CN107216096A - A kind of preparation method of enhanced rubber powder modified concrete asphalt mortar - Google Patents

A kind of preparation method of enhanced rubber powder modified concrete asphalt mortar Download PDF

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Publication number
CN107216096A
CN107216096A CN201710599851.6A CN201710599851A CN107216096A CN 107216096 A CN107216096 A CN 107216096A CN 201710599851 A CN201710599851 A CN 201710599851A CN 107216096 A CN107216096 A CN 107216096A
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China
Prior art keywords
rubber powder
parts
weight
preparation
asphalt mortar
Prior art date
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Pending
Application number
CN201710599851.6A
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Chinese (zh)
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张娟
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Individual
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Individual
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Priority to CN201710599851.6A priority Critical patent/CN107216096A/en
Publication of CN107216096A publication Critical patent/CN107216096A/en
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Classifications

    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B28/00Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
    • C04B28/02Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing hydraulic cements other than calcium sulfates
    • C04B28/04Portland cements
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B40/00Processes, in general, for influencing or modifying the properties of mortars, concrete or artificial stone compositions, e.g. their setting or hardening ability
    • C04B40/0028Aspects relating to the mixing step of the mortar preparation
    • C04B40/0039Premixtures of ingredients
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2111/00Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
    • C04B2111/00474Uses not provided for elsewhere in C04B2111/00
    • C04B2111/0075Uses not provided for elsewhere in C04B2111/00 for road construction
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2111/00Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
    • C04B2111/20Resistance against chemical, physical or biological attack
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2111/00Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
    • C04B2111/50Flexible or elastic materials

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
  • Materials Engineering (AREA)
  • Structural Engineering (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Processes Of Treating Macromolecular Substances (AREA)

Abstract

The invention discloses a kind of preparation method of enhanced rubber powder modified concrete asphalt mortar, first rubber powder and emulsifying agent are added to the water jointly and are uniformly mixing to obtain rubber powder emulsion, then add in rubber powder emulsion and emulsify after silane coupler KH 570 is mixed with asphalt high-temperature, tetraethyl orthosilicate is added dropwise again carries out solgel reaction in situ and obtain rubber powder modified asphalt emulsion, enhanced rubber powder modified concrete asphalt mortar is obtained after being well mixed with the raw material such as portland cement, quartz sand.Cement asphalt mortar produced by the present invention both has excellent elasticity and weatherability, there is higher mechanical strength and stability again, and performance is good, and durability is strong.

