CN107267966A - A kind of continuous chrome-plated process of pin cloth - Google Patents
A kind of continuous chrome-plated process of pin cloth Download PDFInfo
- Publication number
- CN107267966A CN107267966A CN201710514014.9A CN201710514014A CN107267966A CN 107267966 A CN107267966 A CN 107267966A CN 201710514014 A CN201710514014 A CN 201710514014A CN 107267966 A CN107267966 A CN 107267966A
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- Prior art keywords
- pin cloth
- plating
- chrome
- carried out
- pin
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
- C23C18/16—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by reduction or substitution, e.g. electroless plating
- C23C18/52—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by reduction or substitution, e.g. electroless plating using reducing agents for coating with metallic material not provided for in a single one of groups C23C18/32 - C23C18/50
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
- C23C18/16—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by reduction or substitution, e.g. electroless plating
- C23C18/18—Pretreatment of the material to be coated
- C23C18/1803—Pretreatment of the material to be coated of metallic material surfaces or of a non-specific material surfaces
- C23C18/1824—Pretreatment of the material to be coated of metallic material surfaces or of a non-specific material surfaces by chemical pretreatment
- C23C18/1837—Multistep pretreatment
- C23C18/1844—Multistep pretreatment with use of organic or inorganic compounds other than metals, first
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
- C23C18/16—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by reduction or substitution, e.g. electroless plating
- C23C18/18—Pretreatment of the material to be coated
- C23C18/1803—Pretreatment of the material to be coated of metallic material surfaces or of a non-specific material surfaces
- C23C18/1848—Pretreatment of the material to be coated of metallic material surfaces or of a non-specific material surfaces by electrochemical pretreatment
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- Chemical & Material Sciences (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Electrochemistry (AREA)
- Inorganic Chemistry (AREA)
- Electroplating Methods And Accessories (AREA)
Abstract
The invention discloses a kind of continuous chrome-plated process of pin cloth, technology groove is sequentially passed through using system drive pin cloth is unreeled, using chemical plating, chromium plating is carried out to pin cloth surface, the processing step includes, 1) surface treatment, oil removal treatment is carried out to pin cloth surface；2) polish, chemical polishing is carried out to pin cloth surface；3) activate, use volume ratio to carry out activation process, time to pin cloth surface for 30 40% hydrochloric acid：1‑5min；4) chromium plating, in pin cloth chrome-faced, using chemical plating to pin cloth plating hard chromium on surface；5) dry, the continuous plating of pin cloth is realized by supporting unwinding equipment, the chromium plating length of pin cloth can reach endless in theory.
Description
Technical field
The present invention relates to weaving part overlay coating field, more particularly to a kind of continuous chrome-plated process of pin cloth.
Background technology
The chrome-plated process of pin cloth, can only realize the pin cloth chrome-faced of regular length, and length is less than 3 meters, it is impossible to realize pin
The overlength chromium plating of cloth；It is poor using mechanical polishing, surface finish in surface preparation, or electrobrightening, electric current mistake
Greatly, pin cloth structure is destroyed, causes the crown of pin cloth to burn；Chromium plating uses electroplating technique, because current density is uneven, causes plating
Layer is in uneven thickness, influences quality of coating.
Therefore the chrome-plated process of pin cloth is caused, quality is low, efficiency is low, production cost is high.
The content of the invention
The technical problems to be solved by the invention are to provide a kind of continuous chrome-plated process of pin cloth, pass through supporting unwinding equipment
To realize the continuous plating of pin cloth, the chromium plating length of pin cloth can reach endless in theory, caused in the prior art to solve
Above-mentioned multinomial defect.
To achieve the above object, the present invention provides following technical scheme：A kind of continuous chrome-plated process of pin cloth, using unreeling
System drive pin cloth sequentially passes through technology groove, using chemical plating, chromium plating is carried out to pin cloth surface, the processing step includes,
1) it is surface-treated, oil removal treatment is carried out to pin cloth surface；
2) polish, chemical polishing is carried out to pin cloth surface；
3) activate, use volume ratio to carry out activation process, time to pin cloth surface for 30-40% hydrochloric acid：1-5min；
4) chromium plating, in pin cloth chrome-faced, using chemical plating to pin cloth plating hard chromium on surface；
5) dry.
