorship People and inspection product information and supervision counterpart and its product information collection data structure, be by information system typing when system Sequence number, supervision counterpart's title or supervision counterpart name code, supervision counterpart's registration province, city, county (area) administrative area Draw code, supervision counterpart's registration township (town, street) address information code, supervision counterpart property coding, the relative life of supervision The sorting code number of industry battalion, supervision counterpart legal representative title, supervision counterpart legal representative relevant information and contact method generation Code, supervision counterpart quality owner title, supervision counterpart quality owner relevant information and contact method code, product/ Need sample ID, the registration mark of the sample of product/needs detection, product/sample sorting code number, the product approval text of detection Number, whether expire coding, product of product authentication code declare prescription, production technology code and relevant information code, product manufacturing Link supplementary material detail code, product manufacturing link supplementary material lot number, product manufacturing link supplementary material place of production message code, product Date of manufacture, the detection qualitative classification coding of product/sample, inspection condition are to people's title, inspection product counterpart relevant information and contact Mode code, the character of product/sample, specification, packaged information code, production/environmental protection sample lot number, product/inspection Link sorting code number, product/Sample storage humiture limit, keeping life deadline, product/sample storage residing for product (transport) place (position) message code, product/sample whether there is examining report coding, product/inspection product detection project and detection number According to, tester's message code, product/inspection product examine survey and whether qualified encode, detect that sample takes out/censored time, examining report promulgation Time, the grading of supervision counterpart prestige and history prestige rating information code, supervisory organ's title, supervision director title, prison Superintend and direct director's relevant information and contact method code this 38 information units compositions.
5. the method with supervision message management system framework and programming is detected according to claim 1, it is characterised in that standard The information data structure of change is the association mode of the use information code in information data structure, to information carry out 2 grades, 3 grades, 4 Level, 5 grades, 6 grades and the other information of more stages are carefully divided and cut, and are consequently formed multi-level information data structure pattern.
6. the method with supervision message management system framework and programming is detected according to claim 1, it is characterised in that standard The information data structure of change is that the information management system of the information management system and the administrative supervision mechanism that analyze testing agency should be by Supervise the product of counterpart or the title of kind, sample or examine the authority that the title of product is promulgated according to administrative supervision management organization The title of the product classification of the product classification of file or retrieval or national standard or ministry standard or professional standard or trade classification The name of the product classification of convention is referred to as " title ", and is product in information system or kind, sample or the " standard for examining product Title " assigns the code of a uniqueness in information system, and this code can be digital or alphabetical or word, But regular should follow.
7. the method with supervision message management system framework and programming is detected according to claim 1, it is characterised in that standard The information data structure of change is to define the double-digit classifying rules of every grade of Pyatyi as all product in information management system of the present invention The classifying rules of " title " coding of kind/article/inspection product/sample.So-called 1-5 grades can be referred to as meaning 1 grade, 2 grades, 3 grades, 4 grades, 5 grades, it can also be referred to as meaning class, subclass, secondary class, kind, also secondary kind, the side different according to A, B, C, D, E or I, II, III, IV, V etc. Method represents the difference between 1-5 grades.Every grade of (according to the decimal system) 2-3 digit represents, i.e. 001-999 or 01-99, it is recommended to use 01-99 can meet most of exhaustive division demand.
8. the method with supervision message management system framework and programming is detected according to claim 1, it is characterized in that standardization Information data structure be according in the detection product assortment of object/inspection product, examination criteria, examination criteria to analysis examination criteria A specific detection project, the control limit of the detection project as defined in examination criteria, detect specified in examination criteria The order of a kind of detection method of detection object/inspection product specified in a kind of pre-treating method of object (inspection product), examination criteria Enter edlin, and be consequently formed a kind of specific analyze of the specific detection project of detection object/inspection product and detect operating procedure SOP (Standard Operating Procedure), synchronization detects that the SOP's of operating procedure is above-mentioned every to the analysis edited The uniqueness coding that one information unit is standardized, the set of these uniqueness coding just constitutes the uniqueness of the SOP Code, SOP codes are actually the unique identification for detecting that an information unit for detecting operating method of object is integrated, this Individual unique identification just characterizes the full information data structure of this analyzing detecting method of detection object/kind.
9. the method with supervision message management system framework and programming is detected according to claim 1, it is characterised in that standard The information data structure of change is the material information data structure for defining unique identification, recording laboratory consumptive material from procurement request to The change procedure for the whole life cycle that material disappears.Wherein include least unit entry and least unit used in material Under quantity register information data item, the least unit of material is " gram " (g) for solid, is " milli for liquid Rise " (ml), milligram (mg), milliliter (ml) can also be extended to, this for some expensive materials for example reference substance, standard items, For standard reagent, smaller measurement unit is conducive to the management of more fine test consumable and material.
