CN107213862A - A kind of graphene oxide production reduction reactor with environmental-protection adsorption function - Google Patents

A kind of graphene oxide production reduction reactor with environmental-protection adsorption function Download PDF

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Publication number
CN107213862A
CN107213862A CN201710374224.2A CN201710374224A CN107213862A CN 107213862 A CN107213862 A CN 107213862A CN 201710374224 A CN201710374224 A CN 201710374224A CN 107213862 A CN107213862 A CN 107213862A
Authority
CN
China
Prior art keywords
inner bag
kettle
fixedly connected
environmental
gas
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
CN201710374224.2A
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Chinese (zh)
Inventor
刘美君
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Qingyuan Starter Intelligent Technology Co Ltd
Original Assignee
Qingyuan Starter Intelligent Technology Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Qingyuan Starter Intelligent Technology Co Ltd filed Critical Qingyuan Starter Intelligent Technology Co Ltd
Priority to CN201710374224.2A priority Critical patent/CN107213862A/en
Publication of CN107213862A publication Critical patent/CN107213862A/en
Withdrawn legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/34Chemical or biological purification of waste gases
    • B01D53/46Removing components of defined structure
    • B01D53/48Sulfur compounds
    • B01D53/50Sulfur oxides
    • B01D53/501Sulfur oxides by treating the gases with a solution or a suspension of an alkali or earth-alkali or ammonium compound
    • B01D53/504Sulfur oxides by treating the gases with a solution or a suspension of an alkali or earth-alkali or ammonium compound characterised by a specific device
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006Controlling or regulating processes
    • B01J19/002Avoiding undesirable reactions or side-effects, e.g. avoiding explosions, or improving the yield by suppressing side-reactions
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2251/00Reactants
    • B01D2251/30Alkali metal compounds
    • B01D2251/304Alkali metal compounds of sodium
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2251/00Reactants
    • B01D2251/60Inorganic bases or salts
    • B01D2251/604Hydroxides
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2259/00Type of treatment
    • B01D2259/12Methods and means for introducing reactants
    • B01D2259/124Liquid reactants
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00074Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/00099Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor the reactor being immersed in the heat exchange medium
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00132Controlling the temperature using electric heating or cooling elements
    • B01J2219/00135Electric resistance heaters

Abstract

Reduction reactor is produced the invention discloses a kind of graphene oxide with environmental-protection adsorption function, including kettle, the inside of the kettle is fixedly connected with inner bag, the side of the support is fixedly connected with supporting plate, the upper surface of the supporting plate is provided with gas treatment groove, the side lower end of the gas treatment groove is provided with the first control valve, the upper end of the inner bag is fixedly connected with gas pipeline, the other end of the gas pipeline is fixedly connected with gas treatment groove, the side of the gas pipeline is provided with the second control valve, the upper end of the kettle is provided with motor, the motor is connected in series second switch, the rotating shaft of the motor is fixedly connected with agitator, the upper shaft connection kettle and inner bag of the agitator, the inner side of the inner bag is provided with fix bar.This kind has the graphene oxide production reduction reactor of environmental-protection adsorption function, and the gas produced when can be to graphite oxidation handles, it is to avoid gas occurs and sheds situation about being damaged to operator.

