CN107268298A - A kind of new dyeing technique of cotton face fabric - Google Patents

A kind of new dyeing technique of cotton face fabric Download PDF

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Publication number
CN107268298A
CN107268298A CN201710502626.6A CN201710502626A CN107268298A CN 107268298 A CN107268298 A CN 107268298A CN 201710502626 A CN201710502626 A CN 201710502626A CN 107268298 A CN107268298 A CN 107268298A
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CN
China
Prior art keywords
face fabric
cotton face
oyster shell
shell whiting
fabric
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
CN201710502626.6A
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Chinese (zh)
Inventor
叶志进
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Jingning She Nationality Autonomous County Animal Husbandry Arts And Crafts Factory
Original Assignee
Jingning She Nationality Autonomous County Animal Husbandry Arts And Crafts Factory
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Jingning She Nationality Autonomous County Animal Husbandry Arts And Crafts Factory filed Critical Jingning She Nationality Autonomous County Animal Husbandry Arts And Crafts Factory
Priority to CN201710502626.6A priority Critical patent/CN107268298A/en
Publication of CN107268298A publication Critical patent/CN107268298A/en
Withdrawn legal-status Critical Current

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    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/34General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/673Inorganic compounds
    • D06P1/67333Salts or hydroxides
    • D06P1/6735Salts or hydroxides of alkaline or alkaline-earth metals with anions different from those provided for in D06P1/67341
    • DTEXTILES; PAPER
    • D06TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06PDYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P3/00Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
    • D06P3/58Material containing hydroxyl groups
    • D06P3/60Natural or regenerated cellulose

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Coloring (AREA)

Abstract

The invention discloses a kind of new dyeing technique of cotton face fabric, selection calcined shell powder is dyed simultaneously as the carrier of dyestuff to cotton face fabric, good Color can be not only reached, while can dye, sand washing is synchronously completed, assigns fabric special pseudo-classic style of missing old times or old friends;Conventional sand washing can also be avoided to use environmental pollution caused by silica, and the anti-microbial property of cotton face fabric can be strengthened;In dyeing course, by controlling the porosity, particle diameter and usage amount of oyster shell whiting, good Color is reached;In summary, dyeing of the invention is a kind of fabric handling process of novel environment friendly.

