CN107058019A - Staged continuous distillation plant - Google Patents
Staged continuous distillation plant Download PDFInfo
- Publication number
- CN107058019A CN107058019A CN201710144087.3A CN201710144087A CN107058019A CN 107058019 A CN107058019 A CN 107058019A CN 201710144087 A CN201710144087 A CN 201710144087A CN 107058019 A CN107058019 A CN 107058019A
- Authority
- CN
- China
- Prior art keywords
- staged
- retort
- baffle plate
- distillation plant
- continuous distillation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000001944 continuous distillation Methods 0.000 title claims abstract description 16
- 239000007788 liquid Substances 0.000 claims abstract description 25
- 238000000034 method Methods 0.000 claims abstract description 15
- 238000009835 boiling Methods 0.000 claims abstract description 11
- 238000002485 combustion reaction Methods 0.000 claims description 5
- 230000035515 penetration Effects 0.000 claims 1
- 238000004821 distillation Methods 0.000 abstract description 12
- 230000001476 alcoholic effect Effects 0.000 description 18
- 239000007789 gas Substances 0.000 description 13
- 235000014101 wine Nutrition 0.000 description 13
- 238000004519 manufacturing process Methods 0.000 description 12
- 241000196324 Embryophyta Species 0.000 description 10
- 230000001105 regulatory effect Effects 0.000 description 10
- 238000010438 heat treatment Methods 0.000 description 6
- 238000007600 charging Methods 0.000 description 5
- 239000000463 material Substances 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 3
- 241000209094 Oryza Species 0.000 description 3
- 235000007164 Oryza sativa Nutrition 0.000 description 3
- 238000005265 energy consumption Methods 0.000 description 3
- 238000000855 fermentation Methods 0.000 description 3
- 230000004151 fermentation Effects 0.000 description 3
- 239000004615 ingredient Substances 0.000 description 3
- MWUXSHHQAYIFBG-UHFFFAOYSA-N nitrogen oxide Inorganic materials O=[N] MWUXSHHQAYIFBG-UHFFFAOYSA-N 0.000 description 3
- 235000009566 rice Nutrition 0.000 description 3
- 235000020097 white wine Nutrition 0.000 description 3
- 230000009286 beneficial effect Effects 0.000 description 2
- 230000005540 biological transmission Effects 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 239000003245 coal Substances 0.000 description 2
- 239000000796 flavoring agent Substances 0.000 description 2
- 235000019634 flavors Nutrition 0.000 description 2
- 239000012530 fluid Substances 0.000 description 2
- 238000000746 purification Methods 0.000 description 2
- 238000010025 steaming Methods 0.000 description 2
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 1
- 238000000998 batch distillation Methods 0.000 description 1
- 229910002091 carbon monoxide Inorganic materials 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 239000000567 combustion gas Substances 0.000 description 1
- 230000002860 competitive effect Effects 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 238000010924 continuous production Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000004134 energy conservation Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 239000003517 fume Substances 0.000 description 1
- 230000002045 lasting effect Effects 0.000 description 1
- 230000000505 pernicious effect Effects 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 235000019991 rice wine Nutrition 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000004083 survival effect Effects 0.000 description 1
- 239000002912 waste gas Substances 0.000 description 1
- 239000002918 waste heat Substances 0.000 description 1
- 239000002351 wastewater Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12H—PASTEURISATION, STERILISATION, PRESERVATION, PURIFICATION, CLARIFICATION OR AGEING OF ALCOHOLIC BEVERAGES; METHODS FOR ALTERING THE ALCOHOL CONTENT OF FERMENTED SOLUTIONS OR ALCOHOLIC BEVERAGES
- C12H6/00—Methods for increasing the alcohol content of fermented solutions or alcoholic beverages
- C12H6/02—Methods for increasing the alcohol content of fermented solutions or alcoholic beverages by distillation
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Bioinformatics & Cheminformatics (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Health & Medical Sciences (AREA)
- General Engineering & Computer Science (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Food Science & Technology (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Distillation Of Fermentation Liquor, Processing Of Alcohols, Vinegar And Beer (AREA)
Abstract
Staged continuous distillation plant of the present invention, it is related to a kind of field of clean energy resource in terms of continous way distillation technique, including staged retort, infrared gas burner, condenser, the liquid being distilled is in described staged continuous distillation plant from eminence toward lower along the overflow step by step of staged baffle plate, flowed in the way of "the" shape in retort, and flow through each retort, liquid is heated to boiling in flow process by heater, the steam of generation is condensed by each condenser and obtains corresponding distillate respectively, realize that continous way is distilled, the present invention has compact conformation, it is easy to operate, it is reliable, the advantages of high-efficiency environment friendly.