Description

A kind of graphene oxide production reduction reactor with environmental-protection adsorption function
Technical field
The present invention relates to graphene production reactor technical field, specially a kind of oxidation with environmental-protection adsorption function Graphene produces reduction reactor.
Background technology
Graphene be one kind by carbon atom with sp2Hybridized orbit composition hexangle type is in the single flat that honeycomb lattice is arranged to make up Face film, the two-dimensional material of only one of which carbon atom thickness is referred to as the fields such as the 21 century energy, electronics most glittering star, It is international study hotspot in recent years.
At present, it can continue to produce the sour gas such as sulfur dioxide when graphene production reduction, when producing due to graphene Based on artificial operate, therefore gas comes out and easily can cause potential injury to the body of operator.
The content of the invention
Reduction reactor is produced it is an object of the invention to provide a kind of graphene oxide with environmental-protection adsorption function, To solve the problems mentioned in the above background technology.
To achieve the above object, the present invention provides following technical scheme:A kind of graphite oxide with environmental-protection adsorption function Alkene produces reduction reactor, including kettle, and the surface fixed cover of the kettle is connected to support, and the surface of the support is provided with the One switch and second switch, the inside of the kettle are fixedly connected with inner bag, and the upper end of the inner bag is provided with charging aperture, described interior The lower end of courage is provided with discharging opening, and heating chamber is provided between the kettle and inner bag, and the upper end of the heating chamber is provided with water inlet, institute The lower end for stating heating chamber is provided with delivery port, and the surface wrap of the inner bag has heating tube, and the inside of the heating tube is socketed with electricity Heated filament, the heating wire is connected in series first switch, and the side of the support is fixedly connected with supporting plate, the supporting plate it is upper Surface is provided with gas treatment groove, and the side lower end of the gas treatment groove is provided with the first control valve, and the upper end of the inner bag is consolidated Surely gas pipeline is connected with, the other end of the gas pipeline is fixedly connected with gas treatment groove, and the side of the gas pipeline is set There is the second control valve, the upper end of the kettle is provided with motor, and the motor is connected in series second switch, the rotating shaft of the motor Agitator is fixedly connected with, the upper shaft connection kettle and inner bag of the agitator, the inner side of the inner bag are provided with fixation Bar.
It is preferred that, the inside of the gas treatment groove fills sodium hydroxide solution.
It is preferred that, the upper surface of the gas treatment groove is provided with solution inlet port, and the upper end of the solution inlet port is provided with sealing Lid.
It is preferred that, the distance between described fix bar is 3 to 5 centimetres.
Compared with prior art, the beneficial effects of the invention are as follows:The graphene oxide that this kind has environmental-protection adsorption function is given birth to Production reduction is run with reactor by second switch controlled motor, and motor drives agitator to rotate, and agitator can stir inner bag The graphite raw material of bottom, so as to blend the larger graphite of volume with fix bar by agitator, accelerates the oxidation of graphite Speed;Open the inside that the gas inside the second control valve, inner bag enters gas treatment groove by gas pipeline so that titanium dioxide The sour gas such as sulphur are absorbed by sodium hydroxide, it is to avoid gas occur and shed situation about being damaged to operator.
Brief description of the drawings
Fig. 1 is whole for a kind of graphene oxide production reduction reactor with environmental-protection adsorption function of the present invention Body structural front view;
Fig. 2 produces the kettle of reduction reactor for a kind of graphene oxide with environmental-protection adsorption function of the present invention Body sectional view.
Division mark is as follows in accompanying drawing:1st, kettle, 2, support, 3, first switch, 4, second switch, 5, inner bag, 6, heating Chamber, 7, charging aperture, 8, discharging opening, 9, water inlet, 10, delivery port, 11, heating tube, 12, heating wire, 13, gas pipeline, 14, gas Body treatment trough, the 15, first control valve, the 16, second control valve, 17, motor, 18, agitator, 19, fix bar, 20, supporting plate, 21st, solution inlet port, 22, closure.
Embodiment
In conjunction with the accompanying drawings, the present invention is further explained in detail.These accompanying drawings are simplified schematic diagram, only with Illustration illustrates the basic structure of the present invention, therefore it only shows the composition relevant with the present invention.
Fig. 1-2 is referred to, the present invention provides a kind of technical scheme:A kind of graphene oxide life with environmental-protection adsorption function Reduction reactor, including kettle 1 are produced, the surface fixed cover of kettle 1 is connected to support 2, and the surface of support 2 is provided with first switch 3 With second switch 4, first switch 3 and second switch 4 are connected with the circuit connected in series of either inside, and the inside of kettle 1, which is fixed, to be connected Inner bag 5 is connected to, the upper end of inner bag 5 is provided with charging aperture 7, and the lower end of inner bag 5 is provided with discharging opening 8, is provided between kettle 1 and inner bag 5 Heating chamber 6, the upper end of heating chamber 6 is provided with water inlet 9, and the lower end of heating chamber 6 is provided with delivery port 10, and the surface wrap of inner bag 5 has Heating tube 11, the inside of heating tube 11 is socketed with heating wire 12, and heating wire 12 is connected in series first switch 3, passes through delivery port 10 Water is injected to the inside of heating chamber 6, then controls heating wire 12 to heat the water inside heating chamber 6 by first switch 3, from And heat can be provided the reaction inside inner bag 5, the side of support 2 is fixedly connected with supporting plate 20, the upper table of supporting plate 20 Face is provided with gas treatment groove 14, and the upper surface of gas treatment groove 14 is provided with solution inlet port 21, and the upper end of solution inlet port 21 is provided with Closure 22, can be to sodium hydroxide solution be added inside gas treatment groove 14, so as in absorbing by solution inlet port 21 Gas inside courage 5, the side lower end of gas treatment groove 14 is provided with the first control valve 15, can be released by the first control valve 15 Solution inside gas treatment groove 14, is conveniently replaceable, and the upper end of inner bag 5 is fixedly connected with gas pipeline 13, gas pipeline 13 The other end is fixedly connected with gas treatment groove 14, and the inside of gas treatment groove 14 fills sodium hydroxide solution, sodium hydroxide solution energy The gas that produces when enough absorbing graphite oxidation, it is to avoid gas occur and shed situation about being damaged to operator, gas pipeline 13 side is provided with the second control valve 16, and the upper end of kettle 1 is provided with motor 17, the model YS6314 of motor 17, motor 17 Second switch 4 is connected in series, the rotating shaft of motor 17 is fixedly connected with agitator 18, the upper shaft connection He of kettle 1 of agitator 18 Inner bag 5, the inner side of inner bag 5 is provided with fix bar 19, and the distance between fix bar 19 is 3 to 5 centimetres, passes through second switch 4 Controlled motor 17 is run, and motor 17 drives agitator 18 to rotate, and agitator 18 can stir the graphite raw material of the bottom of inner bag 5, from And can be blended the larger graphite of volume by agitator 18 and fix bar 19, accelerate the oxidation rate of graphite.
The present invention is in the specific implementation:When in use, water is injected to the inside of heating chamber 6 by delivery port 10, then passed through The control heating wire 12 of first switch 3 is heated to the water inside heating chamber 6, so as to provide the reaction inside inner bag 5 Heat;Run by the controlled motor 17 of second switch 4, motor 17 drives agitator 18 to rotate, and agitator 18 can stir inner bag 5 The graphite raw material of bottom, so as to blend the larger graphite of volume with fix bar 19 by agitator 18, accelerates graphite Oxidation rate;The gas inside the second control valve 16, inner bag 5 is opened by gas pipeline 13 to enter in gas treatment groove 14 Portion so that the sour gas such as sulfur dioxide is absorbed by sodium hydroxide, it is to avoid gas occur and shed what is damaged to operator Situation.
Using the above-mentioned desirable embodiment according to the present invention as enlightenment, by above-mentioned description, relevant staff is complete Various changes and amendments can be carried out without departing from the scope of the technological thought of the present invention' entirely.The technology of this invention Property scope is not limited to the content on specification, it is necessary to its technical scope is determined according to right.

