CN107238564A - The microcosmos experiment device that a kind of electric field is coalesced with dual drop under shearing field coupling - Google Patents

The microcosmos experiment device that a kind of electric field is coalesced with dual drop under shearing field coupling Download PDF

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Publication number
CN107238564A
CN107238564A CN201710415117.XA CN201710415117A CN107238564A CN 107238564 A CN107238564 A CN 107238564A CN 201710415117 A CN201710415117 A CN 201710415117A CN 107238564 A CN107238564 A CN 107238564A
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electric field
microcosmos experiment
coalesced
microcosmos
drop under
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CN107238564B (en
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孙治谦
王振波
杜联盟
李彬
朱丽云
李强
巩志强
刘兆增
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China University of Petroleum East China
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N15/00Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
    • G01N15/10Investigating individual particles
    • G01N15/1031Investigating individual particles by measuring electrical or magnetic effects

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  • Dispersion Chemistry (AREA)
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Abstract

The microcosmos experiment device that a kind of electric field is coalesced with dual drop under shearing field coupling, belongs to microcosmos experiment apparatus field.It is characterized in that:Microcosmos experiment groove(2)Interior middle part is provided with isolating device, by isolating device by its internal insulation into symmetrically arranged two flowing lumens, oil product circulating direction in two flowing lumens is oppositely arranged, and provided with the collision of reverse oil product gap occurs for the middle part of isolating device, the top that gap occurs for collision is provided with image acquisition and processing device;Microcosmos experiment groove(2)Two side be provided with battery lead plate(12), battery lead plate(12)Connect high voltage high frequency bursts generating means.The present invention can carry out the microcosmos experiment that electric field is coalesced with dual drop under shearing field coupling, probe into coupling off field drop migration, coalescence rule, the experimental study of the deformation, motion and coalescence of drop on micro-scale is carried out, behavior of the dual drop under electric field and shearing field coupling can be studied well on a microscopic scale.

