CN107254230A - A kind of preparation method of environmental protection coating material for underground parking - Google Patents
A kind of preparation method of environmental protection coating material for underground parking Download PDFInfo
- Publication number
- CN107254230A CN107254230A CN201610994717.1A CN201610994717A CN107254230A CN 107254230 A CN107254230 A CN 107254230A CN 201610994717 A CN201610994717 A CN 201610994717A CN 107254230 A CN107254230 A CN 107254230A
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- CN
- China
- Prior art keywords
- preparation
- environmental protection
- coating
- pigment
- underground parking
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D161/00—Coating compositions based on condensation polymers of aldehydes or ketones; Coating compositions based on derivatives of such polymers
- C09D161/04—Condensation polymers of aldehydes or ketones with phenols only
- C09D161/06—Condensation polymers of aldehydes or ketones with phenols only of aldehydes with phenols
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D193/00—Coating compositions based on natural resins; Coating compositions based on derivatives thereof
- C09D193/04—Rosin
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/14—Paints containing biocides, e.g. fungicides, insecticides or pesticides
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
Abstract
The invention discloses a kind of preparation method of the environmental protection coating material for underground parking, its processing step is as follows：（1）Select raw material；（2）Melting is refined；（3）Preceding white silk；（4）It is scattered；（5）Reconcile and mix colours；（6）Filtering；（7）Packaging.It is an object of the invention to provide a kind of to overcome the shortcomings of in prior art; carry out the Paint preparation technology of processing composite effectively and reasonably; its simple to operate, proportioning is stable; one layer of adsorption layer is provided with inside paint can; the volatile materials come out available for an absorption part from coating; the diffusion of gas is inhibited to a certain extent, and protection people's is healthy.
Description
Technical field
The present invention relates to chemical technology field, a kind of preparation side of the environmental protection coating material for underground parking is specifically referred to
Method.
Background technology
Traditional environment-friendly materials mainly have the flexible environment friendly material such as environmentally friendly coiled material, environmental protection coating material, sealing cement, and with water
Based on mud base material, the rigid environment-friendly materials of addition liquid medicine agent and other auxiliary agents.China's major part environment-friendly engineering is using traditional ring
Protect material, Traditional Environmental-protection material exist loss of properties on aging, tensile strength it is low, it is temperature sensitive the shortcomings of.Traditional Environmental-protection is applied
Material is used for roofing environmental protection, easily cause aging, it is dry and cracked, the phenomenon such as deform, fracture, being layered；It is multiple for shape for environmental friendly indoor
Miscellaneous place, constructional difficulties, and to Seepage, quality is more difficult to ensure, people's every few years will spend substantial amounts of fund
Reprocessed with labour, not only confused the normal life, work and the production order of people, and influence whole building building
Service life.
The content of the invention
It is an object of the invention to provide a kind of to overcome the shortcomings of in prior art, the processing carried out effectively and reasonably is answered
The Paint preparation technology of condensation material, its simple to operate, proportioning is stable, and one layer of adsorption layer is provided with inside paint can, be can be used for
The volatile materials that an absorption part comes out from coating, inhibits the diffusion of gas to a certain extent, protects people
It is healthy.
The present invention is achieved through the following technical solutions：A kind of preparation method of environmental protection coating material for underground parking, its
Processing step is as follows：
（1）Select raw material：By weight percentage, emulsion carriers 35-60 parts, 20-45 parts of pigment, 20-40 parts of base-material, auxiliary agent 5-20
Part, the emulsion carriers include phenolic resin, industrial residue, tail from least one of ethanol, methanol, isopropanol, base-material
Ore deposit, rosin, pigment is at least one of chrome oxide green, ultramarine, auxiliary agent include defoamer, film forming agent, dispersant, thickener,
Nertralizer and preservative；
（2）Melting is refined：By above-mentioned phenolic resin, rosin melting, temperature control at 110 DEG C~150 DEG C, and by industrial residue,
Base-material after above-mentioned processing, is then dissolved in ethanol or methanol or isopropanol by mine tailing grind into powder, through filtering, extracts pure
High phenolic resin-waste residue the solution of degree；
（3）Preceding white silk：Pigment, phenolic resin-waste residue solution are reached into uniform exchange by high-speed stirred in preceding experienced groove, it is fully wet
The admixture of profit, obtains graining paste；
（4）It is scattered：By step（3）In obtained graining paste, reach that pigment is dispersed and scattered by the grinding of decentralized medium
Fineness reaches the state of coating requirement；
（5）Reconcile and mix colours：In mediation groove, pass through the input of auxiliary agent and various uses additive, assign the various mechanicalnesses of coating
Energy and other functions, and pass through the secondary input of pigment, adjust the aberration of coating；
（6）Filtering：Filtering through filtration core and silk, filters out the impurity in coating；
（7）Packaging：Coating after above-mentioned filtering is packaged in paint can through bottle placer；
Wherein, phenolic resin is also bakelite, also known as phenolic moulding powder.Originally it was colourless or yellowish-brown transparency, market sale often adds
Toner and in the color such as red, yellow, black, green, brown, blue, have particle, powdered.Weak acid resistant and weak base, meet strong acid and decompose, meet
Highly basic corrodes.It is water insoluble, it is dissolved in the organic solvents such as acetone, alcohol, phenolic resin has good acid resistance, power
Performance, heat resistance are learned, is widely used in the industries such as environment-friendly engineering, adhesive, fire proofing, grinding wheel manufacture；
Rosin is soluble in various organic solvents, and easily film forming, glossy, is one of base stock of coating；Rosin is in paint
In effect be to make paint bright in color, fast drying, paint film is smooth difficult for drop-off.
