CN107223953A - A kind of stability phosphatidylserine micro mist and preparation method for food - Google Patents
A kind of stability phosphatidylserine micro mist and preparation method for food Download PDFInfo
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- CN107223953A CN107223953A CN201710456737.8A CN201710456737A CN107223953A CN 107223953 A CN107223953 A CN 107223953A CN 201710456737 A CN201710456737 A CN 201710456737A CN 107223953 A CN107223953 A CN 107223953A
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
- A23L29/03—Organic compounds
- A23L29/035—Organic compounds containing oxygen as heteroatom
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23C—DAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
- A23C9/00—Milk preparations; Milk powder or milk powder preparations
- A23C9/12—Fermented milk preparations; Treatment using microorganisms or enzymes
- A23C9/13—Fermented milk preparations; Treatment using microorganisms or enzymes using additives
- A23C9/1322—Inorganic compounds; Minerals, including organic salts thereof, oligo-elements; Amino-acids, peptides, protein-hydrolysates or derivatives; Nucleic acids or derivatives; Yeast extract or autolysate; Vitamins; Antibiotics; Bacteriocins
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23C—DAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
- A23C9/00—Milk preparations; Milk powder or milk powder preparations
- A23C9/152—Milk preparations; Milk powder or milk powder preparations containing additives
- A23C9/1526—Amino acids; Peptides; Protein hydrolysates; Nucleic acids; Derivatives thereof
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/52—Adding ingredients
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
- A23L29/03—Organic compounds
- A23L29/045—Organic compounds containing nitrogen as heteroatom
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Abstract
The present invention relates to the technology for producing field of phosphatidylserine, a kind of stability phosphatidylserine micro mist and preparation method for food is specifically related to, the phosphatidylserine micro mist of the stabilization includes following material：Phosphatidylserine, diphosphoinesitide, triphosphoinositide, asparatate, carrier, edible glue；After the present invention mixes phosphatidylserine with diphosphoinesitide and triphosphoinositide, it is complexed with asparatate, further it is carried on by vacuum suction in carrier, by the way that the glue of Arabic gum, gelatin or xanthans is obtained into phosphatidylserine micro mist by being sprayed at silica gel micro mist dry tack free.Asparatate is aided in be complexed by diphosphoinesitide and triphosphoinositide; inactivation of the phosphatidylserine in storage and use is preferably further avoided by the protection of silica gel micro mist, it can be directly added applied to food and for various tablets, pill, granule, pulvis, capsule, emulsion.
Description
Technical field
The present invention relates to the technology for producing field of phosphatidylserine, a kind of stabilization for food is specifically related to
Property phosphatidylserine micro mist and preparation method.
Background technology
Phosphatidylserine（Phosphatidylserine, PS）Also known as composite nerve is sour, and its function is mainly improvement god
Through cell function, the conduction of nerve impulse is adjusted, promotes brain memory function, because it has very strong lipophilicity, after absorption
Blood-brain barrier can be run through and enter brain, vascular smooth muscle cells of releiving are played, increase the effect of brain blood supply.It no matter
Be that certainly, supplement phosphatidylserine can improve long-term memory as medicine or health food, it is long-term cognitive and
Free talk and logicality speech ability.
Phosphatidylserine（PS）Have become many American-European countries's research losses of memory, mood, cognitive behavior and study
The problem of the relevant clinical test of ability.Clinical test results are shown, after supplement phosphatidylserine, on cognitive and memory
Parameter significantly improves.Certainly, supplement phosphatidylserine can improve long-term memory, long-term cognition and freely talk
Tuhe logicality speech ability.Phosphatidylserine（PS）It can be proportionally added into meals, can be by enteron aisle effectively
Promptly it is absorbed into blood, and the finally and successfully nerve cell that intracerebral is reached through blood-brain barrier.
Phosphatidylserine（PS）It can be synthesized by the mankind or animal self-condition, can also be from plant extract, or can
Produced using biocatalysis technology from soybean lecithin.By using phospholipase D（PLDs）Phosphatidyl transfer
（transphosphatidylation）Reaction, easily can be modified the head base of phosphatide.Therefore, phosphatidylserine can
Pass through PLD catalytic productions from phosphatidyl choline or any other mixture of phospholipids with serine.
