CN107252667A - A kind of twin shaft far infrared reactor for producing graphene - Google Patents
A kind of twin shaft far infrared reactor for producing graphene Download PDFInfo
- Publication number
- CN107252667A CN107252667A CN201710488873.5A CN201710488873A CN107252667A CN 107252667 A CN107252667 A CN 107252667A CN 201710488873 A CN201710488873 A CN 201710488873A CN 107252667 A CN107252667 A CN 107252667A
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- CN
- China
- Prior art keywords
- reactor
- agitator
- servomotor
- reactor body
- heater
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
- B01J19/0013—Controlling the temperature of the process
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
- B01J2219/00094—Jackets
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00139—Controlling the temperature using electromagnetic heating
- B01J2219/00146—Infrared radiation
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Carbon And Carbon Compounds (AREA)
Abstract
The present invention relates to a kind of twin shaft far infrared reactor for producing graphene, belong to pressure vessel technology field.The reactor includes reactor body, heater, agitator and reactor support, reactor body is arranged on reactor support, reactor body can be around the central axis being arranged on reactor support, reactor can be rotated in a clockwise direction by the driving of the first servomotor, reactor body outer surface is provided with heat-insulation layer, the far-infrared heater that reactor body peripheral side is set；Agitator is arranged on the center line of axis；Agitator includes the second servomotor, agitating shaft and agitating paddle；Second servomotor is arranged on the top of reactor body, and agitator can be under the driving of the second servomotor along counterclockwise rotates.The present invention is rotated against by reactor body and agitator, increases the heating degree of internal-response kettle so that heating is more uniformly distributed, it is to avoid local heating's overlong time so that the layer key fracture of graphene, and yield rate is improved with this.
Description
Technical field
The present invention relates to a kind of twin shaft far infrared reactor for producing graphene, belong to pressure vessel technology field.
Background technology
At present, the synthetic method of graphene typically is used several raw materials used being put into reactor and reacted.Instead
Meeting neither endothermic nor exothermic during answering, the control of temperature has great role to the selectivity and yield of reactive material.Reacting
All it is continuous feed in journey, and adds related auxiliaries during the course of the reaction, its reaction speed is very sensitive to reaction temperature, temperature
It is higher, react faster, therefore control reaction temperature, be control reaction speed, improve the selectivity and yield of reactive material
One key.Therefore, the designer of the present invention is in view of above-mentioned technological deficiency, it is comprehensive long-term many by concentrating on studies and designing
Year is engaged in the experience and achievement of related industry, and research and design goes out a kind of reactor, to overcome above-mentioned technological deficiency.
The content of the invention
The technical problem to be solved in the present invention is, in view of the shortcomings of the prior art, proposing a kind of pair for producing graphene
Axle far infrared reactor.
The technical scheme that in order to solve the above-mentioned technical problem proposes of the present invention is：A kind of twin shaft far infrared for producing graphene
Reactor, including reactor body, heater, agitator and reactor support, the reactor body are arranged on reactor
On support, the reactor body can be by the first servo around the central axis being arranged on reactor support, the reactor
Motor driving is rotated in a clockwise direction, and the reactor upper end is provided with least one reactor charging aperture, the reactor sheet
The lower end of body is provided with reactor discharging opening, and the reactor body outer surface is provided with heat-insulation layer, the reactor body with
The heater is set between the heat-insulation layer, and the heater is included around the remote of reactor body peripheral side setting
Infrared heater；The agitator is arranged on the center line of axis；The agitator include the second servomotor, agitating shaft and
Agitating paddle；Second servomotor is arranged on the top of reactor body, and the agitator can be in second servomotor
Driving under along counterclockwise rotates；The agitating shaft is connected with the second servomotor；The agitating paddle is arranged on agitating shaft
On；The agitating paddle is welded to connect with agitating shaft.
The improvement of above-mentioned technical proposal is：The reactor bodies top is provided with three reactor charging apertures.
The improvement of above-mentioned technical proposal is：The agitating paddle is frame structure and is fixed with the frame structure some
Crossbeam.
It is of the invention to be using the beneficial effect of above-mentioned technical proposal：Rotated against, increased by reactor body and agitator
Plus the heating degree of internal-response kettle so that heating is more uniformly distributed, it is to avoid local heating's overlong time so that the layer key of graphene
Fracture, yield rate is improved with this.
Brief description of the drawings
The invention will be further described below in conjunction with the accompanying drawings.
Fig. 1 is a kind of twin shaft far infrared reactor structural representation for producing graphene of the embodiment of the present invention.
