CN107138117A - A kind of covalent modified graphite intercalation compound hermetic type rapid expanding retort - Google Patents
A kind of covalent modified graphite intercalation compound hermetic type rapid expanding retort Download PDFInfo
- Publication number
- CN107138117A CN107138117A CN201710375459.3A CN201710375459A CN107138117A CN 107138117 A CN107138117 A CN 107138117A CN 201710375459 A CN201710375459 A CN 201710375459A CN 107138117 A CN107138117 A CN 107138117A
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- China
- Prior art keywords
- tank body
- charge door
- chuck
- hermetic type
- retort
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/0066—Stirrers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/0073—Sealings
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J4/00—Feed or outlet devices; Feed or outlet control devices
- B01J4/001—Feed or outlet devices as such, e.g. feeding tubes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2204/00—Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices
- B01J2204/002—Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices the feeding side being of particular interest
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
- B01J2219/00094—Jackets
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
- B01J2219/00103—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor in a heat exchanger separate from the reactor
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Carbon And Carbon Compounds (AREA)
Abstract
The invention discloses a kind of covalent modified graphite intercalation compound hermetic type rapid expanding retort, including tank body, charge door is provided with front side of the upper surface of the tank body, the inside of the charge door is provided with blanking port, the lower surface of the blanking port is provided with seal groove, the outer surface both sides of the seal groove are provided with lower end charging aperture, the inside of the seal groove slidably connects sealing block by Packing spring, the upper surface both sides of the charge door are provided with neck, the internal slide of the charge door is connected with hopper, the interior surface of neck is connected on the outside of the lower surface of the hopper by dop, the lower surface center of the hopper is provided with sliding eye, the outside of the sliding eye is provided with upper end charging aperture, the internal slide of the sliding eye is connected with push rod, the upper surface of the push rod is fixedly connected with baffle plate, the outer surface of the tank body slidably connects chuck by link slot.This kind of hermetic type rapid expanding retort can greatly improve the ease of use and service life of device.
Description
Technical field
The present invention relates to graphene presoma reaction vessel technical field, specially a kind of covalent modified graphite intercalation chemical combination
Thing hermetic type rapid expanding retort.
Background technology
Conventional at present prepares graphite presoma expansion reaction device, generally comprises on tank body and agitating device, tank body
Chuck is provided with, chuck bottom is provided with hot water or steam inlet, and top is provided with hot water or steam (vapor) outlet, and agitating device includes
Motor and agitating shaft, motor are fixed on tank body top, and agitating shaft is arranged on the middle part of tank body by motor.The present apparatus can make stone
Black intercalation compound is fully contacted with inflation fluid during the course of the reaction, so as to reach that quickening expansion reaction speed, raising reaction are filled
Point property and the purpose of reduction expansion reaction time, but still have some defects when in use, such as using being fixedly connected
It is jacket structured, after a long time use, incrustation scale is inevitably born on inwall, be so not only inconvenient to clear up, and
Cooling effect can be also substantially reduced, then it is exactly to use common feed inlet structure to have, when carrying out reaction production, internal steam
Easily impact charge door, causes the addition of graphene raw material inconvenient.
The content of the invention
It is an object of the invention to provide a kind of covalent modified graphite intercalation compound hermetic type rapid expanding retort, with
The problem of solving to propose in above-mentioned background technology.
To achieve the above object, the present invention provides following technical scheme：A kind of covalent modified graphite intercalation compound is closed
Type rapid expanding retort, including tank body, the lower surface both sides of the tank body are fixedly connected with supporting leg, the lower surface of the tank body
Center is provided with drain hole, and the interior lower end of the tank body is fixedly connected with bearing, and the lower surface of the bearing is provided with groove, institute
The upper surface for stating bearing is rotatably connected to agitating shaft by rotation hole, and the outer surface of the agitating shaft is fixedly connected with paddle
Piece, the upper surface of the agitating shaft is fixedly connected with motor by axle, and the motor is fixedly installed in the upper surface center of tank body
Place, the outer surface upper end of the tank body, which is provided with rear side of connecting seat, the upper surface of the tank body, is provided with venthole, the tank body it is upper
Charge door is provided with front side of surface, the inside of the charge door is provided with blanking port, and the lower surface of the blanking port is provided with seal groove, institute
The outer surface both sides for stating seal groove are provided with lower end charging aperture, and the inside of the seal groove slidably connects sealing by Packing spring
Block, the upper surface both sides of the charge door are provided with neck, and the internal slide of the charge door is connected with hopper, the hopper
Outer side surface is connected in the interior surface of neck by dop, and the lower surface center of the hopper is provided with sliding eye, the cunning
The outside in dynamic hole is provided with upper end charging aperture, and the internal slide of the sliding eye is connected with push rod, and the upper surface of the push rod is fixed
Baffle plate is connected with, the outer surface of the tank body slidably connects chuck by link slot, and the outer surface lower end of the chuck is provided with
Water inlet, the outer surface upper end of the chuck is provided with delivery port, and the upper surface both sides of the chuck are provided with threaded block, the screw thread
Seat is fixedly connected on the inside of connecting seat by screw, and the inside of the chuck is provided with waterway, the inner side table of the link slot
Face is provided with annular groove, and the inside of the annular groove is installed with Gask-O-Seal.
