CN107226991A - A kind of Matte oil-resistant elastomer cable material - Google Patents
A kind of Matte oil-resistant elastomer cable material Download PDFInfo
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- CN107226991A CN107226991A CN201710457091.5A CN201710457091A CN107226991A CN 107226991 A CN107226991 A CN 107226991A CN 201710457091 A CN201710457091 A CN 201710457091A CN 107226991 A CN107226991 A CN 107226991A
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- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L53/00—Compositions of block copolymers containing at least one sequence of a polymer obtained by reactions only involving carbon-to-carbon unsaturated bonds; Compositions of derivatives of such polymers
- C08L53/02—Compositions of block copolymers containing at least one sequence of a polymer obtained by reactions only involving carbon-to-carbon unsaturated bonds; Compositions of derivatives of such polymers of vinyl-aromatic monomers and conjugated dienes
- C08L53/025—Compositions of block copolymers containing at least one sequence of a polymer obtained by reactions only involving carbon-to-carbon unsaturated bonds; Compositions of derivatives of such polymers of vinyl-aromatic monomers and conjugated dienes modified
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- C—CHEMISTRY; METALLURGY
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- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L23/00—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers
- C08L23/02—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers not modified by chemical after-treatment
- C08L23/10—Homopolymers or copolymers of propene
- C08L23/12—Polypropene
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01B—CABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
- H01B3/00—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties
- H01B3/18—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of organic substances
- H01B3/30—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of organic substances plastics; resins; waxes
- H01B3/44—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of organic substances plastics; resins; waxes vinyl resins; acrylic resins
- H01B3/441—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of organic substances plastics; resins; waxes vinyl resins; acrylic resins from alkenes
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01B—CABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
- H01B3/00—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties
- H01B3/18—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of organic substances
- H01B3/30—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of organic substances plastics; resins; waxes
- H01B3/44—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of organic substances plastics; resins; waxes vinyl resins; acrylic resins
- H01B3/442—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of organic substances plastics; resins; waxes vinyl resins; acrylic resins from aromatic vinyl compounds
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
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- C—CHEMISTRY; METALLURGY
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- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2203/00—Applications
- C08L2203/20—Applications use in electrical or conductive gadgets
- C08L2203/202—Applications use in electrical or conductive gadgets use in electrical wires or wirecoating
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- Organic Insulating Materials (AREA)
Abstract
The invention discloses a kind of Matte oil-resistant elastomer cable material, it is prepared by the component raw material of following parts by weight：25 35 parts of hydrogenated styrene butadiene styrene, 15 25 parts of polypropylene, 8 10 parts of nitrile rubber point, 8 12 parts of polyacrylamide resin, 12 16 parts of two tricaprylate of triethylene glycol, 68 parts of triethyl citrate, 24 parts of methyl-silicone oil, 6 10 parts of EP rubbers, 6 12 parts of precipitated calcium carbonate, 13 parts of stearic acid, 13 parts of zinc oxide, 6 12 parts of wollastonite in powder, 13 parts of magnesia, 46 parts of celestine, 46 parts of fluorite, 57 parts of clay, 13 parts of zirconium oxide, 0.6 1.0 parts of antioxidant, 0.4 0.6 parts of triphenyl phosphite, 68 parts of Firebrake ZB, 8 10 parts of ammonium molybdate, 13 parts of cupric oxide, 3 parts of cumyl peroxide DCP1, 10 20 parts of modified filler.The CABLE MATERIALS of machine-shaping of the present invention has good oil resistivity and mechanical performance, further improve the compatilizer of CABLE MATERIALS fusion and eliminate the internal stress existed in material body, and preparation technology is simple, realizes cost-effective and reduce labor intensity, meet actual operation requirements.
Description
Technical field
The present invention relates to a kind of Matte oil-resistant elastomer cable material, belong to CABLE MATERIALS technical field.