Description

The microcosmos experiment device that a kind of electric field is coalesced with dual drop under shearing field coupling
Technical field
The microcosmos experiment device that a kind of electric field is coalesced with dual drop under shearing field coupling, belongs to microcosmos experiment equipment neck Domain.
Background technology
Oil as a kind of precious non-renewable strategic resources, with the development of society, the consumption of oil with Demand is growing day by day.China's major part oil field enters the middle and later periods of recovering the oil, and the difficulty that oil is exploited from stratum is greatly increased, and is led to The method for often taking the tertiary oil recoveries such as chemical flooding, combination flooding, exploits the water content in crude oil come up very high(In the oil field produced oil in part Water content is up to more than 90%)And exist generally in the form of highly stable water-oil emulsion.Crude oil water containing not only increases accumulating During energy consumption, and the burn into of equipment can be caused to rush tower, the reduction negative issue such as heat transfer efficiency, therefore, crude oil enter factory it Before, it is necessary to carry out strict desalting and dewatering processing.
The dehydration of voltolisation knot with it efficiently, the advantages of quick, treating capacity is big, be widely applied.Water droplet is in extra electric field Effect is lower to polarize, mutual Collision coagulation, water droplet coalescence demulsification, so that gathering into big water droplet obtains sedimentation separation.With offshore oil Field is continually developed, and offshore platform load-bearing and area limitation, the continuous type voltolisation knot dehydration device to high-efficiency compact propose demand. In recent years, increasing scholar starts to recognize facilitation of the flowing shearing to drop electrostatic coalescence process, including compact Type electrostatic coalescer(CEC), the electrostatic coalescence equipment such as online electrostatic poly- (IEC) and the built-in electrostatic coalescer of container (VIEC) All more or less will flowing shear action and electric field action.
Under electric field and shearing field coupling, the stress of drop is complicated, and the research to droplet coalescence mechanism is not thorough, especially It is drop on micro-scale deformation, motion and coalescence experimental study almost do not have.But coupled in electric field and shearing field Under effect, the coalescence mechanism of drop has the meaning of directiveness to the design and development of the continuous electrostatic coalescer of high-efficiency compact.It is right The coalescence mechanism research of drop is extremely urgent under electric field and shearing field coupling.
The content of the invention
The technical problems to be solved by the invention are:Overcome the deficiencies in the prior art can be in micro-scale there is provided one kind On study behavior of the dual drop under electric field and shearing field coupling, and then the electric field studied coalescence mechanism well The microcosmos experiment device coalesced with dual drop under shearing field coupling.
The technical solution adopted for the present invention to solve the technical problems is:The electric field and dual drop under shearing field coupling The microcosmos experiment device of coalescence, it is characterised in that:Occur including microcosmos experiment groove, settling tank, oil storage tank and high voltage high frequency bursts Middle part is provided with isolating device in device, microcosmos experiment groove, is flowed its internal insulation into symmetrically arranged two by isolating device Cavity, the two ends of each flowing lumen connect the oil product circulation side in one group of in-line and outlet line, two flowing lumens respectively To oppositely arranged, and provided with the collision of reverse oil product gap occurs for the middle part of isolating device, and the top that gap occurs for collision is provided with Image acquisition and processing device;The in-line of microcosmos experiment groove both sides connects oil storage tank simultaneously, and the outlet line of both sides connects simultaneously The two side for connecing oil product circulating direction in settling tank, microcosmos experiment groove is provided with battery lead plate, and battery lead plate is external by connection High voltage high frequency bursts generating means.
Isolating device is set in microcosmos experiment groove, and isolation forms two flowing lumens, two formed in microcosmos experiment groove The liquid of two bursts of reverse circulateds of flowing in individual flowing lumen, while between occurring at the middle part of isolating device provided with the collision of reverse oil product Gap, occurs gap using the collision and causes the oil product of two bursts of reverse flows to collide to form contacting section in the gap location, and at this Gap location continuous phase oil forms velocity gradient, forms shearing force field;Meanwhile, it is provided with simultaneously in the vertical direction of oil product circulating direction The electric field formed between battery lead plate, now, occurs gap location instillation two in the collision and drips, thus, force microcosmos experiment groove In collision gap location occurs for interior dual drop simultaneously by the collective effect in shearing field and electric field, deforms upon, migrates, coalescence etc. Behavior, recycles the image acquisition and processing device monitored in real time to shoot the motion agglomeration process of record dual drop, then to image Analyzed;The experimental provision of the present invention can carry out the microcosmos experiment that electric field is coalesced with dual drop under shearing field coupling, Probe into coupling off field drop migration, coalescence rule, carry out micro-scale on drop deformation, motion and coalescence experiment Research, behavior of the dual drop under electric field and shearing field coupling can be studied well on a microscopic scale, and then to poly- Knot mechanism is studied, and applies significant to the heavy industrialization of the continuous voltolisation knot of high-efficiency compact.
