CN107117926A - A kind of multifunctional fire-proof door panel and preparation method thereof - Google Patents
A kind of multifunctional fire-proof door panel and preparation method thereof Download PDFInfo
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- CN107117926A CN107117926A CN201710448372.4A CN201710448372A CN107117926A CN 107117926 A CN107117926 A CN 107117926A CN 201710448372 A CN201710448372 A CN 201710448372A CN 107117926 A CN107117926 A CN 107117926A
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
- C04B28/24—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing alkyl, ammonium or metal silicates; containing silica sols
- C04B28/26—Silicates of the alkali metals
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/20—Resistance against chemical, physical or biological attack
- C04B2111/28—Fire resistance, i.e. materials resistant to accidental fires or high temperatures
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Ceramic Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Materials Engineering (AREA)
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Abstract
The invention discloses a kind of multifunctional fire-proof door panel, belong to fire resistant doorsets technical field, include the raw material of following parts by weight：40 50 parts of magnesia, 12 parts of kyanite, 30 40 parts of perlite, 36 parts of carbon fiber, 47 parts of glass fibre, 17 22 parts of flake asbestos, 25 parts of nano zirconium dioxide, 14 parts of Chinese medicine dreg, 12 parts of essence, 45 parts of foaming agent, 35 parts of binding agent；The invention also discloses a kind of preparation method of multifunctional fire-proof door panel.The present invention is prepared simply, is prepared simply, intensity is high, fire protecting performance is good, and free from extraneous odour can bring delicate fragrance to surrounding environment, be also beneficial to the health of people.
Description
Technical field
The present invention relates to fire resistant doorsets technical field, specifically, a kind of multifunctional fire-proof door panel and its preparation relate to
Method.
Background technology
By Ministry of Economic Affaris specify accredited laboratory, according to the new edition fire resistant doorsets standard GB/T of implementation from 1 day January in 2009 _
12955-2008, fire resistant doorsets fire resistance test method test passes, and obtain BSMI core hair checking login certificate and
Authorize mark the knowledgeable, referred to as fire resistant doorsets.Fire resistant doorsets defined in U.S.'s NFPA and IBC specification are that " can provide opening portion jointly
Any fire-proof door leaf of a certain degree of flameproof protection, door cheek, the combination of hardware and other accessories.”
Fire-resistant door core packing material plays main function in the refractory heat-insulating performance of fire resistant doorsets, therefore packing material is fire resistant doorsets
Engineering supervision and the key project checked and accepted.Current fire-resistant door core packing material mainly has perlite fireproof door core board and magnesite anti-
Vent core plate；Perlite fireproof door core board uses expanded perlite for primary raw material, with a certain proportion of inorganic high binder and
Chemical addition agent is mixed, and is processed because the expanded perlite of use is natural peral rock ore in sand form by a whole set of operation, is passed through
1300 DEG C of high temperature above instantaneous expansions, structure be in hollow honeycomb particle spherical, therefore the fire-resistant door core being made
Plate is that a kind of ideal product of natural green environmental protection enters factory to finished product completion from raw material, and whole manufacturing process is all by strict thin
The making and inspection of cause, then adapted fireproof gum, the steel fire-proof wooden door core plate of production through domestic many clients using and after testing
Afterwards, the fire endurance of national new standard first class fire resistant doorsets is reached.
And function only has fire prevention, heat-resisting ability in current anti-fire door core board, without other functions, cause
The market competitiveness of fire resistant doorsets is not enough, it is difficult to attract the sight of people, so needing a kind of multifunctional fire-proof door panel to solve
Above mentioned problem.
In publication number CN201410151491.X patent document, a kind of anti-fire door core board and its preparation side are disclosed
Method.Wherein, the raw material of the anti-fire door core board are counted including following components by weight：1000-1500 parts of magnesium chloride brine,
1000-1200 parts of magnesia, 1-2 parts of sodium methyl silicate, 0.1-0.2 parts of phosphoric acid, 400-600 parts of vegetalitas foaming agent water solution,
10-20 parts of polystyrene fiber, 300-500 parts of flyash；The mass ratio of magnesium chloride and water is 29- wherein in magnesium chloride brine
50∶100；The mass ratio of vegetalitas foaming agent and water is 1-10: 40 in vegetalitas foaming agent water solution.It is anti-that the invention is prepared
Vent core plate uses expanded perlite compared with the anti-fire door core board that raw material is prepared with prior art, without dirt in preparation process
Dye, no waste mine, without dust, the anti-fire door core board density prepared is high, intensity is high, and fire protecting performance is good；But the function of the invention is few,
The market competitiveness can not be effectively improved.
