CN107151095A - A kind of implosion guard and preparation method thereof - Google Patents
A kind of implosion guard and preparation method thereof Download PDFInfo
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- CN107151095A CN107151095A CN201710366940.6A CN201710366940A CN107151095A CN 107151095 A CN107151095 A CN 107151095A CN 201710366940 A CN201710366940 A CN 201710366940A CN 107151095 A CN107151095 A CN 107151095A
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C3/00—Glass compositions
- C03C3/12—Silica-free oxide glass compositions
- C03C3/14—Silica-free oxide glass compositions containing boron
- C03C3/145—Silica-free oxide glass compositions containing boron containing aluminium or beryllium
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B25/00—Annealing glass products
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Adhesives Or Adhesive Processes (AREA)
- Laminated Bodies (AREA)
Abstract
The invention discloses a kind of implosion guard and preparation method thereof, 50 100 parts of Petropols, 20 30 parts of boron oxide, 5 20 parts of Lauryl Alcohol ester, 15 20 parts of dodecane glucosides, 5 10 parts of alundum (Al2O3), 5 parts of silicon phosphatase 11,15 parts of mica powder are taken, mixed material is mixed to obtain；Mixed material is added in crucible, 23 hours are incubated at 850 DEG C, 1,300 1500 DEG C is warming up to and is incubated 12 hours, obtain glass stoste；13 parts of dispersant, 13 parts of adhesive, 12 parts of thickener are added into glass stoste, stirs 10 20 minutes, obtains glass metal；Glass metal is poured into preheated copper coin die for molding, put into be preheated in 600 800 DEG C of Muffle furnace anneal 24 hours after, furnace cooling obtains implosion guard to room temperature.Present invention making raw material is simple and easy to get, and manufacture craft is simple to operation；Gained finished product has high explosion-proof and shock resistance.
Description
Technical field
The present invention relates to a kind of glass, and in particular to a kind of implosion guard and preparation method thereof.
Background technology
With the development of science and technology, needing to use the place of glass becomes variation, have tighter to glass properties index
Lattice and various requirement, wherein, implosion guard is mainly used in preventing glass breaking from scattering everywhere, is difficult to internal staff and furniture
Cause damage, be widely used in finance, charge place, high-level meeting center, luxurious hotel, museum, consulate with
And the occasion such as police military safety devices and private savings villa.However, existing implosion guard, makes complicated, with high costs, and it is anti-
Quick-fried performance needs further raising.
The content of the invention
The technical problem of solution：In view of the shortcomings of the prior art, the invention provides a kind of implosion guard and its preparation side
Method, improves the explosion-proof performance of existing glass.
Technical scheme：A kind of implosion guard that the present invention is provided, is prepared from the following raw materials in parts by weight：Petropols
50-100 parts, 20-30 parts of boron oxide, 5-20 parts of Lauryl Alcohol ester, 15-20 parts of dodecane glucosides, 5-10 parts of alundum (Al2O3), silicon
- 5 parts of phosphatase 11,1-5 parts of mica powder, 1-3 parts of dispersant, 1-3 parts of adhesive, 1-2 parts of thickener.
The dispersant is the mixture from one or both of waterglass, sodium tripolyphosphate, when both are used in mixed way
Mass ratio is 1:1.
The adhesive is the mixture of one or both of polyvinyl alcohol, Vinylidene Chloride, matter when both are used in mixed way
Amount is than being 1:2.
The thickener is the mixture of one or both of polyacrylamide, polyvinyl alcohol, when both are used in mixed way
Mass ratio is 1:1.
A kind of preparation method for implosion guard that the present invention is provided, it includes following preparation process：
（1）Weigh 50-100 parts of Petropols, 20-30 parts of boron oxide, 5-20 parts of Lauryl Alcohol ester, 15-20 parts of dodecane glucosides,
5-10 parts of alundum (Al2O3), -5 parts of silicon phosphatase 11,1-5 parts of mica powder, are well mixed to obtain mixed material；
（2）Said mixture material is added in crucible, 2-3 hours are incubated at 850 DEG C, 1300-1500 DEG C of insulation 1-2 is warming up to small
When, obtain glass stoste；The speed of the heating is 80-100 DEG C/min.