Description

A kind of new dyeing technique of cotton face fabric
Technical field
The present invention relates to a kind of processing method of fabric, belong to field of textiles, and in particular to a kind of new dye of cotton face fabric Color technique.
Background technology
With the raising of living standard, requirement of the consumers in general to the quality and wearability of dress-goods is no longer It is confined to warming, consumer had both needed comfortably, more pursue diversified, personalized and distinctive product.Such as pseudo-classic style of missing old times or old friends Jeans, buttocks and knee is specially made and fades, or even the state galled, this way be typically using decolourant, The special equipment such as sand washing is handled.And for the clothes that cotton face fabric is made, because the fabric of strength ratio jeans is much lower, because This clothes that can not be made using being generally similar to make the method for jeans to woolen fabric carries out doing old processing.
The content of the invention
The purpose of the present invention is that there is provided a kind of new dyeing technique of cotton face fabric to overcome above-mentioned the deficiencies in the prior art.
To achieve the above object, the present invention uses following technical proposals:
A kind of new dyeing technique of cotton face fabric, comprises the following steps:
A, by fresh shell with after salt acid soak, use clear water cleaning, drying, be crushed to particle diameter for 1-3mm;
B, oyster shell whiting calcined into 2-4h under 880-900 DEG C of high temperature;
C, by the oyster shell whiting after calcining and the common wet grinding of natural dye solution to particle diameter it is 200-500 μm, obtains micron order Dye oyster shell whiting;
D, micron order dyed in oyster shell whiting and cotton face fabric addition washing machine, 60-80min is stirred together in 40-50 DEG C of warm water;
E, cotton face fabric is taken out again after, carry out after simply cleaning, then rinsed with clear water, dry under for acid condition, you can.
It is preferred that, in described step B, after calcining, the porosity of oyster shell whiting is 10-20%.
It is preferred that, in described step D, the amount ratio of oyster shell whiting and cotton face fabric is(2-3):10.
It is preferred that, in described step D, the micron order dyeing oyster shell whiting after dyeing is handled is by repeating calcination processing Afterwards, the organic matter such as natural dye can be decomposed, and retrieve calcined shell powder, then by with the common wet grinding of natural dye solution Afterwards, particle diameter is only needed to meet requirement, it is possible to reuse.
It is preferred that, in described step E, described acid condition is the slightly acidic condition that pH is 5.5-6.2.
The new dyeing technique of the present invention, selection calcined shell powder is dyed and sand as the carrier of dyestuff to cotton face fabric Wash, not only can reach good Color while sand washing can be completed, dyeing, sand washing are synchronously completed, healthy, environmentally friendly, low Energy consumption, generation sewage is few, and chemical addition agent usage amount is few, and sewage disposal is simple.
Traditional sand is replaced from calcined shell powder(Silica)Carrier as dyeing and sand washing mainly has as follows Benefit:One is after silica carries out sand washing and dried, to have nano level silica dioxide granule thing and be attached to web surface, one Under fixed condition, these particulate matters meeting air inlet carries out harm environmental and human health impacts, but the main component of oyster shell whiting is carbon Sour calcium, is carried out after pickling, and calcium carbonate reaction is decomposed, and does not result in harm;Two be that calcined shell powder carries out new dye with cotton face fabric After color technique, partial calcination oyster shell whiting is polished to generate nano level little particle, into the inside of cotton face fabric, so as to provide Certain antibacterial effect.
The difficult point of the present invention is:One is the particle diameter and usage amount for controlling oyster shell whiting, can if oyster shell whiting particle diameter is excessive The surface of cotton fiber is damaged, so that low-fiber intensity is dropped, so as to influence the service life of fabric;And oyster shell whiting particle diameter It is too small, just do not reach the effect of sand washing;Two be the porosity for controlling oyster shell whiting, for the purposes of preventing during sand washing to cotton fiber Surface damage, the porosity of oyster shell whiting needs to control more than 10%, therefore the present invention is according in oyster shell whiting calcination process Correlated response formula, the temperature that have selected 880-900 DEG C is calcined, at a temperature of this, will not be by Decomposition of Calcium Carbonate into calcium oxide, together When the stomata of oyster shell whiting can be tried one's best expansion.
Correlated response formula is (under conditions of oxygen is sufficient):
Organic matter=H2O+ carbohydrate+CO2(700 DEG C of >);
CaCO3=CaO+CO2(900 DEG C of >).
Beneficial effects of the present invention:
Present invention selection calcined shell powder is dyed and sand washing as the carrier of dyestuff to cotton face fabric, can not only be reached good Color can dye simultaneously, sand washing is synchronously completed, and assigns fabric special pseudo-classic style of missing old times or old friends;Routine can also be avoided Sand washing uses environmental pollution caused by silica, and can strengthen the anti-microbial property of cotton face fabric;In dyeing course, pass through The porosity, particle diameter and the usage amount of oyster shell whiting are controlled, good Color is reached;Natural dye and calcined shell powder coordinate and made With rear, good anti-bacterial effect;In summary, dyeing of the invention is a kind of fabric handling process of novel environment friendly.