The content of the invention
It is an object of the invention to overcoming above-mentioned the deficiencies in the prior art there is provided a kind of multifunctional fire-proof door panel and its
Preparation method, is prepared simply, intensity is high, fire protecting performance is good, and free from extraneous odour can bring delicate fragrance to surrounding environment, be also beneficial to people
Health.
A kind of multifunctional fire-proof door panel that the present invention is provided, includes the raw material of following parts by weight：
40-50 parts of magnesia, 1-2 parts of kyanite, 30-40 parts of perlite, 3-6 parts of carbon fiber, 4-7 parts of glass fibre, flake asbestos
17-22 parts, 2-5 parts of nano zirconium dioxide, 1-4 parts of Chinese medicine dreg, 1-2 parts of essence, 4-5 parts of foaming agent, 3-5 parts of binding agent.
Preferably, the mesh number of magnesia, kyanite is 100-140 mesh, the mesh number of perlite is 80-100 mesh, flake asbestos
Mesh number be 170-200 mesh, the particle diameter of nano zirconium dioxide is 40-50nm.
Preferably, the length of carbon fiber and glass fibre is 0.5-2mm, a diameter of 0.1-0.5mm.
Preferably, Chinese medicine dreg is quassia, the fleece-flower root, radix bupleuri root, selfheal, black robe, kelp, kalimeris, dried orange peel, Du
Secondary, pseudo-ginseng, Chinese yam rhizome, one or two or more kinds of mixtures of Poria cocos.
Preferably, essence is jasmine flower essence；Binding agent is the mixture of waterglass, cement and epoxy resin, three
Between weight ratio be 3:1:2.
Preferably, foaming agent is the mixture of rosin soap foaming agent and carborundum, weight ratio between the two is 1:
2。
Present invention also offers a kind of preparation method of multifunctional fire-proof door panel, comprise the following steps：
（1）, by above-mentioned parts by weight weigh various raw materials；
（2）, Chinese medicine dreg processing：After the size-reduced machine of Chinese medicine dreg is crushed, 140-170 mesh sieves are crossed, Chinese medicines ground-slag is obtained
End；
（3）, by magnesia, kyanite, perlite, carbon fiber, glass fibre, flake asbestos, nano zirconium dioxide, Chinese medicines ground-slag
End, essence are added to stirring 5-10min in homogenizer, then add foaming agent, binding agent and a certain amount of water, stirring
Fluid mixture is obtained after 10-20min；
（4）, the fluid mixture carried out injection molding, pressurization, depanning, obtains finished product after drying steps；
（5）, packaging.
Wherein,
Step（3）The speed of high speed mixer is 500-700r/min.
A kind of multifunctional fire-proof door panel of the present invention and preparation method thereof, is prepared simply, intensity is high, fire protecting performance is good,
Free from extraneous odour, can bring delicate fragrance to surrounding environment, be also beneficial to the health of people, specifically have the beneficial effect that：
（1）, magnesia, kyanite, perlite, flake asbestos, the addition of nano zirconium dioxide can improve the resistance to of anti-fire door core board
Fire, heat-resisting ability, especially nano zirconium dioxide, good dispersion, with good thermo-chemical stability, pyroconductivity and
Higher intensity and toughness, machinery, calorifics, electricity, optical property are good, and nano zircite particle diameter is small, stability strong, with resistance to
Sour, alkaline-resisting, corrosion-resistant, resistant to elevated temperatures performance；Carbon fiber and glass fibre can also increase the heat-resisting ability of anti-fire door core board, and
And carbon fiber good corrosion resistance, electrical and thermal conductivity performance, electromagnetic wave shielding are good, glass fibre can also increase toughness and impact resistance；
（2）, after Chinese medicine dreg addition, the smell distributed is conducive to the health of people around, and the addition energy dispelling abnormal flavor of essence,
The anti-fire door core board produced can giving out fragrance, can also effectively mosquito proof using jasmine flower essence；
（3）, binding agent adoption rate be 3:1:2 waterglass, cement and epoxy resin, is effective to ensure that between each raw material and fills
Divide mixing, the generation for situations such as preventing fracture, crackle；
（4）, this preparation method it is simple, can stably produce the hybrid energy between anti-fire door core board, each raw material of correspondence ratio
Effectively ensure fire resisting, the heat-resisting ability of anti-fire door core board.