It is preferred that, the stirring vane at least three, and tapered Structural assignments.
It is preferred that, the sealing block is slidably connected to the lower surface of blanking port.
It is preferred that, the upper end charging aperture is located at the underface of blanking port, and positioned at the underface of baffle plate.
Compared with prior art, the beneficial effects of the invention are as follows：This kind of covalent modified graphite intercalation compound hermetic type is fast
Fast expansion reaction tank, with reference to the structure type of Gask-O-Seal, can facilitate mounting box to tear open by setting the chuck being slidably installed
Unload, be convenient to clean incrustation scale, then have exactly by spring sealed charge door combination hopper, can be added in the case of closed
Material, it is to avoid material is dispelled, and can so greatly improve the ease of use and service life of device.
Brief description of the drawings
Fig. 1 is a kind of entirety of covalent modified graphite intercalation compound hermetic type rapid expanding retort of the present invention
Structural representation；
Fig. 2 is a kind of charging of covalent modified graphite intercalation compound hermetic type rapid expanding retort of the present invention
Mouth structure schematic diagram；
Fig. 3 is a kind of chuck of covalent modified graphite intercalation compound hermetic type rapid expanding retort of the present invention
Schematic cross-section.
Division mark is as follows in accompanying drawing：1st, tank body, 11, supporting leg, 12, drain hole, 13, bearing, 14, groove, 15, rotate
Hole, 16, agitating shaft, 17, stirring vane, 18, motor, 19, connecting seat, 2, charge door, 21, blanking port, 22, seal groove, 23, under
Endfeed mouthful, 24, Packing spring, 25, sealing block, 26, neck, 27, venthole, 3, hopper, 31, dop, 32, sliding eye, 33,
Upper end charging aperture, 34, push rod, 35, baffle plate, 4, chuck, 41, link slot, 42, water inlet, 43, delivery port, 44, threaded block, 45,
Waterway, 46, annular groove, 47, Gask-O-Seal.
Embodiment
Below in conjunction with the accompanying drawing in the embodiment of the present invention, the technical scheme in the embodiment of the present invention is carried out clear, complete
Site preparation is described, it is clear that described embodiment is only a part of embodiment of the invention, rather than whole embodiments.It is based on
Embodiment in the present invention, it is every other that those of ordinary skill in the art are obtained under the premise of creative work is not made
Embodiment, belongs to the scope of protection of the invention.
Fig. 1-3 are referred to, the present invention provides a kind of technical scheme：A kind of covalent modified graphite intercalation compound hermetic type is fast
Fast expansion reaction tank, including tank body 1, the outer surface of tank body 1 are smooth surface, convenient to be connected with chuck 4, and can and it is annular
Sealing gasket 47 is contacted well, it is ensured that sealing, the lower surface both sides of tank body 1 are fixedly connected with supporting leg 11, the lower surface of tank body 1
Center is provided with drain hole 12, and the interior lower end of tank body 1 is fixedly connected with bearing 13, and the lower surface of bearing 13 is provided with groove 14,
The upper surface of bearing 13 is rotatably connected to agitating shaft 16 by rotation hole 15, and the outer surface of agitating shaft 16 is fixedly connected with paddle
Piece 17, stirring vane 17 at least three, and tapered Structural assignments, it is ensured that the uniformity of stirring, agitating shaft 16 it is upper
Surface is fixedly connected with motor 18 by axle, and motor 18 is fixedly installed in the upper surface center of tank body 1, the outer surface of tank body 1
Upper end, which is provided with rear side of connecting seat 19, the upper surface of tank body 1, is provided with venthole 27, and charge door 2 is provided with front side of the upper surface of tank body 1,
The inside of charge door 2 is provided with blanking port 21, and the lower surface of blanking port 21 is provided with seal groove 22, and the outer surface both sides of seal groove 22 are set
There is lower end charging aperture 23, the inside of seal groove 22 slidably connects sealing block 25 by Packing spring 24, and sealing block 25, which is slided, to be connected
The lower surface of blanking port 21 is connected to, is sealed when not feeding, the upper surface both sides of charge door 2 are provided with neck 26, charge door 2
Internal slide be connected with hopper 3, the interior surface of neck 26, hopper 3 are connected on the outside of the lower surface of hopper 3 by dop 31
Lower surface center be provided with sliding eye 32, the outside of sliding eye 32 is provided with upper end charging aperture 33, and upper end charging aperture 33 is located to fall
The underface of material mouth 21, and positioned at the underface of baffle plate 35, so ensure that material accurately enters blanking port 21, Ke Yishun
Sharp enters inside tank body 1, and the internal slide of sliding eye 32 is connected with push rod 34, and the upper surface of push rod 34 is fixedly connected with gear
Plate 35, the outer surface of tank body 1 slidably connects chuck 4 by link slot 41, and the outer surface lower end of chuck 4 is provided with water inlet 42,
The outer surface upper end of chuck 4 is provided with delivery port 43, and the upper surface both sides of chuck 4 are provided with threaded block 44, and threaded block 44 passes through screw
The inside of connecting seat 19 is fixedly connected on, the inside of chuck 4 is provided with waterway 45, and the inner surface of link slot 41 is provided with annular groove
46, the inside of annular groove 46 is installed with Gask-O-Seal 47.