（3）1-3 parts of dispersant, 1-3 parts of adhesive, 1-2 parts of thickener are added into above-mentioned glass stoste, 10-20 is stirred
Minute, obtain glass metal；
（4）Above-mentioned glass metal is poured into preheated copper coin die for molding, put into the Muffle furnace for being preheated to 600-800 DEG C
After annealing 2-4 hours, furnace cooling obtains implosion guard to room temperature.
Beneficial effect：A kind of implosion guard that the present invention is provided, making raw material is simple and easy to get, and manufacture craft is simply easily grasped
Make；Gained finished product has high explosion-proof and shock resistance.
Embodiment
The present invention is further illustrated below by the mode of embodiment, but therefore protection scope of the present invention is not confined to
Following embodiments, but limited by description and claims of this specification.
Embodiment 1
A kind of implosion guard, is prepared from the following raw materials in parts by weight：50 parts of Petropols, 20 parts of boron oxide, Lauryl Alcohol ester 5
Part, 15 parts of dodecane glucosides, 5 parts of alundum (Al2O3), silicon phosphatase 11 part, 1 part of mica powder, 1 part of dispersant, 1 part of adhesive, thickening
1 part of agent；Its preparation method is as follows：
（1）Weigh 50 parts of Petropols, 20 parts of boron oxide, 5 parts of Lauryl Alcohol ester, 15 parts of dodecane glucosides, alundum (Al2O3) 5
Part, silicon phosphatase 11 part, 1 part of mica powder, are well mixed to obtain mixed material；
（2）Said mixture material is added in crucible, 2 hours is incubated at 850 DEG C, 1300 is warming up to 80 DEG C/min of speed
DEG C insulation 1 hour, obtain glass stoste；
（3）Add from 1 part of waterglass, 1 part of polyvinyl alcohol, 1 part of polyacrylamide, stir 10 minutes into above-mentioned glass stoste,
Obtain glass metal；
（4）Above-mentioned glass metal is poured into preheated copper coin die for molding, puts into be preheated in 600 DEG C of Muffle furnace and anneals
After 2 hours, furnace cooling obtains implosion guard to room temperature.
Embodiment 2
A kind of implosion guard, is prepared from the following raw materials in parts by weight：80 parts of Petropols, 25 parts of boron oxide, Lauryl Alcohol ester
10 parts, 18 parts of dodecane glucosides, 7 parts of alundum (Al2O3), 2 parts of silicon phosphoric acid, 2 parts of mica powder, 2 parts of dispersant, 2 parts of adhesive, increase
Thick dose 2 parts；Its preparation method is as follows：
（1）Weigh 80 parts of Petropols, 25 parts of boron oxide, 10 parts of Lauryl Alcohol ester, 18 parts of dodecane glucosides, alundum (Al2O3) 7
Part, 2 parts of silicon phosphoric acid, 2 parts of mica powder, are well mixed to obtain mixed material；
（2）Said mixture material is added in crucible, 2.5 hours is incubated at 850 DEG C, is warming up to 90 DEG C/min of speed
1400 DEG C are incubated 1.5 hours, obtain glass stoste；
（3）2 parts of sodium tripolyphosphate, 2 parts of Vinylidene Chloride, 2 parts of polyvinyl alcohol are added into above-mentioned glass stoste, is stirred 15 minutes,
Obtain glass metal；
（4）Above-mentioned glass metal is poured into preheated copper coin die for molding, puts into be preheated in 700 DEG C of Muffle furnace and anneals
After 3 hours, furnace cooling obtains implosion guard to room temperature.
