CN107166998A - A kind of corrosion-resistant and high-temperature resistant is without the quartzy heat-exchanger rig of leakage formula and preparation method - Google Patents

A kind of corrosion-resistant and high-temperature resistant is without the quartzy heat-exchanger rig of leakage formula and preparation method Download PDF

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Publication number
CN107166998A
CN107166998A CN201710512720.XA CN201710512720A CN107166998A CN 107166998 A CN107166998 A CN 107166998A CN 201710512720 A CN201710512720 A CN 201710512720A CN 107166998 A CN107166998 A CN 107166998A
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CN
China
Prior art keywords
heat exchange
heat
shell
resistant
exchanger rig
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710512720.XA
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Chinese (zh)
Inventor
刘广卫
贾泽坤
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
DONGHAI COUNTY KAIKAI QUARTZ PRODUCTS Co Ltd
Original Assignee
DONGHAI COUNTY KAIKAI QUARTZ PRODUCTS Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by DONGHAI COUNTY KAIKAI QUARTZ PRODUCTS Co Ltd filed Critical DONGHAI COUNTY KAIKAI QUARTZ PRODUCTS Co Ltd
Priority to CN201710512720.XA priority Critical patent/CN107166998A/en
Publication of CN107166998A publication Critical patent/CN107166998A/en
Priority to CN201820066845.4U priority patent/CN207881529U/en
Priority to CN201810039097.5A priority patent/CN108106466A/en
Pending legal-status Critical Current

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Classifications

    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F28HEAT EXCHANGE IN GENERAL
    • F28DHEAT-EXCHANGE APPARATUS, NOT PROVIDED FOR IN ANOTHER SUBCLASS, IN WHICH THE HEAT-EXCHANGE MEDIA DO NOT COME INTO DIRECT CONTACT
    • F28D7/00Heat-exchange apparatus having stationary tubular conduit assemblies for both heat-exchange media, the media being in contact with different sides of a conduit wall
    • F28D7/16Heat-exchange apparatus having stationary tubular conduit assemblies for both heat-exchange media, the media being in contact with different sides of a conduit wall the conduits being arranged in parallel spaced relation
    • F28D7/1607Heat-exchange apparatus having stationary tubular conduit assemblies for both heat-exchange media, the media being in contact with different sides of a conduit wall the conduits being arranged in parallel spaced relation with particular pattern of flow of the heat exchange media, e.g. change of flow direction
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F28HEAT EXCHANGE IN GENERAL
    • F28FDETAILS OF HEAT-EXCHANGE AND HEAT-TRANSFER APPARATUS, OF GENERAL APPLICATION
    • F28F19/00Preventing the formation of deposits or corrosion, e.g. by using filters or scrapers
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F28HEAT EXCHANGE IN GENERAL
    • F28FDETAILS OF HEAT-EXCHANGE AND HEAT-TRANSFER APPARATUS, OF GENERAL APPLICATION
    • F28F21/00Constructions of heat-exchange apparatus characterised by the selection of particular materials
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F28HEAT EXCHANGE IN GENERAL
    • F28FDETAILS OF HEAT-EXCHANGE AND HEAT-TRANSFER APPARATUS, OF GENERAL APPLICATION
    • F28F9/00Casings; Header boxes; Auxiliary supports for elements; Auxiliary members within casings
    • F28F9/24Arrangements for promoting turbulent flow of heat-exchange media, e.g. by plates

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  • Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Mechanical Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • Fluid Mechanics (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