Background technology
Electric wire has the effect of power Transmission and information conveyance, and important work is played in people live and produce
With.Low cigarette, low toxicity are designed and make, while but also with excellent fire-retardancy and the CABLE MATERIALS of insulating properties, as current fire-retardant
The focus of research.Traditional magnesium hydroxide and aluminium hydroxide fire retardant, although can assign material good fire resistance, still,
Because the matrix resin of most of CABLE MATERIALSs is nonpolar polyolefin macromolecule, the magnesium hydroxide, aluminium hydroxide with polarity
Compatibility is poor, often reduces the mechanical property and processing characteristics of material.Thus, working out both has good anti-flammability
Can, while have environmental-protecting performance, good machining property, the CABLE MATERIALS material of preferable insulating properties turn into the side of development
To.At present, it is in the prior art compatibility that storeroom is improved by adding modified filler, and then improves the machine of CABLE MATERIALS
Tool processing characteristics, while ensure that the flame-proof environmental protection of CABLE MATERIALS.But, due to the defect of modified filler preparation technology, cause
There is internal stress and unstability in modified filler, and then reduce the compatibility of modified filler, so as to reduce the machine of CABLE MATERIALS
Tool processing characteristics, it is impossible to be further ensured that the flame-proof environmental protection of CABLE MATERIALS.
The content of the invention
The present invention is exactly in view of the deficienciess of the prior art, there is provided a kind of Matte oil-resistant elastomer cable material, this hair
The CABLE MATERIALS of bright machine-shaping has good oil resistivity and mechanical performance, further improve CABLE MATERIALS fusion compatibility and
The internal stress existed in material body is eliminated, and preparation technology is simple, realizes cost-effective and reduces labor intensity, meets
Actual operation requirements.
To solve the above problems, the technical solution used in the present invention is as follows：
A kind of Matte oil-resistant elastomer cable material, is prepared by the component raw material of following parts by weight：Hydrogenated styrene-fourth two
Alkene -25-35 parts of styrene, 15-25 parts of polypropylene, nitrile rubber points 8-10 parts, 8-12 parts of polyacrylamide resin, triethylene glycol
Two 12-16 parts of tricaprylates, 6-8 parts of triethyl citrate, 2-4 parts of methyl-silicone oil, 6-10 parts of EP rubbers, precipitated calcium carbonate 6-
12 parts, 1-3 parts of stearic acid, 1-3 parts of zinc oxide, 6-12 parts of wollastonite in powder, 1-3 parts of magnesia, 4-6 parts of celestine, fluorite 4-6
Part, 5-7 parts of clay, 1-3 parts of zirconium oxide, 0.6-1.0 parts of antioxidant, 0.4-0.6 parts of triphenyl phosphite, 6-8 parts of Firebrake ZB, molybdenum
Sour ammonium 8-10 parts, 1-3 parts of cupric oxide, DCP1-3 parts of cumyl peroxide, 10-20 parts of modified filler；
The preparation method of the modified filler is as follows：
Step（1）：Take 160-180 parts of kaolin, 30-36 parts of medical stone, 1-3 parts of nano-sized carbon, 1-3 parts of ascorbic acid, coix seed oil
1-3 parts, 1-3 parts of aluminum nitride powder, 2-4 parts of zinc gluconate, 2-4 parts of jade powder, 2-4 parts of polyisobutene, aluminate coupling agent 1-3
Part, 2-4 parts of stearic acid, 1-3 parts of antioxidant；
Step（2）：Kaolin, medical stone are calcined into 4-6h at 450-480 DEG C, vacuum cooled to room temperature after taking-up, adds 3-
Ground in 4% sodium hydroxide solution 1-2 hours, then, add 12-16% hydrochloric acid solution, regulation pH value is 4-5, is aged 12-
16 hours, it was neutrality to add sodium hydroxide solution regulation lapping liquid pH, and filtering, drying obtains filler powder；
Step（3）：By step（2）Obtained filler powder is inserted on the bottom electrode medium of plasma device, voltage 12kV, electricity
Flow and irradiated 15~25 seconds under 1.2mA, gap 3mm operating condition；
Step（4）：Above-mentioned gained filler powder is mixed with other residual components, it is air-cooled to room temperature after hot pressing twice, then with
8000-10000r/min high speed is uniformly dispersed, and produces.