Further, the step（2）In, temperature control is at 135 DEG C~145 DEG C.
Further, the step（4）In, device therefor is RS-16 type bitubular sand mills.
Further, the step（5）In, additive can be sodium pyrosulfite or bitumastic solution.
Further, the step（7）In, paint can interior skin is provided with adsorbed film.
The present invention is a kind of Paint preparation technology of processing composite effectively and reasonably, and its simple to operate, proportioning is steady
It is fixed, one layer of adsorption layer is provided with inside paint can, the volatile materials come out available for an absorption part from coating,
The diffusion of gas is inhibited to a certain extent, and protection people's is healthy.
Embodiment
The present invention is described in further detail with reference to embodiment, but the implementation of the present invention is not limited to this,
Without departing from the idea case in the present invention described above, according to ordinary skill knowledge and customary means, various replace is made
Change and change, all should be included within the scope of the invention.
Embodiment 1：
A kind of preparation method of environmental protection coating material for underground parking described in the present embodiment, its processing step is as follows：
（1）Select raw material：By weight percentage, 35 parts of emulsion carriers, 20 parts of pigment, 20 parts of base-material, 5 parts of auxiliary agent, the emulsion
Carrier selects ethanol, and base-material includes phenolic resin, industrial residue, mine tailing, rosin, and pigment is chrome oxide green, and auxiliary agent includes froth breaking
Agent, film forming agent, dispersant, thickener, nertralizer and preservative；
The defoamer is the mixture of brokenly bubble polymer and polysiloxane solution, and the defoamer accounts for the quality hundred of the auxiliary agent
Fraction is 34%；
The film forming agent is diethylene glycol dimethyl ether, and the mass percent that the film forming agent accounts for the auxiliary agent is 34%；
The dispersant is polyacrylic acid sodium salt, and the mass percent that the dispersant accounts for the auxiliary agent is 8%；
The thickener is the swollen polyacrylic acid of anion alkali soluble, and the mass percent that the thickener accounts for the auxiliary agent is 8%；
The nertralizer is low molecule organic amine compound, and the mass percent that the nertralizer accounts for the auxiliary agent is 8%；
The preservative is isothiazolinone derivatives, benzimidazole esters, Dao Weixier -75,1,2- benzisothiazoles -3-
At least one of ketone, the mass percent that the preservative accounts for the auxiliary agent is 8%.
（2）Melting is refined：By above-mentioned phenolic resin, rosin melting, temperature control is at 110 DEG C~150 DEG C, and by industry
Base-material after above-mentioned processing, is then dissolved in ethanol or methanol or isopropanol by waste residue, mine tailing grind into powder, through filtering, carries
Produce the high phenolic resin of purity-waste residue solution；
（3）Preceding white silk：Pigment, phenolic resin-waste residue solution are reached into uniform exchange by high-speed stirred in preceding experienced groove, it is fully wet
The admixture of profit, obtains graining paste；
（4）It is scattered：By step（3）In obtained graining paste, reach that pigment is dispersed and scattered by the grinding of decentralized medium
Fineness reaches the state of coating requirement；
（5）Reconcile and mix colours：In mediation groove, pass through the input of auxiliary agent and various uses additive, assign the various mechanicalnesses of coating
Energy and other functions, and pass through the secondary input of pigment, adjust the aberration of coating；
（6）Filtering：Filtering through filtration core and silk, filters out the impurity in coating；
（7）Packaging：Coating after above-mentioned filtering is packaged in paint can through bottle placer；
Wherein, the step（2）In, temperature control is at 135 DEG C；Step（4）In, device therefor is sanded for the RS-16 types bitubular
Machine；Step（5）In, additive can be sodium pyrosulfite；Step（7）In, paint can interior skin is provided with adsorbed film.
Coating property is tested：
According to country building material industry standard JC/T984-2005 to having done impermeability test using the embodiment of the present invention, by 6.3cm,
It is tested after 6.4cm, 6.5cm shaping, it was demonstrated that its impermeability pressure reaches 3.4MPa, there is good impervious effect.