Phosphatidylserine has been used for all kinds of brain-nourishing health foods, nutrition at present as medicine or the raw material of health food
Product etc..But it is limited to phosphatidylserine to store and easily react with oxidation environment using process.Therefore during storage, use pole
It is easily caused phosphatidyl transfer, the division of serine base, phosphatidylserine inactivation.In particular with phosphatidylserine in milk
Addition is used in powder, Yoghourt, beverage etc., and its environment produces influence to the activity of phosphatidylserine.Therefore, how phosphorus is ensured
Stability of the acyl serine in storage and in using turns into its key used as health product raw material large-scale promotion.
The content of the invention
In view of the shortcomings of the prior art, it is an object of the invention to provide a kind of stability phosphorus acyl silk ammonia for food
Sour micro mist, with good storage stability, has a wide range of application, and can be added in a variety of environment such as milk powder, Yoghourt, beverage makes
With.Further provide for the preparation method of the stability phosphatidylserine micro mist.
To achieve the above object, the concrete scheme of use is as follows：
A kind of preparation method of stability phosphatidylserine micro mist for food, comprises the following steps：
A, phosphatidylserine, diphosphoinesitide, triphosphoinositide be well mixed in the solution, then to mixing
Asparatate complexing is added in solution, mixed system 1 is obtained；
B, by mixed system 1 and silica gel micro mist in vacuum condition 30 ~ 60min of ultrasonic disperse, mixed system 1 is micro- silica gel micro mist
Loaded in hole, obtain compound 2；
C, edible glue and compound 2 be mixed, by spray drying, edible glue is fixed on silica gel micro mist surface, that is, obtains one kind
Stability phosphatidylserine micro mist for food.
According to the present invention, the stability of phosphatidylserine micro mist depends on the content of each material in micro mist, it is preferred that institute
State and prepare stable phosphatidylserine micro mist, required raw material includes the material of following parts by weight：Phosphatidylserine 5 ~ 25
Part, 8 ~ 16 parts of diphosphoinesitide, 5 ~ 25 parts of triphosphoinositide, 6 ~ 20 parts of asparatate, silica gel micro mist 10 ~ 30
Part, 5 ~ 25 parts of edible glue.
In the present invention phosphatidylserine can in the presence of diphosphoinesitide and triphosphoinositide with day
Complex reaction occurs for L-aminobutanedioic acid, it is to avoid phosphatidyl transfer, the division of serine base, phosphatidyl silk ammonia occur for phosphatidylserine
The phenomenon of acid inactivation, improves the stability of phosphatidylserine.
In the present invention, silica gel micro mist can load phosphatidylserine, be the carrier nontoxic to human body.
In the present invention, phosphatidylserine can be fixed on carrier by edible glue, it is to avoid phosphatidylserine is from carrier
On come off, the edible glue can be the art personnel Chang Zhi edible glue, it is preferred that the edible glue for draw primary
At least one of glue, gelatin, algin or xanthans.
It is preferred that, it can also be added in emulsifying agent, antioxidant, disintegrant, lubricant, preservative at least in step B
It is a kind of.
In the present invention, used specific emulsifying agent to emulsify phosphatidylserine, the emulsifying agent includes Sucrose Fatty Acid Ester
One in fat acid esters S-570, polyglyceryl fatty acid ester, glycerin monostearate, diglycerine fatty acid ester and stearoyl lactate
Plant or a variety of.
According to the present invention, in order to improve the inoxidizability of phosphatidylserine micro mist, extend the storage of phosphatidylserine
Time, it is preferred that also contain antioxidant and/or preservative in the phosphatidylserine micro mist, it is further preferred that described
Butylated hydroxy anisole that antioxidant is, dibutyl hydroxy toluene, propylgallate, tert-butylhydroquinone, tocopherol
At least one of with ascorbic acid.