Description
Technical field
Patent of the present invention is related to continuous with clean energy resource progress continous way distillation technique field, more particularly to a kind of staged
Distilling apparatus, it is characterised in that including the staged continuous distillation plant being in series by multiple staged retorts, be distilled
Liquid described staged continuous distillation plant from eminence toward lower along staged baffle plate step by step overflow flow, with " it " word
The type of flow of shape is flowed in retort, and flows through each retort, and liquid is heated in flow process by heater
Boiling, the steam of generation is condensed by each condenser and obtains corresponding distillate respectively.
Background technology
During current liquor production, distillation technique mainly uses single retort based on batch distillation mode,
Production efficiency is relatively low, and labor strength is big, the substantial amounts of energy is consumed in whole production process, the energy consumption of still-process is accounted for
More than the 70% of liquor production total energy consumption, and still-process produces steam mainly by burning raw coal and provides the mode of heat energy to white wine
Distilled, heat energy produces larger heat loss after multiple conversion and transmission, reduce the utilization rate of the energy, burn coal
When produce substantial amounts of waste gas waste water, aggravate environmental pollution, endanger environment for human survival, the life of white liquor distilling is carried out with live (open) steam
Production mode brings substantial amounts of steam condensate (SC) to mash, greatly reduces the organic concentration of mash, is unfavorable for liquor flavor
The distillation and purification of material, comprehensive utilization of the substantial amounts of steam condensate (SC) to vinasse cause bigger difficulty, how to reduce white wine
The energy resource consumption of Spirit production, improves the big problem that distillation efficiency has become liquor industry, improves distillation technique, application
Clean energy resource is distilled, energy-saving and emission-reduction, is to reduce the effective way of liquor production energy consumption, straight using infrared gas burner
The staged continuous distillation plant distilled spirit of mode of heating is connect, energy conversion and heat energy transmission link, reduction production energy is reduced
Consumption, improves production efficiency, overcomes the problem of producing a large amount of steam condensate (SC)s in still-process, and height is carried out to the flavor substance of white wine
The distillation and purification of effect, Improving The Quality of Products reduce the moisture of vinasse, are more beneficial for the comprehensive utilization of vinasse, reduction life
Cost is produced, competitive power of product is lifted.
The content of the invention
Patent of the present invention is to directly heat the staged continuous distillation plant of mode white using infrared gas burner
Application in terms of wine distillation technique, its principle is：The liquor fermentation mash being distilled is in described staged continuous distillation plant
From eminence toward lower along staged baffle plate overflow and the flow down step by step in the way of "the" shape step by step, each distillation is flowed through
Keep seething with excitement by heater heating in rice steamer, flow process of the fermentation liquid in each retort, the alcohol in fermentation liquid
Composition volatilization turns into steam, and the steam of generation is condensed by each condenser and obtains corresponding distilled spirit respectively.
The beneficial effects of the invention are as follows, the staged continuous distillation plant, compact conformation is easy to operate, reliable,
It is energy-efficient, realize that continous way is distilled, improve production automation degree, reduce labor strength, improving production efficiency can root
Various concentrations, differently flavoured Liquor Products are directly distilled out according to different product specification requirements, different consumer demands are met,
Still-process directly heats mode with infrared gas burner, and infrared gas burner belongs to full premixed combustion heating
The surface combustion of burner is close in mode, combustion gas, is non flame combustion mode, and burning area is big, burns more abundant, uniform, with
The mode of heat radiation is conducted heat, and waste heat discharge is few, and energy-saving efficiency reaches more than 30% compared with other mode of heatings, and fume emission is few,
The discharge capacity of the pernicious gases such as carbon monoxide, nitrogen oxides is very low, present apparatus compact conformation, easy to operate, reliable, energy-conservation
Environmental protection.
Brief description of the drawings：
The present invention is further described with reference to the accompanying drawings and examples.
Fig. 1 is the schematic diagram of staged continuous distillation plant of the present invention.
Fig. 2 is the partial top view of staged continuous distillation plant of the present invention.
