CN107099110A - A kind of renewable building thermal insulation material and preparation method thereof - Google Patents
A kind of renewable building thermal insulation material and preparation method thereof Download PDFInfo
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- CN107099110A CN107099110A CN201710411090.7A CN201710411090A CN107099110A CN 107099110 A CN107099110 A CN 107099110A CN 201710411090 A CN201710411090 A CN 201710411090A CN 107099110 A CN107099110 A CN 107099110A
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L33/00—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- C08L33/02—Homopolymers or copolymers of acids; Metal or ammonium salts thereof
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2217—Oxides; Hydroxides of metals of magnesium
- C08K2003/222—Magnesia, i.e. magnesium oxide
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/014—Additives containing two or more different additives of the same subgroup in C08K
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Abstract
The invention discloses a kind of renewable building thermal insulation material and preparation method thereof, insulation material component includes 10 20 parts of bentonite by weight, 5 10 parts of talcum powder, 10 18 parts of expanded perlite, 3 10 parts of centrifugal glass fibre, 28 parts of hydroxymethyl-propyl cellulose, 6 12 parts of magnesia, 6 16 parts of expanded vermiculite, 3 10 parts of negative ion powder for building, 2 10 parts of kaolin, 10 20 parts of silane coupler, 12 25 parts of 5 15 parts of active micro silicon powder and acrylic acid vinylidene chloride emulsion, preparation method of the present invention is simple, preparation process is environment friendly and pollution-free, obtained insulation material good environmental protection, with certain heat insulation effect, it is also equipped with superior resistance to compression simultaneously, impact resistance, service life is long.
Description
Technical field
The present invention relates to insulation material preparing technical field, specially a kind of renewable building thermal insulation material and its preparation side
Method.
Background technology
Modern society's energy resource consumption increasingly increases, and consumes ample resources.As people gradually recognize the limited of resource
Property the environmental crisis that causes with energy resource consumption, energy-conservation turns into environmental protection and one of the important content that economizes on resources, insulation skill
Art is widely applied in each field, but domestic heat insualting building coating in the market is present function is single, effect is limited and
The problem of term of validity is short, it is difficult to extensive use.
The content of the invention
It is an object of the invention to provide a kind of renewable building thermal insulation material and preparation method thereof, to solve above-mentioned background
The problem of being proposed in technology.
To achieve the above object, the present invention provides following technical scheme：A kind of renewable building thermal insulation material, insulation material
Component includes 10-20 parts of bentonite, 5-10 parts of talcum powder, 10-18 parts of expanded perlite, centrifugal glass fibre 3- by weight
10 parts, 2-8 parts of hydroxymethyl-propyl cellulose, 6-12 parts of magnesia, 6-16 parts of expanded vermiculite, negative ion powder 3-10 parts for building,
2-10 parts of kaolin, 10-20 parts of silane coupler, 5-15 parts of active micro silicon powder and acrylic acid-vinylidene chloride emulsion 12-25
Part.
It is preferred that, composition proportion preferably is：15 parts of bentonite, 8 parts of talcum powder, 14 parts of expanded perlite, rotary glass
7 parts of fiber, 5 parts of hydroxymethyl-propyl cellulose, 9 parts of magnesia, 11 parts of expanded vermiculite, 7 parts of negative ion powder for building, kaolin 6
Part, 15 parts of silane coupler, 10 parts of active micro silicon powder and acrylic acid -18 parts of vinylidene chloride emulsion.
It is preferred that, its preparation method comprises the following steps：
A, will bentonite, talcum powder, expanded perlite, magnesia, expanded vermiculite, kaolin mix after add grinder in grind
Mill, milling time is 20min, obtains mixture A；
B, addition centrifugal glass fibre, hydroxymethyl-propyl cellulose, negative ion powder for building, silane coupler in mixture A,
Add in stirred tank and stir after mixing, stir speed (S.S.) is 2000 revs/min, and mixing time is 20min, obtains mixture B；
C, add to add in reactor after active micro silicon powder, the mixing of acrylic acid-vinylidene chloride emulsion in mixture B and carry out low temperature
Stirring, heating-up temperature is 40 DEG C, and the heat time is 20min, is slowly cooled to room temperature afterwards, stands 5h, that is, obtains insulation material.