Embodiment
With reference to embodiment, the present invention will be further elaborated, it should explanation, the description below merely to The present invention is explained, its content is not defined.
Tested below using natural dye of gordon euryale seed shell.
Embodiment 1
A kind of new dyeing technique of cotton face fabric, comprises the following steps:
A, by fresh shell with after salt acid soak, use clear water cleaning, drying, be crushed to particle diameter for 1-3mm;
B, oyster shell whiting calcined into 2.5h under 890 DEG C of high temperature;
C, by the oyster shell whiting after calcining and the common wet grinding of natural dye solution to particle diameter it is 200-500 μm, obtains micron order Dye oyster shell whiting;
D, micron order dyed in oyster shell whiting and cotton face fabric addition washing machine, 75min is stirred together in 45 DEG C of warm water;
E, cotton face fabric is taken out again after, carry out after simply cleaning, then rinsed with clear water, dry under for acid condition, you can.
In described step B, after calcining, the porosity of oyster shell whiting is 18-20%.
In described step C, the solid content of natural dye solution is 30%, and the mass ratio with oyster shell whiting is 10:1.
In described step D, the amount ratio of oyster shell whiting and cotton face fabric is 2.5:10.
In described step E, described acid condition is the slightly acidic condition that pH is 6.0.
Embodiment 2
A kind of new dyeing technique of cotton face fabric, comprises the following steps:
A, by fresh shell with after salt acid soak, use clear water cleaning, drying, be crushed to particle diameter for 1-3mm;
B, oyster shell whiting calcined into 4h under 900 DEG C of high temperature;
C, by the oyster shell whiting after calcining and the common wet grinding of natural dye solution to particle diameter it is 200-500 μm, obtains micron order Dye oyster shell whiting;
D, micron order dyed in oyster shell whiting and cotton face fabric addition washing machine, 60min is stirred together in 50 DEG C of warm water;
E, cotton face fabric is taken out again after, carry out after simply cleaning, then rinsed with clear water, dry under for acid condition, you can.
In described step B, after calcining, the porosity of oyster shell whiting is 10-12%.
In described step C, the solid content of natural dye solution is 40%, and the mass ratio with oyster shell whiting is 5:1.
In described step D, the amount ratio of oyster shell whiting and cotton face fabric is 3:10.
In described step E, described acid condition is the slightly acidic condition that pH is 5.5.
Embodiment 3
A kind of new dyeing technique of cotton face fabric, comprises the following steps:
A, by fresh shell with after salt acid soak, use clear water cleaning, drying, be crushed to particle diameter for 1-3mm;
B, oyster shell whiting calcined into 2h under 880 DEG C of high temperature;
C, by the oyster shell whiting after calcining and the common wet grinding of natural dye solution to particle diameter it is 200-500 μm, obtains micron order Dye oyster shell whiting;
D, micron order dyed in oyster shell whiting and cotton face fabric addition washing machine, 80min is stirred together in 40 DEG C of warm water;
E, cotton face fabric is taken out again after, carry out after simply cleaning, then rinsed with clear water, dry under for acid condition, you can.
In described step B, after calcining, the porosity of oyster shell whiting is 12-15%.
In described step C, the solid content of natural dye solution is 25%, and the mass ratio with oyster shell whiting is 6:1.
In described step D, the amount ratio of oyster shell whiting and cotton face fabric is 2:10.
In described step E, described acid condition is the slightly acidic condition that pH is 6.2.
Comparative example 1
Calcining heat in embodiment 1 is improved to 910 DEG C, remaining preparation condition is constant.
Comparative example 2
Calcination time in embodiment 1 is shortened, so as to be 5-8% by the porosity of oyster shell whiting, remaining preparation condition is constant.
Comparative example 3
By the size controlling of the oyster shell whiting in the step C in embodiment 1 at 600-800 μm;Remaining preparation condition is constant.
Comparative example 4
Natural dye of gordon euryale seed shell in embodiment 1 is replaced with into reactive dye, remaining preparation condition is constant.
After testing, embodiment 1-3 and the sample of comparative example 1, before and after dyeing, the tensile strength and tearing resistance of cotton face fabric are equal Without obvious difference;But the sample of comparative example 2 and 3, before and after dyeing, the tensile strength and tearing resistance of cotton face fabric decline super Cross 20%.
After testing, embodiment 1-3 and comparative example 2-3 sample, to Escherichia coli, Candida albicans and golden yellow grape The bacteriostasis rate of coccus is more than 95%;And it is less than 20%, comparative example without the bacteriostasis rate of the cotton face fabric of dyeing processing in embodiment 1 The bacteriostasis rate of 1 sample is less than 50%, and the bacteriostasis rate of the sample of comparative example 4 is between 80-90%.
After testing, the WASHING COLOR FASTNESS of 1-3 of the embodiment of the present invention and the sample of comparative example 1,3,4 can reach 4 grades, right The WASHING COLOR FASTNESS of the sample of ratio 2 can also reach 3 grades.
The foregoing is only a preferred embodiment of the present invention, but protection scope of the present invention be not limited thereto, Any one skilled in the art the invention discloses technical scope in, technique according to the invention scheme and its Inventive concept is subject to equivalent substitution or change, should all be included within the scope of the present invention.

