CN107049915A - A kind of snake gall jessamine and its ageing - Google Patents
A kind of snake gall jessamine and its ageing Download PDFInfo
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- CN107049915A CN107049915A CN201710168542.3A CN201710168542A CN107049915A CN 107049915 A CN107049915 A CN 107049915A CN 201710168542 A CN201710168542 A CN 201710168542A CN 107049915 A CN107049915 A CN 107049915A
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- perfume
- snake gall
- absolute ethyl
- ethyl alcohol
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/342—Alcohols having more than seven atoms in an unbroken chain
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q13/00—Formulations or additives for perfume preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
Abstract
A kind of snake gall jessamine and its ageing, rose 8~12, Lavender 8~12, fresh jasmine 6~10, geraniol 18~22, Oleum Ligni Santali 10~14, linalool 16~20, propane diols 48~52, snake gall leaching liquor 48~52, citric acid 10000~14000, hydroxycitronellal 8~12, absolute ethyl alcohol 500~700.First, the preparation of snake gall leaching liquor；2nd, the preparation of the basic essential oil of perfume；3rd, perfume is aged；10 parts of the essential oil in perfume basis is settled to 50 with absolute ethyl alcohol, 100~140min of heating water bath in 30 DEG C~70 DEG C water-baths, it is cooled to room temperature, then 70~74h is placed in subzero 4~6 DEG C, taking-up allows its clear-cutting forestland to normal temperature, 46~50h is stood, places 28~32 days and produces at normal temperatures after sealing.Its advantage is the micro- Huang of perfume color and luster after ageing, and transparency is good；Head perfume has dense autumn breath, is not pungent, influential；The plump perfection of body note, bottom note continues for a long time, of puzzling aftertaste.The perfume fungistatic effect drawn after ageing is good.
Description
Technical field
The present invention relates to the material obtained containing animal, it is related to the cosmetics from animal or similar dressing is prepared
Product, espespecially a kind of snake gall jessamine and its ageing.
Background technology
With the development of society, people increasingly increase the demand of perfume, medicinal or other property with research perfume are paid close attention to
Can, the multiple fragrance that exploitation embodies different levels is the direction of perfume development.Snake industry is supported just in vigorous growth in current Yongzhou, opens
The new application of hair snake gall is the need for supporting the development of snake industry.There is snake gall refrigerant improving eyesight, removing toxic substances to remove miliaria, delay the work(of body aging
Effect, snake gall is added to and added in the perfume of essential oil, using the high osmosis of essential oil, human body is more easily absorbed having for snake gall
Composition is imitated, and utilizes the volatility speed difference of different cultivars essential oil, the modulated perfume with multi-level fragrance.
In addition, a perfect perfume is, it is necessary to by ageing, coarse smell be reconciled to make one the vintage of spirit and QI cleaning
Fougere.The perfume newly prepared is pungent, fragrance is discord, it is soft to owe, and promotes the esterification of perfume by ageing, makes the fragrance of perfume rich
Profit, it is soft.
The content of the invention
In view of the shortcomings of the prior art with market the need for, it is an object of the invention to provide a kind of snake gall jessamine and
It is aged.
One of the technical solution adopted for the present invention to solve the technical problems is：A kind of snake gall jessamine is provided, it is special
Levy and be that its component includes following parts by weight（Non- percentage）：
Rose 8~12, Lavender 8~12, fresh jasmine 6~10, geraniol 18~22, Oleum Ligni Santali 10~14, agalloch eaglewood
Alcohol 16~20, propane diols 48~52, snake gall leaching liquor 48~52, citric acid 10~14, hydroxycitronellal 8~12, absolute ethyl alcohol
500~700.
The two of the technical solution adopted for the present invention to solve the technical problems are：A kind of ageing of snake gall jessamine is provided
Method, it is characterised in that comprise the following steps：
First, the preparation of snake gall leaching liquor；The fresh parts by weight of snake gall 4~6 are taken plus 18~22 parts by weight absolute ethyl alcohol grindings, then with 4~6
Parts by weight absolute ethyl alcohol is washed 3 times, standby；
2nd, the preparation of the basic essential oil of perfume；Take rose 8~12, Lavender 8~12, fresh jasmine 6~8, geraniol 18
~22, Oleum Ligni Santali 10~14, linalool 16~20, the absolute ethyl alcohol of citric acid 10~14, hydroxycitronellal 8~12, Jia 80~120
Dissolving, then Jia 48~52 propane diols and 48~52 snake gall leaching liquors, is sufficiently mixed, standby；
3rd, perfume is aged；Basic 8~12 parts of the essential oil of perfume of step 2 configuration is settled to 50 with absolute ethyl alcohol, 30 DEG C~70
100~140min of heating water bath in DEG C water-bath, is cooled to room temperature, and 70~74h is then placed in subzero 4~6 DEG C, and taking-up allows
Its clear-cutting forestland stands 46~50h, places 28~32 days and produce at normal temperatures after sealing to normal temperature.