A kind of corrosion-resistant and high-temperature resistant is without the quartzy heat-exchanger rig of leakage formula:Including shell and some heat exchange inner tubes, heat exchange inner tube two ends are respectively connected by one piece of connecting partition, two pieces of connecting partitions are connected on outer casing inner wall, heat exchange shell chamber, some heat exchange inner tubes formation heat exchange tube chamber relatively independent with heat exchange shell chamber are formed between connecting partition, between heat exchange inner tube and shell;Material inlet/outlet pipe is respectively equipped with heat exchange shell chamber, heat exchange tube chamber, the material-heat-exchanging shell side and tube side of quartzy heat-exchanger rig is consequently formed;Shell, heat exchange inner tube, material inlet/outlet pipe are made of quartz material and seamless welding is into a single integrated structure.The invention also discloses the preparation method of the device.The integrative-structure of the full quartz material of the device and seamless welding, greatly reinforces its corrosion resistance;The seamless welding of tube side and shell side is into a single integrated structure, thoroughly solves the problems, such as the evaporating, emitting, dripping or leaking of liquid or gas of heat-exchanger rig, substantially increases the application of the present invention, apparatus of the present invention is applied in chemical field.

Description

A kind of corrosion-resistant and high-temperature resistant is without the quartzy heat-exchanger rig of leakage formula and preparation method
Technical field
The present invention relates to a kind of heat transmission equipment, more particularly to a kind of corrosion-resistant and high-temperature resistant is without leakage formula quartz heat exchange dress Put.The invention further relates to a kind of preparation method of the corrosion-resistant and high-temperature resistant without the quartzy heat-exchanger rig of leakage formula.
Background technology
Heat exchanger(heat exchanger), it is the equipment that the partial heat of hot fluid is passed to cold fluid, it is also known as hot Exchanger.Heat exchanger occupies critical role in chemical industry, oil, power, food and other many industrial productions, and it gives birth in chemical industry Heat exchanger can be widely used as heater, cooler, condenser, evaporator and reboiler etc. in production.
Heat exchanger be it is a kind of realize material between two or more fluid of different temperatures between heat transfer section Energy equipment, is heat is passed to the relatively low fluid of temperature by the higher fluid of temperature, fluid temperature (F.T.) is reached flow specification Index, the need for meeting process conditions, while being also to improve one of capital equipment of energy utilization rate.Heat exchanger industry is related to HVAC, pressure vessel, sewerage disposing equipment, chemical industry, nearly 30 multi industries such as oil.
Suitable for different medium, different operating mode, different temperatures, different pressures heat exchanger, structural shape is also different, heat exchange Device is classified as follows by heat transfer theory:
1st, dividing wall type heat exchanger
Dividing wall type heat exchanger is that two kinds of different fluids of temperature flow in the space separated by wall, by the heat conduction of wall and Fluid is exchanged heat between wall surface convection current, two kinds of fluids.Dividing wall type heat exchanger has shell-and-tube, bushing type and other patterns Heat exchanger.Dividing wall type heat exchanger is the heat exchanger being most widely used at present.
2nd, heat regenerator
Heat, is passed to cryogen, heat is situated between by the heat storage that heat regenerator is made up of solid matter from high temperature fluid Matter first passes through heating solid matter and reached after certain temperature, and cold medium is heated by solid matter again, makes up to heat biography The purpose passed.Heat regenerator have rotatably, valve transfer formula etc..
3rd, indirect type heat exchanger is fluidly connected
Indirect type heat exchanger is fluidly connected, is by changing that the heat carrier circulated wherein is connected two surface-type heat exchangers Hot device, heat carrier is circulated between high temperature fluid heat exchanger and cryogen, is received heat in high temperature fluid, is changed in cryogen Heat is released to cryogen by hot device.
4th, direct-contact heat exchanger
Be otherwise known as direct contact heat exchanger, and this heat exchanger is that two kinds of fluids are directly contacted, and be mixed with each other the equipment exchanged heat, For example, cooling column, gas condenser etc..
5th, composite heat exchanger
The equipment for having vapour surface type indirect heat exchange and water water two kinds of heat exchange modes of direct mixed flow heat exchange concurrently.Changed indirectly with vapour surface type Heat is compared, with higher heat exchange efficiency;There is higher stability and relatively low unit compared with the direct mixed heat transfer of carbonated drink Noise.
In the prior art, no matter being by metal material or ceramic material or gold using the heat exchanger of which kind of principle Category is made with ceramic material, using split type tube side shell side structure, assembled shaping.The shortcoming of this heat exchanger is:Can The operating temperature range of adaptation is small, it is impossible to high temperature resistant, is not suitable for a variety of Application in Chemical Engineering, and anticorrosion ability is poor, at assembly connection Easily leakage.
The content of the invention
It is an object of the invention to overcome the above-mentioned problems in the prior art more to be closed there is provided a kind of structure design Reason, strong adaptability, it is possible to achieve corrosion-resistant, high temperature resistant, dead-tight quartzy heat-exchanger rig.