The preservative is benzoic acid and salt, potassium sorbate, dehydroactic acid sodium, propylparaben, calcium propionate, double
In sodium acetate, sodium lactate, streptococcus lactis, natamycin, hydrogen peroxide, sulfur dioxide, sulphite and nitrite etc.
It is at least one.
It is disintegrated rapidly in human body for the ease of phosphatidylserine, is easy to absorption of human body, the phosphatidylserine is micro-
Also contain disintegrant in powder, the disintegrant can be dried starch, sodium carboxymethyl starch, low-substituted hydroxypropyl cellulose, crosslinking
At least one of mixture, Ac-Di-Sol of polyvinylpyrrolidone, sodium acid carbonate and citric acid composition etc..
A kind of stability phosphatidylserine micro mist for food, is prepared by the above method, is deposited with good
Stability is stored up, is had a wide range of application, can be added and use in a variety of environment such as milk powder, Yoghourt, beverage.
In the present invention, for the ease of the storage of phosphatidylserine micro mist, transport and use, it is preferred that will in the present invention
Medicament has been made in phosphatidylserine micro mist, is then vacuum-packed, and the present invention does not have special requirement to the species of medicament,
The medicament additive that can often know for one of ordinary skill in the art, can be used for tablet, pill, granule, pulvis, capsule
One kind in agent, emulsion.Or for food milk powder, Yoghourt etc..
A kind of stability phosphatidylserine micro mist for food, compared with prior art, the present invention have following skill
Art effect：
After the present invention mixes phosphatidylserine with diphosphoinesitide and triphosphoinositide, with asparatate network
Close, be further carried on by vacuum suction in carrier, by by the glue of Arabic gum, gelatin or xanthans by being sprayed at
Silica gel micro mist dry tack free obtains phosphatidylserine micro mist.Day is aided in by diphosphoinesitide and triphosphoinositide
L-aminobutanedioic acid is complexed, and further preferably avoids mistake of the phosphatidylserine in storage and use by the protection of silica gel micro mist
It is living, it can be directly added applied to food and for various tablets, pill, granule, pulvis, capsule, emulsion.
Embodiment
Technical scheme is clearly and completely described below in conjunction with embodiment, it is clear that described reality
It is only a part of embodiment of the invention to apply example, rather than whole embodiments.Based on the embodiment in the present invention, this area is general
The every other embodiment that logical technical staff is obtained under the premise of creative work is not made, belongs to what the present invention was protected
Scope.
Embodiment 1
A kind of stability phosphatidylserine micro mist for food, includes the raw material of substance of following parts by weight：Phosphatidyl silk ammonia
12 parts of acid, 13 parts of diphosphoinesitide, 15 parts of triphosphoinositide, 10 parts of asparatate, 20 parts of silica gel micro mist, La Bai
15 parts of glue；
Also contain glycerin monostearate, sucrose fatty ester S-570, butylhydroxy fennel in the phosphatidylserine micro mist
The mixture that ether, benzoic acid, sodium acid carbonate and citric acid are constituted；
A kind of preparation method of above-mentioned stability phosphatidylserine micro mist for food, comprises the following steps：
A, phosphatidylserine, diphosphoinesitide, triphosphoinositide be well mixed in the solution, then to mixing
Asparatate is added in solution, mixed system 1 is obtained；
B, by mixed system 1, silica gel micro mist, glycerin monostearate, sucrose fatty ester S-570, butylated hydroxy anisole, benzene
The mixture of formic acid, sodium acid carbonate and citric acid composition obtains compound 2 in vacuum condition ultrasonic disperse 40min;
C, by the surface for drawing primary glue to be sprayed to compound 2, after drying, that is, obtain a kind of stability phosphorus acyl thread ammonia for food
Sour micro mist.