10. the method with supervision message management system framework and programming is detected according to claim 1, it is characterised in that standard The information data structure of change is to analyze testing agency to carry out the rule that progress equipment in the room or separate space of experiment places station Draw and assign uniqueness code identification to the station of each placement equipment,
11. the method with supervision message management system framework and programming is detected according to claim 1, it is characterised in that standard The information data structure of change is to carry out uniqueness to the active equipment that analysis testing result can be had influence in analysis testing agency Code identification, the code identification includes the information of the station uniqueness coding of active equipment.
12. the method with supervision message management system framework and programming is detected according to claim 1, it is characterised in that standard The information data structure of change is by experimentation links form in Laboratory Operation System comprising experiment original record Change data inputting, complete experimentation track record, first choice recommends the tabular recording mode of the form of a thing one, and each form Possess uniqueness serial number coding in each test data sheet, identification means are provided for the editor of laboratory report.
13. according to claim 3 Laboratory Operation System be by digital (data) collection and equipment management system is incidental has Source is equipped, it is characterised in that can be using electricity between active equipment and Laboratory Operation System that Laboratory Operation System is administered Cable communication, fiber optic communications (data/address bus) and wireless telecommunications, recommended in the case where condition is permitted wireless communication mode with And wireless and wired (data/address bus) mashed up communication mode or wired (data/address bus) communication mode.Wireless digital transmission communicates skill Art mainly using those short distances low cost wireless digital transmission pattern, recommend using ZigBee, bluetooth, infrared ray, WiFi, UWB, RFID, NFC, preferred wireless communication data transmission mode and the mashed up data-transmission mode of Wireless-wire, wireless mode are first Select ZigBee, WiFi.
14. it can be adopted between the active equipment and Laboratory Operation System administered according to claim 3 Laboratory Operation System With cable communication, fiber optic communications (data/address bus) and wireless telecommunications, it is characterised in that the digital collection in Laboratory Operation System Need to carry out periodic information exchange with the active equipment in equipment management system and Laboratory Operation System compass of competency Increase periodic clock alignment link in program, by the digital collection and equipment management system in Laboratory Operation System according to Active equipment of the clock frequency of oneself into domain sends active equipment in clock alignment signal, domain and carries out response adjustment, makes this The information gathering and instruction of communication cycle are sent to be carried out according to the fiducial time order of clock alignment signal.
15. according to claim 3 Laboratory Operation System be by digital (data) collection and equipment management system is incidental has Source is equipped, it is characterised in that the active dress for being administered intelligent power socket and intelligent power distribution cabinet/case as experiment management system Stand-by power source supply port.
16. according to claim 3 Laboratory Operation System be by digital (data) collection and equipment management system is incidental has Source is equipped, it is characterised in that Laboratory Operation System takes form to disguise active equipment parameter setting link in process of the test The pattern of standby parameter settings data carries out the setting of equipment parameter, and a kind of each numeral dress of equipment parameter setting form correspondence Standby communications protocol.
17. according to claim 3 Laboratory Operation System be by digital (data) collection and equipment management system is incidental has Source is equipped, it is characterized in that the equipment that the active equipment in Laboratory Operation System region within the jurisdiction must be into Laboratory Operation System Management system carry out information registering, registration will be made up of two parts, one be the equipment newly used equipment parameter setting table The table registration of equipment parameter setting is carried out in Laboratory Operation System, another is to be equipped in when active after energization starts immediately to institute The Laboratory Operation System of administration sends revival notification, and thus starts the information friendship of equipment and Laboratory Operation System Mutually.
18. according to claim 3 Laboratory Operation System be by digital (data) collection and equipment management system is incidental has Various conventional analytical instruments in the equipment of source, it is characterized in that what Laboratory Operation System was equipped to there is the analytical instrument class of work station Testing result take work station output file take passages and using work station testing result output file as attachment management pattern.
19. according to claim 3 Laboratory Operation System be by digital (data) collection and equipment management system is incidental has Various conventional analytical instruments in the equipment of source, it is characterized in that Laboratory Operation System in detection and analysis operating process to being related to phase The electrical operation parameter information for closing equipment is recorded, and proves analysis as the attached report supporting with analysis examining report It is true and reliable that the analysis detection that examining report is relied on is operated.
