CN107213862A - A kind of graphene oxide production reduction reactor with environmental-protection adsorption function - Google Patents
A kind of graphene oxide production reduction reactor with environmental-protection adsorption function Download PDFInfo
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- CN107213862A CN107213862A CN201710374224.2A CN201710374224A CN107213862A CN 107213862 A CN107213862 A CN 107213862A CN 201710374224 A CN201710374224 A CN 201710374224A CN 107213862 A CN107213862 A CN 107213862A
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- Prior art keywords
- inner bag
- kettle
- fixedly connected
- environmental
- gas
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/34—Chemical or biological purification of waste gases
- B01D53/46—Removing components of defined structure
- B01D53/48—Sulfur compounds
- B01D53/50—Sulfur oxides
- B01D53/501—Sulfur oxides by treating the gases with a solution or a suspension of an alkali or earth-alkali or ammonium compound
- B01D53/504—Sulfur oxides by treating the gases with a solution or a suspension of an alkali or earth-alkali or ammonium compound characterised by a specific device
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
- B01J19/002—Avoiding undesirable reactions or side-effects, e.g. avoiding explosions, or improving the yield by suppressing side-reactions
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2251/00—Reactants
- B01D2251/30—Alkali metal compounds
- B01D2251/304—Alkali metal compounds of sodium
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2251/00—Reactants
- B01D2251/60—Inorganic bases or salts
- B01D2251/604—Hydroxides
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2259/00—Type of treatment
- B01D2259/12—Methods and means for introducing reactants
- B01D2259/124—Liquid reactants
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
- B01J2219/00099—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor the reactor being immersed in the heat exchange medium
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00132—Controlling the temperature using electric heating or cooling elements
- B01J2219/00135—Electric resistance heaters
Abstract
Reduction reactor is produced the invention discloses a kind of graphene oxide with environmental-protection adsorption function, including kettle, the inside of the kettle is fixedly connected with inner bag, the side of the support is fixedly connected with supporting plate, the upper surface of the supporting plate is provided with gas treatment groove, the side lower end of the gas treatment groove is provided with the first control valve, the upper end of the inner bag is fixedly connected with gas pipeline, the other end of the gas pipeline is fixedly connected with gas treatment groove, the side of the gas pipeline is provided with the second control valve, the upper end of the kettle is provided with motor, the motor is connected in series second switch, the rotating shaft of the motor is fixedly connected with agitator, the upper shaft connection kettle and inner bag of the agitator, the inner side of the inner bag is provided with fix bar.This kind has the graphene oxide production reduction reactor of environmental-protection adsorption function, and the gas produced when can be to graphite oxidation handles, it is to avoid gas occurs and sheds situation about being damaged to operator.
Description
Technical field
The present invention relates to graphene production reactor technical field, specially a kind of oxidation with environmental-protection adsorption function
Graphene produces reduction reactor.
Background technology
Graphene be one kind by carbon atom with sp2Hybridized orbit composition hexangle type is in the single flat that honeycomb lattice is arranged to make up
Face film, the two-dimensional material of only one of which carbon atom thickness is referred to as the fields such as the 21 century energy, electronics most glittering star,
It is international study hotspot in recent years.
At present, it can continue to produce the sour gas such as sulfur dioxide when graphene production reduction, when producing due to graphene
Based on artificial operate, therefore gas comes out and easily can cause potential injury to the body of operator.
The content of the invention
Reduction reactor is produced it is an object of the invention to provide a kind of graphene oxide with environmental-protection adsorption function,
To solve the problems mentioned in the above background technology.
To achieve the above object, the present invention provides following technical scheme:A kind of graphite oxide with environmental-protection adsorption function
Alkene produces reduction reactor, including kettle, and the surface fixed cover of the kettle is connected to support, and the surface of the support is provided with the
One switch and second switch, the inside of the kettle are fixedly connected with inner bag, and the upper end of the inner bag is provided with charging aperture, described interior
The lower end of courage is provided with discharging opening, and heating chamber is provided between the kettle and inner bag, and the upper end of the heating chamber is provided with water inlet, institute
The lower end for stating heating chamber is provided with delivery port, and the surface wrap of the inner bag has heating tube, and the inside of the heating tube is socketed with electricity
Heated filament, the heating wire is connected in series first switch, and the side of the support is fixedly connected with supporting plate, the supporting plate it is upper
Surface is provided with gas treatment groove, and the side lower end of the gas treatment groove is provided with the first control valve, and the upper end of the inner bag is consolidated
Surely gas pipeline is connected with, the other end of the gas pipeline is fixedly connected with gas treatment groove, and the side of the gas pipeline is set
There is the second control valve, the upper end of the kettle is provided with motor, and the motor is connected in series second switch, the rotating shaft of the motor
Agitator is fixedly connected with, the upper shaft connection kettle and inner bag of the agitator, the inner side of the inner bag are provided with fixation
Bar.