It is a further object to provide corrosion-resistant and high-temperature resistant as described above without the quartzy heat-exchanger rig of leakage formula A kind of preparation method.
The technical problems to be solved by the invention are realized by following technical scheme.The present invention is a kind of corrosion resistant High temperature resistant is lost without the quartzy heat-exchanger rig of leakage formula, is characterized in:The heat-exchanger rig includes shell and some heat exchange inner tubes, described to change Hot inner tube two ends are respectively connected by one piece of connecting partition, and two pieces of described connecting partitions are connected on outer casing inner wall, connection Heat exchange shell chamber is formed between dividing plate, between heat exchange inner tube and shell, some heat exchange inner tubes formation and heat exchange shell chamber are relatively independent Exchange heat tube chamber;Material inlet/outlet pipe is respectively equipped with the heat exchange shell chamber, heat exchange tube chamber, the material of quartzy heat-exchanger rig is consequently formed Exchange heat shell side and tube side;The shell, heat exchange inner tube, material inlet/outlet pipe are made of quartz material and seamless welding is integral Structure.
Corrosion-resistant and high-temperature resistant of the present invention is without the quartzy heat-exchanger rig of leakage formula, its further preferred technical scheme It is:Some deflection plates are interval with according to design and operational requirement in heat exchange shell intracavitary, described deflection plate uses quartz material It is made and local welding is fixed on the inwall of shell, shape between the baffle section and outer casing inner wall do not closed with outer casing inner wall Into baffling material channel, adjacent baffling material channel is in be staggered.
Corrosion-resistant and high-temperature resistant of the present invention is without the quartzy heat-exchanger rig of leakage formula, its further preferred technical scheme It is:It is be arranged in parallel between described some deflection plates.
Corrosion-resistant and high-temperature resistant of the present invention is without the quartzy heat-exchanger rig of leakage formula, its further preferred technical scheme It is:Described some heat exchange inner tubes are arranged in shell using section in cellular mode.
Corrosion-resistant and high-temperature resistant of the present invention is without the quartzy heat-exchanger rig of leakage formula, its further preferred technical scheme It is:Outer shell outer wall in heat exchange shell cavity segment is provided with silicon rubber or fluorubber layer of protective material.
Corrosion-resistant and high-temperature resistant of the present invention is without the quartzy heat-exchanger rig of leakage formula, its further preferred technical scheme It is:It is provided with heat exchange shell chamber or heat exchanger tube intracavitary and uses quartz with the integrally formed intubation of quartzy heat-exchanger rig, the intubation Material is made, and temperature sensor is provided with intubation.
Corrosion-resistant and high-temperature resistant described in more than one technical scheme any one of the invention is without the quartzy heat-exchanger rig of leakage formula Preparation method, be characterized in, its step is as follows:
(1)Prepare shell, heat exchange inner tube, material inlet/outlet pipe that quartz raw material is made, provided with deflection plate and intubation, then prepare folding Plate and intubation are flowed, deflection plate is manufactured into through hole by design requirement;
(2)Heat exchange inner tube is sequentially passed through in the through hole of deflection plate, using nanoscale melting welding silica flour by heat exchange inner tube and folding Flow plate and carry out thermal weld shaping according to design requirement, redundance is then subjected to accurate cutting, part I is made;
(3)Part I is loaded in shell, shell and part I are subjected to heat according to design requirement using nanoscale melting welding silica flour Welding fabrication, then carries out accurate cutting by redundance, while the corresponding material inlet pipe of thermoforming, material outlet pipe and intubation, Part II is made;
(4)Acid treatment is carried out to part II, cleaning, flame polish, high annealing eliminates stress, finished product is made.
Above-described preparation method, its further preferred technical scheme is:High temperature anneal temperature described in step (4) For 1100 DEG C -1250 DEG C.
Compared with prior art, the beneficial effects of the invention are as follows:
1st, the present invention is a kind of quartzy heat-exchanger rig, it is possible to achieve the liquid of heat exchange shell intracavitary is exchanged heat.Heat exchange inner tube is installed On connecting partition, the differentiation of tube side and shell side is realized.Shell, heat exchange inner tube, feed tube and drain pipe are using quartzy material Material is made and seamless welding is into a single integrated structure.So so that the present invention has the stress ability of higher high temperature resistant and the resistance to temperature difference, It is adapted to operating temperature range at -50 DEG C -1000 DEG C or so.It is additionally, since the one knot of full quartz material and seamless welding Structure, greatly reinforces its corrosion resistance;The seamless welding of tube side and shell side is into a single integrated structure, thoroughly solves heat-exchanger rig Evaporating, emitting, dripping or leaking of liquid or gas problem, substantially increases the application of the present invention, apparatus of the present invention is applied in chemical field.
