CN107151929A - A kind of stamp releasing soaping agent and preparation method thereof - Google Patents
A kind of stamp releasing soaping agent and preparation method thereof Download PDFInfo
- Publication number
- CN107151929A CN107151929A CN201710383055.9A CN201710383055A CN107151929A CN 107151929 A CN107151929 A CN 107151929A CN 201710383055 A CN201710383055 A CN 201710383055A CN 107151929 A CN107151929 A CN 107151929A
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- parts
- soaping agent
- stamp
- releasing soaping
- stamp releasing
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Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/02—After-treatment
- D06P5/04—After-treatment with organic compounds
- D06P5/06—After-treatment with organic compounds containing nitrogen
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/16—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using dispersed, e.g. acetate, dyestuffs
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/39—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using acid dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/02—Material containing basic nitrogen
- D06P3/04—Material containing basic nitrogen containing amide groups
- D06P3/06—Material containing basic nitrogen containing amide groups using acid dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/02—Material containing basic nitrogen
- D06P3/04—Material containing basic nitrogen containing amide groups
- D06P3/14—Wool
- D06P3/16—Wool using acid dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/02—Material containing basic nitrogen
- D06P3/04—Material containing basic nitrogen containing amide groups
- D06P3/24—Polyamides; Polyurethanes
- D06P3/241—Polyamides; Polyurethanes using acid dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/34—Material containing ester groups
- D06P3/52—Polyesters
- D06P3/521—Polyesters using acid dyes
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/02—After-treatment
- D06P5/04—After-treatment with organic compounds
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/02—After-treatment
- D06P5/04—After-treatment with organic compounds
- D06P5/08—After-treatment with organic compounds macromolecular
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Dispersion Chemistry (AREA)
- Coloring (AREA)
Abstract
The present invention provides a kind of stamp releasing soaping agent, is made up of each component of following parts by weight：20 45 parts of aliphatic amine polyoxyethylene ether, 25 35 parts of polyoxyethylene, 10 20 parts of Dodecyl Polyoxyethylene Ether, 15 parts of sorbierite, 0.1 2 parts of methylisothiazolinone, 12 25 parts of water.The stamp releasing soaping agents of GS 929 are by having the chemicals of strong affinity to be formed with adjuvant compounding to dyestuff.Strong detergency, dispersion effect are good, thus the ability that there is splendid anti-white background to stain to PRINTED FABRIC.Soil resistant for the nylon after acid dyes stamp, silk, wool etc. is soaped.PRINTED FABRIC form and aspect after being soaped through it are distinct, and staining will not be produced between a variety of colors, and color fastness is excellent, is a kind of preferable stamp releasing soaping agent.
Description
Technical field
The invention belongs to textile auxiliary field, a kind of stamp releasing soaping agent and its preparation side are specifically related to
Method.
Background technology
Acid dyes（Acid Dyes）It is the water-soluble dye that acidic-group is carried on a class formation, in acid medium
Dyed.Most of acid dyes contains sulfonate sodium, can be dissolved in water, and bright in colour, chromatogram is complete.Be mainly used in wool,
Silk and polyamide fibre etc. are dyed, it can also be used in terms of leather, paper, ink.To the general non-coloring power of cellulose fibre.By some
The metal complexes such as acid dyes and chromium, cobalt are formed.Water-soluble, its dye product sun-proof, light fastness are excellent.Its dye matrix and
Acid mordant dye is similar, but when preparing dyestuff, metallic atom is introduced into Azo dye, metallic atom and dyestuff
Molecular proportion is 1:1, therefore also known as 1:1 premetallized dye.It need not be handled again with mordant during dyeing.Such as acid complexing Huang GR
（That is C.I. acid yellow 99s）.
Sulfonic group is not contained in another kind of acidic complex dye molecule, and contains the hydrophilic radicals such as sulfonamido, in molecule
Metallic atom is 1 with dye molecule ratio:2, therefore also known as 1:2 premetallized dyes.It is dyed in neutral or weak acidic medium, institute
To be referred to as neutral dye.Such as neutral ash 2BL（That is C.I. acid blacks 60）.
Acid dyes has azo-type, anthraquinone type, triaryl methane type etc., but major part belongs to azo dyes.Acidity complexing dye
The production of material is similar to general dyestuff, but must increase a step and the technique of metal complex, such as neutral ash 2BL, first by 2- ammonia
Base phenol -4- sulfonamide diazotising, is coupled with 1- acetylaminohydroxyphenylarsonic acid 7- naphthols, is then formed again with the complexing of chromium salicylate sodium.
