CN107188548A - Abrasive brick and preparation method thereof - Google Patents
Abrasive brick and preparation method thereof Download PDFInfo
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- CN107188548A CN107188548A CN201710576230.6A CN201710576230A CN107188548A CN 107188548 A CN107188548 A CN 107188548A CN 201710576230 A CN201710576230 A CN 201710576230A CN 107188548 A CN107188548 A CN 107188548A
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- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
- C04B35/10—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on aluminium oxide
- C04B35/101—Refractories from grain sized mixtures
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3418—Silicon oxide, silicic acids, or oxide forming salts thereof, e.g. silica sol, fused silica, silica fume, cristobalite, quartz or flint
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3427—Silicates other than clay, e.g. water glass
- C04B2235/3463—Alumino-silicates other than clay, e.g. mullite
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/38—Non-oxide ceramic constituents or additives
- C04B2235/3817—Carbides
- C04B2235/3826—Silicon carbides
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- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/42—Non metallic elements added as constituents or additives, e.g. sulfur, phosphor, selenium or tellurium
- C04B2235/428—Silicon
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/60—Aspects relating to the preparation, properties or mechanical treatment of green bodies or pre-forms
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
- C04B2235/656—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
- C04B2235/96—Properties of ceramic products, e.g. mechanical properties such as strength, toughness, wear resistance
Abstract
The present invention relates to a kind of abrasive brick and preparation method thereof, it is made up of the raw material of following parts by weight:Granularity is 3 1mm and 1 0mm 35 40 parts of 85 alumina of JGAL, and granularity is 3 1mm and 1 0mm 20 25 parts of mullite synthesizing, and granularity is 0.5 0mm and 200# 5 10 parts of SiC, and granularity is 5um 10 15 parts of high temperature alumina, and granularity is 2um f SiO235 parts, granularity is 35 parts of the Si powder of 200 mesh, 35 parts of 325 mesh of clay, 0.4 part of curing agent, 34 parts of bonding agent resin.The present invention improves product consistency, and acceleration of sintering improves the anti-wear performance of product.To reach product properties index request.The present invention greatly improves dry coke quenching cooling section service life, reduces enterprise operation cost, intensity and anti-wear-resisting is better than BM bricks.
Description
Technical field
The present invention relates to a kind of abrasive brick and preparation method thereof.
Background technology
At present, the resistance to material of dry coke quenching cooling end uses B grades of mullite bricks (BM), service life about 4~5 years.This position
The height of the wearability of resistance to material, directly decides the length of service life.
Since Wuhan Iron and Steel Plant dry coke quenching in 2002, the country occurred in that substantial amounts of dry coke quenching engineering project.Dry coke quenching year in recent years
Checking maintenance situation, one of the problem of existing is that the dry room cooling end material that puts out has different degrees of abrasion, and mainly material is resistance to
Mill property difference causes abrasion overweight.Domestic dry coke quenching cooling end uses (Q) BM materials at present.Japanese dry coke quenching project, cooling end
Majority uses H31LL, also has and uses N53-M materials.Its index performance of the BM mullite bricks that cooling chamber is used at present is relatively low,
Mismatched with the performance indications required for actual bad working environments in coke dry quenching furnace, especially original BM mullite bricks are to normal temperature wearing coefficient
Less demanding, wherein normal temperature wear extent is<10cc index is too low, do not adapt to coke in coke dry quenching furnace rub for a long time generation mill
Damage, so causing cooling chamber brick large area wear damage.
The content of the invention
It is an object of the invention to provide a kind of abrasive brick and preparation method thereof, product consistency is improved, acceleration of sintering is improved
The anti-wear performance of product.To reach product properties index request, dry coke quenching cooling section service life, reduction enterprise fortune are greatly improved
Row cost.
A kind of abrasive brick of the present invention, is made up of the raw material of following parts by weight:
Granularity is 3-1mm and 1-0mm 35-40 parts of JGAL-85 alumina, and granularity is 3-1mm and 1-0mm mullite synthesizing
20-25 parts, granularity is 0.5-0mm and 200# 5-10 parts of SiC, and granularity is 5um 10-15 parts of high temperature alumina, and granularity is
2um f-SiO23-5 parts, granularity is 3-5 parts of the Si powder of 200 mesh, 3-5 parts of 325 mesh of clay, 0.4 part of curing agent, bonding agent tree
3-4 parts of fat.