Compared with prior art, implementation result of the invention is as follows by the present invention：
The invention provides a kind of Matte oil-resistant elastomer cable material, the CABLE MATERIALS of machine-shaping of the present invention has good oil resistant
Property and mechanical performance, further improve the compatilizer of CABLE MATERIALS fusion and eliminate the internal stress existed in material body, and
Preparation technology is simple, realizes cost-effective and reduces labor intensity, meets actual operation requirements.
Note：CABLE MATERIALS produced by the present invention also has extremely excellent ultraviolet resistance, resistance to ozone and chemical-resistant characteristic and tensile strength
And fracture elongation is big.
Embodiment
Illustrate present disclosure below in conjunction with specific embodiments.
Embodiment 1：
A kind of Matte oil-resistant elastomer cable material, is prepared by the component raw material of following parts by weight：Hydrogenated styrene-fourth two
Alkene -25-35 parts of styrene, 15-25 parts of polypropylene, nitrile rubber points 8-10 parts, 8-12 parts of polyacrylamide resin, triethylene glycol
Two 12-16 parts of tricaprylates, 6-8 parts of triethyl citrate, 2-4 parts of methyl-silicone oil, 6-10 parts of EP rubbers, precipitated calcium carbonate 6-
12 parts, 1-3 parts of stearic acid, 1-3 parts of zinc oxide, 6-12 parts of wollastonite in powder, 1-3 parts of magnesia, 4-6 parts of celestine, fluorite 4-6
Part, 5-7 parts of clay, 1-3 parts of zirconium oxide, 0.6-1.0 parts of antioxidant, 0.4-0.6 parts of triphenyl phosphite, 6-8 parts of Firebrake ZB, molybdenum
Sour ammonium 8-10 parts, 1-3 parts of cupric oxide, DCP1-3 parts of cumyl peroxide, 10-20 parts of modified filler；
The preparation method of the modified filler is as follows：Step（1）：Take 160-180 parts of kaolin, 30-36 parts of medical stone, nano-sized carbon
1-3 parts, it is 1-3 parts of ascorbic acid, 1-3 parts of coix seed oil, 1-3 parts of aluminum nitride powder, 2-4 parts of zinc gluconate, 2-4 parts of jade powder, poly-
2-4 parts of isobutene, 1-3 parts of aluminate coupling agent, 2-4 parts of stearic acid, 1-3 parts of antioxidant；Step（2）：By kaolin, medical stone
4-6h is calcined at 450-480 DEG C, vacuum cooled to room temperature after taking-up, adds grinding 1-2 in 3-4% sodium hydroxide solution small
When, then, 12-16% hydrochloric acid solution is added, regulation pH value is 4-5, is aged 12-16 hours, adds sodium hydroxide solution tune
It is neutrality to save lapping liquid pH, and filtering, drying obtains filler powder；Step（3）：By step（2）Obtained filler powder is inserted
On the bottom electrode medium of ion body device, voltage 12kV is irradiated 15~25 seconds under electric current 1.2mA, gap 3mm operating condition；
Step（4）：Above-mentioned gained filler powder is mixed with other residual components, it is air-cooled to room temperature after hot pressing twice, then with 8000-
10000r/min high speed is uniformly dispersed, and produces.
The CABLE MATERIALS of machine-shaping of the present invention has good oil resistivity and mechanical performance, further improves CABLE MATERIALS fusion
Compatilizer and the internal stress for eliminating presence in material body, and preparation technology is simple, realizes cost-effective and reduction and works
Intensity, meets actual operation requirements.
Note：CABLE MATERIALS produced by the present invention also has extremely excellent ultraviolet resistance, resistance to ozone and chemical-resistant characteristic and tensile strength
And fracture elongation is big.