It is preferred that, in the surface treatment step, including electrochemical deoiling and electrochemical degreasing.
It is preferred that, the electrochemical deoiling uses alkaline degreaser, and oil removing agent concentration is 50-70g/L, and temperature is 50-70 DEG C,
Time is 5-30min.
It is preferred that, the electrochemical degreasing uses alkaline degreaser, and degreaser negative electrode concentration is 30-60g/L, and degreaser is cloudy
Pole concentration is 50-80g/L, and temperature is 50-70 DEG C, and the time is 15-180sec, and current density is 1-10ASD, and electrode is using stainless
Steel or graphite.
It is preferred that, in the polishing step, the mode for using impregnated ground agent carries out electrochemical deoiling, and temperature control exists
17 DEG C, pH value is 2.0-3.5, time 1-3min, stings erosion speed 2-7 μm/minute.
It is preferred that, carry out adverse current washing between the surface treatment and polishing；Adverse current washing is carried out between activation and chromium plating；
Adverse current washing is carried out between chromium plating and drying.
It is preferred that, adverse current washing is carried out using pure water between the chromium plating and drying.
Beneficial effect using above technical scheme is：The continuous chrome-plated process of pin cloth of the present invention, using unwinding equipment and right
The special chrome plating equipment for answering the technology groove of each processing step to constitute carries out chromium plating, realizes the continuous plating of pin cloth, in theory pin cloth
Chromium plating length can reach endless, substantially increase the efficiency of pin cloth chromium plating, realize automation mechanized operation, reduction is produced into
This.
Chemical polishing, the quality of chromium plating after raising, while using chemical plating come hard chrome plating are used before chromium plating, it is ensured that
Coating on pin cloth is uniform.
Embodiment
The following detailed description of the preferred embodiment of the present invention.
Embodiment 1
A kind of continuous chrome-plated process of pin cloth, technology groove is sequentially passed through using system drive pin cloth is unreeled, right using chemical plating
Pin cloth surface carries out chromium plating, and the processing step includes,
1) it is surface-treated, oil removal treatment is carried out to pin cloth surface；Including electrochemical deoiling and electrochemical degreasing.
Electrochemical deoiling uses alkaline degreaser, and oil removing agent concentration is 50g/L, and temperature is 70 DEG C, and the time is 30min.
Electrochemical degreasing uses alkaline degreaser, and degreaser negative electrode concentration is 30g/L, and degreaser negative electrode concentration is 50g/L,
Temperature is 70 DEG C, and the time is 180sec, and current density is 10ASD, and electrode uses stainless steel or graphite.
2) polish, chemical polishing is carried out to pin cloth surface；In polishing step, the mode for using impregnated ground agent is carried out
Electrochemical deoiling, temperature control is at 17 DEG C, and pH value is 2.0, time 3min, stings erosion μm/minute of speed 2.
3) activate, use volume ratio to carry out activation process, time to pin cloth surface for 30% hydrochloric acid：5min；
4) chromium plating, in pin cloth chrome-faced, using chemical plating to pin cloth plating hard chromium on surface；
5) dry.
Embodiment 2
A kind of continuous chrome-plated process of pin cloth, technology groove is sequentially passed through using system drive pin cloth is unreeled, right using chemical plating
Pin cloth surface carries out chromium plating, and the processing step includes,
1) it is surface-treated, oil removal treatment is carried out to pin cloth surface；Including electrochemical deoiling and electrochemical degreasing.
Electrochemical deoiling uses alkaline degreaser, and oil removing agent concentration is 70g/L, and temperature is 50 DEG C, and the time is 5min.
Electrochemical degreasing uses alkaline degreaser, and degreaser negative electrode concentration is 60g/L, and degreaser negative electrode concentration is 80g/L,
Temperature is 50 DEG C, and the time is 15sec, and current density is 1ASD, and electrode uses stainless steel or graphite.
2) polish, chemical polishing is carried out to pin cloth surface；In polishing step, the mode for using impregnated ground agent is carried out
Electrochemical deoiling, temperature control is at 17 DEG C, and pH value is 3.5, time 1min, stings erosion μm/minute of speed 7.