2nd, the present invention can not only play by installing some deflection plates additional at heat exchange shell intracavitary interval and strengthen shell side intensity Effect, and the stroke of shell side can be extended by baffling passage, improve heat transfer effect.By the deflection plate that be arranged in parallel, simultaneously Make adjacent baffling passage in being staggered up and down, can further improve its heat transfer effect.
3rd, currently preferred some heat exchange inner tubes are arranged in shell using section in cellular mode, not only favorably With improving device intensity, and the heat exchange efficiency also improved to a certain extent.
4th, the present invention preferably on the outer shell outer wall in heat exchange shell cavity segment provided with silicon rubber or fluorubber by protecting Material layer.Safety protection function can be played, the security of device is improved.Make the present invention in the heating for chemical field Many one layer of safety guarantee.
5th, the quartzy heat-exchanger rig of the present invention is using Integratively formed, has had high temperature resistant after shaping concurrently, anti-leak, corrosion-resistant Effect, can also by docking realize multimachine connect.
Brief description of the drawings
Fig. 1 is a kind of structural representation of the invention.
Embodiment
Referring to the drawings, the concrete technical scheme of the present invention is further described, in order to which those skilled in the art enters One step the present invention is understood, without constituting the limitation to its right.
Embodiment 1, reference picture 1, a kind of corrosion-resistant and high-temperature resistant is without the quartzy heat-exchanger rig of leakage formula:The heat-exchanger rig includes outer Shell 1 and some heat exchange inner tubes 2, the two ends of heat exchange inner tube 2 are respectively connected by one piece of connecting partition 3, two pieces of described companies Connect dividing plate 3 to be connected on the inwall of shell 1, heat exchange shell chamber 4 is formed between connecting partition 3, between heat exchange inner tube 2 and shell 1, it is some The formation of the heat exchange inner tube 2 heat exchange tube chamber 8 relatively independent with heat exchange shell chamber 4;It is respectively equipped with the heat exchange shell chamber 4, heat exchange tube chamber 8 Material inlet/outlet pipe 5, is consequently formed the material-heat-exchanging shell side and tube side of quartzy heat-exchanger rig;The shell 1, heat exchange inner tube 2, material Inlet/outlet pipe 5 is made of quartz material and seamless welding is into a single integrated structure.
Embodiment 2, the corrosion-resistant and high-temperature resistant described in embodiment 1 is without in the quartzy heat-exchanger rig of leakage formula:In heat exchange shell chamber 4 Some deflection plates 6 are interval with according to design and operational requirement, described deflection plate 6 is made and local welding of quartz material Baffling material is formed between the part of deflection plate 6 do not closed on the inwall for being fixed on shell 1 with the inwall of shell 1 and the inwall of shell 1 Passage 7, adjacent baffling material channel 7 is in be staggered.
Embodiment 3, the corrosion-resistant and high-temperature resistant described in embodiment 1 or 2 is without in the quartzy heat-exchanger rig of leakage formula:Described is some It is be arranged in parallel between deflection plate 6.
Embodiment 4, the corrosion-resistant and high-temperature resistant described in embodiment 1-3 any one is without in the quartzy heat-exchanger rig of leakage formula:Institute Some heat exchange inner tubes 2 stated are arranged in shell 1 using section in cellular mode.
Embodiment 5, the corrosion-resistant and high-temperature resistant described in embodiment 1-4 any one is without in the quartzy heat-exchanger rig of leakage formula:Place The outer wall of shell 1 in heat exchange shell chamber 4 part is provided with silicon rubber or fluorubber layer of protective material.
Embodiment 6, the corrosion-resistant and high-temperature resistant described in embodiment 1-5 any one is without in the quartzy heat-exchanger rig of leakage formula: It is provided with heat exchange shell chamber 4 or the tube chamber 8 that exchanges heat and uses quartzy material with the integrally formed intubation 9 of quartzy heat-exchanger rig, described be intubated Matter is made, and temperature sensor is provided with intubation 9.
Embodiment 7, a kind of corrosion-resistant and high-temperature resistant as described in embodiment 1-6 any one is without leakage formula quartz heat exchange dress The preparation method put, its step is as follows:
(1)Prepare shell, heat exchange inner tube, material inlet/outlet pipe that quartz raw material is made, provided with deflection plate and intubation, then prepare folding Plate and intubation are flowed, deflection plate is manufactured into through hole by design requirement;
(2)Heat exchange inner tube is sequentially passed through in the through hole of deflection plate, using nanoscale melting welding silica flour by heat exchange inner tube and folding Flow plate and carry out thermal weld shaping according to design requirement, redundance is then subjected to accurate cutting, part I is made;
(3)Part I is loaded in shell, shell and part I are subjected to heat according to design requirement using nanoscale melting welding silica flour Welding fabrication, then carries out accurate cutting by redundance, while the corresponding material inlet pipe of thermoforming, material outlet pipe and intubation, Part II is made;
(4)Acid treatment is carried out to part II, cleaning, flame polish, high annealing eliminates stress, finished product is made.Step (4) institute The high temperature anneal temperature stated is 1100 DEG C -1250 DEG C.