Compared with prior art, the beneficial effects of the invention are as follows：Preparation method of the present invention is simple, preparation process is environmentally friendly without dirt
Dye, obtained insulation material good environmental protection, with certain heat insulation effect, while being also equipped with superior resistance to compression, shock resistance energy
Power, service life is long, it is adaptable to various building fields.
Embodiment
The technical scheme in the embodiment of the present invention is clearly and completely described below, it is clear that described embodiment
Only a part of embodiment of the invention, rather than whole embodiments.Based on the embodiment in the present invention, the common skill in this area
The every other embodiment that art personnel are obtained under the premise of creative work is not made, belongs to the model that the present invention is protected
Enclose.
The present invention provides following technical scheme：A kind of renewable building thermal insulation material, insulation material component is by weight
Including 10-20 parts of bentonite, 5-10 parts of talcum powder, 10-18 parts of expanded perlite, 3-10 parts of centrifugal glass fibre, methylol third
2-8 parts of base cellulose, 6-12 parts of magnesia, 6-16 parts of expanded vermiculite, negative ion powder 3-10 parts for building, 2-10 parts of kaolin,
10-20 parts of silane coupler, 5-15 parts of active micro silicon powder and acrylic acid -12-25 parts of vinylidene chloride emulsion.
Embodiment one：
It is fine that insulation material component includes 10 parts of bentonite, 5 parts of talcum powder, 10 parts of expanded perlite, rotary glass by weight
Dimension 3 parts, 2 parts of hydroxymethyl-propyl cellulose, 6 parts of magnesia, 6 parts of expanded vermiculite, 3 parts of negative ion powder for building, 2 parts of kaolin,
10 parts of silane coupler, 5 parts of active micro silicon powder and acrylic acid -12 parts of vinylidene chloride emulsion.
The preparation method of the present embodiment comprises the following steps：
A, will bentonite, talcum powder, expanded perlite, magnesia, expanded vermiculite, kaolin mix after add grinder in grind
Mill, milling time is 20min, obtains mixture A；
B, addition centrifugal glass fibre, hydroxymethyl-propyl cellulose, negative ion powder for building, silane coupler in mixture A,
Add in stirred tank and stir after mixing, stir speed (S.S.) is 2000 revs/min, and mixing time is 20min, obtains mixture B；
C, add to add in reactor after active micro silicon powder, the mixing of acrylic acid-vinylidene chloride emulsion in mixture B and carry out low temperature
Stirring, heating-up temperature is 40 DEG C, and the heat time is 20min, is slowly cooled to room temperature afterwards, stands 5h, that is, obtains insulation material.
Embodiment two：
It is fine that insulation material component includes 20 parts of bentonite, 10 parts of talcum powder, 18 parts of expanded perlite, rotary glass by weight
10 parts of dimension, 8 parts of hydroxymethyl-propyl cellulose, 12 parts of magnesia, 16 parts of expanded vermiculite, 10 parts of negative ion powder for building, kaolin
10 parts, 20 parts of silane coupler, 15 parts of active micro silicon powder and acrylic acid -25 parts of vinylidene chloride emulsion.
The preparation method of the present embodiment comprises the following steps：
A, will bentonite, talcum powder, expanded perlite, magnesia, expanded vermiculite, kaolin mix after add grinder in grind
Mill, milling time is 20min, obtains mixture A；
B, addition centrifugal glass fibre, hydroxymethyl-propyl cellulose, negative ion powder for building, silane coupler in mixture A,
Add in stirred tank and stir after mixing, stir speed (S.S.) is 2000 revs/min, and mixing time is 20min, obtains mixture B；
C, add to add in reactor after active micro silicon powder, the mixing of acrylic acid-vinylidene chloride emulsion in mixture B and carry out low temperature
Stirring, heating-up temperature is 40 DEG C, and the heat time is 20min, is slowly cooled to room temperature afterwards, stands 5h, that is, obtains insulation material.