3) activate, use volume ratio to carry out activation process, time to pin cloth surface for 40% hydrochloric acid：1min；
4) chromium plating, in pin cloth chrome-faced, using chemical plating to pin cloth plating hard chromium on surface；
5) dry.
Embodiment 3
A kind of continuous chrome-plated process of pin cloth, it is characterised in that sequentially pass through technology groove using system drive pin cloth is unreeled, adopt
With chemical plating, chromium plating is carried out to pin cloth surface, the processing step includes,
1) it is surface-treated, oil removal treatment is carried out to pin cloth surface；Including electrochemical deoiling and electrochemical degreasing.
Electrochemical deoiling uses alkaline degreaser, and oil removing agent concentration is 60g/L, and temperature is 60 DEG C, and the time is 18min.
Electrochemical degreasing uses alkaline degreaser, and degreaser negative electrode concentration is 45g/L, and degreaser negative electrode concentration is 65g/L,
Temperature is 60 DEG C, and the time is 90sec, and current density is 5ASD, and electrode uses stainless steel or graphite.
2) polish, chemical polishing is carried out to pin cloth surface；In polishing step, the mode for using impregnated ground agent is carried out
Electrochemical deoiling, temperature control is at 17 DEG C, and pH value is 2.8, time 2min, stings erosion μm/minute of speed 4.
3) activate, use volume ratio to carry out activation process, time to pin cloth surface for 35% hydrochloric acid：3min；
4) chromium plating, in pin cloth chrome-faced, using chemical plating to pin cloth plating hard chromium on surface；
5) dry.
Adverse current washing is carried out between surface treatment and polishing；Adverse current washing is carried out between activation and chromium plating；Chromium plating and drying
Between carry out adverse current washing, wherein, chromium plating and drying between using pure water carry out adverse current washing.
Electrochemical deoiling agent uses a kind of multi-functional, the not non-foam powder degreaser of phosphate-containing and silicate, can
It is effective to remove stainless steel, zinc, nickel, a variety of lubricants and grease of copper and its alloy surface.
In adding procedure, the determination of the addition to adding degreaser, point following several steps,
1) 10ml tank liquor is drawn, is placed in beaker, 100mlDI water is added；
2) 4-6 drop phenolphthalein indicators are added；
3) titrated with 1.0N hydrochloric acid standard solution by red to colourless as terminal；
4) addition of degreaser is the addition of 7 times of hydrochloric acid standard solution.
Electrolytic degreasing agent one kind is multi-functional, and the non-foam powder degreaser of phosphate-containing and silicate, can not go effectively
Except stainless steel, zinc, nickel, a variety of lubricants and grease of copper and its alloy surface.
In adding procedure, the determination of the addition to adding electrolytic degreasing agent, point following several steps,
1) 10ml tank liquor is drawn, is placed in beaker, 100mlDI water is added；
2) 4-6 drop phenolphthalein indicators are added；
3) titrated with 1.0N hydrochloric acid standard solution by red to colourless as terminal；
4) addition of degreaser is the addition of 8.28 times of hydrochloric acid standard solution.
The grinding preparation of reagents mode has two ways,
A kind of water for first injecting 1/3 volume cell body, addition 8-12% (v/v) grinding reagent；
Another is the water for first injecting 1/3 volume cell body, addition 12-13.5% (v/v) grinding reagent and 25% (v/
V) hydrogen peroxide.
-- -- washing -- polishing -- washing, in polishing using 30-40% (v/v) hydrochloric acid activation that specific step is washing
It is preceding thoroughly to clean and remove surface oxide layer by activation.
The continuous chrome-plated process of pin cloth of the present invention, using unwinding equipment and each processing step of correspondence technology groove composition it is special
Chromium plating is carried out with chrome plating equipment, the continuous plating of pin cloth is realized, the chromium plating length of pin cloth can reach endless in theory, carry significantly
The high efficiency of pin cloth chromium plating, realizes automation mechanized operation, reduces production cost.
Chemical polishing, the quality of chromium plating after raising, while using chemical plating come hard chrome plating are used before chromium plating, it is ensured that
Coating on pin cloth is uniform.