According to country building material industry standard JC/T984-2005 to being tested using the shrinkage factor of the embodiment of the present invention,
Shrinkage factor is 0.03%.
According to country building material industry standard JC/T958-2005 to having carried out abrasion test using the embodiment of the present invention, in mill
When wiping 200 times, 0.05g only have lost.
According to country building material industry standard JC/T894-2001 to having carried out degradation using the embodiment of the present invention, 3 are done
Block 10 × 10 × 40CM test blocks, its compression strength is tested after 45 degree of ultraviolets irradiate 250 hours, and for 67.6MPa, (blank is real
Block is 45.2MPa).
The experiment of freeze thawing resistance Rapid Circulation has been carried out to what is be made using the embodiment of the present invention according to GBJ82-85 national standards,
Its mass loss 0%, relative resilient modulus 81.4%.
Embodiment 2：
A kind of preparation method of environmental protection coating material for underground parking described in the present embodiment, its processing step is as follows：
（1）Select raw material：By weight percentage, 55 parts of emulsion carriers, 40 parts of pigment, 30 parts of base-material, 15 parts of auxiliary agent, the emulsion
Carrier selects isopropanol, and base-material includes phenolic resin, industrial residue, mine tailing, rosin, and pigment is ultramarine, auxiliary agent include defoamer,
Film forming agent, dispersant, thickener, nertralizer and preservative；
The defoamer is the mixture of brokenly bubble polymer and polysiloxane solution, and the defoamer accounts for the quality hundred of the auxiliary agent
Fraction is 34%；
The film forming agent is diethylene glycol dimethyl ether, and the mass percent that the film forming agent accounts for the auxiliary agent is 34%；
The dispersant is polyacrylic acid sodium salt, and the mass percent that the dispersant accounts for the auxiliary agent is 8%；
The thickener is the swollen polyacrylic acid of anion alkali soluble, and the mass percent that the thickener accounts for the auxiliary agent is 8%；
The nertralizer is low molecule organic amine compound, and the mass percent that the nertralizer accounts for the auxiliary agent is 8%；
The preservative is isothiazolinone derivatives, benzimidazole esters, Dao Weixier -75,1,2- benzisothiazoles -3-
At least one of ketone, the mass percent that the preservative accounts for the auxiliary agent is 8%.
（2）Melting is refined：By above-mentioned phenolic resin, rosin melting, temperature control is at 110 DEG C~150 DEG C, and by industry
Base-material after above-mentioned processing, is then dissolved in ethanol or methanol or isopropanol by waste residue, mine tailing grind into powder, through filtering, carries
Produce the high phenolic resin of purity-waste residue solution；
（3）Preceding white silk：Pigment, phenolic resin-waste residue solution are reached into uniform exchange by high-speed stirred in preceding experienced groove, it is fully wet
The admixture of profit, obtains graining paste；
（4）It is scattered：By step（3）In obtained graining paste, reach that pigment is dispersed and scattered by the grinding of decentralized medium
Fineness reaches the state of coating requirement；
（5）Reconcile and mix colours：In mediation groove, pass through the input of auxiliary agent and various uses additive, assign the various mechanicalnesses of coating
Energy and other functions, and pass through the secondary input of pigment, adjust the aberration of coating；
（6）Filtering：Filtering through filtration core and silk, filters out the impurity in coating；
（7）Packaging：Coating after above-mentioned filtering is packaged in paint can through bottle placer；
Wherein, the step（2）In, temperature control is at 145 DEG C；Step（4）In, device therefor is sanded for the RS-16 types bitubular
Machine；Step（5）In, additive is bitumastic solution；Step（7）In, paint can interior skin is provided with adsorbed film.
Coating property is tested：
According to country building material industry standard JC/T984-2005 to having done impermeability test using the embodiment of the present invention, by 6.3cm,
It is tested after 6.4cm, 6.5cm shaping, it was demonstrated that its impermeability pressure reaches 3.2MPa, there is good impervious effect.
According to country building material industry standard JC/T984-2005 to being tested using the shrinkage factor of the embodiment of the present invention,
Shrinkage factor is 0.04%.
According to country building material industry standard JC/T958-2005 to having carried out abrasion test using the embodiment of the present invention, in mill
When wiping 200 times, 0.06g only have lost.
According to country building material industry standard JC/T894-2001 to having carried out degradation using the embodiment of the present invention, 3 are done
Block 10 × 10 × 40CM test blocks, its compression strength is tested after 45 degree of ultraviolets irradiate 250 hours, and for 62.7MPa, (blank is real
Block is 45.2MPa).