Embodiment
Invention is described in further detail below in conjunction with specific embodiment.
Embodiment 1
A kind of multifunctional fire-proof door panel of the present embodiment, includes the raw material of following parts by weight：
40 parts of magnesia, 1 part of kyanite, 30 parts of perlite, 3 parts of carbon fiber, 4 parts of glass fibre, 17 parts of flake asbestos, nano-silica
Change 2 parts of zirconium, 1 part of Chinese medicine dreg, 1 part of essence, 4 parts of foaming agent, 3 parts of binding agent.
In the present embodiment, magnesia, the mesh number of kyanite are 100 mesh, and the mesh number of perlite is 80 mesh, the mesh number of flake asbestos
For 170 mesh, the particle diameter of nano zirconium dioxide is 40nm.
In the present embodiment, the length of carbon fiber and glass fibre is 0.5mm, a diameter of 0.1mm.
In the present embodiment, Chinese medicine dreg is quassia, the fleece-flower root, radix bupleuri root, selfheal, black robe, kelp, kalimeris, dried orange peel, Du
Secondary, pseudo-ginseng, Chinese yam rhizome, the mixture of Poria cocos.
In the present embodiment, essence is jasmine flower essence；Binding agent is the mixture of waterglass, cement and epoxy resin, three
Weight ratio between person is 3:1:2.
In the present embodiment, foaming agent is the mixture of rosin soap foaming agent and carborundum, and weight ratio between the two is
1:2。
The present embodiment additionally provides a kind of preparation method of multifunctional fire-proof door panel, comprises the following steps：
（1）, by above-mentioned parts by weight weigh various raw materials；
（2）, Chinese medicine dreg processing：After the size-reduced machine of Chinese medicine dreg is crushed, 140 mesh sieves are crossed, Chinese medicine dreg powder is obtained；
（3）, by magnesia, kyanite, perlite, carbon fiber, glass fibre, flake asbestos, nano zirconium dioxide, Chinese medicines ground-slag
End, essence are added to stirring 5min in homogenizer, then add foaming agent, binding agent and a certain amount of water, stir 10min
After obtain fluid mixture；
（4）, the fluid mixture carried out injection molding, pressurization, depanning, obtains finished product after drying steps；
（5）, packaging.
Wherein,
Step（3）The speed of high speed mixer is 500r/min.
Embodiment 2
A kind of multifunctional fire-proof door panel of the present embodiment, includes the raw material of following parts by weight：
45 parts of magnesia, 1.5 parts of kyanite, 35 parts of perlite, 4.5 parts of carbon fiber, 5.5 parts of glass fibre, 19 parts of flake asbestos, receive
3 parts of zirconium dioxide of rice, 3 parts of Chinese medicine dreg, 1.5 parts of essence, 4.5 parts of foaming agent, 4 parts of binding agent.
In the present embodiment, magnesia, the mesh number of kyanite are 100-140 mesh, and the mesh number of perlite is 100 mesh, flake asbestos
Mesh number be 170 mesh, the particle diameter of nano zirconium dioxide is 50nm.
In the present embodiment, the length of carbon fiber and glass fibre is 1.5mm, a diameter of 0.3mm.
In the present embodiment, Chinese medicine dreg is quassia, the fleece-flower root, radix bupleuri root, selfheal, black robe, kelp, kalimeris, dried orange peel, Du
Secondary, pseudo-ginseng, Chinese yam rhizome, the mixture of Poria cocos.
In the present embodiment, essence is jasmine flower essence；Binding agent is the mixture of waterglass, cement and epoxy resin, three
Weight ratio between person is 3:1:2.
In the present embodiment, foaming agent is the mixture of rosin soap foaming agent and carborundum, and weight ratio between the two is
1:2。
The present embodiment additionally provides a kind of preparation method of multifunctional fire-proof door panel, comprises the following steps：
（1）, by above-mentioned parts by weight weigh various raw materials；
（2）, Chinese medicine dreg processing：After the size-reduced machine of Chinese medicine dreg is crushed, 170 mesh sieves are crossed, Chinese medicine dreg powder is obtained；
（3）, by magnesia, kyanite, perlite, carbon fiber, glass fibre, flake asbestos, nano zirconium dioxide, Chinese medicines ground-slag
End, essence are added to stirring 8min in homogenizer, then add foaming agent, binding agent and a certain amount of water, stir 15min
After obtain fluid mixture；
（4）, the fluid mixture carried out injection molding, pressurization, depanning, obtains finished product after drying steps；
（5）, packaging.