Nylon, terylene, silk, wool after acid dyes stamp etc. carry out soil resistant soap with existing releasing soaping agent
Wash, PRINTED FABRIC color is not mutually distinct enough, and staining can be produced between a variety of colors, and color fastness is inadequate.
The content of the invention
The invention provides a kind of stamp releasing soaping agent, to realize that purpose scheme is as follows：
A kind of stamp releasing soaping agent, described stamp releasing soaping agent is made up of each component of following parts by weight：Stearyl Amine
20-45 parts, 25-35 parts of polyoxyethylene, 10-20 parts of Dodecyl Polyoxyethylene Ether, 1-5 parts of sorbierite, methylisothiazolinone
0.1-2 parts, 12-25 parts of water.
Preferably, described stamp releasing soaping agent is made up of each component of following parts by weight：20-40 parts of Stearyl Amine,
25-30 parts of polyoxyethylene, 10-18 parts of Dodecyl Polyoxyethylene Ether, 1-5 parts of sorbierite, 0.1-2 parts of methylisothiazolinone, water
12-25 parts.
It is further preferred that described stamp releasing soaping agent is made up of each component of following parts by weight：Stearyl Amine 25-
40 parts, 26-30 parts of polyoxyethylene, 12-18 parts of Dodecyl Polyoxyethylene Ether, 1-4 parts of sorbierite, methylisothiazolinone 0.1-1
Part, 15-25 parts of water.
It is further preferred that described stamp releasing soaping agent is made up of each component of following parts by weight：Stearyl Amine 30
Part, 30 parts of polyoxyethylene, 15 parts of Dodecyl Polyoxyethylene Ether, 3 parts of sorbierite, 0.5 part of methylisothiazolinone, 21.5 parts of water.
It is further preferred that described stamp releasing soaping agent is made up of each component of following parts by weight：Stearyl Amine 32
Part, 28 parts of polyoxyethylene, 15 parts of Dodecyl Polyoxyethylene Ether, 3 parts of sorbierite, 0.3 part of methylisothiazolinone, 21.7 parts of water.
It is further preferred that the ratio of weight and number of the Dodecyl Polyoxyethylene Ether and sorbierite is 3：1.
A kind of preparation method of stamp releasing soaping agent, it is characterised in that：The each component of proportional quantity is mixed, stirring is equal
It is even, chelated 15-20 minutes in the case where reactor temperature is 200-300 DEG C, prepare stamp releasing soaping agent.
Described stamp releasing soaping agent, for the nylon after acid dyes stamp, terylene, silk, wool releasing
Dirt is soaped, and is soaped while being also applied for the releasing after Disperse Printing.
The advantage of the invention is that：
1st, GS-929 stamps releasing soaping agent is by having the chemicals of strong affinity and adjuvant compounding to form to dyestuff.Decontamination
Power is strong, dispersion effect is good, thus the ability that there is splendid anti-white background to stain to PRINTED FABRIC.For after acid dyes stamp
The soil resistant of nylon, terylene, silk, wool etc. soap, soaped while being also applied for the releasing after Disperse Printing.Through it
PRINTED FABRIC form and aspect after soaping are distinct, and staining will not be produced between a variety of colors, and color fastness is excellent, are a kind of preferable
Stamp releasing soaping agent.
2nd, specifically designed for after acid dyes stamp or Disperse Printing fabric soap, can efficiently remove loose colour and
Printing gum, while returning again for dyestuff can be prevented to be stained with well, with excellent soap ability and anti-white background contamination performance.
3rd, the coloured light of PRINTED FABRIC is had little to no effect, it is ensured that coloured light is pure after soaping.
4th, with low bubble, it can avoid due to contamination problems caused by foam；
5th, not phosphorous and APEO, complies fully with International Environmental Protection standard.
6th, the ratio of weight and number of Dodecyl Polyoxyethylene Ether and sorbierite is 3：Ability of being soaped when 1 and anti-white background stain performance
Most preferably.