Embodiment three：
It is fine that insulation material component includes 12 parts of bentonite, 6 parts of talcum powder, 11 parts of expanded perlite, rotary glass by weight
Dimension 4 parts, 3 parts of hydroxymethyl-propyl cellulose, 7 parts of magnesia, 7 parts of expanded vermiculite, 4 parts of negative ion powder for building, 3 parts of kaolin,
12 parts of silane coupler, 7 parts of active micro silicon powder and acrylic acid -14 parts of vinylidene chloride emulsion.
The preparation method of the present embodiment comprises the following steps：
A, will bentonite, talcum powder, expanded perlite, magnesia, expanded vermiculite, kaolin mix after add grinder in grind
Mill, milling time is 20min, obtains mixture A；
B, addition centrifugal glass fibre, hydroxymethyl-propyl cellulose, negative ion powder for building, silane coupler in mixture A,
Add in stirred tank and stir after mixing, stir speed (S.S.) is 2000 revs/min, and mixing time is 20min, obtains mixture B；
C, add to add in reactor after active micro silicon powder, the mixing of acrylic acid-vinylidene chloride emulsion in mixture B and carry out low temperature
Stirring, heating-up temperature is 40 DEG C, and the heat time is 20min, is slowly cooled to room temperature afterwards, stands 5h, that is, obtains insulation material.
Example IV：
It is fine that insulation material component includes 18 parts of bentonite, 9 parts of talcum powder, 16 parts of expanded perlite, rotary glass by weight
9 parts of dimension, 7 parts of hydroxymethyl-propyl cellulose, 10 parts of magnesia, 14 parts of expanded vermiculite, 8 parts of negative ion powder for building, kaolin 8
Part, 16 parts of silane coupler, 13 parts of active micro silicon powder and acrylic acid -22 parts of vinylidene chloride emulsion.
The preparation method of the present embodiment comprises the following steps：
A, will bentonite, talcum powder, expanded perlite, magnesia, expanded vermiculite, kaolin mix after add grinder in grind
Mill, milling time is 20min, obtains mixture A；
B, addition centrifugal glass fibre, hydroxymethyl-propyl cellulose, negative ion powder for building, silane coupler in mixture A,
Add in stirred tank and stir after mixing, stir speed (S.S.) is 2000 revs/min, and mixing time is 20min, obtains mixture B；
C, add to add in reactor after active micro silicon powder, the mixing of acrylic acid-vinylidene chloride emulsion in mixture B and carry out low temperature
Stirring, heating-up temperature is 40 DEG C, and the heat time is 20min, is slowly cooled to room temperature afterwards, stands 5h, that is, obtains insulation material.
Embodiment five：
It is fine that insulation material component includes 15 parts of bentonite, 8 parts of talcum powder, 14 parts of expanded perlite, rotary glass by weight
Dimension 7 parts, 5 parts of hydroxymethyl-propyl cellulose, 9 parts of magnesia, 11 parts of expanded vermiculite, 7 parts of negative ion powder for building, 6 parts of kaolin,
15 parts of silane coupler, 10 parts of active micro silicon powder and acrylic acid -18 parts of vinylidene chloride emulsion.
The preparation method of the present embodiment comprises the following steps：
A, will bentonite, talcum powder, expanded perlite, magnesia, expanded vermiculite, kaolin mix after add grinder in grind
Mill, milling time is 20min, obtains mixture A；
B, addition centrifugal glass fibre, hydroxymethyl-propyl cellulose, negative ion powder for building, silane coupler in mixture A,
Add in stirred tank and stir after mixing, stir speed (S.S.) is 2000 revs/min, and mixing time is 20min, obtains mixture B；
C, add to add in reactor after active micro silicon powder, the mixing of acrylic acid-vinylidene chloride emulsion in mixture B and carry out low temperature
Stirring, heating-up temperature is 40 DEG C, and the heat time is 20min, is slowly cooled to room temperature afterwards, stands 5h, that is, obtains insulation material.
Preparation method of the present invention is simple, preparation process is environment friendly and pollution-free, obtained insulation material good environmental protection, with one
Fixed heat insulation effect, while being also equipped with superior resistance to compression, impact resistance, service life is long, it is adaptable to various building fields.
Although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
A variety of changes, modification can be carried out to these embodiments, replace without departing from the principles and spirit of the present invention by understanding
And modification, the scope of the present invention is defined by the appended.