Embodiment 2
A kind of stability phosphatidylserine micro mist for food, includes the material of following parts by weight：Phosphatidylserine 8
Part, 10 parts of diphosphoinesitide, 12 parts of triphosphoinositide, 8 parts of asparatate, 18 parts of silica gel micro mist, 10 parts of gelatin；
Also contain sucrose fatty ester S-570, diglycerine fatty acid ester, butylated hydroxy-a in the phosphatidylserine micro mist
Benzene, sodium benzoate, sodium carboxymethyl starch；
A kind of preparation method of above-mentioned stability phosphatidylserine micro mist for food, comprises the following steps：
A, phosphatidylserine, diphosphoinesitide, triphosphoinositide be well mixed in the solution, then to mixing
Asparatate is added in solution, mixed system 1 is obtained；
B, by mixed system 1, silica gel micro mist, sucrose fatty ester S-570, diglycerine fatty acid ester, dibutyl hydroxy toluene, benzene
Sodium formate, sodium carboxymethyl starch obtain compound 2 in vacuum condition ultrasonic disperse 40min;
C, the surface that gelatin is sprayed to compound 2, after drying, that is, obtain a kind of stability phosphatidylserine for food
Micro mist.
Embodiment 3
A kind of stability phosphatidylserine micro mist for food, includes the material of following parts by weight：Phosphatidylserine 16
Part, 15 parts of diphosphoinesitide, 18 parts of triphosphoinositide, 15 parts of asparatate, 26 parts of silica gel micro mist, algin 20
Part；
Also contain sucrose fatty ester S-570, polyglyceryl fatty acid ester, sodium sulfite, spy in the phosphatidylserine micro mist
Butylhydroquinone, dehydroactic acid sodium, low-substituted hydroxypropyl cellulose；
A kind of preparation method of above-mentioned stability phosphatidylserine micro mist for food, comprises the following steps：
A, phosphatidylserine, diphosphoinesitide, triphosphoinositide be well mixed in the solution, then to mixing
Asparatate is added in solution, mixed system 1 is obtained；
B, by mixed system 1, silica gel micro mist, sucrose fatty ester S-570, polyglyceryl fatty acid ester, sodium sulfite, tertiary butyl pair
Benzenediol, dehydroactic acid sodium, low-substituted hydroxypropyl cellulose obtain compound 2 in vacuum condition ultrasonic disperse 40min;
C, the surface that algin is sprayed to compound 2, after drying, that is, obtain a kind of stability phosphorus acyl thread ammonia for food
Sour micro mist.
Embodiment 4
A kind of stability phosphatidylserine micro mist for food, includes the material of following parts by weight：Phosphatidylserine 5
Part, 8 parts of diphosphoinesitide, 5 parts of triphosphoinositide, 6 parts of asparatate, 10 parts of silica gel micro mist, 5 parts of algin；
Also contain disintegrant, lubricant, sucrose fatty ester S-570, P-hydroxybenzoic acid in the phosphatidylserine micro mist
Propyl ester, PVPP；
A kind of preparation method of above-mentioned stability phosphatidylserine micro mist for food, comprises the following steps：
A, phosphatidylserine, diphosphoinesitide, triphosphoinositide be well mixed in the solution, then to mixing
Asparatate is added in solution, mixed system 1 is obtained；
B, by mixed system 1, silica gel micro mist, disintegrant, lubricant, sucrose fatty ester S-570, propylparaben,
PVPP obtains compound 2 in vacuum condition ultrasonic disperse 40min；
C, the surface that algin is sprayed to compound 2, after drying, that is, obtain a kind of stability phosphorus acyl thread ammonia for food
Sour micro mist.
Embodiment 5
A kind of stability phosphatidylserine micro mist for food, includes the material of following parts by weight：Phosphatidylserine 25
Part, 16 parts of diphosphoinesitide, 25 parts of triphosphoinositide, 20 parts of asparatate, 30 parts of silica gel micro mist, xanthans 25
Part；
Also contain disintegrant, lubricant, propylgallate, sucrose fatty ester S-570 in the phosphatidylserine micro mist；
A kind of preparation method of above-mentioned stability phosphatidylserine micro mist for food, comprises the following steps：
A, phosphatidylserine, diphosphoinesitide, triphosphoinositide be well mixed in the solution, then to mixing
Asparatate is added in solution, mixed system 1 is obtained；
B, by mixed system 1, silica gel micro mist, disintegrant, lubricant, propylgallate, sucrose fatty ester S-570 in vacuum
Condition ultrasonic disperse 40min, obtains compound 2；
C, the surface that xanthans is sprayed to compound 2, after drying, that is, obtain a kind of stability phosphorus acyl thread ammonia for food
Sour micro mist.
