CN107240507A - A kind of nanoporous nickel nickel electrode material for super capacitor and preparation method thereof - Google Patents
A kind of nanoporous nickel nickel electrode material for super capacitor and preparation method thereof Download PDFInfo
- Publication number
- CN107240507A CN107240507A CN201710583968.5A CN201710583968A CN107240507A CN 107240507 A CN107240507 A CN 107240507A CN 201710583968 A CN201710583968 A CN 201710583968A CN 107240507 A CN107240507 A CN 107240507A
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- CN
- China
- Prior art keywords
- nickel
- alloy
- nanoporous
- electrode material
- nickel oxide
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- 239000007772 electrode material Substances 0.000 title claims abstract description 46
- 238000002360 preparation method Methods 0.000 title claims abstract description 29
- XIKYYQJBTPYKSG-UHFFFAOYSA-N nickel Chemical compound [Ni].[Ni] XIKYYQJBTPYKSG-UHFFFAOYSA-N 0.000 title claims abstract description 28
- 239000003990 capacitor Substances 0.000 title claims abstract description 23
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims abstract description 147
- 229910000480 nickel oxide Inorganic materials 0.000 claims abstract description 73
- 229910052759 nickel Inorganic materials 0.000 claims abstract description 65
- GNRSAWUEBMWBQH-UHFFFAOYSA-N oxonickel Chemical compound [Ni]=O GNRSAWUEBMWBQH-UHFFFAOYSA-N 0.000 claims abstract description 57
- 238000010438 heat treatment Methods 0.000 claims abstract description 25
- 238000000034 method Methods 0.000 claims abstract description 24
- 229910000808 amorphous metal alloy Inorganic materials 0.000 claims abstract description 16
- 238000007654 immersion Methods 0.000 claims abstract description 13
- 239000011149 active material Substances 0.000 claims abstract description 9
- 239000000203 mixture Substances 0.000 claims abstract description 6
- 239000012792 core layer Substances 0.000 claims abstract 2
- 239000000956 alloy Substances 0.000 claims description 67
- 229910045601 alloy Inorganic materials 0.000 claims description 66
- 239000010936 titanium Substances 0.000 claims description 23
- 239000000243 solution Substances 0.000 claims description 21
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 claims description 16
- 238000002844 melting Methods 0.000 claims description 16
- 230000008018 melting Effects 0.000 claims description 16
- 230000003647 oxidation Effects 0.000 claims description 16
- 238000007254 oxidation reaction Methods 0.000 claims description 16
- KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 claims description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 11
- 229910052760 oxygen Inorganic materials 0.000 claims description 10
- 239000001301 oxygen Substances 0.000 claims description 10
- 239000008367 deionised water Substances 0.000 claims description 9
- 229910021641 deionized water Inorganic materials 0.000 claims description 9
- 239000002994 raw material Substances 0.000 claims description 9
- 229910052786 argon Inorganic materials 0.000 claims description 8
- 239000007789 gas Substances 0.000 claims description 8
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims description 7
- 238000005266 casting Methods 0.000 claims description 7
- 229910052802 copper Inorganic materials 0.000 claims description 7
- 239000010949 copper Substances 0.000 claims description 7
- 239000011259 mixed solution Substances 0.000 claims description 7
- 239000007788 liquid Substances 0.000 claims description 6
- 229910052719 titanium Inorganic materials 0.000 claims description 6
- 229910000838 Al alloy Inorganic materials 0.000 claims description 5
- 230000008859 change Effects 0.000 claims description 5
- 239000002253 acid Substances 0.000 claims description 4
- 239000011261 inert gas Substances 0.000 claims description 4
- 229910052751 metal Inorganic materials 0.000 claims description 4
- 239000002184 metal Substances 0.000 claims description 4
- 229910052782 aluminium Inorganic materials 0.000 claims description 3
- 238000007664 blowing Methods 0.000 claims description 3
- 229910052726 zirconium Inorganic materials 0.000 claims description 3
- 238000004140 cleaning Methods 0.000 claims description 2
- 238000007712 rapid solidification Methods 0.000 claims description 2
- MYMOFIZGZYHOMD-UHFFFAOYSA-N Dioxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 claims 1
- 239000000126 substance Substances 0.000 abstract description 9
- 239000003153 chemical reaction reagent Substances 0.000 abstract description 2
- 238000011031 large-scale manufacturing process Methods 0.000 abstract description 2
- 238000004519 manufacturing process Methods 0.000 abstract description 2