Claims (8)

1. a kind of corrosion-resistant and high-temperature resistant is without the quartzy heat-exchanger rig of leakage formula, it is characterised in that:If the heat-exchanger rig include shell and Dry heat exchange inner tube, the heat exchange inner tube two ends are respectively connected by one piece of connecting partition, described two pieces of connecting partitions connection On outer casing inner wall, heat exchange shell chamber is formed between connecting partition, between heat exchange inner tube and shell, some heat exchange inner tubes formation are with changing The relatively independent heat exchange tube chamber of hot shell chamber;Material inlet/outlet pipe is respectively equipped with the heat exchange shell chamber, heat exchange tube chamber, stone is consequently formed The material-heat-exchanging shell side and tube side of English heat-exchanger rig;The shell, heat exchange inner tube, material inlet/outlet pipe are made of quartz material And seamless welding is into a single integrated structure.
2. corrosion-resistant and high-temperature resistant according to claim 1 is without the quartzy heat-exchanger rig of leakage formula, it is characterised in that:In heat exchange shell Intracavitary is interval with some deflection plates according to design and operational requirement, and described deflection plate is made of quartz material and locally welded Connect on the inwall for being fixed on shell, forming baffling material between the baffle section and outer casing inner wall do not closed with outer casing inner wall leads to Road, adjacent baffling material channel is in be staggered.
3. corrosion-resistant and high-temperature resistant according to claim 2 is without the quartzy heat-exchanger rig of leakage formula, it is characterised in that:If described It is be arranged in parallel between dry deflection plate.
4. corrosion-resistant and high-temperature resistant according to claim 1 is without the quartzy heat-exchanger rig of leakage formula, it is characterised in that:If described Dry heat exchange inner tube is arranged in shell using section in cellular mode.
5. corrosion-resistant and high-temperature resistant according to claim 1 is without the quartzy heat-exchanger rig of leakage formula, it is characterised in that:In heat exchange The outer shell outer wall of shell cavity segment is provided with silicon rubber or fluorubber layer of protective material.
6. corrosion-resistant and high-temperature resistant according to claim 1 is without the quartzy heat-exchanger rig of leakage formula, it is characterised in that:In heat exchange shell Chamber or heat exchanger tube intracavitary are provided with to be made with the integrally formed intubation of quartzy heat-exchanger rig, the intubation of quartz material, Temperature sensor is provided with intubation.
7. a kind of preparation of corrosion-resistant and high-temperature resistant as described in claim 1-6 any one without the quartzy heat-exchanger rig of leakage formula Method, it is characterised in that its step is as follows:
(1)Prepare shell, heat exchange inner tube, material inlet/outlet pipe that quartz raw material is made, provided with deflection plate and intubation, then prepare folding Plate and intubation are flowed, deflection plate is manufactured into through hole by design requirement;
(2)Heat exchange inner tube is sequentially passed through in the through hole of deflection plate, using nanoscale melting welding silica flour by heat exchange inner tube and folding Flow plate and carry out thermal weld shaping according to design requirement, redundance is then subjected to accurate cutting, part I is made;
(3)Part I is loaded in shell, shell and part I are subjected to heat according to design requirement using nanoscale melting welding silica flour Welding fabrication, then carries out accurate cutting by redundance, while the corresponding material inlet pipe of thermoforming, material outlet pipe and intubation, Part II is made;
(4)Acid treatment is carried out to part II, cleaning, flame polish, high annealing eliminates stress, finished product is made.
8. preparation method according to claim 7, it is characterised in that the high temperature anneal temperature described in step (4) is 1100 DEG C -1250 DEG C.
CN201710512720.XA 2017-02-22 2017-06-29 A kind of corrosion-resistant and high-temperature resistant is without the quartzy heat-exchanger rig of leakage formula and preparation method Pending CN107166998A (en)