20. according to the experimental implementation terminal C of claim 3 Laboratory Operation System, it is characterized in that in the C of Laboratory Operation System When terminal landing experimental implementation management system and entrance experimental implementation interface, the interface of terminal C computer screen is divided into two Individual part a, part is used for concrete operation step (SOP, the standard operation of analysis detection experiment for showing analysis detection experiment Program), another part is used to analyze the original data record in detection test operation flow.
Supervised 21. the information data structure standardized according to claim 6 is the information management system for analyzing testing agency with administrative The product classification of the information management system of mechanism is superintended and directed, it is characterized in that when occurring different have due to the difference of professional etiquette or standard When authoritative product classification pattern and different " title ", information management system and the administrative supervision of testing agency are analyzed The information management system of mechanism should design correlation retrieval and specification subroutine, solve different classifications and different " title " it Between in information management system information exchange inquiry and exchange substitution problem.
22. according to the full information data structure of claim 8 analyzing detecting method, it is characterized in that in the full letter of analyzing detecting method Cease the information unit that structuring food prods safety standard is distinguished based on the code of the provincial administrative region of China stroke in data structure code To distinguish four kinds of above-mentioned standards systems.Wherein regulation 00 is state food safety standard, and 99 be that state food is safely and fast fixed Property examination criteria, be used to distinguish with the front two code of the provincial administrative division of representative in six digits of china administration zoning code Food security company standard in the local food security standard of provincial promulgation and the province region.
23. according to the material information data structure of claim 9 unique identification, it is characterized in that definition has unique identification's Material goods yard information data structure, recording laboratory consumptive material (comprising expendable material, equipment accessory, can also include office, after Duty waits not the directly material and consumptive material related to experiment, or abbreviation material) the whole Life Cycle of the disappearance from procurement request to material The change in location information of phase.
24. according to the material information data structure of claim 9 unique identification, it is characterized in that material is in information management system Sequence number using order arranging and encoding successively, sequence number is upgraded and used when material is called automatically after material disappearance The retrieval of " first in first out, the last-in, last-out " of storehouse recalls pattern.Sequence number in material typing information management system should be adopted With order arranging and encoding successively, when the material of typing in information management system is using finishing, the information of the material is in letter Sequence code during breath management system typing will disappear automatically, and material sequence code followed by will be promoted automatically, while message tube The automatic transfer history of the information of the material is stored and preserves information management system when maximum is no more than the time of 24 months by reason system System is purged again.
25. the change of the whole life cycle disappeared according to claim 9 recording laboratory consumptive material from procurement request to material Journey, it is characterized in that regarding the ratio of the theoretical consumption of test consumable and actual consumption amount as examination analysis detection experiment preciseness Important performance assessment criteria.
26. according to the full information data structure of claim 8 analyzing detecting method, it is characterized in that full information data structure is by eating Product classification model code, food Sort Code, geographic code, the standard code of quick determination method standard, one-level detection project Code, secondary detection item code, three-level detection project code, level Four detection project code, detection control limit data code, Locate before inspection product pre-treating method one-level code, inspection product pre-treating method secondary code, inspection product pre-treating method three-level code, inspection product Reason method level Four code, one-level analyzing detecting method code, secondary analysis detection method code, three-level analyzing detecting method generation This 17 information units of code, level Four analyzing detecting method code are constituted.
27. according to the material information data structure of claim 9 unique identification, it is characterized in that material information data structure be by The sequence numbering of material, Classification of materials name of an article code, buyer codes, apply to purchase authorizer's code, apply to purchase approver's code, adopt Purchase/preparation handler code, specification information code, monovalent message code, purchase quantity code, material total price message code, life Produce company-information code, material auxiliary information code, material manufacturer production lot number/code, material quality guarantee period overdue expiration date Phase, material package message code, the storage temperature limit of material, log-on message management system/entry time, check and accept/check people Code, custodian's code, material storage room code, material storage room station code, material deposit position code, minimum list Position message code, calculate material quantity or code, material by least unit and receive people's code, material and receive person approving's code, thing Material receive approver's code, material receive handler's code, material receive material under time, least unit receive quantity/code, Whether be that Self-made reagent is identified, material whether there is identifies this 32 information units compositions.
28. it is by testing in Laboratory Operation System according to the original data record of claim 12,16 test data sheets Journey links tabular data inputting, it is characterized in that complete experiment original record form system is constituted by four kinds of forms, The specific data structure of these four record forms is:
(1) active (electrical equipment) equipment electrical control parameter set form as:
(2) the test data sheet form that solution is prepared is:
(3) the test data sheet form weighed is:
(4) form of experiment determination data record is:
A B C D * * The numbering of this form Testing result title As a result 1 As a result 2 …… As a result n ……
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