- 239000000463 material Substances 0.000 description 16
- 238000005516 engineering process Methods 0.000 description 10
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 9
- 230000000052 comparative effect Effects 0.000 description 7
- 239000003708 ampul Substances 0.000 description 6
- 230000008569 process Effects 0.000 description 6
- 239000010453 quartz Substances 0.000 description 6
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 6
- 239000003575 carbonaceous material Substances 0.000 description 4
- NUJOXMJBOLGQSY-UHFFFAOYSA-N manganese dioxide Chemical compound O=[Mn]=O NUJOXMJBOLGQSY-UHFFFAOYSA-N 0.000 description 4
- 229910044991 metal oxide Inorganic materials 0.000 description 4
- 150000004706 metal oxides Chemical class 0.000 description 4
- 229920000767 polyaniline Polymers 0.000 description 4
- 238000001228 spectrum Methods 0.000 description 4
- 238000001291 vacuum drying Methods 0.000 description 4
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 3
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 3
- 239000002131 composite material Substances 0.000 description 3
- 238000002484 cyclic voltammetry Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 230000005611 electricity Effects 0.000 description 3
- 239000006260 foam Substances 0.000 description 3
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 3
- 229910052737 gold Inorganic materials 0.000 description 3
- 239000010931 gold Substances 0.000 description 3
- 238000001027 hydrothermal synthesis Methods 0.000 description 3
- 230000001681 protective effect Effects 0.000 description 3
- WOCIAKWEIIZHES-UHFFFAOYSA-N ruthenium(iv) oxide Chemical compound O=[Ru]=O WOCIAKWEIIZHES-UHFFFAOYSA-N 0.000 description 3
- 230000002000 scavenging effect Effects 0.000 description 3
- 241000209094 Oryza Species 0.000 description 2
- 235000007164 Oryza sativa Nutrition 0.000 description 2
- 238000005275 alloying Methods 0.000 description 2
- 230000005540 biological transmission Effects 0.000 description 2
- 238000001354 calcination Methods 0.000 description 2
- 238000005234 chemical deposition Methods 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 229920001940 conductive polymer Polymers 0.000 description 2
- 239000013078 crystal Substances 0.000 description 2
- 238000009826 distribution Methods 0.000 description 2
- 238000004070 electrodeposition Methods 0.000 description 2
- 238000004146 energy storage Methods 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 239000002105 nanoparticle Substances 0.000 description 2
- 150000002815 nickel Chemical class 0.000 description 2
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 2
- 235000013855 polyvinylpyrrolidone Nutrition 0.000 description 2
- 229920000036 polyvinylpyrrolidone Polymers 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 235000009566 rice Nutrition 0.000 description 2
- 238000004062 sedimentation Methods 0.000 description 2
- 238000010183 spectrum analysis Methods 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 229910021607 Silver chloride Inorganic materials 0.000 description 1
- 239000012670 alkaline solution Substances 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 238000006701 autoxidation reaction Methods 0.000 description 1
- 239000011230 binding agent Substances 0.000 description 1
- 230000033228 biological regulation Effects 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 238000009388 chemical precipitation Methods 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000002322 conducting polymer Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 125000004122 cyclic group Chemical group 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000005137 deposition process Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000005518 electrochemistry Effects 0.000 description 1
- 239000003792 electrolyte Substances 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 239000002803 fossil fuel Substances 0.000 description 1
- 238000011065 in-situ storage Methods 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 210000003041 ligament Anatomy 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 229910001338 liquidmetal Inorganic materials 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 238000010295 mobile communication Methods 0.000 description 1
- -1 nanometer sheet Substances 0.000 description 1
- 239000002073 nanorod Substances 0.000 description 1
- 239000002070 nanowire Substances 0.000 description 1
- AOPCKOPZYFFEDA-UHFFFAOYSA-N nickel(2+);dinitrate;hexahydrate Chemical compound O.O.O.O.O.O.[Ni+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O AOPCKOPZYFFEDA-UHFFFAOYSA-N 0.000 description 1
- BFDHFSHZJLFAMC-UHFFFAOYSA-L nickel(ii) hydroxide Chemical compound [OH-].[OH-].[Ni+2] BFDHFSHZJLFAMC-UHFFFAOYSA-L 0.000 description 1
