CN107057174A - A kind of preparation method of the elastic plastic-wood composite floor capstock with vermins-proof effect - Google Patents

A kind of preparation method of the elastic plastic-wood composite floor capstock with vermins-proof effect Download PDF

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Publication number
CN107057174A
CN107057174A CN201710248965.6A CN201710248965A CN107057174A CN 107057174 A CN107057174 A CN 107057174A CN 201710248965 A CN201710248965 A CN 201710248965A CN 107057174 A CN107057174 A CN 107057174A
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capstock
preparation
vermins
composite floor
elastic plastic
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CN201710248965.6A
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Inventor
王同文
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Zhejiang Motomori State Wood Polytron Technologies Inc
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Zhejiang Motomori State Wood Polytron Technologies Inc
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Priority to CN201710248965.6A priority Critical patent/CN107057174A/en
Publication of CN107057174A publication Critical patent/CN107057174A/en
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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L23/00—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers
    • C08L23/02—Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers not modified by chemical after-treatment
    • C08L23/04—Homopolymers or copolymers of ethene
    • C08L23/08—Copolymers of ethene
    • C08L23/0807—Copolymers of ethene with unsaturated hydrocarbons only containing more than three carbon atoms
    • C08L23/0815—Copolymers of ethene with aliphatic 1-olefins
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08—Magnoliopsida [dicotyledons]
    • A01N65/20—Fabaceae or Leguminosae [Pea or Legume family], e.g. pea, lentil, soybean, clover, acacia, honey locust, derris or millettia
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/40—Liliopsida [monocotyledons]
    • E—FIXED CONSTRUCTIONS
    • E04—BUILDING
    • E04F—FINISHING WORK ON BUILDINGS, e.g. STAIRS, FLOORS
    • E04F15/00—Flooring
    • E04F15/02—Flooring or floor layers composed of a number of similar elements
    • E04F15/10—Flooring or floor layers composed of a number of similar elements of other materials, e.g. fibrous or chipped materials, organic plastics, magnesite tiles, hardboard, or with a top layer of other materials
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2201/00—Properties
    • C08L2201/08—Stabilised against heat, light or radiation or oxydation
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00—Polymer mixtures characterised by other features
    • C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00—Polymer mixtures characterised by other features
    • C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
    • C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2207/00—Properties characterising the ingredient of the composition
    • C08L2207/06—Properties of polyethylene
    • C08L2207/062—HDPE

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  • Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Dentistry (AREA)
  • Wood Science & Technology (AREA)
  • Agronomy & Crop Science (AREA)
  • Biotechnology (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Plant Pathology (AREA)
  • Architecture (AREA)
  • Environmental Sciences (AREA)
  • Zoology (AREA)
  • Chemical & Material Sciences (AREA)
  • Structural Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Civil Engineering (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Catching Or Destruction (AREA)

Abstract

The invention provides a kind of preparation method of the elastic plastic-wood composite floor capstock with vermins-proof effect, the main component of the capstock is：TPE, wood powder, maleic anhydride grafted polyethylene, lubricant, antioxidant, ultra-violet absorber, natural plants are modified pest repellant and HDPE, and the capstock cementability is strong, are difficult delamination, wear-resisting, corrosion-resistant, anti-skidding, expelling parasite, uvioresistant, anti-aging；Surface can sanding, embossing, polishing, wire drawing etc.；After shaping, imitation wood, imitative stone and other effects can be made, also with preferable elasticity；The present invention selects cattail wool as the main component of pest repellant, not only with extraordinary anthelminthic effect, and the also pure and fresh effect calmed the nerves.