Embodiment
Following embodiment facilitates a better understanding of the present invention, but does not limit the experiment in the present invention, following embodiments
Method, such as without special circumstances, is accordingly to be regarded as conventional method.
| Stearyl Amine（Kg) | Polyoxyethylene（Kg) | Dodecyl Polyoxyethylene Ether（Kg) | Sorbierite（Kg) | Methylisothiazolinone（Kg) | Water（Kg) | |
| Embodiment 1 | 35 | 25 | 15 | 3 | 0.2 | 21.8 |
| Embodiment 2 | 32 | 29 | 15 | 3 | 0.5 | 20.5 |
| Embodiment 3 | 30 | 30 | 15 | 3 | 0.5 | 21.5 |
| Embodiment 4 | 28 | 32 | 15 | 3 | 0.8 | 21.5 |
| Embodiment 5 | 25 | 35 | 15 | 3 | 1 | 20.5 |
| Comparative example 1 | 32 | 28 | 13 | 5 | 0.5 | 21.5 |
| Comparative example 2 | 30 | 30 | 12 | 6 | 1 | 21.5 |
Through overtesting, the formula and preparation method of the equal subordinate present invention of various embodiments above 1-5, are that outward appearance is light yellow
Liquid, pH value is 6.0-8.0（1% aqueous solution）Stamp releasing soaping agent.According to consumption 2-5g/L, and comparative example 1,2 is not belonging to
The formula of the present invention.
By the actual test of being soaped of stamp releasing soaping agent made above, different soaping method usage amounts is different.
The soaping agent of each embodiment tests following methods once.
First, infusion process（Soaped for nylon printing）
1st, light color flower is soaped
GS-929 2-3g/L
Soda ash 1.5g/L
Normal temperature X 10-15 minutes
2nd, middle dyeing defect is soaped
GS-929 3-4g/L
Soda ash 1.5g/L
Normal temperature X 20-30 minutes
3rd, dark flower is soaped
GS-929 3-5g/L
Soda ash 1.5g/L
Normal temperature X 30 minutes
2nd, padding method（Soaped for nylon printing）
First groove, normal temperature wash water
Second groove, normal temperature wash water
3rd groove, 50 degree, GS-929 2-5g/l soda ash 1-2g/l
4th groove, 50 degree, GS-929 2-5g/l soda ash 1-2g/l
5th groove, 50 degree, wash water
6th groove, normal temperature cleaning
7th groove, normal temperature cleaning
8th groove, fixation treatment GS-213 4-20g/L 60-70 DEG C
3rd, soaped for printed polyester
1st, light color flower is soaped
GS-929 2-3g/L
Soda ash 3.0g/L
10-15 minutes → reduction cleanings of normal temperature X
2nd, middle dyeing defect is soaped
GS-929 2-4g/L
Soda ash 3.0g/L
10-20 minutes → reduction cleanings of normal temperature X
3rd, dark flower is soaped（Soaped it is recommended that first making normal temperature soda ash, then do 70 degree of caustic soda and soaped）
Soda ash is washed:
GS-929 3-5g/L
Soda ash 3.0g/L
Normal temperature X 10-20 minutes
Caustic soda is washed:
GS-929 3-5g/L
Caustic soda 3.0g/L
10-20 minutes → reduction cleanings of 70 DEG C of X
Tested more than, it is found that embodiment 1-5 soaping agent strong detergency, dispersion effect is good, thus had to PRINTED FABRIC
The ability that splendid anti-white background stains.PRINTED FABRIC form and aspect after being soaped through it are distinct, and staining will not be produced between a variety of colors,
And color fastness is excellent.And comparative example 1-2 soaping agent effect is substantially not so good as embodiment 1-5 soaping agent.
Finally it should be noted that：The preferred embodiment of invention is the foregoing is only, the limitation present invention is not intended as, to the greatest extent
The present invention is described in detail with reference to the foregoing embodiments for pipe, for those skilled in the art, and it still can be with
Technical scheme described in foregoing embodiments is modified, or equivalent substitution is carried out to which part technical characteristic.It is all
Within the spirit and principles in the present invention, any modification, equivalent substitution and improvements made etc. should be included in the protection of the present invention
Within the scope of.
Claims (8)
1. a kind of stamp releasing soaping agent, it is characterised in that；Described stamp releasing soaping agent by following parts by weight each component
Composition：20-45 parts of Stearyl Amine, 25-35 parts of polyoxyethylene, 10-20 parts of Dodecyl Polyoxyethylene Ether, 1-5 parts of sorbierite, first
0.1-2 parts of base OIT, 12-25 parts of water.
2. the stamp releasing soaping agent according to claims 1, it is characterised in that：Described stamp releasing soaping agent by with
The each component composition of lower parts by weight：20-40 parts of Stearyl Amine, 25-30 parts of polyoxyethylene, Dodecyl Polyoxyethylene Ether 10-18
Part, 1-5 parts of sorbierite, 0.1-2 parts of methylisothiazolinone, 12-25 parts of water.