It is preferred that, the inside of the gas treatment groove fills sodium hydroxide solution.
It is preferred that, the upper surface of the gas treatment groove is provided with solution inlet port, and the upper end of the solution inlet port is provided with sealing
Lid.
It is preferred that, the distance between described fix bar is 3 to 5 centimetres.
Compared with prior art, the beneficial effects of the invention are as follows:The graphene oxide that this kind has environmental-protection adsorption function is given birth to
Production reduction is run with reactor by second switch controlled motor, and motor drives agitator to rotate, and agitator can stir inner bag
The graphite raw material of bottom, so as to blend the larger graphite of volume with fix bar by agitator, accelerates the oxidation of graphite
Speed;Open the inside that the gas inside the second control valve, inner bag enters gas treatment groove by gas pipeline so that titanium dioxide
The sour gas such as sulphur are absorbed by sodium hydroxide, it is to avoid gas occur and shed situation about being damaged to operator.
Brief description of the drawings
Fig. 1 is whole for a kind of graphene oxide production reduction reactor with environmental-protection adsorption function of the present invention
Body structural front view;
Fig. 2 produces the kettle of reduction reactor for a kind of graphene oxide with environmental-protection adsorption function of the present invention
Body sectional view.
Division mark is as follows in accompanying drawing:1st, kettle, 2, support, 3, first switch, 4, second switch, 5, inner bag, 6, heating
Chamber, 7, charging aperture, 8, discharging opening, 9, water inlet, 10, delivery port, 11, heating tube, 12, heating wire, 13, gas pipeline, 14, gas
Body treatment trough, the 15, first control valve, the 16, second control valve, 17, motor, 18, agitator, 19, fix bar, 20, supporting plate,
21st, solution inlet port, 22, closure.
Embodiment
In conjunction with the accompanying drawings, the present invention is further explained in detail.These accompanying drawings are simplified schematic diagram, only with
Illustration illustrates the basic structure of the present invention, therefore it only shows the composition relevant with the present invention.
Fig. 1-2 is referred to, the present invention provides a kind of technical scheme:A kind of graphene oxide life with environmental-protection adsorption function
Reduction reactor, including kettle 1 are produced, the surface fixed cover of kettle 1 is connected to support 2, and the surface of support 2 is provided with first switch 3
With second switch 4, first switch 3 and second switch 4 are connected with the circuit connected in series of either inside, and the inside of kettle 1, which is fixed, to be connected
Inner bag 5 is connected to, the upper end of inner bag 5 is provided with charging aperture 7, and the lower end of inner bag 5 is provided with discharging opening 8, is provided between kettle 1 and inner bag 5
Heating chamber 6, the upper end of heating chamber 6 is provided with water inlet 9, and the lower end of heating chamber 6 is provided with delivery port 10, and the surface wrap of inner bag 5 has
Heating tube 11, the inside of heating tube 11 is socketed with heating wire 12, and heating wire 12 is connected in series first switch 3, passes through delivery port 10
Water is injected to the inside of heating chamber 6, then controls heating wire 12 to heat the water inside heating chamber 6 by first switch 3, from
And heat can be provided the reaction inside inner bag 5, the side of support 2 is fixedly connected with supporting plate 20, the upper table of supporting plate 20
Face is provided with gas treatment groove 14, and the upper surface of gas treatment groove 14 is provided with solution inlet port 21, and the upper end of solution inlet port 21 is provided with
Closure 22, can be to sodium hydroxide solution be added inside gas treatment groove 14, so as in absorbing by solution inlet port 21
Gas inside courage 5, the side lower end of gas treatment groove 14 is provided with the first control valve 15, can be released by the first control valve 15
Solution inside gas treatment groove 14, is conveniently replaceable, and the upper end of inner bag 5 is fixedly connected with gas pipeline 13, gas pipeline 13
The other end is fixedly connected with gas treatment groove 14, and the inside of gas treatment groove 14 fills sodium hydroxide solution, sodium hydroxide solution energy
The gas that produces when enough absorbing graphite oxidation, it is to avoid gas occur and shed situation about being damaged to operator, gas pipeline
13 side is provided with the second control valve 16, and the upper end of kettle 1 is provided with motor 17, the model YS6314 of motor 17, motor 17
Second switch 4 is connected in series, the rotating shaft of motor 17 is fixedly connected with agitator 18, the upper shaft connection He of kettle 1 of agitator 18
Inner bag 5, the inner side of inner bag 5 is provided with fix bar 19, and the distance between fix bar 19 is 3 to 5 centimetres, passes through second switch 4
Controlled motor 17 is run, and motor 17 drives agitator 18 to rotate, and agitator 18 can stir the graphite raw material of the bottom of inner bag 5, from
And can be blended the larger graphite of volume by agitator 18 and fix bar 19, accelerate the oxidation rate of graphite.