Description

A kind of preparation method of the elastic plastic-wood composite floor capstock with vermins-proof effect
Technical field
The present invention relates to Wood-plastic floor technical field, it particularly relates to which a kind of elasticity modeling wood with vermins-proof effect is multiple Close the preparation method of floor layered material.
Background technology
Wood plastic composite（Wood~polymer Composites, abridge WPC）, be using wood-fibred or string as Key component, a kind of new material for being allowed to be combined into theRMOPLASTIC RESINS or other materials by pretreatment.It is this Material can give full play to the advantage of each component in material, overcome the shortcoming of homogenous material, can not only improve the physics of material Mechanical property and processing characteristics, reduce cost and expand application, also improve the added value of material.Because product is in crystallization State（Wood-fibred or string）And disordered state（Resin）Multiphase state, make it that both there is the high-strength of wood-fibred or string Degree, high resiliency, the high tenacity with polymeric matrix, and excellent in cushion effect, thermal expansion and water imbibition compare timber Small, good stability of the dimension, it is wear-resisting, resistant to chemical etching, be not afraid of damage by worms, non-flammable, the dual processing characteristics for having timber and plastics concurrently. It can be by moulding process such as such as hot-forming, injection molding, extrusion moldings, and the product of wood plastic composite is made, i.e., Wood-plastic composite section bar.
The chrysanthemum esters insect-proof agent of chemical synthesis being used the insect-prevention method of traditional indoor furniture, although the insect-proof agent effect more It is good, but in some specific occasions, such as hotel, due to security consideration, window opening is smaller, room ventilation effect is very Difference, these chemical compositions can be remained largely causes certain harm to human body indoors, therefore being necessary that research is a kind of has insect prevention The composite floor board capstock of effect.
The content of the invention
In view of this, it is an object of the invention to provide a kind of elastic plastic-wood composite floor capstock with vermins-proof effect Preparation method.
A kind of preparation method of the elastic plastic-wood composite floor capstock with vermins-proof effect, is carried out as steps described below：
A, each raw material put into high-speed mixer and be mixed, temperature is 80~120 DEG C, and incorporation time is 10~15min, mixed Conjunction rotating speed is 1000~1200rpm；
B, the 3rd step, mixed material is granulated through special comminutor；Temperature is 160~180 DEG C, and screw speed is 150~300rpm；
C, using extruder by the material extrusion molding after granulation, you can, extrusion temperature is 160~180 DEG C.
It is preferred that, the raw material in described step A includes the composition of following percentage by weight：
TPE（Elastic polyethylene）30~40%
Wood powder 8~12%
Maleic anhydride grafted polyethylene 1.5~2.5%
Lubricant 0.8~1.5%
Antioxidant 0.3~0.6%
Ultra-violet absorber 0.3~0.6%
Natural plants are modified pest repellant 1~2%
HDPE（High density polyethylene (HDPE)）Surplus.
It is further preferred that the raw material in described step A, includes the composition of following percentage by weight：
TPE 36%
Wood powder 10%
Maleic anhydride grafted polyethylene 2%
Lubricant 1%
Antioxidant 0.5%
Ultra-violet absorber 0.5%
Natural plants are modified pest repellant 1.5%
HDPE surpluses.
It is preferred that, the particle diameter of described wood powder is 100 mesh.
It is preferred that, the main component that described natural plants are modified pest repellant is cattail wool and expanded vermiculite powder.
It is preferred that, described natural plants are modified the preparation method of pest repellant, comprise the following steps：
Inflorescence on a, clip cattail, takes the cattail wool on inflorescence；
B, cattail wool soaked after 2~3h in clear water, carry out 5~8h of subzero less than 20 DEG C freezings, and placed it in container and rise 2.5~3MPa is depressed into, is kept after 10~15min, rapid release pressure is crushed to normal pressure in 0.3~0.5s；