3. the stamp releasing soaping agent according to claims 1, it is characterised in that：Described stamp releasing soaping agent by with
The each component composition of lower parts by weight：25-40 parts of Stearyl Amine, 26-30 parts of polyoxyethylene, Dodecyl Polyoxyethylene Ether 12-18
Part, 1-4 parts of sorbierite, 0.1-1 parts of methylisothiazolinone, 15-25 parts of water.
4. the stamp releasing soaping agent according to claims 1, it is characterised in that：Described stamp releasing soaping agent by with
The each component composition of lower parts by weight：30 parts of Stearyl Amine, 30 parts of polyoxyethylene, 15 parts of Dodecyl Polyoxyethylene Ether, sorbierite 3
Part, 0.5 part of methylisothiazolinone, 21.5 parts of water.
5. the stamp releasing soaping agent according to claims 1, it is characterised in that：Described stamp releasing soaping agent by with
The each component composition of parts by weight：32 parts of Stearyl Amine, 28 parts of polyoxyethylene, 15 parts of Dodecyl Polyoxyethylene Ether, 3 parts of sorbierite,
0.3 part of methylisothiazolinone, 21.7 parts of water.
6. the stamp releasing soaping agent according to claims 1, it is characterised in that：The Dodecyl Polyoxyethylene Ether and mountain
The ratio of weight and number of pears alcohol is 3：1.
7. the preparation method of stamp releasing soaping agent described in a kind of claim 1-6 any one, it is characterised in that：By proportional quantity
Each component mixing, stir, reactor temperature be 100-120 DEG C at chelate 200-300 minutes, prepare stamp
Releasing soaping agent.
8. the stamp releasing soaping agent according to claim 1-6, for the nylon after acid dyes stamp, terylene, true
Silk, the soil resistant of wool are soaped, and are soaped while being also applied for the releasing after Disperse Printing.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710383055.9A CN107151929A (en) | 2017-05-26 | 2017-05-26 | A kind of stamp releasing soaping agent and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710383055.9A CN107151929A (en) | 2017-05-26 | 2017-05-26 | A kind of stamp releasing soaping agent and preparation method thereof |
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| Publication Number | Publication Date |
|---|---|
| CN107151929A true CN107151929A (en) | 2017-09-12 |
Family
ID=59794475
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|---|---|---|---|
| CN201710383055.9A Pending CN107151929A (en) | 2017-05-26 | 2017-05-26 | A kind of stamp releasing soaping agent and preparation method thereof |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110331603A (en) * | 2019-08-06 | 2019-10-15 | 广东科峰新材料科技有限公司 | A kind of acid dyeing and calico-printer's soap detergent composition and preparation method thereof |
| CN111118935A (en) * | 2019-12-11 | 2020-05-08 | 广东德润纺织有限公司 | Non-floating color flat screen printing process |
| CN111733023A (en) * | 2020-07-01 | 2020-10-02 | 广东德美精细化工集团股份有限公司 | Wax printing soaping agent and preparation method thereof |
| CN111764186A (en) * | 2019-03-31 | 2020-10-13 | 江苏海云花新材料有限公司 | Preparation method of soaping agent for polyester-polyurethane fastness |
| CN114045692A (en) * | 2021-11-25 | 2022-02-15 | 多恩生物科技有限公司 | Active anti-staining soaping agent |
| CN116083179A (en) * | 2022-12-29 | 2023-05-09 | 江苏华达新材料科技有限公司 | Fabric anti-flooding cleaning agent and anti-flooding method thereof |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111764186A (en) * | 2019-03-31 | 2020-10-13 | 江苏海云花新材料有限公司 | Preparation method of soaping agent for polyester-polyurethane fastness |
| CN110331603A (en) * | 2019-08-06 | 2019-10-15 | 广东科峰新材料科技有限公司 | A kind of acid dyeing and calico-printer's soap detergent composition and preparation method thereof |
| CN111118935A (en) * | 2019-12-11 | 2020-05-08 | 广东德润纺织有限公司 | Non-floating color flat screen printing process |
| CN111733023A (en) * | 2020-07-01 | 2020-10-02 | 广东德美精细化工集团股份有限公司 | Wax printing soaping agent and preparation method thereof |
| CN114045692A (en) * | 2021-11-25 | 2022-02-15 | 多恩生物科技有限公司 | Active anti-staining soaping agent |
| CN116083179A (en) * | 2022-12-29 | 2023-05-09 | 江苏华达新材料科技有限公司 | Fabric anti-flooding cleaning agent and anti-flooding method thereof |
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Application publication date: 20170912 |