The beneficial effects of the invention are as follows：The micro- Huang of perfume color and luster after ageing, transparency is good；Head perfume has dense autumn gas
Breath, is not pungent, influential；The plump perfection of body note, bottom note continues for a long time, of puzzling aftertaste.The perfume drawn after ageing is antibacterial
Work well, to staphylococcus aureus inhibition zone up to 1.9cm, escherichia coli inhibition zone reaches 2.8cm, by withered grass bud bag bacillus
Design sketch understands that inhibition zone reaches 2.3cm.
Brief description of the drawings
Fig. 1 is bacteriostatic test result table of the present invention.
Fig. 2 is the GC-MS collection of illustrative plates before perfume ageing of the present invention.
Fig. 3 is GC-MS collection of illustrative plates after perfume ageing of the present invention.
Fig. 4 is the material figure of composition contrast new life before and after perfume ageing of the present invention.
Embodiment
There is provided a kind of snake gall jessamine in the first embodiment of the invention, it is characterised in that its component includes following weight
Measure part（Non- percentage）：
Rose 8, Lavender 8, fresh jasmine 6, geraniol 18, Oleum Ligni Santali 10, linalool 16, propane diols 48, snake gall leaching
Extract 48, citric acid 10, hydroxycitronellal 8, absolute ethyl alcohol 500.
There is provided a kind of aging method of snake gall jessamine, it is characterised in that comprise the following steps：
First, the preparation of snake gall leaching liquor；The fresh parts by weight of snake gall 4 plus 18 parts by weight absolute ethyl alcohols are taken to grind, then it is anhydrous with 4 parts by weight
Ethanol is washed 3 times, standby；
2nd, the preparation of the basic essential oil of perfume；Take rose 8, Lavender 8, fresh jasmine 6, geraniol 18, Oleum Ligni Santali 10,
Linalool 16, citric acid 10, hydroxycitronellal 8 plus the dissolving of 80 absolute ethyl alcohols, then add 48 propane diols and 48 snake gall leaching liquors, fill
Divide mixing, it is standby；
3rd, perfume is aged；Basic 8 parts of the essential oil of perfume of step 2 configuration is settled to 50 with absolute ethyl alcohol, in 30 DEG C~70 DEG C water
100~140min of heating water bath in bath, is cooled to room temperature, and 70~74h is then placed in subzero 4~6 DEG C, and taking-up allows it certainly
So recover to normal temperature, stand 46~50h, place 28~32 days and produce at normal temperatures after sealing.
There is provided a kind of snake gall jessamine in second embodiment of the invention, it is characterised in that its component includes following weight
Measure part（Non- percentage）：
Rose 12, Lavender 12, fresh jasmine 10, geraniol 22, Oleum Ligni Santali 14, linalool 20, propane diols 52, snake gall
Leaching liquor 52, citric acid 14, hydroxycitronellal 12, absolute ethyl alcohol 700.
There is provided a kind of aging method of snake gall jessamine, it is characterised in that comprise the following steps：
First, the preparation of snake gall leaching liquor；The fresh parts by weight of snake gall 6 plus 22 parts by weight absolute ethyl alcohols are taken to grind, then it is anhydrous with 6 parts by weight
Ethanol is washed 3 times, standby；
2nd, the preparation of the basic essential oil of perfume；Take rose 12, Lavender 12, fresh jasmine 8, geraniol 22, Oleum Ligni Santali
14, linalool 20, citric acid 14, hydroxycitronellal 12 plus the dissolving of 120 absolute ethyl alcohols, then add 52 propane diols and the extraction of 52 snake galls
Liquid, is sufficiently mixed, standby；
3rd, perfume is aged；Basic 12 parts of the essential oil of perfume of step 2 configuration is settled to 50 with absolute ethyl alcohol, in 30 DEG C~70 DEG C water
100~140min of heating water bath in bath, is cooled to room temperature, and 70~74h is then placed in subzero 4~6 DEG C, and taking-up allows it certainly
So recover to normal temperature, stand 46~50h, place 28~32 days and produce at normal temperatures after sealing.