The present invention is in the specific implementation:When in use, water is injected to the inside of heating chamber 6 by delivery port 10, then passed through
The control heating wire 12 of first switch 3 is heated to the water inside heating chamber 6, so as to provide the reaction inside inner bag 5
Heat;Run by the controlled motor 17 of second switch 4, motor 17 drives agitator 18 to rotate, and agitator 18 can stir inner bag 5
The graphite raw material of bottom, so as to blend the larger graphite of volume with fix bar 19 by agitator 18, accelerates graphite
Oxidation rate;The gas inside the second control valve 16, inner bag 5 is opened by gas pipeline 13 to enter in gas treatment groove 14
Portion so that the sour gas such as sulfur dioxide is absorbed by sodium hydroxide, it is to avoid gas occur and shed what is damaged to operator
Situation.
Using the above-mentioned desirable embodiment according to the present invention as enlightenment, by above-mentioned description, relevant staff is complete
Various changes and amendments can be carried out without departing from the scope of the technological thought of the present invention' entirely.The technology of this invention
Property scope is not limited to the content on specification, it is necessary to its technical scope is determined according to right.
Claims (4)
1. a kind of graphene oxide production reduction reactor with environmental-protection adsorption function, including kettle (1), its feature exist
In:The surface fixed cover of the kettle (1) is connected to support (2), and the surface of the support (2) is provided with first switch (3) and second
Switch (4), the inside of the kettle (1) is fixedly connected with inner bag (5), and the upper end of the inner bag (5) is provided with charging aperture (7), institute
The lower end for stating inner bag (5) is provided with discharging opening (8), and heating chamber (6), the heating chamber are provided between the kettle (1) and inner bag (5)
(6) upper end is provided with water inlet (9), and the lower end of the heating chamber (6) is provided with delivery port (10), and the surface of the inner bag (5) is twined
Heating tube (11) is wound with, the inside of the heating tube (11) is socketed with heating wire (12), and the heating wire (12) is connected in series
One switch (3);
The side of the support (2) is fixedly connected with supporting plate (20), and the upper surface of the supporting plate (20) is provided with gas
Groove (14) is managed, the side lower end of the gas treatment groove (14) is provided with the first control valve (15), and the upper end of the inner bag (5) is fixed
Gas pipeline (13) is connected with, the other end of the gas pipeline (13) is fixedly connected with gas treatment groove (14), the flue
The side in road (13) is provided with the second control valve (16), and the upper end of the kettle (1) is provided with motor (17), motor (17) string
Connection connection second switch (4), the rotating shaft of the motor (17) is fixedly connected with agitator (18), the upper end of the agitator (18)
Axle connection kettle (1) and inner bag (5), the inner side of the inner bag (5) are provided with fix bar (19).
2. a kind of graphene oxide production reduction reactor with environmental-protection adsorption function according to claim 1, its
It is characterised by:The inside of the gas treatment groove (14) fills sodium hydroxide solution.
3. a kind of graphene oxide production reduction reactor with environmental-protection adsorption function according to claim 1, its
It is characterised by:The upper surface of the gas treatment groove (14) is provided with solution inlet port (21), and the upper end of the solution inlet port (21) is set
There is closure (22).
4. a kind of graphene oxide production reduction reactor with environmental-protection adsorption function according to claim 1, its
It is characterised by:The distance between described fix bar (19) is 3 to 5 centimetres.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201710374224.2A CN107213862A (en) | 2017-05-24 | 2017-05-24 | A kind of graphene oxide production reduction reactor with environmental-protection adsorption function |
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CN201710374224.2A CN107213862A (en) | 2017-05-24 | 2017-05-24 | A kind of graphene oxide production reduction reactor with environmental-protection adsorption function |
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Publication Number | Publication Date |
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CN107213862A true CN107213862A (en) | 2017-09-29 |
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CN201710374224.2A Withdrawn CN107213862A (en) | 2017-05-24 | 2017-05-24 | A kind of graphene oxide production reduction reactor with environmental-protection adsorption function |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN114432992A (en) * | 2022-01-19 | 2022-05-06 | 深圳市鸿盛天诚电子有限公司 | High-efficient new forms of energy lithium battery material preparation facilities |
-
2017
- 2017-05-24 CN CN201710374224.2A patent/CN107213862A/en not_active Withdrawn
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN114432992A (en) * | 2022-01-19 | 2022-05-06 | 深圳市鸿盛天诚电子有限公司 | High-efficient new forms of energy lithium battery material preparation facilities |
CN114432992B (en) * | 2022-01-19 | 2023-11-03 | 常州厚德再生资源科技有限公司 | High-efficient new forms of energy lithium battery material preparation facilities |
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Application publication date: 20170929 |