Wherein,
Step（3）The speed of high speed mixer is 600r/min.
Embodiment 3
A kind of multifunctional fire-proof door panel of the present embodiment, includes the raw material of following parts by weight：
50 parts of magnesia, 2 parts of kyanite, 40 parts of perlite, 6 parts of carbon fiber, 7 parts of glass fibre, 22 parts of flake asbestos, nano-silica
Change 5 parts of zirconium, 4 parts of Chinese medicine dreg, 2 parts of essence, 5 parts of foaming agent, 5 parts of binding agent.
In the present embodiment, magnesia, the mesh number of kyanite are 140 mesh, and the mesh number of perlite is 100 mesh, the mesh of flake asbestos
Number is 200 mesh, and the particle diameter of nano zirconium dioxide is 50nm.
In the present embodiment, the length of carbon fiber and glass fibre is 2mm, a diameter of 0.5mm.
In the present embodiment, Chinese medicine dreg is quassia, the fleece-flower root, radix bupleuri root, selfheal, black robe, kelp, kalimeris, dried orange peel, Du
Secondary, pseudo-ginseng, Chinese yam rhizome, the mixture of Poria cocos.
In the present embodiment, essence is jasmine flower essence；Binding agent is the mixture of waterglass, cement and epoxy resin, three
Weight ratio between person is 3:1:2.
In the present embodiment, foaming agent is the mixture of rosin soap foaming agent and carborundum, and weight ratio between the two is
1:2。
The present embodiment additionally provides a kind of preparation method of multifunctional fire-proof door panel, comprises the following steps：
（1）, by above-mentioned parts by weight weigh various raw materials；
（2）, Chinese medicine dreg processing：After the size-reduced machine of Chinese medicine dreg is crushed, 140-170 mesh sieves are crossed, Chinese medicines ground-slag is obtained
End；
（3）, by magnesia, kyanite, perlite, carbon fiber, glass fibre, flake asbestos, nano zirconium dioxide, Chinese medicines ground-slag
End, essence are added to stirring 10min in homogenizer, then add foaming agent, binding agent and a certain amount of water, stirring
Fluid mixture is obtained after 20min；
（4）, the fluid mixture carried out injection molding, pressurization, depanning, obtains finished product after drying steps；
（5）, packaging.
Wherein,
Step（3）The speed of high speed mixer is 700r/min.
Described above is only the preferred embodiment of the present invention, and protection scope of the present invention is not limited merely to above-mentioned implementation
Example, all technical schemes belonged under thinking of the present invention belong to protection scope of the present invention.It should be pointed out that for the art
Those of ordinary skill for, some improvements and modifications without departing from the principles of the present invention, these improvements and modifications
It should be regarded as protection scope of the present invention.
Claims (8)
1. a kind of multifunctional fire-proof door panel, it is characterised in that：Include the raw material of following parts by weight：
40-50 parts of magnesia, 1-2 parts of kyanite, 30-40 parts of perlite, 3-6 parts of carbon fiber, 4-7 parts of glass fibre, flake asbestos
17-22 parts, 2-5 parts of nano zirconium dioxide, 1-4 parts of Chinese medicine dreg, 1-2 parts of essence, 4-5 parts of foaming agent, 3-5 parts of binding agent.
2. multifunctional fire-proof door panel according to claim 1, it is characterised in that：Magnesia, the mesh number of kyanite are
100-140 mesh, the mesh number of perlite is 80-100 mesh, and the mesh number of flake asbestos is 170-200 mesh, and the particle diameter of nano zirconium dioxide is
40-50nm。
3. multifunctional fire-proof door panel according to claim 1, it is characterised in that：The length of carbon fiber and glass fibre is
0.5-2mm, a diameter of 0.1-0.5mm.
4. multifunctional fire-proof door panel according to claim 1, it is characterised in that：Chinese medicine dreg is quassia, the fleece-flower root, bavin
Hu Gen, selfheal, black robe, kelp, kalimeris, dried orange peel, the bark of eucommia, pseudo-ginseng, Chinese yam rhizome, one or two or more kinds of mixing of Poria cocos
Thing.