Claims (5)

1. the new dyeing technique of a kind of cotton face fabric, it is characterised in that comprise the following steps:
A, by fresh shell with after salt acid soak, use clear water cleaning, drying, be crushed to particle diameter for 1-3mm;
B, oyster shell whiting calcined into 2-4h under 880-900 DEG C of high temperature;
C, by the oyster shell whiting after calcining and the common wet grinding of natural dye solution to particle diameter it is 200-500 μm, obtains micron order Dye oyster shell whiting;
D, micron order dyed in oyster shell whiting and cotton face fabric addition washing machine, 60-80min is stirred together in 40-50 DEG C of warm water;
E, cotton face fabric is taken out again after, carry out after simply cleaning, then rinsed with clear water, dry under for acid condition, you can.
2. the new dyeing technique of cotton face fabric as claimed in claim 1, it is characterised in that in described step B, after calcining, The porosity of oyster shell whiting is 10-20%.
3. the new dyeing technique of cotton face fabric as claimed in claim 1, it is characterised in that in described step D, oyster shell whiting with The amount ratio of cotton face fabric is(2-3):10.
4. the new dyeing technique of cotton face fabric as claimed in claim 1, it is characterised in that in described step E, described acid Property condition is the slightly acidic condition that pH is 5.5-6.2.
5. the new dyeing technique of cotton face fabric as claimed in claim 1, it is characterised in that in described step D, by dyeing Micron order dyeing oyster shell whiting after processing may be reused after repeating calcination processing.
CN201710502626.6A 2017-06-27 2017-06-27 A kind of new dyeing technique of cotton face fabric Withdrawn CN107268298A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201710502626.6A CN107268298A (en) 2017-06-27 2017-06-27 A kind of new dyeing technique of cotton face fabric

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Application Number Priority Date Filing Date Title
CN201710502626.6A CN107268298A (en) 2017-06-27 2017-06-27 A kind of new dyeing technique of cotton face fabric

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108660795A (en) * 2018-06-12 2018-10-16 江西京东实业有限公司 A kind of environment protection type dye method of pure cotton knitting face fabric
CN108909074A (en) * 2018-07-09 2018-11-30 绍兴市柯桥皓质华琚纺织品设计有限公司 A kind of fire-retardant, waterproof, radiation protection, gold stampped shell fabric and its preparation process

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106012591A (en) * 2016-06-21 2016-10-12 湖州新隆龙丝绸印花有限公司 Environment-friendly sand washing and dyeing technology for habotai real silk fabric
CN106087470A (en) * 2016-06-21 2016-11-09 湖州新隆龙丝绸印花有限公司 A kind of environment-friendly type terylene fabric sand washing dyeing
CN106835681A (en) * 2016-12-30 2017-06-13 长兴宝诺纺织科技有限公司 A kind of silk fabric granite-wash technique

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106012591A (en) * 2016-06-21 2016-10-12 湖州新隆龙丝绸印花有限公司 Environment-friendly sand washing and dyeing technology for habotai real silk fabric
CN106087470A (en) * 2016-06-21 2016-11-09 湖州新隆龙丝绸印花有限公司 A kind of environment-friendly type terylene fabric sand washing dyeing
CN106835681A (en) * 2016-12-30 2017-06-13 长兴宝诺纺织科技有限公司 A kind of silk fabric granite-wash technique

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
四川省纺织工业厅科技情报中心站编: "《织物后整理新工艺新技术选编》", 31 December 1994 *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108660795A (en) * 2018-06-12 2018-10-16 江西京东实业有限公司 A kind of environment protection type dye method of pure cotton knitting face fabric
CN108909074A (en) * 2018-07-09 2018-11-30 绍兴市柯桥皓质华琚纺织品设计有限公司 A kind of fire-retardant, waterproof, radiation protection, gold stampped shell fabric and its preparation process

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Application publication date: 20171020

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