Claims (4)

1. a kind of graphene oxide production reduction reactor with environmental-protection adsorption function, including kettle (1), its feature exist In:The surface fixed cover of the kettle (1) is connected to support (2), and the surface of the support (2) is provided with first switch (3) and second Switch (4), the inside of the kettle (1) is fixedly connected with inner bag (5), and the upper end of the inner bag (5) is provided with charging aperture (7), institute The lower end for stating inner bag (5) is provided with discharging opening (8), and heating chamber (6), the heating chamber are provided between the kettle (1) and inner bag (5) (6) upper end is provided with water inlet (9), and the lower end of the heating chamber (6) is provided with delivery port (10), and the surface of the inner bag (5) is twined Heating tube (11) is wound with, the inside of the heating tube (11) is socketed with heating wire (12), and the heating wire (12) is connected in series One switch (3);
The side of the support (2) is fixedly connected with supporting plate (20), and the upper surface of the supporting plate (20) is provided with gas Groove (14) is managed, the side lower end of the gas treatment groove (14) is provided with the first control valve (15), and the upper end of the inner bag (5) is fixed Gas pipeline (13) is connected with, the other end of the gas pipeline (13) is fixedly connected with gas treatment groove (14), the flue The side in road (13) is provided with the second control valve (16), and the upper end of the kettle (1) is provided with motor (17), motor (17) string Connection connection second switch (4), the rotating shaft of the motor (17) is fixedly connected with agitator (18), the upper end of the agitator (18) Axle connection kettle (1) and inner bag (5), the inner side of the inner bag (5) are provided with fix bar (19).
2. a kind of graphene oxide production reduction reactor with environmental-protection adsorption function according to claim 1, its It is characterised by:The inside of the gas treatment groove (14) fills sodium hydroxide solution.
3. a kind of graphene oxide production reduction reactor with environmental-protection adsorption function according to claim 1, its It is characterised by:The upper surface of the gas treatment groove (14) is provided with solution inlet port (21), and the upper end of the solution inlet port (21) is set There is closure (22).
4. a kind of graphene oxide production reduction reactor with environmental-protection adsorption function according to claim 1, its It is characterised by:The distance between described fix bar (19) is 3 to 5 centimetres.
CN201710374224.2A 2017-05-24 2017-05-24 A kind of graphene oxide production reduction reactor with environmental-protection adsorption function Withdrawn CN107213862A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201710374224.2A CN107213862A (en) 2017-05-24 2017-05-24 A kind of graphene oxide production reduction reactor with environmental-protection adsorption function

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201710374224.2A CN107213862A (en) 2017-05-24 2017-05-24 A kind of graphene oxide production reduction reactor with environmental-protection adsorption function

Publications (1)

Publication Number Publication Date
CN107213862A true CN107213862A (en) 2017-09-29

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CN201710374224.2A Withdrawn CN107213862A (en) 2017-05-24 2017-05-24 A kind of graphene oxide production reduction reactor with environmental-protection adsorption function

Country Status (1)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114432992A (en) * 2022-01-19 2022-05-06 深圳市鸿盛天诚电子有限公司 High-efficient new forms of energy lithium battery material preparation facilities

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114432992A (en) * 2022-01-19 2022-05-06 深圳市鸿盛天诚电子有限公司 High-efficient new forms of energy lithium battery material preparation facilities
CN114432992B (en) * 2022-01-19 2023-11-03 常州厚德再生资源科技有限公司 High-efficient new forms of energy lithium battery material preparation facilities

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Application publication date: 20170929