Described microcosmos experiment groove is the clamping plate connected between rectangular housing, including the end cap and two end cap of both sides, described Clamping plate be two layers of superposition, install between two laminated planks and connection in-line opened up on battery lead plate, described end cap and fuel-displaced The oil inlet and oil-out of pipeline, bearing rib of the inner side provided with connection isolating device of end cap.
Opposition set two clamping plates on battery lead plate is installed so that form electric field between two clamping plates, at the same with two clamping plates Oil inlet and oil-out are set on end cap connected vertically so that the flow direction of oil product and the direction of electric field are perpendicular, that is, compeled Oil product is passed perpendicularly through electric field during flowing, particularly when occurring gap by colliding, while by electric field and The collective effect of shearing force, the behavior that two-way drop is sheared when colliding, may occur after electric field action all collects In collision occur gap in, be more convenient for Centralizing inspection and record are easy to data acquisition and experimental study.
Described isolating device includes two groups of symmetrically arranged quartzy thin slice necks, quartzy thin slice and liquid distribution plate, two cloth liquid Plate is arranged on battery lead plate both sides, and liquid distribution plate two ends are vertically connected in the two side that microcosmos experiment groove is provided with battery lead plate, liquid distribution plate Installed in the quartzy thin slice neck of portion's right angle setting, quartzy thin slice neck and leave described touch between quartzy thin slice, two quartzy thin slices Hit generation gap.
For the ease of fixed quartzy thin slice using quartzy thin slice neck, the oil entered by setting liquid distribution plate to make from oil inlet And the oil of oil-out outflow being capable of Uniform Flow, reduction local turbulent, raising experiment accuracy.
It is 10mm that gap, which occurs, for the collision that the thickness of described quartzy thin slice is less than between 0.1mm, two quartzy thin slices, microcosmic The length 200mm of experimental tank.
The thickness very little of quartzy thin slice, less than 0.1mm, the thickness of quartzy thin slice is thin as far as possible, can reduce in quartz The influence that the flow cross-section areas change of thin slice intermediate region is flowed to oil product;The distance between two quartzy thin slices are relative to drop Particle diameter is very big, but the very little again for the size of microcosmos experiment groove.Avoid the flowing to the oil product of flowing from producing interference, protect The oil product for demonstrate,proving flowing being capable of Uniform Flow, reduction local turbulent, further raising experiment accuracy.
The distance between two described liquid distribution plates are more than or equal to the length in oil product circulating direction of battery lead plate.
Described image acquisition and processing device includes high-speed camera and image collection processing system.
Described high voltage high frequency bursts generating means includes high voltage high frequency bursts power supply, and high voltage high frequency bursts power supply passes through electricity Magnetic coil connects two battery lead plates being oppositely arranged respectively.
Described also to include switch board, described switch board is arranged on in-line and outlet line by connection Flow regulator.
Described flow regulator includes flowmeter, the delivery valve in outlet line and installed in in-line On inlet valve.
Compared with prior art, the present invention is had an advantageous effect in that:The present invention in microcosmos experiment groove by setting Isolating device, forms two strands of flowing in two flowing lumens, two flowing lumens formed in microcosmos experiment groove reverse using isolation The liquid of circulation, while occurring gap provided with the collision of reverse oil product at the middle part of isolating device, occurring gap using the collision makes The oil product for obtaining two bursts of reverse flows collides to form contacting section in the gap location, and forms speed ladder in gap location continuous phase oil Degree, forms shearing force field;Meanwhile, it is provided with the electric field formed between battery lead plate simultaneously in the vertical direction of oil product circulating direction, this When, occur gap location instillation two in the collision and drip, thus, force the dual drop in microcosmos experiment groove to occur gap in collision The behaviors such as place by the collective effect in shearing field and electric field, deforms upon, migrated simultaneously, coalescence, recycle the figure monitored in real time As acquisition processing device shoots the motion agglomeration process of record dual drop, then image is analyzed;The experiment dress of the present invention The microcosmos experiment that electric field is coalesced with dual drop under shearing field coupling can be carried out by putting, and probed into the drop of coupling off field and moved Shifting, coalescence rule, carry out the experimental study of the deformation, motion and coalescence of drop on micro-scale, can on a microscopic scale very Behavior of the dual drop under electric field and shearing field coupling is studied well, and then coalescence mechanism is studied, to efficiently tight Gather continuous voltolisation knot heavy industrialization using significant.
Brief description of the drawings
Fig. 1 is the microcosmos experiment apparatus structure schematic diagram that electric field is coalesced with dual drop under shearing field coupling.
Fig. 2 is microcosmos experiment slot structure schematic diagram.
Wherein, 1, switch board 2, microcosmos experiment groove 201, end cap 202, bearing rib 203, clamping plate 3, at a high speed Photographic apparatus 4, image collection processing system 5, high voltage high frequency bursts power supply 6, settling tank 7, oil storage tank 8, pump 9th, flowmeter 10, quartzy thin slice neck 11, quartzy thin slice 12, battery lead plate 13, liquid distribution plate 14, the first oil-out 15th, the first oil inlet 16, the second oil-out 17, the second oil inlet 18, delivery valve 19, inlet valve 20, monitoring section.
Embodiment
Fig. 1 ~ 2 are highly preferred embodiment of the present invention, and 1 ~ 2 the present invention will be further described below in conjunction with the accompanying drawings.