It is obvious to a person skilled in the art that the invention is not restricted to the details of above-mentioned one exemplary embodiment, Er Qie
In the case of without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, embodiment all should be regarded as exemplary, and be nonrestrictive, the scope of the present invention is by appended power
Profit is required rather than described above is limited, it is intended that all in the implication and scope of the equivalency of claim by falling
Change is included in the present invention.
Claims (9)
1. a kind of preparation method of stability phosphatidylserine micro mist for food, comprises the following steps：
A, phosphatidylserine, diphosphoinesitide, triphosphoinositide be well mixed in the solution, then to mixing
Asparatate complexing is added in solution, mixed system 1 is obtained；
B, by mixed system 1 and silica gel micro mist in vacuum condition 30 ~ 60min of ultrasonic disperse, mixed system 1 is micro- silica gel micro mist
Loaded in hole, obtain compound 2；
C, edible glue and compound 2 be mixed, by spray drying, edible glue is fixed on silica gel micro mist surface, that is, obtains one kind
Stability phosphatidylserine micro mist for food.
2. a kind of preparation method of stability phosphatidylserine micro mist for food, its feature according to claim 1
It is：Described to prepare stable phosphatidylserine micro mist, required raw material includes the material of following parts by weight：Phosphatidyl silk ammonia
5 ~ 25 parts of acid, 8 ~ 16 parts of diphosphoinesitide, 5 ~ 25 parts of triphosphoinositide, 6 ~ 20 parts of asparatate, silica gel micro mist
10 ~ 30 parts, 5 ~ 25 parts of edible glue.
3. a kind of preparation method of stability phosphatidylserine micro mist for food, its feature according to claim 1
It is：The edible glue is at least one of the primary glue of drawing, gelatin, algin or xanthans.
4. a kind of preparation method of stability phosphatidylserine micro mist for food, its feature according to claim 1
It is：Emulsifying agent, antioxidant, disintegrant, lubricant, at least one of the preservatives are added in step B.
5. a kind of preparation method of stability phosphatidylserine micro mist for food, its feature according to claim 4
It is：The emulsifying agent includes sucrose fatty ester S-570, polyglyceryl fatty acid ester, glycerin monostearate, diglycerine fatty
One or more in acid esters and stearoyl lactate.
6. a kind of preparation method of stability phosphatidylserine micro mist for food, its feature according to claim 4
It is：Butylated hydroxy anisole that the antioxidant is, dibutyl hydroxy toluene, propylgallate, tertiary butyl are to benzene two
At least one of phenol, tocopherol and ascorbic acid.
7. a kind of preparation method of stability phosphatidylserine micro mist for food, its feature according to claim 4
It is：The preservative is benzoic acid and salt, potassium sorbate, dehydroactic acid sodium, propylparaben, calcium propionate, double second
In sour sodium, sodium lactate, streptococcus lactis, natamycin, hydrogen peroxide, sulfur dioxide, sulphite and nitrite at least
It is a kind of.
8. a kind of preparation method of stability phosphatidylserine micro mist for food, its feature according to claim 1
It is：The disintegrant is dried starch, sodium carboxymethyl starch, low-substituted hydroxypropyl cellulose, PVPP, carbon
At least one of mixture that sour hydrogen sodium and citric acid are constituted, Ac-Di-Sol.
9. a kind of stability phosphatidylserine micro mist for food, it is characterised in that：The stability phosphatidylserine
Micro mist is prepared by any one of claim 1-8 methods described.
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Cited By (1)
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| CN113317488A (en) * | 2021-06-30 | 2021-08-31 | 四川省食品发酵工业研究设计院有限公司 | Composite quality modifier, composite preservative and application of composite preservative in preparation of phylla cakes |
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| CN107223953B (en) | 2019-12-17 |
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