Embodiment 2：
The preparation technology of Matte oil-resistant elastomer cable material：
Each constitutive material is weighed by formula rate, constitutive material is put into homogenizer mixing 6-8 minutes, blowing will be mixed
The material got togather is put into double screw extruder, and extruding pelletization is entered back into after being dried in air drier, produces cloudy surface
Oil resistant elastomer cable material, double screw extruder temperature is set to during extrusion：114 DEG C of feeding section, 175 DEG C of melt zone, melt conveying
175-182 DEG C of section, 185 DEG C of mixing section, 185 DEG C of head metering section.
The performance test results of CABLE MATERIALS made from the present embodiment such as following table：
Above content is made for the present invention in conjunction with specific embodiments describes in detail, it is impossible to assert present invention specific implementation only
It is limited to these explanations.For those skilled in the art, without departing from the inventive concept of the premise,
Some simple deduction or replace can also be made, the scope of protection of the invention should be all considered as belonging to.
Claims (2)
1. a kind of Matte oil-resistant elastomer cable material, it is characterised in that：It is prepared by the component raw material of following parts by weight：Hydrogenation
25-35 parts of s-B-S, 15-25 parts of polypropylene, nitrile rubber point 8-10 parts, polyacrylamide resin 8-12
Part, 12-16 parts of two tricaprylate of triethylene glycol, 6-8 parts of triethyl citrate, 2-4 parts of methyl-silicone oil, 6-10 parts of EP rubbers,
6-12 parts of precipitated calcium carbonate, 1-3 parts of stearic acid, 1-3 parts of zinc oxide, 6-12 parts of wollastonite in powder, 1-3 parts of magnesia, celestine 4-6
Part, 4-6 parts of fluorite, 5-7 parts of clay, 1-3 parts of zirconium oxide, 0.6-1.0 parts of antioxidant, 0.4-0.6 parts of triphenyl phosphite, boric acid
6-8 parts of zinc, 8-10 parts of ammonium molybdate, 1-3 parts of cupric oxide, DCP1-3 parts of cumyl peroxide, 10-20 parts of modified filler；
The preparation method of the modified filler is as follows：
Step（1）：Take 160-180 parts of kaolin, 30-36 parts of medical stone, 1-3 parts of nano-sized carbon, 1-3 parts of ascorbic acid, coix seed oil
1-3 parts, 1-3 parts of aluminum nitride powder, 2-4 parts of zinc gluconate, 2-4 parts of jade powder, 2-4 parts of polyisobutene, aluminate coupling agent 1-3
Part, 2-4 parts of stearic acid, 1-3 parts of antioxidant；
Step（2）：Kaolin, medical stone are calcined into 4-6h at 450-480 DEG C, vacuum cooled to room temperature after taking-up, adds 3-
Ground in 4% sodium hydroxide solution 1-2 hours, then, add 12-16% hydrochloric acid solution, regulation pH value is 4-5, is aged 12-
16 hours, it was neutrality to add sodium hydroxide solution regulation lapping liquid pH, and filtering, drying obtains filler powder；
Step（3）：By step（2）Obtained filler powder is inserted on the bottom electrode medium of plasma device, voltage 12kV, electricity
Flow and irradiated 15~25 seconds under 1.2mA, gap 3mm operating condition；
Step（4）：Above-mentioned gained filler powder is mixed with other residual components, it is air-cooled to room temperature after hot pressing twice, then with
8000-10000r/min high speed is uniformly dispersed, and produces.