The present invention is in the specific implementation：From model YEJ-M20 motor 18, and it is connected in series to working power
On switch, raw material, and the good quantitative inflation fluid of configuration in 1 body 1 are then added into tank body 1 by charge door 2 in proportion, so
After add graphite intercalation compound powder, graphite intercalation compound is floated on liquid level after being contacted with inflation fluid, is taken place swollen
Swollen reaction, the reaction is static process (gathering heat of reaction, accelerate the progress of reaction), touches the graphite intercalation of inflation fluid
Compound first participates in reaction, but with the progress of reaction, material bed increasingly thicker, upper materials can not be touched by siphonage
Inflation fluid, can now start motor 18 and drive agitating shaft 16 to mix the solid-liquid phase materials in tank body, about stirring a few minutes
Zhong Hou, stops stirring, continues to react, until graphite intercalation compound reacts completely.It can be produced the multiple short time in course of reaction
A large amount of steam, in time can be discharged steam by gas outlet 27, and when needing to add materials during the course of the reaction, can be by material
It is placed into hopper 3, then hopper 3 is put into inside charge door 2, the clamping of dop 31 can be entered and be consolidated in neck 26
Fixed, push rod 34 can touch sealing block 25 first, persistently advance downwardly, and can open sealing block 25, also just can be by blanking
Mouthfuls 21 connects with lower end charging aperture 23, and sealing block 25 is reached behind bottom, then proceed to propulsion, and push rod 34 can not be moved down will be to
Upper movement, baffle plate 35 can be pushed up open upwards, also can just be opened upper end blanking port 33, be so located at the material in hopper 3
It can be entered from blanking port 21 inside tank body 1, both ensure that sealing, material addition, very safe ready can be carried out again.
And heat can be produced in reaction, reaction rate is easily influenceed, at this moment water inlet 42 and delivery port 43 circulation can be connected to
In water loop, cooling water can be passed through in chuck 4, such cooling water is connect in waterway 45 in the outer surface of tank body 1
Touch, it is ensured that the temperature of inflation fluid can condense incrustation scale in OK range after long-time use, on the inwall of waterway 45,
At this moment chuck 4 can be disassembled and is cleared up, can reused, and ensure the efficiency of water cooling, production can be accelerated
Efficiency, releases product when that after completion of the reaction, can open drain hole 12.
Although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
A variety of changes, modification can be carried out to these embodiments, replace without departing from the principles and spirit of the present invention by understanding
And modification, the scope of the present invention is defined by the appended.