There is provided a kind of snake gall jessamine in the preferred embodiment, it is characterised in that its component includes as follows
Parts by weight（Non- percentage）：
Rose 10, Lavender 10, fresh jasmine 8, geraniol 20, Oleum Ligni Santali 12, linalool 18, propane diols 50, snake gall
Leaching liquor 50, citric acid 12, hydroxycitronellal 10, absolute ethyl alcohol 600.
There is provided a kind of aging method of snake gall jessamine, it is characterised in that comprise the following steps：
First, the preparation of snake gall leaching liquor；Take the fresh absolute ethyl alcohol of snake gall 5 plus 20 to be ground in mortar, be transferred in 50ml volumetric flasks,
Washed 3 times, and be transferred in volumetric flask with 5 absolute ethyl alcohols, use absolute ethyl alcohol constant volume, it is standby；
2nd, the preparation of the basic essential oil of perfume；Rose 10 is taken, lavender 10, fresh jasmine 8, geraniol 20, Oleum Ligni Santali 12 sinks
Aromatic 18, citric acid 12, hydroxycitronellal 10 plus 100 absolute ethyl alcohols dissolve, then add 50 propane diols and 50 snake gall leaching liquors, with nothing
Water-ethanol is settled to 500ml, standby；
3rd, perfume is aged；Basic 10 parts of the essential oil of perfume of step 2 configuration is settled to 50 ml with absolute ethyl alcohol, 30 DEG C~70
100~140min of heating water bath in DEG C water-bath, is cooled to room temperature, and 70~74h is then placed in subzero 4~6 DEG C, and taking-up allows
Its clear-cutting forestland stands 46~50h, places 28~32 days and produce at normal temperatures after sealing to normal temperature.
Bacteriostatic experiment
Actication of culture
Bacillus subtilis, staphylococcus aureus, Escherichia coli are activated first, then transferred into the test tube slant prepared
On culture medium, 24h is cultivated in the environment of 37 DEG C in constant incubator.With the ring thalline of oese picking one, it is put into and is equipped with
In the conical flask of 10mL sterilized waters, fully shake up, bacteria suspension is made, it is standby.
The bacteria suspension that 1mL has been prepared is drawn with 1mL aseptic straws, is accurately put in 0.5mL to No. 1 test tube, this is
For 10 times of dilutions.Unnecessary bacterium solution is put back in original bacteria liquid.Separately taking a 1mL suction pipe to insert in No. 1 test tube, pressure-vaccum bacterium is hanged back and forth
Liquid three times, thalline is further disperseed, mixed, the bacterium solution 1mL of 10 times of dilutions are drawn with this suction pipe, 0.5mL to No. 2 is accurately put
In test tube, this is 100 times of dilutions.Remaining the like.200uL is separately added into each flat board for pouring into culture medium to have made
It, is uniformly applied on the flat board of culture medium, in aseptic operating platform by the bacteria suspension for the 100000 times of dilutions got ready with spreading rod
It is standby after upper placement a period of time.
The assay method of bacteriostatic activity
Filter paper dick is broken into 4mm disk with puncher, in an oven after autoclaving, placed it in perfume and blank
30min is soaked in the water of control, unnecessary test solution is drained, filter paper is gripped with aseptic nipper, the culture for coating bacterium solution is put into
On base flat board.It is placed in culture 48h in 37 DEG C of constant incubators.Culture terminate after, with ruler measure culture medium in inhibition zone it is straight
Footpath (diameter for removing filter paper).
Bacteriostatic experiment result
Referring to Fig. 1, Fig. 1 is biocidal property experimental result picture, and perfume is obvious to staphylococcus aureus fungistatic effect, inhibition zone
Up to 19mm；Perfume group is also very good to Escherichia coli fungistatic effect, and inhibition zone is up to 2.8cm；Perfume group is to withered grass bud bag bacillus
Preferably, inhibition zone is up to 2.3cm for effect.Effect size to bacterial strain is：Escherichia coli>Bacillus subtilis>Golden yellow grape
Coccus.Illustrate that this perfume has relatively good fungistatic effect.
GC-MS detections before and after perfume ageing
Determined by experimenter's sense organ, fragrance is more miscellaneous before perfume ageing, is a little pungent, and being aged back perfume (or spice) has dense autumn gas
Breath, and be not pungent, it is influential；The plump perfection of body note, bottom note continues for a long time, of puzzling aftertaste；It is all fragrant harmonious；So we will be old
Perfume before and after changing carries out GC-MS constituent analyses.