Embodiment 3
A kind of implosion guard, is prepared from the following raw materials in parts by weight：100 parts of Petropols, 30 parts of boron oxide, Lauryl Alcohol ester
20 parts, 20 parts of dodecane glucosides, 10 parts of alundum (Al2O3), 5 parts of silicon phosphoric acid, 5 parts of mica powder, 3 parts of dispersant, 3 parts of adhesive, increase
Thick dose 2 parts；Its preparation method is as follows：
（1）Weigh 100 parts of Petropols, 30 parts of boron oxide, 20 parts of Lauryl Alcohol ester, 20 parts of dodecane glucosides, alundum (Al2O3)
10 parts, 5 parts of silicon phosphoric acid, 5 parts of mica powder, be well mixed to obtain mixed material；
（2）Said mixture material is added in crucible, 3 hours is incubated at 850 DEG C, 1500 is warming up to 100 DEG C/min of speed
DEG C insulation 2 hours, obtain glass stoste；
（3）3 parts of sodium tripolyphosphate, 3 parts of polyvinyl alcohol, 2 parts of polyacrylamide are added into above-mentioned glass stoste, 20 points are stirred
Clock, obtains glass metal；
（4）Above-mentioned glass metal is poured into preheated copper coin die for molding, puts into be preheated in 800 DEG C of Muffle furnace and anneals
After 4 hours, furnace cooling obtains implosion guard to room temperature.
Embodiment 4
A kind of implosion guard, is prepared from the following raw materials in parts by weight：85 parts of Petropols, 27 parts of boron oxide, Lauryl Alcohol ester
18 parts, 16 parts of dodecane glucosides, 9 parts of alundum (Al2O3), silicon phosphatase 24 part, 2 parts of mica powder, from 1 part of waterglass, sodium tripolyphosphate 1
Part, 1 part of polyvinyl alcohol, 2 parts of Vinylidene Chloride, 1 part of polyacrylamide, 1 part of polyvinyl alcohol；Its preparation method is as follows：
（1）Weigh 85 parts of Petropols, 27 parts of boron oxide, 18 parts of Lauryl Alcohol ester, 16 parts of dodecane glucosides, alundum (Al2O3) 9
Part, silicon phosphatase 24 part, 2 parts of mica powder, are well mixed to obtain mixed material；
（2）Said mixture material is added in crucible, 2.5 hours is incubated at 850 DEG C, is warming up to 100 DEG C/min of speed
1500 DEG C are incubated 1.5 hours, obtain glass stoste；
（3）Added into above-mentioned glass stoste from 1 part of waterglass, 1 part of sodium tripolyphosphate, 1 part of polyvinyl alcohol, 2 parts of Vinylidene Chloride,
1 part of polyacrylamide, 1 part of polyvinyl alcohol, stir 15 minutes, obtain glass metal；
（4）Above-mentioned glass metal is poured into preheated copper coin die for molding, puts into be preheated in 700 DEG C of Muffle furnace and anneals
After 2.5 hours, furnace cooling obtains implosion guard to room temperature.
Using universal testing machine to made from above-described embodiment implosion guard carry out mechanical performance measure, and with common glass
Glass compares, and concrete outcome see the table below：
| Toughness/MPa | Tensile strength/MPa | |
| Embodiment 1 | 820 | 720 |
| Embodiment 2 | 835 | 732 |
| Embodiment 3 | 850 | 741 |
| Embodiment 4 | 860 | 756 |
| Simple glass | 460 | 500 |
From upper table it can be found that implosion guard toughness prepared by the present invention is big, tensile strength is big, with excellent Mechanics of Machinery
Performance.
Claims (6)
1. a kind of implosion guard, it is characterised in that be prepared from the following raw materials in parts by weight：50-100 parts of Petropols, boron oxide
20-30 parts, 5-20 parts of Lauryl Alcohol ester, 15-20 parts of dodecane glucosides, 5-10 parts of alundum (Al2O3), -5 parts of silicon phosphatase 11, mica
1-5 parts of powder, 1-3 parts of dispersant, 1-3 parts of adhesive, 1-2 parts of thickener.
2. a kind of implosion guard according to claim 1, it is characterised in that：The dispersant is from waterglass, trimerization phosphorus
The mixture of one or both of sour sodium, mass ratio is 1 when both are used in mixed way:1.
3. a kind of implosion guard according to claim 1, it is characterised in that：The adhesive is polyvinyl alcohol, crosses chloroethene
The mixture of one or both of alkene, mass ratio is 1 when both are used in mixed way:2.