The experiment of freeze thawing resistance Rapid Circulation has been carried out to what is be made using the embodiment of the present invention according to GBJ82-85 national standards,
Its mass loss 0%, relative resilient modulus 79.1%.
The other parts of the present embodiment are same as the previously described embodiments, repeat no more.
Although an embodiment of the present invention has been shown and described, it will be understood by those skilled in the art that：Not
A variety of change, modification, replacement and modification can be carried out to these embodiments by departing under the principle and objective of the present invention, of the invention
Scope is limited by claim and its equivalent.
Claims (5)
1. the preparation method of a kind of environmental protection coating material for underground parking, it is characterised in that its processing step is as follows：
（1）Select raw material：By weight percentage, emulsion carriers 35-60 parts, 20-45 parts of pigment, 20-40 parts of base-material, auxiliary agent 5-20
Part, the emulsion carriers include phenolic resin, industrial residue, tail from least one of ethanol, methanol, isopropanol, base-material
Ore deposit, rosin, pigment is at least one of chrome oxide green, ultramarine, auxiliary agent include defoamer, film forming agent, dispersant, thickener,
Nertralizer and preservative；
（2）Melting is refined：By above-mentioned phenolic resin, rosin melting, temperature control at 110 DEG C~150 DEG C, and by industrial residue,
Base-material after above-mentioned processing, is then dissolved in ethanol or methanol or isopropanol by mine tailing grind into powder, through filtering, extracts pure
High phenolic resin-waste residue the solution of degree；
（3）Preceding white silk：Pigment, phenolic resin-waste residue solution are reached into uniform exchange by high-speed stirred in preceding experienced groove, it is fully wet
The admixture of profit, obtains graining paste；
（4）It is scattered：By step（3）In obtained graining paste, reach that pigment is dispersed and scattered by the grinding of decentralized medium
Fineness reaches the state of coating requirement；
（5）Reconcile and mix colours：In mediation groove, pass through the input of auxiliary agent and various uses additive, assign the various mechanicalnesses of coating
Energy and other functions, and pass through the secondary input of pigment, adjust the aberration of coating；
（6）Filtering：Filtering through filtration core and silk, filters out the impurity in coating；
（7）Packaging：Coating after above-mentioned filtering is packaged in paint can through bottle placer.
2. a kind of preparation method of environmental protection coating material for underground parking according to claim 1, it is characterised in that
The step（2）In, temperature control is at 135 DEG C~145 DEG C.
3. a kind of preparation method of environmental protection coating material for underground parking according to claim 1, it is characterised in that
The step（4）In, device therefor is RS-16 type bitubular sand mills.
4. a kind of preparation method of environmental protection coating material for underground parking according to claim 1, it is characterised in that
The step（5）In, additive can be sodium pyrosulfite or bitumastic solution.
5. a kind of preparation method of environmental protection coating material for underground parking according to claim 1, it is characterised in that
The step（7）In, paint can interior skin is provided with adsorbed film.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610994717.1A CN107254230A (en) | 2016-11-11 | 2016-11-11 | A kind of preparation method of environmental protection coating material for underground parking |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610994717.1A CN107254230A (en) | 2016-11-11 | 2016-11-11 | A kind of preparation method of environmental protection coating material for underground parking |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107254230A true CN107254230A (en) | 2017-10-17 |
Family
ID=60027436
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610994717.1A Withdrawn CN107254230A (en) | 2016-11-11 | 2016-11-11 | A kind of preparation method of environmental protection coating material for underground parking |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107254230A (en) |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102702967A (en) * | 2012-06-12 | 2012-10-03 | 天长市巨龙车船涂料有限公司 | Waterproof coating |
| CN103421427A (en) * | 2013-08-22 | 2013-12-04 | 欧美龙（南通）重防腐涂料有限公司 | Anticorrosion phenol-formaldehyde resin compressive coating |
| CN103540198A (en) * | 2013-09-22 | 2014-01-29 | 苏州市湘园特种精细化工有限公司 | Paint preparation technology |
| CN104530839A (en) * | 2014-12-31 | 2015-04-22 | 广西大学 | Coating preparation process |
-
2016
- 2016-11-11 CN CN201610994717.1A patent/CN107254230A/en not_active Withdrawn
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102702967A (en) * | 2012-06-12 | 2012-10-03 | 天长市巨龙车船涂料有限公司 | Waterproof coating |
| CN103421427A (en) * | 2013-08-22 | 2013-12-04 | 欧美龙（南通）重防腐涂料有限公司 | Anticorrosion phenol-formaldehyde resin compressive coating |
| CN103540198A (en) * | 2013-09-22 | 2014-01-29 | 苏州市湘园特种精细化工有限公司 | Paint preparation technology |
| CN104530839A (en) * | 2014-12-31 | 2015-04-22 | 广西大学 | Coating preparation process |
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| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20171017 |
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