5. multifunctional fire-proof door panel according to claim 1, it is characterised in that：Essence is jasmine flower essence；Binding agent
For the mixture of waterglass, cement and epoxy resin, the weight ratio between three is 3:1:2.
6. multifunctional fire-proof door panel according to claim 1, it is characterised in that：Foaming agent be rosin soap foaming agent and
The mixture of carborundum, weight ratio between the two is 1:2.
7. a kind of preparation method of multifunctional fire-proof door panel according to claim 1-6 any one, it is characterised in that：
Comprise the following steps：
（1）, by above-mentioned parts by weight weigh various raw materials；
（2）, Chinese medicine dreg processing：After the size-reduced machine of Chinese medicine dreg is crushed, 140-170 mesh sieves are crossed, Chinese medicines ground-slag is obtained
End；
（3）, by magnesia, kyanite, perlite, carbon fiber, glass fibre, flake asbestos, nano zirconium dioxide, Chinese medicines ground-slag
End, essence are added to stirring 5-10min in homogenizer, then add foaming agent, binding agent and a certain amount of water, stirring
Fluid mixture is obtained after 10-20min；
（4）, the fluid mixture carried out injection molding, pressurization, depanning, obtains finished product after drying steps；
（5）, packaging.
8. the preparation method of multifunctional fire-proof door panel according to claim 7, it is characterised in that：Step（3）High speed
The speed of mixer is 500-700r/min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201710448372.4A CN107117926A (en) | 2017-06-14 | 2017-06-14 | A kind of multifunctional fire-proof door panel and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710448372.4A CN107117926A (en) | 2017-06-14 | 2017-06-14 | A kind of multifunctional fire-proof door panel and preparation method thereof |
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| Publication Number | Publication Date |
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| CN107117926A true CN107117926A (en) | 2017-09-01 |
Family
ID=59719001
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| CN201710448372.4A Withdrawn CN107117926A (en) | 2017-06-14 | 2017-06-14 | A kind of multifunctional fire-proof door panel and preparation method thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111662064A (en) * | 2020-06-09 | 2020-09-15 | 河北工程大学 | Method for preparing low-shrinkage high-performance concrete by using tailings and traditional Chinese medicine residues |
| CN112617504A (en) * | 2020-12-28 | 2021-04-09 | 浙江晶富科技有限公司 | Health-care zirconium oxide mattress and manufacturing method thereof |
| CN112851262A (en) * | 2021-02-25 | 2021-05-28 | 杭州钱神商品混凝土有限公司 | Self-compacting concrete and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101781113A (en) * | 2009-12-31 | 2010-07-21 | 李同生 | Inorganic fire-resistant foam filling material for door core board |
| CN102584115A (en) * | 2011-12-20 | 2012-07-18 | 汪洋 | Fireproof material, preparation method thereof and fireproof door |
| CN103880369A (en) * | 2014-02-10 | 2014-06-25 | 安徽众凯架业有限责任公司 | Traditional Chinese medicine residue heat preserving mortar and preparation method thereof |
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2017
- 2017-06-14 CN CN201710448372.4A patent/CN107117926A/en not_active Withdrawn
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101781113A (en) * | 2009-12-31 | 2010-07-21 | 李同生 | Inorganic fire-resistant foam filling material for door core board |
| CN102584115A (en) * | 2011-12-20 | 2012-07-18 | 汪洋 | Fireproof material, preparation method thereof and fireproof door |
| CN103880369A (en) * | 2014-02-10 | 2014-06-25 | 安徽众凯架业有限责任公司 | Traditional Chinese medicine residue heat preserving mortar and preparation method thereof |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111662064A (en) * | 2020-06-09 | 2020-09-15 | 河北工程大学 | Method for preparing low-shrinkage high-performance concrete by using tailings and traditional Chinese medicine residues |
| CN112617504A (en) * | 2020-12-28 | 2021-04-09 | 浙江晶富科技有限公司 | Health-care zirconium oxide mattress and manufacturing method thereof |
| CN112851262A (en) * | 2021-02-25 | 2021-05-28 | 杭州钱神商品混凝土有限公司 | Self-compacting concrete and preparation method thereof |
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Application publication date: 20170901 |