C, 30~40min of immersion is put into cassia seed extract solution, with expanded vermiculite powder co-ground, mistake repeatedly after spray drying 325 mesh sieves, you can.
It is preferred that, the elastic plastic-wood composite floor capstock with vermins-proof effect of the invention is applied to behind floor and floor heating Equipment is used in conjunction with, better.
Cattail wool alias：Water candle, Calceolaria, wild candle, raupo, hair wax（Shaanxi call）Deng the Gu at the western side of Shandong Weishan Lake Abundant ground.Abounded with lake among the vegetation such as various reeds, the stem or leaf of cattail, wetland shallow water.2 month weather gradually warm up surface, start life It is long, just it is cattail pollen, through being grown to the cattail's spike eight, September, its tiny fine hair is fluffy such as cotton, the cattail's spike parched after the autumn cattail's spike is completely dry Without when must not can touch, even a little scratching, the cattail's spike has been reformed into " Magic wand ", the Pu of a piece consolidation of moment Rod has just popped into a glob of cattail wool, whiffet, and that cattail wool just floats in the air, grab all grab less than.In every late autumn, work as breeze Cross, local tiny fine hair is danced in the air over the sky, as a kind of landscape, make it is many come this poet, singer be all reluctant to leave lyric, Zhong Duoyou People sees all cannot forget for a long time after this scape.
Current cattail wool is applied to pillow and core mostly as filler, compared with silk and eider down, cattail wool is light and short, It is strongly small, it is traditional pillow inserts.Many people both know about《Book on Chinese herbal medicine》In for cattail wool record some benefits, say its pacify God is relieving convulsion, and clearing heat and cooling blood effect is good, most suitable to old man for children.
Beneficial effects of the present invention：
The present invention selects cattail wool as the main component of pest repellant, not only with extraordinary anthelminthic effect, and also pure and fresh The effect calmed the nerves；Using cryogenic freezing and boost it is modified by the way of the internal structure of cattail wool fiber can be modified, and have Beneficial to the volatilization of expelling parasite active ingredient, so as to further improve its anthelminthic effect；Simultaneously by being expanded to fibrous inside, have It is to allow cattail wool with expanded vermiculite powder co-ground so as to improve anthelminthic effect beneficial to the immersion of follow-up cassia seed extract solution Fiber is penetrated into inside the interlayer structure of vermiculite, so as to reach certain slow release effect, improves the duration of anthelminthic effect.
Elastic plastic-wood composite floor capstock provided by the present invention with vermins-proof effect, main component is：TPE, wood Powder, maleic anhydride grafted polyethylene, lubricant, antioxidant, ultra-violet absorber, natural plants are modified pest repellant and HDPE, The capstock cementability is strong, is difficult delamination, wear-resisting, corrosion-resistant, anti-skidding, expelling parasite, uvioresistant, anti-aging；Surface can sanding, pressure Flower, polishing, wire drawing etc.；After shaping, imitation wood, imitative stone and other effects can be made, also with preferable elasticity.
Embodiment
Embodiment 1
A kind of preparation method of the elastic plastic-wood composite floor capstock with vermins-proof effect, is carried out as steps described below：
A, will each raw material put into high-speed mixer in be mixed, temperature be 100 DEG C, incorporation time is 12min, mix rotating speed be 1120rpm；
B, the 3rd step, mixed material is granulated through special comminutor；Temperature is 175 DEG C, and screw speed is 220rpm；
C, using extruder by the material extrusion molding after granulation, you can, extrusion temperature is 170 DEG C.
Raw material in described step A, includes the composition of following percentage by weight：
TPE 36%
Wood powder 10%
Maleic anhydride grafted polyethylene 2%
Lubricant 1%
Antioxidant 0.5%
Ultra-violet absorber 0.5%
Natural plants are modified pest repellant 1.5%
HDPE surpluses.
The particle diameter of described wood powder is 100 mesh.
The main component that described natural plants are modified pest repellant is cattail wool and expanded vermiculite powder.
Described natural plants are modified the preparation method of pest repellant, comprise the following steps：