4. a kind of implosion guard according to claim 1, it is characterised in that：The thickener is polyacrylamide, poly- second
The mixture of one or both of enol, mass ratio is 1 when both are used in mixed way:1.
5. a kind of preparation method of implosion guard as claimed in claim 1, it is characterised in that including following preparation process：
（1）Weigh 50-100 parts of Petropols, 20-30 parts of boron oxide, 5-20 parts of Lauryl Alcohol ester, 15-20 parts of dodecane glucosides,
5-10 parts of alundum (Al2O3), -5 parts of silicon phosphatase 11,1-5 parts of mica powder, are well mixed to obtain mixed material；
（2）Said mixture material is added in crucible, 2-3 hours are incubated at 850 DEG C, 1300-1500 DEG C of insulation 1-2 is warming up to small
When, obtain glass stoste；
（3）1-3 parts of dispersant, 1-3 parts of adhesive, 1-2 parts of thickener are added into above-mentioned glass stoste, is stirred 10-20 minutes,
Obtain glass metal；
（4）Above-mentioned glass metal is poured into preheated copper coin die for molding, put into the Muffle furnace for being preheated to 600-800 DEG C
After annealing 2-4 hours, furnace cooling obtains implosion guard to room temperature.
6. a kind of preparation method of implosion guard according to claim 5, it is characterised in that：Step（2）Described in heat up
Speed be 80-100 DEG C/min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710366940.6A CN107151095A (en) | 2017-05-23 | 2017-05-23 | A kind of implosion guard and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710366940.6A CN107151095A (en) | 2017-05-23 | 2017-05-23 | A kind of implosion guard and preparation method thereof |
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| Publication Number | Publication Date |
|---|---|
| CN107151095A true CN107151095A (en) | 2017-09-12 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710366940.6A Pending CN107151095A (en) | 2017-05-23 | 2017-05-23 | A kind of implosion guard and preparation method thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110839134A (en) * | 2018-08-16 | 2020-02-25 | 单晓 | Explosion-proof television screen and preparation process of explosion-proof glass thereof |
| CN113206161A (en) * | 2021-05-06 | 2021-08-03 | 浙江合特光电有限公司 | Colorful high-light-transmission solar panel and preparation method thereof |
| CN113585925A (en) * | 2021-08-24 | 2021-11-02 | 安徽鸿玻玻璃科技有限公司 | Production process of heat-insulation explosion-proof hollow glass |
| CN114031294A (en) * | 2021-12-21 | 2022-02-11 | 苏州晶生新材料有限公司 | High-refractive-index optical material and preparation method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105753318A (en) * | 2016-03-04 | 2016-07-13 | 苏州圣谱拉新材料科技有限公司 | Heatproof anti-explosion nano glass material and preparation method thereof |
| CN106365445A (en) * | 2016-09-07 | 2017-02-01 | 安徽金生金世电子科技有限公司 | Explosion-proof glass and preparation method thereof |
-
2017
- 2017-05-23 CN CN201710366940.6A patent/CN107151095A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105753318A (en) * | 2016-03-04 | 2016-07-13 | 苏州圣谱拉新材料科技有限公司 | Heatproof anti-explosion nano glass material and preparation method thereof |
| CN106365445A (en) * | 2016-09-07 | 2017-02-01 | 安徽金生金世电子科技有限公司 | Explosion-proof glass and preparation method thereof |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110839134A (en) * | 2018-08-16 | 2020-02-25 | 单晓 | Explosion-proof television screen and preparation process of explosion-proof glass thereof |
| CN113206161A (en) * | 2021-05-06 | 2021-08-03 | 浙江合特光电有限公司 | Colorful high-light-transmission solar panel and preparation method thereof |
| CN113585925A (en) * | 2021-08-24 | 2021-11-02 | 安徽鸿玻玻璃科技有限公司 | Production process of heat-insulation explosion-proof hollow glass |
| CN114031294A (en) * | 2021-12-21 | 2022-02-11 | 苏州晶生新材料有限公司 | High-refractive-index optical material and preparation method thereof |
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Application publication date: 20170912 |