Referring to the drawings 1:The microcosmos experiment device that a kind of electric field is coalesced with dual drop under shearing field coupling, including it is microcosmic Middle part is provided with isolating device in experimental tank 2, settling tank 6, oil storage tank 7 and high voltage high frequency bursts generating means, microcosmos experiment groove 2, By isolating device by its internal insulation into symmetrically arranged two flowing lumens, the two ends of each flowing lumen connect one group and entered respectively Oil product circulating direction in oil pipe line and outlet line, two flowing lumens is oppositely arranged, and the middle part of isolating device is provided with anti- Occurs gap to oil product collision, the top that gap occurs for collision is provided with image acquisition and processing device;Microcosmos experiment groove 2 both sides are entered Oil pipe line connects oil storage tank 7 simultaneously, and the outlet line of both sides connects oil product circulating direction in settling tank 6, microcosmos experiment groove 2 simultaneously Two side be provided with battery lead plate 12, battery lead plate 12 passes through the external high voltage high frequency bursts generating means of connection.
Image acquisition and processing device includes high-speed camera 3 and image collection processing system 4.High voltage high frequency bursts are filled Put including high voltage high frequency bursts power supply 5, high voltage high frequency bursts power supply 5 connects two electrodes being oppositely arranged by magnet coil respectively Plate 12.
Present invention additionally comprises switch board 1, switch board 1 is arranged on in-line and the flow of outlet line by connection Adjusting means.Flow regulator includes flowmeter 9, the delivery valve 18 in outlet line and on in-line Inlet valve 19.
Referring to the drawings 2:Microcosmos experiment groove 2 is to be connected between rectangular housing, including the end cap 201 and two end cap 201 of both sides Clamping plate 203, clamping plate 203 is two layers of superposition, install between two laminated planks 203 opened up on battery lead plate 12, end cap 201 connect into The oil inlet and oil-out of oil pipe line and outlet line, bearing rib 202 of the inner side provided with connection isolating device of end cap 201.
Wherein, the first oil-out 14 and the second oil inlet 17 are offered on a wherein end cap 201 for microcosmos experiment groove 2, The first oil inlet 15 and the second oil-out 16, the first oil-out 14 and the second oil-out are offered on the end cap 201 of opposite side Delivery valve 18 is respectively equipped with the flowline of 16 connections;On first oil inlet 15 and the oil inlet pipe of the second oil inlet 17 connection respectively Provided with inlet valve 19, the side of two inlet valves 19 is respectively provided with a flowmeter 9, and two flowmeters 9 connect switch board 1, entered jointly The first oil inlet 15 and the second oil inlet 17 of oil pipe line connection connect oil storage tank 7 by pump 8, and the first oil-out 14 and second goes out Hydraulic fluid port 16 connects settling tank 6 by delivery valve 18.
Isolating device includes two groups of symmetrically arranged quartzy thin slice necks 10, quartzy thin slice 11 and liquid distribution plate 13, two cloth liquid Plate 13 is arranged on the both sides of battery lead plate 12, and the two ends of liquid distribution plate 13 vertically connect the two side that microcosmos experiment groove 2 is provided with battery lead plate 12, Quartzy thin slice 11, two quartzy thin slices are installed in the quartzy thin slice neck 10 of the middle part right angle setting of liquid distribution plate 13, quartzy thin slice neck 10 Collision is left between 11 and occurs gap.The thickness of quartzy thin slice 11 is less than between the collision generation between 0.1mm, two quartzy thin slices 11 Gap is 10mm, the length 200mm of microcosmos experiment groove 2.The distance between two liquid distribution plates 13 are more than or equal to battery lead plate 12 in oil product The length of circulating direction.
The course of work and operation principle:Appropriate oil product is injected into microcosmos experiment groove 2 first, using micropipettor to The micron order water droplet of two appropriate particle diameters is moved into microcosmos experiment groove 2 equipped with oil-continuous phase, water droplet is placed on two quartzy thin slices In monitoring section 20 between 11, the position of dual drop can be adjusted according to requirement of experiment;High voltage high frequency bursts power supply 5 and battery lead plate 12 Connection, can produce electric field in microcosmos experiment groove 2;Everything in readiness, opens the oil of the continuous phase in pump 8, oil storage tank 7 and passes through flow The 9, first oil inlet 15 of meter is sent in microcosmos experiment groove 2 by pump 8;Flowmeter 9 is connected with switch board 1, is controlled by switch board 1 Flowmeter 9, so as to control the oily amount entered in the first oil inlet 15 and the second oil inlet 17;From the first oil inlet 15 and second The continuous phase speed oil that oil inlet 17 enters microcosmos experiment groove 2 is in opposite direction, flow is identical, by two liquid distribution plates 13 of both sides Even flow field after uniform cloth liquid, liquid distribution plate 13;Region between two quartzy thin slices 11, continuous phase oil forms velocity gradient, Drop is by shearing force field;Drop in microcosmos experiment groove 2 by the collective effect in shearing field and electric field, deform upon, migrate, The behaviors such as coalescence, the motion agglomeration process for recording dual drop, later-stage utilization image acquisition and processing system are shot using high-speed camera 3 4 pairs of images of system are analyzed, and oil product enters settling tank 6 after being flowed out by the first oil-out 14 and the second oil-out 16.
The above described is only a preferred embodiment of the present invention, being not the limitation for making other forms to the present invention, appoint What those skilled in the art changed or be modified as possibly also with the technology contents of the disclosure above equivalent variations etc. Imitate embodiment.But it is every without departing from technical solution of the present invention content, the technical spirit according to the present invention is to above example institute Any simple modification, equivalent variations and the remodeling made, still fall within the protection domain of technical solution of the present invention.

