CN107033510A - A kind of highly-efficient glass thermal isolation film - Google Patents

A kind of highly-efficient glass thermal isolation film Download PDF

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Publication number
CN107033510A
CN107033510A CN201710366939.3A CN201710366939A CN107033510A CN 107033510 A CN107033510 A CN 107033510A CN 201710366939 A CN201710366939 A CN 201710366939A CN 107033510 A CN107033510 A CN 107033510A
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China
Prior art keywords
parts
highly
thermal isolation
isolation film
glass thermal
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Pending
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CN201710366939.3A
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Chinese (zh)
Inventor
孙祯彬
苏复
赵庆
孙俊
佟鹏飞
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Jurong Yaopi Glass Technology Development Co Ltd
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Jurong Yaopi Glass Technology Development Co Ltd
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Priority to CN201710366939.3A priority Critical patent/CN107033510A/en
Publication of CN107033510A publication Critical patent/CN107033510A/en
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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L33/00—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J5/00—Manufacture of articles or shaped materials containing macromolecular substances
    • C08J5/18—Manufacture of films or sheets
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2333/00—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Derivatives of such polymers
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2423/00—Characterised by the use of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Derivatives of such polymers
    • C08J2423/02—Characterised by the use of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Derivatives of such polymers not modified by chemical after treatment
    • C08J2423/04—Homopolymers or copolymers of ethene
    • C08J2423/06—Polyethene
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2423/00—Characterised by the use of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Derivatives of such polymers
    • C08J2423/02—Characterised by the use of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Derivatives of such polymers not modified by chemical after treatment
    • C08J2423/10—Homopolymers or copolymers of propene
    • C08J2423/12—Polypropene
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2423/00—Characterised by the use of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Derivatives of such polymers
    • C08J2423/26—Characterised by the use of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Derivatives of such polymers modified by chemical after-treatment
    • C08J2423/30—Characterised by the use of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Derivatives of such polymers modified by chemical after-treatment by oxidation
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2429/00—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an alcohol, ether, aldehydo, ketonic, acetal, or ketal radical; Hydrolysed polymers of esters of unsaturated alcohols with saturated carboxylic acids; Derivatives of such polymer
    • C08J2429/02—Homopolymers or copolymers of unsaturated alcohols
    • C08J2429/04—Polyvinyl alcohol; Partially hydrolysed homopolymers or copolymers of esters of unsaturated alcohols with saturated carboxylic acids
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2433/00—Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Derivatives of such polymers
    • C08J2433/24—Homopolymers or copolymers of amides or imides
    • C08J2433/26—Homopolymers or copolymers of acrylamide or methacrylamide
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2483/00—Characterised by the use of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon with or without sulfur, nitrogen, oxygen, or carbon only; Derivatives of such polymers
    • C08J2483/04—Polysiloxanes
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K2201/00—Specific properties of additives
    • C08K2201/014—Additives containing two or more different additives of the same subgroup in C08K
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2203/00—Applications
    • C08L2203/16—Applications used for films
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00—Polymer mixtures characterised by other features
    • C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00—Polymer mixtures characterised by other features
    • C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
    • C08L2205/025—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group containing two or more polymers of the same hierarchy C08L, and differing only in parameters such as density, comonomer content, molecular weight, structure
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00—Polymer mixtures characterised by other features
    • C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
    • C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Manufacturing & Machinery (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Laminated Bodies (AREA)
  • Compositions Of Macromolecular Compounds (AREA)

Abstract

The invention discloses a kind of highly-efficient glass thermal isolation film, 20~30 parts of acrylic resin, 10~20 parts of bentonite, 5~15 parts of kaolin are mixed at 55~65 DEG C, stirred；15 parts of dispersant, 13 parts of levelling agent, 12 parts of thickener are sequentially added into mixture, is stirred continuously until to form finely dispersed dope；Above-mentioned dope is sent into film laminator, film is pressed into, highly-efficient glass thermal isolation film finished product is produced after static cooling.Present invention making raw material is simple and easy to get, and manufacture craft is simple to operation；Gained finished product is easy to use, and effect of heat insulation is obvious.