In figure：
1st, Gas Pipe 2, gas control valve 3, infrared gas burner 4, charging regulating valve
5th, mash basin 6, staged baffle plate 7, retort 8, a condenser
9th, temperature controller 10, pod apertures 11, No. two retorts 12, No. three retorts
13rd, No. four retorts 14, feed pipe 15, No. five retorts 16, No. six retorts
17th, fluid level controller 18, the poor regulating valve 19 of row, overfall
Embodiment：
In Fig. 1, using alcoholic strength as 13%（v/v）Rice wine fermenting mash exemplified by, the mash of mash basin 5 is through feeding regulating valve 4
The first order ladder entered into staged continuous distillation plant, mash in a retort 7, is filled after first order ladder along rank
The overfall 19 on the top of ladder type baffle plate 6 flows into next stage ladder, so down to the overflow material feeding step by step of every grade of ladder, until one
Minimum step is filled after material in number retort 7, and mash passes through overfall, and mash passes through the pod apertures 10 at retort bottom, led
The first order ladder that discharge orifice 10 enters in No. two retorts 11 less than liquid level and in fluid-tight state, mash, along ladder after filling
The overfall on formula baffle plate top flows into next stage ladder, and mash is so down noted step by step along the mode of staged baffle plate overflow step by step
Material, until all ladders of each retort are filled into mash, now closes charging regulating valve 4, the poor regulating valve 18 of row, which is in, closes
Closed state, opens the infrared gas burner 3 of each retort bottom, and mash comes to life when being heated to 91.1 DEG C, production
Raw alcohol steam, alcohol steam obtains wine liquid in the condensation of condenser 8, and condenser 8 is preheated to mash, and condenser 8 starts stream
The alcoholic strength for going out wine liquid is 65%（v/v）, with the lasting progress of still-process, the alcoholic strength of distillate is gradually reduced, when distillating
The alcoholic strength of liquid is 50%（v/v）When, mash temperature is stepped up to 92.6 DEG C, is now opened charging regulating valve 4 and is fed, and root
Inlet amount is adjusted according to mash temperature variations, allows mash to flow downward into each ladder and be burnt by infrared gas combustion step by step
Device heating keeps fluidized state, and mash is distilled step by step by each retort, by the alcoholic ingredient of the mash of ebuillition of heated
Progressively it is distilled off, when mash reaches the lees outlet of afterbody retort, the alcoholic ingredient of mash is distilled substantially
Finish, vinasse spirituosity composition is 0.2%（v/v）Hereinafter, when the liquid level rise of lees outlet, by the row of control of fluid level controller 17
Poor regulating valve 18, the poor regulating valve 18 of the row of unlatching, discharges vinasse, allows vinasse liquid level to keep stable state, and lees outlet is accordingly in liquid
Envelope state.
In still-process, by carrying out effective control to gas control valve 2, charging regulating valve 4, the poor regulating valve 18 of row
System, mash keeps dynamic balance state, each retort institute from charging, heating, distillation to the continuous process of distillation that vinasse are discharged
The alcoholic strength of the wine liquid distilled out and other fraction contents are also maintained at certain scope, and the wine that retort at different levels is distilled out
The alcoholic strength of liquid and other fraction contents are also different, and alcoholic strength therein is in downward trend step by step, corresponding steamings at different levels
The mash boiling temperature evaporated in rice steamer is also different, in the trend stepped up.
In Fig. 1, a retort 7 distills out wine liquid alcoholic strength for 51-65%（v/v）, mash boiling point is 91.1-92.6
℃；No. two retorts 11 distill out wine liquid alcoholic strength for 41-50%（v/v）, mash boiling point is 92.7-94.1 DEG C；No. three retorts
12 distill out wine liquid alcoholic strength for 31-40%（v/v）, mash boiling point is 94.2-95.6 DEG C；No. four retorts 13 distill out wine liquid
Alcoholic strength is 21-30%（v/v）, mash boiling point is 95.7-97.1 DEG C；No. five retorts 15 distill out wine liquid alcoholic strength for 11-
20%（v/v）, mash boiling point is 97.2-98.6 DEG C；No. six retorts 16 distill out wine liquid alcoholic strength for 3-10%（v/v）, mash
Boiling point is 98.7-100 DEG C, and each retort sets temperature controller 9 respectively, according to the temperature variations of mash in rice steamer to red
The gas control valve 2 of outside line gas burner 3 is adjusted, and allows the boiling temperature of mash to reach predetermined requirement, distillation is obtained
Alcoholic strength meet predetermined index request, finally the alcoholic ingredient continuous still in mash is finished, to fourth, fifth, No. six
Retort distills out the relatively low wine liquid of alcoholic strength, can according to the design requirement of end product quality, used as collocation with wine or
It is used as the multiple steaming processing that flows back.