Inflorescence on a, clip cattail, takes the cattail wool on inflorescence；
B, cattail wool soaked after 2.5h in clear water, carry out subzero 22 DEG C of freezings 7h, and placed it in container and boost to 2.8MPa, keeps after 13min, and 0.4s discharges rapidly pressure to normal pressure, crushes；
C, it is put into cassia seed extract solution and soaks 35min, with expanded vermiculite powder co-ground repeatedly after spray drying, crosses 325 mesh Sieve, you can.
Embodiment 2
A kind of preparation method of the elastic plastic-wood composite floor capstock with vermins-proof effect, is carried out as steps described below：
A, will each raw material put into high-speed mixer in be mixed, temperature be 80 DEG C, incorporation time is 15min, mix rotating speed be 1000rpm；
B, the 3rd step, mixed material is granulated through special comminutor；Temperature is 180 DEG C, and screw speed is 150rpm；
C, using extruder by the material extrusion molding after granulation, you can, extrusion temperature is 180 DEG C.
Raw material in described step A, includes the composition of following percentage by weight：
TPE（Elastic polyethylene） 30%
Wood powder 12%
Maleic anhydride grafted polyethylene 1.5%
Lubricant 1.5%
Antioxidant 0.3%
Ultra-violet absorber 0.6%
Natural plants are modified pest repellant 1%
HDPE（High density polyethylene (HDPE)）Surplus.
The particle diameter of described wood powder is 100 mesh.
The main component that described natural plants are modified pest repellant is cattail wool and expanded vermiculite powder.
Described natural plants are modified the preparation method of pest repellant, comprise the following steps：
Inflorescence on a, clip cattail, takes the cattail wool on inflorescence；
B, cattail wool soaked after 2h in clear water, carry out subzero less than 28 DEG C and freeze 8h, and placed it in container and boost to 2.5MPa, keeps after 15min, and 0.3s discharges rapidly pressure to normal pressure, crushes；
C, it is put into cassia seed extract solution and soaks 40min, with expanded vermiculite powder co-ground repeatedly after spray drying, crosses 325 mesh Sieve, you can.
Embodiment 3
A kind of preparation method of the elastic plastic-wood composite floor capstock with vermins-proof effect, is carried out as steps described below：
A, will each raw material put into high-speed mixer in be mixed, temperature be 120 DEG C, incorporation time is 10min, mix rotating speed be 1200rpm；
B, the 3rd step, mixed material is granulated through special comminutor；Temperature is 160 DEG C, and screw speed is 300rpm；
C, using extruder by the material extrusion molding after granulation, you can, extrusion temperature is 160 DEG C.
Raw material in described step A, includes the composition of following percentage by weight：
TPE（Elastic polyethylene） 40%
Wood powder 8%
Maleic anhydride grafted polyethylene 2.5%
Lubricant 0.8%
Antioxidant 0.6%
Ultra-violet absorber 0.3%
Natural plants are modified pest repellant 2%
HDPE（High density polyethylene (HDPE)）Surplus.
The particle diameter of described wood powder is 100 mesh.
The main component that described natural plants are modified pest repellant is cattail wool and expanded vermiculite powder.
Described natural plants are modified the preparation method of pest repellant, comprise the following steps：
Inflorescence on a, clip cattail, takes the cattail wool on inflorescence；
B, cattail wool soaked after 3h in clear water, carries out subzero 20.5 DEG C of freezings 8h, and placed it in 3MPa is boosted in container, Keep after 10min, 0.5s discharges rapidly pressure to normal pressure, crushes；
C, it is put into cassia seed extract solution and soaks 30min, with expanded vermiculite powder co-ground repeatedly after spray drying, crosses 325 mesh Sieve, you can.
After tested, the elastic plastic-wood composite floor capstock with vermins-proof effect of preparation of the invention is applied to floor Afterwards, there is the anthelminthic effect of more than 5 years to termite, fly, mosquito etc..
The foregoing is only a preferred embodiment of the present invention, but protection scope of the present invention be not limited thereto, Any one skilled in the art the invention discloses technical scope in, technique according to the invention scheme and its Inventive concept is subject to equivalent substitution or change, should all be included within the scope of the present invention.