Description

A kind of highly-efficient glass thermal isolation film
Technical field
The present invention relates to a kind of thermal isolation film, and in particular to a kind of highly-efficient glass thermal isolation film.
Background technology
Glass is that a kind of transparent, intensity and hardness are quite high, and air-locked material is widely used in various architectural.To protect The good translucency of card, now widely used glass is mostly individual layer plate glass, but effect of heat insulation is poor, is especially existed Hot summer, it is impossible to effectively stop that the heat of outdoor sunshine is got in, so as to cause indoor temperature higher.For having thrown Enter the building used, change glass cost higher, it is necessary to take effective provision for thermal insulation on the basis of existing.
The content of the invention
The technical problem of solution：In view of the shortcomings of the prior art, the invention provides a kind of highly-efficient glass thermal isolation film, save Cost, improves the effect of heat insulation of glass.
Technical scheme：A kind of highly-efficient glass thermal isolation film that the present invention is provided, is prepared from the following raw materials in parts by weight：Propylene 20-30 parts of acid resin, 10-20 parts of bentonite, 5-15 parts of kaolin, 1-5 parts of dispersant, 1-3 parts of levelling agent, 1-2 parts of thickener. The thickness of the glass heat-proof film is 6,8 or 12.
The dispersant is the mixture of one or both of Tissuemat E, polypropylene wax, matter when both are used in mixed way Amount is than being 2:3.
The levelling agent is the mixture of one or both of dimethyl silicone polymer, PSI, two Mass ratio is 1 when person is used in mixed way:2.
The thickener is the mixture of one or both of polyacrylamide, polyvinyl alcohol, polyethylene glycol oxide, both Mass ratio is 1 when being used in mixed way:1.
A kind of preparation method for highly-efficient glass thermal isolation film that the present invention is provided, it includes following preparation process：
（1）20~30 parts of acrylic resin, 10~20 parts of bentonite, 5~15 parts of kaolin are mixed at 55~65 DEG C, fully Stir；
（2）1-5 parts of dispersant, 1-3 parts of levelling agent, 1-2 parts of thickener are sequentially added into said mixture, is stirred continuously until Form finely dispersed dope；
（3）Above-mentioned dope is sent into film laminator, film is pressed into, highly-efficient glass thermal isolation film finished product is produced after static cooling.
Beneficial effect：A kind of highly-efficient glass thermal isolation film that the present invention is provided, making raw material is simple and easy to get, and manufacture craft is simple It is easy to operate；Gained finished product is easy to use, and effect of heat insulation is obvious.
Embodiment
The present invention is further illustrated below by the mode of embodiment, but therefore protection scope of the present invention is not confined to Following embodiments, but limited by description and claims of this specification.
Embodiment 1
A kind of highly-efficient glass thermal isolation film, is prepared from the following raw materials in parts by weight：20 parts of acrylic resin, 10 parts of bentonite, height 5 parts of ridge soil, 1 part of Tissuemat E, 1 part of dimethyl silicone polymer, 1 part of polyacrylamide；Its making step is as follows：
（1）20 parts of acrylic resin, 10 parts of bentonite, 5 parts of kaolin are mixed at 55 DEG C, stirred；
（2）1 part of Tissuemat E, 1 part of dimethyl silicone polymer, 1 part of polyacrylamide are sequentially added into said mixture, is continued Stirring is until form finely dispersed dope；
（3）Above-mentioned dope is sent into film laminator, 6 films is pressed into, highly-efficient glass thermal isolation film finished product is produced after static cooling.
Embodiment 2
A kind of highly-efficient glass thermal isolation film, is prepared from the following raw materials in parts by weight：25 parts of acrylic resin, 15 parts of bentonite, height 10 parts of ridge soil, 3 parts of polypropylene wax, 2 parts of PSI, 2 parts of polyvinyl alcohol；Its making step is as follows：
（1）25 parts of acrylic resin, 15 parts of bentonite, 10 parts of kaolin are mixed at 60 DEG C, stirred；
（2）3 parts of polypropylene wax, 2 parts of PSI, 2 parts of polyvinyl alcohol are sequentially added into said mixture, is continued Stirring is until form finely dispersed dope；
（3）Above-mentioned dope is sent into film laminator, 8 films is pressed into, highly-efficient glass thermal isolation film finished product is produced after static cooling.
Embodiment 3
A kind of highly-efficient glass thermal isolation film, is prepared from the following raw materials in parts by weight：30 parts of acrylic resin, 20 parts of bentonite, height 15 parts of ridge soil, 5 parts of Tissuemat E, 3 parts of PSI, 2 parts of polyethylene glycol oxide；Its making step is as follows：
（1）30 parts of acrylic resin, 20 parts of bentonite, 15 parts of kaolin are mixed at 65 DEG C, stirred；
（2）5 parts of Tissuemat E, 3 parts of PSI, 2 parts of polyethylene glycol oxide are sequentially added into said mixture, is held Continuous stirring is until form finely dispersed dope；
（3）Above-mentioned dope is sent into film laminator, 12 films is pressed into, highly-efficient glass thermal isolation film finished product is produced after static cooling.
Embodiment 4
A kind of highly-efficient glass thermal isolation film, is prepared from the following raw materials in parts by weight：26 parts of acrylic resin, 18 parts of bentonite, height 12 parts of ridge soil, 2 parts of Tissuemat E, 3 parts of polypropylene wax, 1 part of dimethyl silicone polymer, 2 parts of PSI, polypropylene 1 part of acid amides, 1 part of polyvinyl alcohol；Its making step is as follows：
（1）26 parts of acrylic resin, 18 parts of bentonite, 12 parts of kaolin are mixed at 60 DEG C, stirred；
（2）2 parts of Tissuemat E, 3 parts of polypropylene wax, 1 part of dimethyl silicone polymer, poly- methyl are sequentially added into said mixture 2 parts of phenyl siloxane, 1 part of polyacrylamide, 1 part of polyvinyl alcohol, are stirred continuously until to form finely dispersed dope；
（3）Above-mentioned dope is sent into film laminator, 8 films is pressed into, highly-efficient glass thermal isolation film finished product is produced after static cooling.
Above-described embodiment finished product is overlying on the outside of glass of building, under different outside air temperatures, indoor and outdoor temperature, knot is contrasted Fruit is as shown in table 1：
Table 1
From upper table it can be found that embodiment 1-4 highly-efficient glass thermal isolation film finished thermal insulation effect is obvious, indoor temperature compares outdoor temp Spend low 5-9 DEG C.