GC-MS conditions
GC conditions：DB-1 fused-silica capillary columns（30m×0.25mm×0.25μm）；Stationary phase is 5% phenyl and 95% diformazan
Based polysiloxane；Carrier gas is the kPa of pressure 47 before high-purity helium, post, and split ratio is 1:50.Three rank temperature programmings：70 DEG C of column temperature,
Maintain 1 min；120 DEG C are warming up to 3 DEG C/min, 1 min is maintained；180 DEG C are warming up to 5 DEG C/min again, 1 is maintained
min；It is last to be warming up to 250 DEG C with 8 DEG C/min, maintain 5 min.
MS conditions：EI ion guns, the eV of electron energy 70, the kV of electron multiplier 1.5, the min of solvent delay 2, scanning range
30~470 amu, full scan mode, sample size is 1 μ L.
Referring to Fig. 4, GC-MS detections are operated before and after being aged according to perfume, and the composition before being aged to perfume and after ageing is contrasted.
Front and rear GC-MC figure contrasts are aged from perfume to can be seen that, there are four kinds of new materials to produce after perfume ageing, are respectively
R (+)-glycidol, 4- isopropyl -1,2- cyclohexanediols, benzyl acetate, 3- pi-allyl -2- metoxyphenol percentages contain
Amount is 0.15%, 0.23%, 0.18%, 9.95% respectively, when this four kinds of materials are perfume ageings, reaction generation.
Claims (2)
1. a kind of snake gall jessamine, it is characterised in that its component includes following parts by weight：
Rose 8~12, Lavender 8~12, fresh jasmine 6~10, geraniol 18~22, Oleum Ligni Santali 10~14, agalloch eaglewood
Alcohol 16~20, propane diols 48~52, snake gall leaching liquor 48~52, citric acid 10~14, hydroxycitronellal 8~12, absolute ethyl alcohol
500~700.
2. the aging method of snake gall jessamine according to claim 1, it is characterised in that comprise the following steps：
First, the preparation of snake gall leaching liquor；The fresh parts by weight of snake gall 4~6 are taken plus 18~22 parts by weight absolute ethyl alcohol grindings, then with 4~6
Parts by weight absolute ethyl alcohol is washed 3 times, standby；
2nd, the preparation of the basic essential oil of perfume；Take rose 8~12, Lavender 8~12, fresh jasmine 6~8, geraniol 18
~22, Oleum Ligni Santali 10~14, linalool 16~20, the absolute ethyl alcohol of citric acid 1~14, hydroxycitronellal 8~12, Jia 80~120
Dissolving, then Jia 48~52 propane diols and 48~52 snake gall leaching liquors, is sufficiently mixed, standby；
3rd, perfume is aged；Basic 8~12 parts of the essential oil of perfume of step 2 configuration is settled to 48~52 with absolute ethyl alcohol, at 30 DEG C
100~140min of heating water bath in~70 DEG C of water-baths, is cooled to room temperature, and 70~74h is then placed in subzero 4~6 DEG C, is taken
Its clear-cutting forestland is sold to normal temperature, 46~50h is stood, places 28~32 days and produce at normal temperatures after sealing.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710168542.3A CN107049915A (en) | 2017-03-21 | 2017-03-21 | A kind of snake gall jessamine and its ageing |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710168542.3A CN107049915A (en) | 2017-03-21 | 2017-03-21 | A kind of snake gall jessamine and its ageing |
Publications (1)
| Publication Number | Publication Date |
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| CN107049915A true CN107049915A (en) | 2017-08-18 |
Family
ID=59620806
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| CN201710168542.3A Pending CN107049915A (en) | 2017-03-21 | 2017-03-21 | A kind of snake gall jessamine and its ageing |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107519118A (en) * | 2017-08-31 | 2017-12-29 | 广西小燕蛇业有限公司 | A kind of snake gall eye mask and preparation method thereof |
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2017
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| 朱洪法等编: "《精细化学产品配方与制造 第7册》", 31 October 2001, 北京金盾出版社 * |
| 王淑君等: "《美容产品制剂学》", 31 January 2012, 辽宁科学技术出版社 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107519118A (en) * | 2017-08-31 | 2017-12-29 | 广西小燕蛇业有限公司 | A kind of snake gall eye mask and preparation method thereof |
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Application publication date: 20170818 |