Claims (6)

1. a kind of preparation method of the elastic plastic-wood composite floor capstock with vermins-proof effect, it is characterised in that according to following Step is carried out：
A, each raw material put into high-speed mixer and be mixed, temperature is 80~120 DEG C, and incorporation time is 10~15min, mixed Conjunction rotating speed is 1000~1200rpm；
B, the 3rd step, mixed material is granulated through special comminutor；Temperature is 160~180 DEG C, and screw speed is 150~300rpm；
C, using extruder by the material extrusion molding after granulation, you can, extrusion temperature is 160~180 DEG C.
2. there is the preparation method of the elastic plastic-wood composite floor capstock of vermins-proof effect, its feature as claimed in claim 1 It is that the raw material in described step A includes the composition of following percentage by weight：
TPE 30~40%
Wood powder 8~12%
Maleic anhydride grafted polyethylene 1.5~2.5%
Lubricant 0.8~1.5%
Antioxidant 0.3~0.6%
Ultra-violet absorber 0.3~0.6%
Natural plants are modified pest repellant 1~2%
HDPE surpluses.
3. there is the preparation method of the elastic plastic-wood composite floor capstock of vermins-proof effect, its feature as claimed in claim 2 It is that the raw material in described step A includes the composition of following percentage by weight：
TPE 36%
Wood powder 10%
Maleic anhydride grafted polyethylene 2%
Lubricant 1%
Antioxidant 0.5%
Ultra-violet absorber 0.5%
Natural plants are modified pest repellant 1.5%
HDPE surpluses.
4. there is the preparation method of the elastic plastic-wood composite floor capstock of vermins-proof effect, its feature as claimed in claim 2 It is, the particle diameter of described wood powder is 100 mesh.
5. there is the preparation method of the elastic plastic-wood composite floor capstock of vermins-proof effect, its feature as claimed in claim 2 It is, the main component that described natural plants are modified pest repellant is cattail wool and expanded vermiculite powder.
6. there is the preparation method of the elastic plastic-wood composite floor capstock of vermins-proof effect, its feature as claimed in claim 2 It is, described natural plants are modified the preparation method of pest repellant, comprise the following steps：
Inflorescence on a, clip cattail, takes the cattail wool on inflorescence；
B, cattail wool soaked after 2~3h in clear water, carry out 5~8h of subzero less than 20 DEG C freezings, and placed it in container and rise 2.5~3MPa is depressed into, is kept after 10~15min, rapid release pressure is crushed to normal pressure in 0.3~0.5s；
C, 30~40min of immersion is put into cassia seed extract solution, with expanded vermiculite powder co-ground, mistake repeatedly after spray drying 325 mesh sieves, you can.
CN201710248965.6A 2017-04-17 2017-04-17 A kind of preparation method of the elastic plastic-wood composite floor capstock with vermins-proof effect Pending CN107057174A (en)

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CN109057231A (en) * 2018-07-03 2018-12-21 合肥华盖光伏科技有限公司 A kind of preparation method of environmental protection abrasive floor
CN111961351A (en) * 2020-09-02 2020-11-20 湖州南浔超盛金属制品有限公司 Preparation method of elastic wood-plastic sectional material for decoration
CN113981669A (en) * 2021-11-02 2022-01-28 安徽农业大学 Cattail wool material, cattail wool foam material, application of cattail wool foam material and pillow

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109057231A (en) * 2018-07-03 2018-12-21 合肥华盖光伏科技有限公司 A kind of preparation method of environmental protection abrasive floor
CN111961351A (en) * 2020-09-02 2020-11-20 湖州南浔超盛金属制品有限公司 Preparation method of elastic wood-plastic sectional material for decoration
CN113981669A (en) * 2021-11-02 2022-01-28 安徽农业大学 Cattail wool material, cattail wool foam material, application of cattail wool foam material and pillow

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