- 229910000510 noble metal Inorganic materials 0.000 description 1
- 238000011017 operating method Methods 0.000 description 1
- 230000008520 organization Effects 0.000 description 1
- 239000012071 phase Substances 0.000 description 1
- 229910052697 platinum Inorganic materials 0.000 description 1
- 239000001267 polyvinylpyrrolidone Substances 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 229910001925 ruthenium oxide Inorganic materials 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 239000004065 semiconductor Substances 0.000 description 1
- HKZLPVFGJNLROG-UHFFFAOYSA-M silver monochloride Chemical compound [Cl-].[Ag+] HKZLPVFGJNLROG-UHFFFAOYSA-M 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- 238000010301 surface-oxidation reaction Methods 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 229910000314 transition metal oxide Inorganic materials 0.000 description 1
Classifications
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES, LIGHT-SENSITIVE OR TEMPERATURE-SENSITIVE DEVICES OF THE ELECTROLYTIC TYPE
- H01G11/00—Hybrid capacitors, i.e. capacitors having different positive and negative electrodes; Electric double-layer [EDL] capacitors; Processes for the manufacture thereof or of parts thereof
- H01G11/22—Electrodes
- H01G11/30—Electrodes characterised by their material
- H01G11/46—Metal oxides
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES, LIGHT-SENSITIVE OR TEMPERATURE-SENSITIVE DEVICES OF THE ELECTROLYTIC TYPE
- H01G11/00—Hybrid capacitors, i.e. capacitors having different positive and negative electrodes; Electric double-layer [EDL] capacitors; Processes for the manufacture thereof or of parts thereof
- H01G11/22—Electrodes
- H01G11/24—Electrodes characterised by structural features of the materials making up or comprised in the electrodes, e.g. form, surface area or porosity; characterised by the structural features of powders or particles used therefor
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES, LIGHT-SENSITIVE OR TEMPERATURE-SENSITIVE DEVICES OF THE ELECTROLYTIC TYPE
- H01G11/00—Hybrid capacitors, i.e. capacitors having different positive and negative electrodes; Electric double-layer [EDL] capacitors; Processes for the manufacture thereof or of parts thereof
- H01G11/22—Electrodes
- H01G11/26—Electrodes characterised by their structure, e.g. multi-layered, porosity or surface features
- H01G11/28—Electrodes characterised by their structure, e.g. multi-layered, porosity or surface features arranged or disposed on a current collector; Layers or phases between electrodes and current collectors, e.g. adhesives
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES, LIGHT-SENSITIVE OR TEMPERATURE-SENSITIVE DEVICES OF THE ELECTROLYTIC TYPE
- H01G11/00—Hybrid capacitors, i.e. capacitors having different positive and negative electrodes; Electric double-layer [EDL] capacitors; Processes for the manufacture thereof or of parts thereof
- H01G11/66—Current collectors
- H01G11/68—Current collectors characterised by their material
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01G—CAPACITORS; CAPACITORS, RECTIFIERS, DETECTORS, SWITCHING DEVICES, LIGHT-SENSITIVE OR TEMPERATURE-SENSITIVE DEVICES OF THE ELECTROLYTIC TYPE
- H01G11/00—Hybrid capacitors, i.e. capacitors having different positive and negative electrodes; Electric double-layer [EDL] capacitors; Processes for the manufacture thereof or of parts thereof
- H01G11/84—Processes for the manufacture of hybrid or EDL capacitors, or components thereof
- H01G11/86—Processes for the manufacture of hybrid or EDL capacitors, or components thereof specially adapted for electrodes
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/13—Energy storage using capacitors
Landscapes
- Engineering & Computer Science (AREA)
- Power Engineering (AREA)
- Microelectronics & Electronic Packaging (AREA)
- Chemical & Material Sciences (AREA)
- Materials Engineering (AREA)
- Electric Double-Layer Capacitors Or The Like (AREA)
- Manufacturing & Machinery (AREA)
Abstract
Description
Claims (3)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201710583968.5A CN107240507B (en) | 2017-07-18 | 2017-07-18 | A kind of nanoporous nickel nickel electrode material for super capacitor and preparation method thereof |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201710583968.5A CN107240507B (en) | 2017-07-18 | 2017-07-18 | A kind of nanoporous nickel nickel electrode material for super capacitor and preparation method thereof |
Publications (2)
Publication Number | Publication Date |
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CN107240507A true CN107240507A (en) | 2017-10-10 |
CN107240507B CN107240507B (en) | 2019-02-22 |