Described abrasive brick, is preferably constituted by the raw material of following parts by weight:
15-20 parts of the JGAL-85 alumina that 15-20 parts of the JGAL-85 alumina that granularity is 3-1mm, granularity are 1-0mm, granularity
8-10 parts of mullite synthesizing for being 1-0mm for 3-1mm 13-18 parts of mullite synthesizing, granularity, granularity is 0.5-0mm SiC
6-7 parts, 2-3 parts of the SiC that granularity is 200#, granularity are 10um 4-6 parts of andalusite, and granularity is 5um high temperature alumina 13-
15 parts, granularity is 2um f-SiO22-4 parts, granularity is 3-5 parts of the Si powder of 200 mesh, 5-7 parts of 325 mesh of clay, curing agent 0.2-
0.5 part, 3-4 parts of bonding agent.
Curing agent is methenamine.
Bonding agent is resin.
The preparation method of described abrasive brick, raw material is well mixed, and uses forcing press weight, is dried, and moisture content is dried in control
< 1%, tunnel cave is burnt till.
The present invention is uniform using high speed mixing smelting machine mixing.Using 500t forcing press weight, product consistency is improved, tunnel is used
Road formula drier is dried, and moisture content < 1% is dried in control.Burnt till using tunnel cave, firing temperature is 1400-1430 DEG C.
Firing temperature is 1400-1450 DEG C.
Firing temperature is preferably 1400-1430 DEG C.
Burnt till using 1400-1430 DEG C, it is ensured that the wearability in the reaction of each raw material, and product use.Control and burn till
Temperature is also most important.
Alumina of the present invention, mullite, carborundum are primary raw material, by the application of micro mist, select rational grain size of raw material,
Fine material grain mixture ratio, good compatible proportioning is formed using with bonding agent, improves product consistency, and acceleration of sintering is improved
The anti-wear performance of product is to reach product properties index request.
It is primary raw material that alumina and mullite material are preferably homogenized from wearability.Generally existing chemistry in refractory material
Reaction and crystal transfer, they have a huge impact to product properties.To reach product high-wearing feature, add wear-resisting raw material and
Addition.
From critical materials of the carborundum for raising Wear Resistance.
Plasticizer promotes each raw material reaction, improves product strength.
Dry coke quenching cooling section Plastic phase bonded abrasive brick of the present invention, intensity improves a lot compared with BM.Carried significantly using scope
It is high.
BM bricks intensity is in 85Mpa, Plastic phase bonded abrasive brick intensity > 150Mpa, because being combined using reaction in-situ, increases
The intensity of product is added.
Carborundum is added, wearability is enhanced.
Generally existing chemical reaction and crystal transfer in refractory material, and they have a huge impact to product properties.
To reach product high-wearing feature, wear-resisting raw material is added.
Abrasive brick of the present invention is widely used, and is preferred for coke dry quenching furnace, the more excellent cooling section for coke dry quenching furnace.
Compared with prior art, the invention has the advantages that:
The present invention improves product consistency, and acceleration of sintering improves the anti-wear performance of product.To reach that product properties index will
Ask.The present invention greatly improves dry coke quenching cooling section service life, reduces enterprise operation cost, intensity and anti-wear-resisting is better than BM bricks.
Embodiment
With reference to embodiment, the present invention is further illustrated.
Embodiment 1
Abrasive brick of the present invention, is made up of the raw material of following parts by weight:
18 parts of the JGAL-85 alumina that 19 parts of the JGAL-85 alumina that granularity is 3-1mm, granularity are 1-0mm, granularity is 3-1mm
15 parts of mullite synthesizing, granularity be 1-0mm 9 parts of mullite synthesizing, 5 parts of the SiC that granularity is 0.5-0mm, granularity are 200#
2 parts of SiC, granularity be 10um 5 parts of andalusite, granularity be 5um 14 parts of high temperature alumina, granularity be 2um f-SiO2 3
Part, granularity is 4 parts of the Si powder of 200 mesh, 6 parts of 325 mesh of clay, 0.4 part of curing agent (methenamine), 3-4 parts of bonding agent (resin).
It is uniform using high speed mixing smelting machine mixing.Using 500t forcing press weight, product consistency is improved, it is dry using tunnel type
Dry device is dried, and moisture content < 1% is dried in control.Burnt till using tunnel cave, firing temperature is 1400 DEG C.
Embodiment 2
Abrasive brick, it is characterised in that be made up of the raw material of following parts by weight:
20 parts of the JGAL-85 alumina that 17 parts of the JGAL-85 alumina that granularity is 3-1mm, granularity are 1-0mm, granularity is 3-1mm
17 parts of mullite synthesizing, granularity be 1-0mm 7 parts of mullite synthesizing, 5 parts of the SiC that granularity is 0.5-0mm, granularity are 200#
2 parts of SiC, granularity be 10um 5 parts of andalusite, granularity be 5um 14 parts of high temperature alumina, granularity be 2um f-SiO2 3
Part, granularity is 4 parts of the Si powder of 200 mesh, 6 parts of 325 mesh of clay, 0.4 part of curing agent (methenamine), 3-4 parts of bonding agent (resin).