Claims (9)

1. the microcosmos experiment device that a kind of electric field is coalesced with dual drop under shearing field coupling, it is characterised in that:Including microcosmic Experimental tank(2), settling tank(6), oil storage tank(7)With high voltage high frequency bursts generating means, microcosmos experiment groove(2)Interior middle part be provided with every From device, by isolating device by its internal insulation into symmetrically arranged two flowing lumens, the two ends of each flowing lumen connect respectively The oil product circulating direction connect in one group of in-line and outlet line, two flowing lumens is oppositely arranged, and in isolating device Gap occurs for the collision of oil product of the middle part provided with reverse circulated, and the top that gap occurs for collision is provided with image acquisition and processing device; Microcosmos experiment groove(2)The in-line of both sides connects oil storage tank simultaneously(7), the outlet line of both sides is while connect settling tank(6), Microcosmos experiment groove(2)The two side of interior oil product circulating direction is provided with battery lead plate(12), battery lead plate(12)Outside by connection The high voltage high frequency bursts generating means put.
2. the microcosmos experiment device that a kind of electric field according to claim 1 is coalesced with dual drop under shearing field coupling, It is characterized in that:Described microcosmos experiment groove(2)For the end cap of rectangular housing, including both sides(201)And two end cap(201)Between The clamping plate of connection(203), described clamping plate(203)For two layers of superposition, two laminated planks(203)Between battery lead plate is installed(12), Described end cap(201)On open up connection in-line and outlet line oil inlet and oil-out, end cap(201)Inner side set There is the bearing rib of connection isolating device(202).
3. the microcosmos experiment device that a kind of electric field according to claim 1 is coalesced with dual drop under shearing field coupling, It is characterized in that:Described isolating device includes two groups of symmetrically arranged quartzy thin slice necks(10), quartzy thin slice(11)And cloth Liquid plate(13), two liquid distribution plates(13)It is arranged on battery lead plate(12)Both sides, liquid distribution plate(13)Two ends vertically connect microcosmos experiment groove(2) Battery lead plate is installed(12)Two side, liquid distribution plate(13)The quartzy thin slice neck of middle part right angle setting(10), quartzy thin slice neck (10)It is interior that quartzy thin slice is installed(11), two quartzy thin slices(11)Between leave described collision and occur gap.
4. the microcosmos experiment device that a kind of electric field according to claim 3 is coalesced with dual drop under shearing field coupling, It is characterized in that:Described quartzy thin slice(11)Thickness be less than 0.1mm, two quartzy thin slices(11)Between collision occur gap For 10mm, microcosmos experiment groove(2)Length 200mm.
5. the microcosmos experiment device that a kind of electric field according to claim 3 is coalesced with dual drop under shearing field coupling, It is characterized in that:Two described liquid distribution plates(13)The distance between be more than or equal to battery lead plate(12)The length in oil product circulating direction Degree.
6. the microcosmos experiment device that a kind of electric field according to claim 1 is coalesced with dual drop under shearing field coupling, It is characterized in that:Described image acquisition and processing device includes high-speed camera(3)And image collection processing system(4).
7. the microcosmos experiment device that a kind of electric field according to claim 1 is coalesced with dual drop under shearing field coupling, It is characterized in that:Described high voltage high frequency bursts generating means includes high voltage high frequency bursts power supply(5), high voltage high frequency bursts power supply (5)Connect two battery lead plates being oppositely arranged respectively by magnet coil(12).
8. the microcosmos experiment device that a kind of electric field according to claim 1 is coalesced with dual drop under shearing field coupling, It is characterized in that:Also include switch board(1), described switch board(1)In-line and flowline are arranged on by connection The flow regulator on road.
9. the microcosmos experiment device that a kind of electric field according to claim 8 is coalesced with dual drop under shearing field coupling, It is characterized in that:Described flow regulator includes flowmeter(9), delivery valve in outlet line(18)And installation Inlet valve on in-line(19).
CN201710415117.XA 2017-06-05 2017-06-05 A kind of microcosmos experiment device that electric field is coalesced with dual drop under shearing field coupling Active CN107238564B (en)

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Cited By (2)

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CN108562518A (en) * 2018-02-12 2018-09-21 浙江大学 A kind of device and method for studying heavy metal ion traveling locus in the Polluted Soil that electric osmose is handled
CN109903820A (en) * 2019-03-25 2019-06-18 重庆工商大学 A kind of method of determining double-field coupled dehydration device optimal operation parameter

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Cited By (3)

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Publication number Priority date Publication date Assignee Title
CN108562518A (en) * 2018-02-12 2018-09-21 浙江大学 A kind of device and method for studying heavy metal ion traveling locus in the Polluted Soil that electric osmose is handled
CN108562518B (en) * 2018-02-12 2023-06-30 浙江大学 Device and method for researching migration track of heavy metal ions in electroosmosis treated polluted soil
CN109903820A (en) * 2019-03-25 2019-06-18 重庆工商大学 A kind of method of determining double-field coupled dehydration device optimal operation parameter

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