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CN201710583968.5A Active CN107240507B (en) | 2017-07-18 | 2017-07-18 | A kind of nanoporous nickel nickel electrode material for super capacitor and preparation method thereof |
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CN (1) | CN107240507B (en) |
Cited By (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108054022A (en) * | 2017-12-07 | 2018-05-18 | 安徽工业大学 | A kind of non-crystaline amorphous metal combination electrode of surface layer porous structure nickel cobalt oxide and preparation method thereof |
CN108493000A (en) * | 2018-03-23 | 2018-09-04 | 中国科学院宁波材料技术与工程研究所 | A kind of flexible nano porous metals/oxide super capacitor electrode material and preparation method thereof |
CN108707922A (en) * | 2018-05-03 | 2018-10-26 | 北京科技大学 | A kind of flexible nano is porous/amorphous composite material and preparation method thereof |
CN109023412A (en) * | 2018-08-24 | 2018-12-18 | 北京科技大学 | A kind of nanoporous ambrose alloy/amorphous combination electrode material and preparation method thereof |
CN109935888A (en) * | 2017-12-19 | 2019-06-25 | 成都亦道科技合伙企业(有限合伙) | Current collector structure, lithium battery electric core and its lithium battery |
CN110379647A (en) * | 2019-08-14 | 2019-10-25 | 河北工业大学 | A kind of nanoporous nickel nickel loads the preparation method of ultra-thin cobalt hydroxide nanometer sheet flexible electrode material |
CN110706939A (en) * | 2019-09-06 | 2020-01-17 | 暨南大学 | Nano porous nickel alloy/manganese dioxide electrode material and preparation method and application thereof |
CN113416974A (en) * | 2021-03-22 | 2021-09-21 | 辽宁石油化工大学 | Method for rapidly preparing efficient porous silver electrocatalyst |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102013470A (en) * | 2010-11-17 | 2011-04-13 | 哈尔滨工业大学 | Foam metal matrix oxide electrode used in lithium-ion battery cathode and preparation method thereof |
-
2017
- 2017-07-18 CN CN201710583968.5A patent/CN107240507B/en active Active
Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102013470A (en) * | 2010-11-17 | 2011-04-13 | 哈尔滨工业大学 | Foam metal matrix oxide electrode used in lithium-ion battery cathode and preparation method thereof |
Non-Patent Citations (3)
Title |
---|
QINMIN PAN等: "Facile fabrication of porous NiO films for lithium-ion batteries with high reversibility and rate capability", 《J SOLID STATE ELECTROCHEM》 * |
王丽娟: "纳米多孔镍/氧化镍的制备及其性能的研究", 《中国优秀硕士学位论文全文数据库工程科技I辑》 * |
蔡荆等: "多孔氧化镍膜的制备及其赝电容性能", 《中国科技论文》 * |
Cited By (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108054022A (en) * | 2017-12-07 | 2018-05-18 | 安徽工业大学 | A kind of non-crystaline amorphous metal combination electrode of surface layer porous structure nickel cobalt oxide and preparation method thereof |
CN109935888A (en) * | 2017-12-19 | 2019-06-25 | 成都亦道科技合伙企业(有限合伙) | Current collector structure, lithium battery electric core and its lithium battery |
CN108493000A (en) * | 2018-03-23 | 2018-09-04 | 中国科学院宁波材料技术与工程研究所 | A kind of flexible nano porous metals/oxide super capacitor electrode material and preparation method thereof |
CN108707922A (en) * | 2018-05-03 | 2018-10-26 | 北京科技大学 | A kind of flexible nano is porous/amorphous composite material and preparation method thereof |
CN109023412A (en) * | 2018-08-24 | 2018-12-18 | 北京科技大学 | A kind of nanoporous ambrose alloy/amorphous combination electrode material and preparation method thereof |
CN110379647A (en) * | 2019-08-14 | 2019-10-25 | 河北工业大学 | A kind of nanoporous nickel nickel loads the preparation method of ultra-thin cobalt hydroxide nanometer sheet flexible electrode material |
CN110379647B (en) * | 2019-08-14 | 2021-04-30 | 河北工业大学 | Preparation method of nano-porous nickel/nickel oxide loaded ultrathin cobalt hydroxide nanosheet flexible electrode material |
CN110706939A (en) * | 2019-09-06 | 2020-01-17 | 暨南大学 | Nano porous nickel alloy/manganese dioxide electrode material and preparation method and application thereof |
CN113416974A (en) * | 2021-03-22 | 2021-09-21 | 辽宁石油化工大学 | Method for rapidly preparing efficient porous silver electrocatalyst |
Also Published As
Publication number | Publication date |
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CN107240507B (en) | 2019-02-22 |
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Inventor after: Qin Chunling Inventor after: Zheng Donghui Inventor after: Zhu Jiangsai Inventor after: Zhu Mo Inventor after: Wang Zhifeng Inventor after: Yu Hui Inventor after: Zhao Weimin Inventor before: Qin Chunling Inventor before: Zhu Jiangsai Inventor before: Zhu Mo Inventor before: Zheng Donghui Inventor before: Wang Zhifeng Inventor before: Yu Hui Inventor before: Zhao Weimin |
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