Claims (3)
1. a kind of renewable building thermal insulation material, it is characterised in that：Insulation material component includes bentonite 10-20 by weight
Part, 5-10 parts of talcum powder, 10-18 parts of expanded perlite, 3-10 parts of centrifugal glass fibre, 2-8 parts of hydroxymethyl-propyl cellulose, oxygen
Change 6-12 parts of magnesium, 6-16 parts of expanded vermiculite, negative ion powder 3-10 parts for building, 2-10 parts of kaolin, silane coupler 10-20
Part, 5-15 parts of active micro silicon powder and acrylic acid -12-25 parts of vinylidene chloride emulsion.
2. a kind of renewable building thermal insulation material according to claim 1, it is characterised in that：It is preferred that composition proportion be：
15 parts of bentonite, 8 parts of talcum powder, 14 parts of expanded perlite, 7 parts of centrifugal glass fibre, 5 parts of hydroxymethyl-propyl cellulose, oxidation
9 parts of magnesium, 11 parts of expanded vermiculite, 7 parts of negative ion powder for building, 6 parts of kaolin, 15 parts of silane coupler, 10 parts of active micro silicon powder
And acrylic acid -18 parts of vinylidene chloride emulsion.
3. realize a kind of preparation method of renewable building thermal insulation material described in claim 1, it is characterised in that：Its preparation side
Method comprises the following steps：
A, will bentonite, talcum powder, expanded perlite, magnesia, expanded vermiculite, kaolin mix after add grinder in grind
Mill, milling time is 20min, obtains mixture A；
B, addition centrifugal glass fibre, hydroxymethyl-propyl cellulose, negative ion powder for building, silane coupler in mixture A,
Add in stirred tank and stir after mixing, stir speed (S.S.) is 2000 revs/min, and mixing time is 20min, obtains mixture B；
C, add to add in reactor after active micro silicon powder, the mixing of acrylic acid-vinylidene chloride emulsion in mixture B and carry out low temperature
Stirring, heating-up temperature is 40 DEG C, and the heat time is 20min, is slowly cooled to room temperature afterwards, stands 5h, that is, obtains insulation material.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201710411090.7A CN107099110A (en) | 2017-06-05 | 2017-06-05 | A kind of renewable building thermal insulation material and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201710411090.7A CN107099110A (en) | 2017-06-05 | 2017-06-05 | A kind of renewable building thermal insulation material and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107674248A (en) * | 2017-10-24 | 2018-02-09 | 蚌埠市莱特汽车配件有限公司 | Automobile filter shell cleaning device insulation material |
| CN107695005A (en) * | 2017-10-24 | 2018-02-16 | 蚌埠市莱特汽车配件有限公司 | Automobile filter shell cleaning device |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104072085A (en) * | 2014-07-11 | 2014-10-01 | 福建农林大学 | Method for preparing ultralight foam material by using vinyl chloride-vinylidene chloride copolymer emulsion |
| CN104876517A (en) * | 2015-05-11 | 2015-09-02 | 青岛百千川海洋生态科技有限公司 | Renewable building thermal-insulation material |
| CN106588108A (en) * | 2016-11-10 | 2017-04-26 | 南宁市大江保温材料有限公司 | Building heat preservation material |
-
2017
- 2017-06-05 CN CN201710411090.7A patent/CN107099110A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104072085A (en) * | 2014-07-11 | 2014-10-01 | 福建农林大学 | Method for preparing ultralight foam material by using vinyl chloride-vinylidene chloride copolymer emulsion |
| CN104876517A (en) * | 2015-05-11 | 2015-09-02 | 青岛百千川海洋生态科技有限公司 | Renewable building thermal-insulation material |
| CN106588108A (en) * | 2016-11-10 | 2017-04-26 | 南宁市大江保温材料有限公司 | Building heat preservation material |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107674248A (en) * | 2017-10-24 | 2018-02-09 | 蚌埠市莱特汽车配件有限公司 | Automobile filter shell cleaning device insulation material |
| CN107695005A (en) * | 2017-10-24 | 2018-02-16 | 蚌埠市莱特汽车配件有限公司 | Automobile filter shell cleaning device |
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Application publication date: 20170829 |