It is uniform using high speed mixing smelting machine mixing.Using 500t forcing press weight, product consistency is improved, it is dry using tunnel type
Dry device is dried, and moisture content < 1% is dried in control.Burnt till using tunnel cave, firing temperature is 1410 DEG C.
Embodiment 3
Abrasive brick, it is characterised in that be made up of the raw material of following parts by weight:
17 parts of the JGAL-85 alumina that 20 parts of the JGAL-85 alumina that granularity is 3-1mm, granularity are 1-0mm, granularity is 3-1mm
14 parts of mullite synthesizing, granularity be 1-0mm 10 parts of mullite synthesizing, 5 parts of the SiC that granularity is 0.5-0mm, granularity are
2 parts of 200# SiC, granularity is 10um 5 parts of andalusite, and granularity is 5um 14 parts of high temperature alumina, and granularity is 2um f-
3 parts of SiO2, granularity is 4 parts of the Si powder of 200 mesh, 6 parts of 325 mesh of clay, 0.4 part of curing agent (methenamine), bonding agent (resin)
3-4 parts.
It is uniform using high speed mixing smelting machine mixing.Using 500t forcing press weight, product consistency is improved, it is dry using tunnel type
Dry device is dried, and moisture content < 1% is dried in control.Burnt till using tunnel cave, firing temperature is 1420 DEG C.
Claims (7)
1. a kind of abrasive brick, it is characterised in that be made up of the raw material of following parts by weight:
Granularity is 3-1mm and 1-0mm 35-40 parts of JGAL-85 alumina, and granularity is 3-1mm and 1-0mm mullite synthesizing 20-
25 parts, granularity is 0.5-0mm and 200# 5-10 parts of SiC, and granularity is 5um 10-15 parts of high temperature alumina, and granularity is 2um's
f-SiO23-5 parts, granularity is 3-5 parts of the Si powder of 200 mesh, 3-5 parts of 325 mesh of clay, 0.4 part of curing agent, bonding agent resin 3-4
Part.
2. abrasive brick according to claim 1, it is characterised in that be made up of the raw material of following parts by weight:
15-20 parts of the JGAL-85 alumina that 15-20 parts of the JGAL-85 alumina that granularity is 3-1mm, granularity are 1-0mm, granularity is 3-
1mm 13-18 parts of mullite synthesizing, 8-10 parts of the mullite synthesizing that granularity is 1-0mm, granularity is 0.5-0mm SiC 6-7
Part, 2-3 parts of the SiC that granularity is 200#, granularity are 10um 4-6 parts of andalusite, and granularity is 5um high temperature alumina 13-15
Part, granularity is 2um f-SiO22-4 parts, granularity is 3-5 parts of the Si powder of 200 mesh, 5-7 parts of 325 mesh of clay, curing agent 0.2-
0.5 part, 3-4 parts of bonding agent.
3. abrasive brick according to claim 1, it is characterised in that curing agent is methenamine.
4. abrasive brick according to claim 1, it is characterised in that bonding agent is resin.
5. the preparation method of the abrasive brick described in a kind of claim 1, it is characterised in that be well mixed raw material, uses forcing press
Weight, is dried, and moisture content < 1% is dried in control, and tunnel cave is burnt till.
6. the preparation method of abrasive brick according to claim 5, it is characterised in that firing temperature is 1400-1450 DEG C.
7. the preparation method of abrasive brick according to claim 6, it is characterised in that firing temperature is 1400-1430 DEG C.
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CN201710576230.6A CN107188548B (en) | 2017-07-14 | 2017-07-14 | Wear-resistant brick and preparation method thereof |
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CN201710576230.6A CN107188548B (en) | 2017-07-14 | 2017-07-14 | Wear-resistant brick and preparation method thereof |
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CN107188548B CN107188548B (en) | 2021-09-17 |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN117263662A (en) * | 2023-11-21 | 2023-12-22 | 山东耐材集团鲁耐窑业有限公司 | Low-internal-stress dry quenching column part brick and preparation method thereof |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN117263662A (en) * | 2023-11-21 | 2023-12-22 | 山东耐材集团鲁耐窑业有限公司 | Low-internal-stress dry quenching column part brick and preparation method thereof |
CN117263662B (en) * | 2023-11-21 | 2024-02-27 | 山东耐材集团鲁耐窑业有限公司 | Low-internal-stress dry quenching column part brick and preparation method thereof |
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