Existing similar-type products on the market, black pin cloth (being by processing, only surface polishing) unit price 200/m members；
400 yuan/m of white pin cloth (passing through simple process) unit price；High standard pin cloth unit price 800-900 members/m, are made using the application technique
Pin cloth, high standard pin cloth is equal in quality, and theoretic processing cost is 200 yuan/endless.
The cost price of product is greatly reduced, great economic benefit is produced.
Above-described is only the preferred embodiment of the present invention, it is noted that for one of ordinary skill in the art
For, without departing from the concept of the premise of the invention, various modifications and improvements can be made, these belong to the present invention
Protection domain.
Claims (7)
1. a kind of continuous chrome-plated process of pin cloth, it is characterised in that sequentially pass through technology groove using system drive pin cloth is unreeled, is used
Chemical plating, chromium plating is carried out to pin cloth surface, and the processing step includes,
1) it is surface-treated, oil removal treatment is carried out to pin cloth surface；
2) polish, chemical polishing is carried out to pin cloth surface；
3) activate, use volume ratio to carry out activation process, time to pin cloth surface for 30-40% hydrochloric acid：1-5min；
4) chromium plating, in pin cloth chrome-faced, using chemical plating to pin cloth plating hard chromium on surface；
5) dry.
2. the continuous chrome-plated process of pin cloth according to claim 1, it is characterised in that in the surface treatment step, including
Electrochemical deoiling and electrochemical degreasing.
3. the continuous chrome-plated process of pin cloth according to claim 2, it is characterised in that the electrochemical deoiling uses alkaline degreasing
Agent, oil removing agent concentration is 50-70g/L, and temperature is 50-70 DEG C, and the time is 5-30min.
4. the continuous chrome-plated process of pin cloth according to claim 2, it is characterised in that the electrochemical degreasing is removed using alkalescence
Finish, degreaser negative electrode concentration is 30-60g/L, and degreaser negative electrode concentration is 50-80g/L, and temperature is 50-70 DEG C, and the time is
15-180sec, current density is 1-10ASD, and electrode uses stainless steel or graphite.
5. the continuous chrome-plated process of pin cloth according to claim 1, it is characterised in that in the polishing step, use
The mode of impregnated ground agent carries out electrochemical deoiling, and temperature control is at 17 DEG C, and pH value is 2.0-3.5, time 1-3min, stings erosion speed
2-7 μm/minute.
6. the continuous chrome-plated process of pin cloth according to claim 1, it is characterised in that enter between the surface treatment and polishing
Row adverse current is washed；Adverse current washing is carried out between activation and chromium plating；Adverse current washing is carried out between chromium plating and drying.
7. the continuous chrome-plated process of pin cloth according to claim 6, it is characterised in that using pure between the chromium plating and drying
Water carries out adverse current washing.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710514014.9A CN107267966A (en) | 2017-06-29 | 2017-06-29 | A kind of continuous chrome-plated process of pin cloth |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710514014.9A CN107267966A (en) | 2017-06-29 | 2017-06-29 | A kind of continuous chrome-plated process of pin cloth |
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| CN107267966A true CN107267966A (en) | 2017-10-20 |
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| CN201710514014.9A Pending CN107267966A (en) | 2017-06-29 | 2017-06-29 | A kind of continuous chrome-plated process of pin cloth |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111364073A (en) * | 2020-02-25 | 2020-07-03 | 光山白鲨针布有限公司 | Preparation process and product of anticorrosive wear-resistant chromium-based card clothing |
| CN115821577A (en) * | 2022-09-21 | 2023-03-21 | 光山白鲨针布有限公司 | Surface treatment method of elastic card clothing and anti-corrosion wear-resistant coating elastic card clothing |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111364073A (en) * | 2020-02-25 | 2020-07-03 | 光山白鲨针布有限公司 | Preparation process and product of anticorrosive wear-resistant chromium-based card clothing |
| CN111364073B (en) * | 2020-02-25 | 2021-06-04 | 光山白鲨针布有限公司 | Preparation process and product of anticorrosive wear-resistant chromium-based card clothing |
| CN115821577A (en) * | 2022-09-21 | 2023-03-21 | 光山白鲨针布有限公司 | Surface treatment method of elastic card clothing and anti-corrosion wear-resistant coating elastic card clothing |
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