Claims (4)
1. a kind of covalent modified graphite intercalation compound hermetic type rapid expanding retort, including tank body (1), it is characterised in that：
The lower surface both sides of the tank body (1) are fixedly connected with supporting leg (11), and the lower surface center of the tank body (1) is provided with drain hole
(12), the interior lower end of the tank body (1) is fixedly connected with bearing (13), and the lower surface of the bearing (13) is provided with groove
(14), the upper surface of the bearing (13) is rotatably connected to agitating shaft (16) by rotation hole (15), the agitating shaft (16)
Outer surface is fixedly connected with stirring vane (17), and the upper surface of the agitating shaft (16) is fixedly connected with motor (18) by axle,
The motor (18) is fixedly installed in the upper surface center of tank body (1), and the outer surface upper end of the tank body (1) is provided with connecting seat
(19), it is provided with rear side of the upper surface of the tank body (1) on front side of venthole (27), the upper surface of the tank body (1) and is provided with charge door
(2), the inside of the charge door (2) is provided with blanking port (21), and the lower surface of the blanking port (21) is provided with seal groove (22)；
The outer surface both sides of the seal groove (22) are provided with lower end charging aperture (23), and the inside of the seal groove (22) passes through sealing
Spring (24) slidably connects sealing block (25), and the upper surface both sides of the charge door (2) are provided with neck (26), the charge door
(2) internal slide is connected with the outside of hopper (3), the lower surface of the hopper (3) and is connected in neck (26) by dop (31)
Interior surface, the lower surface center of the hopper (3) is provided with sliding eye (32), and the outside of the sliding eye (32) is provided with upper
Endfeed mouthful (33), the internal slide of the sliding eye (32) is connected with push rod (34), and the upper surface of the push rod (34) is fixed
It is connected with baffle plate (35)；
The outer surface of the tank body (1) is slidably connected under chuck (4), the outer surface of the chuck (4) by link slot (41)
End is provided with water inlet (42), and the outer surface upper end of the chuck (4) is provided with delivery port (43), the upper surface two of the chuck (4)
Side is provided with threaded block (44), and the threaded block (44) is fixedly connected on the inside of connecting seat (19), the chuck (4) by screw
Inside be provided with waterway (45), the inner surface of the link slot (41) is provided with annular groove (46), the annular groove (46)
Inside is installed with Gask-O-Seal (47).
2. a kind of covalent modified graphite intercalation compound hermetic type rapid expanding retort according to claim 1, it is special
Levy and be：The stirring vane (17) at least three, and tapered Structural assignments.
3. a kind of covalent modified graphite intercalation compound hermetic type rapid expanding retort according to claim 1, it is special
Levy and be：The sealing block (25) is slidably connected to the lower surface of blanking port (21).
4. a kind of covalent modified graphite intercalation compound hermetic type rapid expanding retort according to claim 1, it is special
Levy and be：The upper end charging aperture (33) is located at the underface of blanking port (21), and positioned at the underface of baffle plate (35).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710375459.3A CN107138117A (en) | 2017-05-24 | 2017-05-24 | A kind of covalent modified graphite intercalation compound hermetic type rapid expanding retort |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710375459.3A CN107138117A (en) | 2017-05-24 | 2017-05-24 | A kind of covalent modified graphite intercalation compound hermetic type rapid expanding retort |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107138117A true CN107138117A (en) | 2017-09-08 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710375459.3A Withdrawn CN107138117A (en) | 2017-05-24 | 2017-05-24 | A kind of covalent modified graphite intercalation compound hermetic type rapid expanding retort |
Country Status (1)
| Country | Link |
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| CN (1) | CN107138117A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111483105A (en) * | 2020-04-23 | 2020-08-04 | 合肥荣丰包装制品有限公司 | EPS foam material forming device and process |
| CN113083199A (en) * | 2021-04-25 | 2021-07-09 | 江西禾益化工股份有限公司 | Energy-concerving and environment-protective formula production iprodione's device |
| CN114432992A (en) * | 2022-01-19 | 2022-05-06 | 深圳市鸿盛天诚电子有限公司 | High-efficient new forms of energy lithium battery material preparation facilities |
-
2017
- 2017-05-24 CN CN201710375459.3A patent/CN107138117A/en not_active Withdrawn
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111483105A (en) * | 2020-04-23 | 2020-08-04 | 合肥荣丰包装制品有限公司 | EPS foam material forming device and process |
| CN111483105B (en) * | 2020-04-23 | 2021-09-24 | 合肥荣丰包装制品有限公司 | EPS foam material forming device and process |
| CN113083199A (en) * | 2021-04-25 | 2021-07-09 | 江西禾益化工股份有限公司 | Energy-concerving and environment-protective formula production iprodione's device |
| CN113083199B (en) * | 2021-04-25 | 2022-08-02 | 江西禾益化工股份有限公司 | Energy-concerving and environment-protective formula production iprodione's device |
| CN114432992A (en) * | 2022-01-19 | 2022-05-06 | 深圳市鸿盛天诚电子有限公司 | High-efficient new forms of energy lithium battery material preparation facilities |
| CN114432992B (en) * | 2022-01-19 | 2023-11-03 | 常州厚德再生资源科技有限公司 | High-efficient new forms of energy lithium battery material preparation facilities |
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Application publication date: 20170908 |
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