Priority Applications (3)

Application Number Priority Date Filing Date Title
CN201710512720.XA CN107166998A (en) 2017-06-29 2017-06-29 A kind of corrosion-resistant and high-temperature resistant is without the quartzy heat-exchanger rig of leakage formula and preparation method
CN201820066845.4U CN207881529U (en) 2017-02-22 2018-01-16 A kind of corrosion-resistant and high-temperature resistant is without leakage formula quartz heat-exchanger rig
CN201810039097.5A CN108106466A (en) 2017-02-22 2018-01-16 A kind of corrosion-resistant and high-temperature resistant is without leakage formula quartz heat-exchanger rig and preparation method

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201710512720.XA CN107166998A (en) 2017-06-29 2017-06-29 A kind of corrosion-resistant and high-temperature resistant is without the quartzy heat-exchanger rig of leakage formula and preparation method

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Publication Number Publication Date
CN107166998A true CN107166998A (en) 2017-09-15

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108106466A (en) * 2017-02-22 2018-06-01 东海县凯凯石英制品有限公司 A kind of corrosion-resistant and high-temperature resistant is without leakage formula quartz heat-exchanger rig and preparation method
CN108759519A (en) * 2018-05-23 2018-11-06 吴玉婷 A kind of chemical industry heat exchanger

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108106466A (en) * 2017-02-22 2018-06-01 东海县凯凯石英制品有限公司 A kind of corrosion-resistant and high-temperature resistant is without leakage formula quartz heat-exchanger rig and preparation method
CN108759519A (en) * 2018-05-23 2018-11-06 吴玉婷 A kind of chemical industry heat exchanger

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Application publication date: 20170915