Reference：Reactor body 1, heater 2, agitator 3, reactor charging aperture 1-1, reactor discharging opening 1-
2nd, heat-insulation layer 1-3, the first servomotor 1-4, the second servomotor 3-1, agitating shaft 3-2, agitating paddle 3-3.
Embodiment
Embodiment
A kind of twin shaft far infrared reactor for producing graphene of the present embodiment, as shown in figure 1, including reactor body 1,
Heater 2, agitator 3 and reactor support, reactor body 1 are arranged on reactor support, and reactor body 1 can winding
The central axis being placed on reactor support, reactor can be rotated in a clockwise direction by the first servomotor 1-4 drivings, be reacted
Kettle upper end is provided with least one reactor charging aperture 1-2, and the lower end of reactor body 1 is provided with a reactor discharging opening, reaction
The outer surface of kettle body 1 is provided with heat-insulation layer 1-3, and heater 2, heater 2 are set between reactor body 1 and heat-insulation layer 1-3
Including the far-infrared heater set around the outer circumferential side of reactor body 1；Agitator 3 is arranged on the center line of axis；Agitator 3
Including the second servomotor 3-1, agitating shaft 3-2 and agitating paddle 3-3；Second servomotor 3-1 is arranged on the top of reactor body 1
Portion, agitator 3 can be under the second servomotor 3-1 driving along counterclockwise rotates；Agitating shaft 3-2 and the second servomotor
3-1 connections；Agitating paddle 3-3 is arranged on agitating shaft 3-2；Agitating paddle 3-3 is welded to connect with agitating shaft 3-2.
The top of reactor body 1 of the present embodiment is provided with three reactor charging aperture 1-2.
The agitating paddle 3-3 of the present embodiment is frame structure and some crossbeams is fixed with frame structure.
The present invention is not limited to above-described embodiment.The technical scheme of all use equivalent substitution formation, all falling within the present invention will
The protection domain asked.
Claims (3)
1. a kind of twin shaft far infrared reactor for producing graphene, including reactor body, heater, agitator and reactor
Support, it is characterised in that：The reactor body is arranged on reactor support, and the reactor body can be around being arranged at reaction
Central axis on kettle support, the reactor can be rotated in a clockwise direction by the driving of the first servomotor, the reactor
Upper end is provided with least one reactor charging aperture, and the lower end of the reactor body is described anti-provided with a reactor discharging opening
Answer kettle body outer surface to be provided with heat-insulation layer, the heater is set between the reactor body and the heat-insulation layer, it is described
Heater includes the far-infrared heater set around the reactor body peripheral side；The agitator is arranged in axis
On heart line；The agitator includes the second servomotor, agitating shaft and agitating paddle；Second servomotor is arranged on reactor
The top of body, the agitator can be under the driving of second servomotor along counterclockwise rotates；The agitating shaft
It is connected with the second servomotor；The agitating paddle is arranged on agitating shaft；The agitating paddle is welded to connect with agitating shaft.
2. the twin shaft far infrared reactor of graphene is produced according to claim 1, it is characterised in that：The reactor body
Top is provided with three reactor charging apertures.
3. the twin shaft far infrared reactor of graphene is produced according to claim 1, it is characterised in that：The agitating paddle is side
Mount structure is simultaneously fixed with some crossbeams in the frame structure.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710488873.5A CN107252667A (en) | 2017-06-23 | 2017-06-23 | A kind of twin shaft far infrared reactor for producing graphene |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710488873.5A CN107252667A (en) | 2017-06-23 | 2017-06-23 | A kind of twin shaft far infrared reactor for producing graphene |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107252667A true CN107252667A (en) | 2017-10-17 |
Family
ID=60024304
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710488873.5A Pending CN107252667A (en) | 2017-06-23 | 2017-06-23 | A kind of twin shaft far infrared reactor for producing graphene |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107252667A (en) |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2055408U (en) * | 1989-10-13 | 1990-04-04 | 重庆电器电瓷厂 | Far infrared electric heating reaction tank |
| CN105983359A (en) * | 2015-02-11 | 2016-10-05 | 江苏康鹏农化有限公司 | Pesticide production agitator tank with improved structure |
-
2017
- 2017-06-23 CN CN201710488873.5A patent/CN107252667A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2055408U (en) * | 1989-10-13 | 1990-04-04 | 重庆电器电瓷厂 | Far infrared electric heating reaction tank |
| CN105983359A (en) * | 2015-02-11 | 2016-10-05 | 江苏康鹏农化有限公司 | Pesticide production agitator tank with improved structure |
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| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20171017 |