2. a kind of Matte oil-resistant elastomer cable material according to claim 1, it is characterised in that：By the component of following parts by weight
Raw material is prepared：30 parts of hydrogenated styrene-butadiene-styrene, 20 parts of polypropylene, nitrile rubber point 9 parts, polyacrylamide
10 parts of resin, 14 parts of two tricaprylate of triethylene glycol, 7 parts of triethyl citrate, 3 parts of methyl-silicone oil, 8 parts of EP rubbers, lightweight
9 parts of calcium carbonate, 2 parts of stearic acid, 2 parts of zinc oxide, 9 parts of wollastonite in powder, 2 parts of magnesia, 5 parts of celestine, 5 parts of fluorite, clay 6
Part, 2 parts of zirconium oxide, 0.8 part of antioxidant, 0.5 part of triphenyl phosphite, 7 parts of Firebrake ZB, 9 parts of ammonium molybdate, 2 parts of cupric oxide, peroxide
Change DCP2 parts of diisopropylbenzene (DIPB), 15 parts of modified filler；
The preparation method of the modified filler is as follows：
Step（1）：Take 170 parts of kaolin, 33 parts of medical stone, 2 parts of nano-sized carbon, 2 parts of ascorbic acid, 2 parts of coix seed oil, aluminum nitride powder
2 parts, 3 parts of zinc gluconate, 3 parts of jade powder, 3 parts of polyisobutene, 2 parts of aluminate coupling agent, 3 parts of stearic acid, 2 parts of antioxidant；
Step（2）：Kaolin, medical stone are calcined into 5h at 465 DEG C, vacuum cooled to room temperature after taking-up, adds 3-4% hydrogen
Ground in sodium hydroxide solution 1.5 hours, then, add 12-16% hydrochloric acid solution, regulation pH value is 4-5, is aged 14 hours, then
It is neutrality to add sodium hydroxide solution regulation lapping liquid pH, and filtering, drying obtains filler powder；
Step（3）：By step（2）Obtained filler powder is inserted on the bottom electrode medium of plasma device, voltage 12kV, electricity
Flow and irradiated 20 seconds under 1.2mA, gap 3mm operating condition；
Step（4）：Above-mentioned gained filler powder is mixed with other residual components, it is air-cooled to room temperature after hot pressing twice, then with
9000r/min high speed is uniformly dispersed, and produces.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710457091.5A CN107226991A (en) | 2017-06-16 | 2017-06-16 | A kind of Matte oil-resistant elastomer cable material |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710457091.5A CN107226991A (en) | 2017-06-16 | 2017-06-16 | A kind of Matte oil-resistant elastomer cable material |
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| CN107226991A true CN107226991A (en) | 2017-10-03 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108677223A (en) * | 2018-06-21 | 2018-10-19 | 广东嘉元科技股份有限公司 | A kind of manufacturing method of the super book electrolytic copper foil of new energy resource power battery |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103509308A (en) * | 2013-10-12 | 2014-01-15 | 绿宝电缆（集团）有限公司 | Matte oil-resistant elastomer cable material |
| CN103865223A (en) * | 2014-03-19 | 2014-06-18 | 安徽电缆股份有限公司 | Surface-frosted oilproof elastomer cable material |
| CN106380869A (en) * | 2016-08-29 | 2017-02-08 | 上海至正道化高分子材料股份有限公司 | 125-degree irradiation-crosslinked elastomer cable material used for new energy automobile high-voltage cable and manufacture method of elastomer cable material |
-
2017
- 2017-06-16 CN CN201710457091.5A patent/CN107226991A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103509308A (en) * | 2013-10-12 | 2014-01-15 | 绿宝电缆（集团）有限公司 | Matte oil-resistant elastomer cable material |
| CN103865223A (en) * | 2014-03-19 | 2014-06-18 | 安徽电缆股份有限公司 | Surface-frosted oilproof elastomer cable material |
| CN106380869A (en) * | 2016-08-29 | 2017-02-08 | 上海至正道化高分子材料股份有限公司 | 125-degree irradiation-crosslinked elastomer cable material used for new energy automobile high-voltage cable and manufacture method of elastomer cable material |
Non-Patent Citations (1)
| Title |
|---|
| 沈新元等: "《高分子材料加工原理》", 31 December 2014, 中国纺织出版社 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108677223A (en) * | 2018-06-21 | 2018-10-19 | 广东嘉元科技股份有限公司 | A kind of manufacturing method of the super book electrolytic copper foil of new energy resource power battery |
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