Description

A kind of preparation method of enhanced rubber powder modified concrete asphalt mortar
Technical field
The present invention relates to cement mortar material technical field, more particularly to a kind of enhanced modifying rubber powder cement pitch sand The preparation method of slurry.
Background technology
Cement asphalt mortar is that one kind is made up of raw material such as cement, emulsified asphalt, fine aggregate, water and a variety of additives, Through hydrated cementitious hardening and a kind of new organic/inorganic composite material formed by the cementing collective effect of pitch demulsification, in high-speed iron Elastic insert is served as in the ballastless track structure of road, plays a part of filling adjustment, load power transmission.With China's high-speed iron in recent years The fast development of road infrastructure, cement asphalt mortar has also obtained increasing concern.Due to emulsified asphalt exist it is weather-proof Property difference defect, and improve elastic performance it is limited, have research will have high resiliency and wide material sources, cheap rubber Rubber powder is compounded to improve the weatherability of mortar with emulsified asphalt.CN200710133454 is disclosed for cement asphalt mortar Rubber powder-asphalt emulsion, by the way that rubber powder and emulsified asphalt are carried out into the weatherability that compounding improves elastic mortar.However, The mechanical strength of rubber powder modified concrete asphalt mortar is relatively low, influences its performance and durability, it is necessary to make improvements.
The content of the invention
The object of the invention is exactly that there is provided a kind of enhanced modifying rubber powder cement pitch in order to make up the defect of prior art The preparation method of mortar.
The present invention is achieved by the following technical solutions:
A kind of preparation method of enhanced rubber powder modified concrete asphalt mortar, comprises the following steps:
(1)By 2-4 parts by weight anionic emulsifier, 0.5-1 parts by weight nonionic emulsifier, 0.1-1 parts by weight stabilizers 600-1000r/min stirrings 5-10min in 20-30 parts by weight water is added, 5-15 parts by weight of rubber powder is then added and turns in same Speed is lower to be continued to stir 20-30min, obtains rubber powder emulsion;
(2)1-2 parts by weight Silane coupling reagent KH-570 is added in 30-40 parts by weight pitches in 110-160 DEG C of mixed processing 5- 10min, then adds step(1)60-70 DEG C of high-speed stirred 20-30min in obtained rubber powder emulsion, being cooled to after normal temperature will PH is adjusted to 8-8.5, and 3-5 parts by weight tetraethyl orthosilicate and stirring reaction 12-24h is slowly added dropwise, and obtains rubber powder-modified pitch breast Liquid;
(3)By step(2)Obtained rubber powder-modified pitch emulsion and 100-150 parts by weight silicate cement, 150-200 weights Measure part quartz sand, 0.5-1 parts by weight water reducer, 0.05-0.1 parts by weight defoamer, 20-30 parts by weight water to be well mixed, obtain Enhanced rubber powder modified concrete asphalt mortar.
The anionic emulsifier is in neopelex, sodium lignin sulfonate, lauryl sodium sulfate It is one or more of.
The nonionic emulsifier is the one or more in NPE, Tween-80, Arlacel-80.
The stabilizer is the one or more in hydroxyethyl cellulose, carboxymethyl cellulose, polyvinyl alcohol.
The rubber powder is 100-200 mesh.
The water reducer is polycarboxylic acids dehydragent.
The defoamer is polysiloxane-based defoamer.
It is an advantage of the invention that:
Rubber powder and emulsifying agent are first added to the water by the present invention jointly is uniformly mixing to obtain rubber powder emulsion, then will be silane coupled Agent KH-570 is added in rubber powder emulsion after being mixed with asphalt high-temperature and emulsified, then tetraethyl orthosilicate is added dropwise carries out colloidal sol in situ-solidifying Glue is reacted, and inorganic nano layer is introduced on emulsified asphalt surface, rubber powder-modified pitch emulsion is obtained, with portland cement, quartz Enhanced rubber powder modified concrete asphalt mortar is obtained after the raw materials such as sand are well mixed.The present invention passes through newborn to rubber powder-pitch Inorganic constituents nano silicon is introduced in liquid, the three-dimensional netted knot of rubber-silica-pitch can be formed in mortar Structure, with certain physical and chemical stability, there is good enhancing effect to mortar, has made obtained cement asphalt mortar both With excellent elasticity and weatherability, there are higher mechanical strength and stability again, performance is good, and durability is strong.
Embodiment
A kind of preparation method of enhanced rubber powder modified concrete asphalt mortar, comprises the following steps:
(1)2 parts by weight anionic emulsifier, 0.5 parts by weight nonionic emulsifier, 0.1 parts by weight stabilizer are added 20 600r/min stirs 5min in parts by weight water, then adds 5 parts by weight of rubber powder in continuing to stir 20min under same rotating speed, obtains To rubber powder emulsion;
(2)1 parts by weight Silane coupling reagent KH-570 is added in 30 parts by weight 70# pitches in 110 DEG C of mixed processing 5min, then Add 40 parts by weight steps(1)60 DEG C of high-speed stirred 20min, are cooled to after normal temperature pH being adjusted to 8 in described rubber powder emulsion, 3 parts by weight tetraethyl orthosilicates and stirring reaction 12h is slowly added dropwise, rubber powder-modified pitch emulsion is obtained;
(3)By step(2)Obtained rubber powder-modified pitch emulsion and 100 parts by weight silicate cement, 150 parts by weight quartz Sand, 0.5 parts by weight water reducer, 0.05 parts by weight defoamer, 20 parts by weight water are well mixed, and obtain enhanced modifying rubber powder water Mud asphalt mortar, bituminous mortar.
The anionic emulsifier is neopelex.
The nonionic emulsifier is NPE.
The stabilizer is hydroxyethyl cellulose.
The rubber powder is 100 mesh.
The water reducer is LG polycarboxylate water-reducers CP-WRM.
The defoamer is dimethyl polysiloxane.

Claims (7)