Claims (5)
1. a kind of staged continuous distillation plant, including staged retort, heater, condenser, it is characterised in that：The rank
Ladder type retort bottom sets staged baffle plate, and adjacent staged retort is connected with the pod apertures of bottom, is distilled
Liquid flows toward underflow stream step by step in described staged retort along staged baffle plate, the penetration by liquid staged being distilled
The pod apertures of retort bottom enter quilt in the staged retort of next stage, flow process of the liquid in staged retort
Heater is heated to boiling, and the steam of generation is condensed by the condenser and obtains corresponding distillate.
2. staged continuous distillation plant according to claim 1, it is characterised in that：The staged baffle plate top is set
Overfall.
3. staged baffle plate according to claim 1, it is characterised in that：Staggered with longitudinal direction on the staged baffle plate top
Mode sets overfall.
4. ladder type continuous distillation plant according to claim 1, it is characterised in that：The heater sets combustion type to heat
Device.
5. gas fired heater according to claim 4, it is characterised in that：The gas fired heater sets infrared ray to fire
Air burner.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710144087.3A CN107058019A (en) | 2017-03-13 | 2017-03-13 | Staged continuous distillation plant |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710144087.3A CN107058019A (en) | 2017-03-13 | 2017-03-13 | Staged continuous distillation plant |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107058019A true CN107058019A (en) | 2017-08-18 |
Family
ID=59621689
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710144087.3A Pending CN107058019A (en) | 2017-03-13 | 2017-03-13 | Staged continuous distillation plant |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107058019A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN117165781A (en) * | 2023-11-01 | 2023-12-05 | 南通市海门常乐粉末冶金厂 | Distillation furnace for treating zinc hydrometallurgy leaching residues |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2091858U (en) * | 1990-06-19 | 1992-01-01 | 中国科学院广州能源研究所 | Enamel solar still with inclined steps |
| JP2005160329A (en) * | 2003-11-28 | 2005-06-23 | Nippon Shuzo Kumiai Chiyuuoukai | Method for multi-stage distillation of shochu and apparatus therefor |
| CN1745867A (en) * | 2005-08-17 | 2006-03-15 | 郑顺清 | Multi-stage distillation equipment |
| CN202961927U (en) * | 2012-12-05 | 2013-06-05 | 向明强 | Continuous type modularized distiller |
| CN103589620A (en) * | 2013-11-11 | 2014-02-19 | 河南景源果业有限责任公司 | Triple-effect wine distilling process |
| CN205133573U (en) * | 2015-11-30 | 2016-04-06 | 杨立志 | Continuous type white spirit distilling machinery |
-
2017
- 2017-03-13 CN CN201710144087.3A patent/CN107058019A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2091858U (en) * | 1990-06-19 | 1992-01-01 | 中国科学院广州能源研究所 | Enamel solar still with inclined steps |
| JP2005160329A (en) * | 2003-11-28 | 2005-06-23 | Nippon Shuzo Kumiai Chiyuuoukai | Method for multi-stage distillation of shochu and apparatus therefor |
| CN1745867A (en) * | 2005-08-17 | 2006-03-15 | 郑顺清 | Multi-stage distillation equipment |
| CN202961927U (en) * | 2012-12-05 | 2013-06-05 | 向明强 | Continuous type modularized distiller |
| CN103589620A (en) * | 2013-11-11 | 2014-02-19 | 河南景源果业有限责任公司 | Triple-effect wine distilling process |
| CN205133573U (en) * | 2015-11-30 | 2016-04-06 | 杨立志 | Continuous type white spirit distilling machinery |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN117165781A (en) * | 2023-11-01 | 2023-12-05 | 南通市海门常乐粉末冶金厂 | Distillation furnace for treating zinc hydrometallurgy leaching residues |
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| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20170818 |
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| WD01 | Invention patent application deemed withdrawn after publication |