1. a kind of preparation method of enhanced rubber powder modified concrete asphalt mortar, it is characterised in that comprise the following steps:
(1)By 2-4 parts by weight anionic emulsifier, 0.5-1 parts by weight nonionic emulsifier, 0.1-1 parts by weight stabilizers 600-1000r/min stirrings 5-10min in 20-30 parts by weight water is added, 5-15 parts by weight of rubber powder is then added and turns in same Speed is lower to be continued to stir 20-30min, obtains rubber powder emulsion;
(2)1-2 parts by weight Silane coupling reagent KH-570 is added in 30-40 parts by weight pitches in 110-160 DEG C of mixed processing 5- 10min, then adds step(1)60-70 DEG C of high-speed stirred 20-30min in obtained rubber powder emulsion, being cooled to after normal temperature will PH is adjusted to 8-8.5, and 3-5 parts by weight tetraethyl orthosilicate and stirring reaction 12-24h is slowly added dropwise, and obtains rubber powder-modified pitch breast Liquid;
(3)By step(2)Obtained rubber powder-modified pitch emulsion and 100-150 parts by weight silicate cement, 150-200 weights Measure part quartz sand, 0.5-1 parts by weight water reducer, 0.05-0.1 parts by weight defoamer, 20-30 parts by weight water to be well mixed, obtain Enhanced rubber powder modified concrete asphalt mortar.
2. a kind of preparation method of high strength anti-abrasion rubber asphalt waterproof coating according to claim 1, it is characterised in that The anionic emulsifier is one kind or several in neopelex, sodium lignin sulfonate, lauryl sodium sulfate Kind.
3. a kind of preparation method of high strength anti-abrasion rubber asphalt waterproof coating according to claim 1, it is characterised in that The nonionic emulsifier is the one or more in NPE, Tween-80, Arlacel-80.
4. a kind of preparation method of high strength anti-abrasion rubber asphalt waterproof coating according to claim 1, it is characterised in that The stabilizer is the one or more in hydroxyethyl cellulose, carboxymethyl cellulose, polyvinyl alcohol.
5. a kind of preparation method of enhanced rubber powder modified concrete asphalt mortar according to claim 1, its feature exists In the rubber powder is 100-200 mesh.
6. a kind of preparation method of enhanced rubber powder modified concrete asphalt mortar according to claim 1, its feature exists In the water reducer is polycarboxylic acids dehydragent.
7. a kind of preparation method of enhanced rubber powder modified concrete asphalt mortar according to claim 1, its feature exists In the defoamer is polysiloxane-based defoamer.
CN201710599851.6A 2017-07-21 2017-07-21 A kind of preparation method of enhanced rubber powder modified concrete asphalt mortar Pending CN107216096A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201710599851.6A CN107216096A (en) 2017-07-21 2017-07-21 A kind of preparation method of enhanced rubber powder modified concrete asphalt mortar

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201710599851.6A CN107216096A (en) 2017-07-21 2017-07-21 A kind of preparation method of enhanced rubber powder modified concrete asphalt mortar

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CN107216096A true CN107216096A (en) 2017-09-29

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110372937A (en) * 2019-08-02 2019-10-25 王云莲 Organosilicon-emulsified asphalt glue powder material, Roof system and preparation method thereof
CN111875814A (en) * 2020-08-03 2020-11-03 安徽理工大学 Preparation method of modified rubber powder by sol-gel method
CN112759943A (en) * 2021-01-22 2021-05-07 熊彪 Emulsified asphalt and preparation method thereof
CN114685121A (en) * 2022-04-11 2022-07-01 山东仝聚建筑节能科技有限公司 Composite mortar and production process thereof

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101173106A (en) * 2007-09-30 2008-05-07 江苏博特新材料有限公司 Rubber powder-asphalt emulsion for concrete asphalt mortar and method for producing the same
CN101948623A (en) * 2010-09-14 2011-01-19 江苏省苏安能节能建材科技有限公司 Rubber powder modified emulsified asphalt and preparation method thereof and CA mortar prepared by emulsified asphalt

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101173106A (en) * 2007-09-30 2008-05-07 江苏博特新材料有限公司 Rubber powder-asphalt emulsion for concrete asphalt mortar and method for producing the same
CN101948623A (en) * 2010-09-14 2011-01-19 江苏省苏安能节能建材科技有限公司 Rubber powder modified emulsified asphalt and preparation method thereof and CA mortar prepared by emulsified asphalt

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
李俊: "国内橡胶粉界面改性方法及其表征的研究现状", 《城市道桥与防洪》 *

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110372937A (en) * 2019-08-02 2019-10-25 王云莲 Organosilicon-emulsified asphalt glue powder material, Roof system and preparation method thereof
CN111875814A (en) * 2020-08-03 2020-11-03 安徽理工大学 Preparation method of modified rubber powder by sol-gel method
CN112759943A (en) * 2021-01-22 2021-05-07 熊彪 Emulsified asphalt and preparation method thereof
CN114685121A (en) * 2022-04-11 2022-07-01 山东仝聚建筑节能科技有限公司 Composite mortar and production process thereof
CN114685121B (en) * 2022-04-11 2023-02-28 山东仝聚建筑节能科技有限公司 Composite mortar and production process thereof

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Application publication date: 20170929

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