Claims (6)

1. a kind of highly-efficient glass thermal isolation film, it is characterised in that be prepared from the following raw materials in parts by weight：Acrylic resin 20-30 Part, 10-20 parts of bentonite, 5-15 parts of kaolin, 1-5 parts of dispersant, 1-3 parts of levelling agent, 1-2 parts of thickener.
2. a kind of highly-efficient glass thermal isolation film according to claim 1, it is characterised in that：The dispersant be Tissuemat E, The mixture of one or both of polypropylene wax, mass ratio is 2 when both are used in mixed way:3.
3. a kind of highly-efficient glass thermal isolation film according to claim 1, it is characterised in that：The levelling agent is poly dimethyl silicon The mixture of one or both of oxygen alkane, PSI, mass ratio is 1 when both are used in mixed way:2.
4. a kind of highly-efficient glass thermal isolation film according to claim 1, it is characterised in that：The thickener is polyacrylamide The mixture of one or both of amine, polyvinyl alcohol, polyethylene glycol oxide, mass ratio is 1 when both are used in mixed way:1.
5. a kind of highly-efficient glass thermal isolation film according to claim 1, it is characterised in that：The thickness of the glass heat-proof film is 6,8 or 12.
6. a kind of preparation method of highly-efficient glass thermal isolation film as claimed in claim 1, it is characterised in that prepare step including following Suddenly：
（1）20~30 parts of acrylic resin, 10~20 parts of bentonite, 5~15 parts of kaolin are mixed at 55~65 DEG C, fully Stir；
（2）1-5 parts of dispersant, 1-3 parts of levelling agent, 1-2 parts of thickener are sequentially added into said mixture, is stirred continuously until Form finely dispersed dope；
（3）Above-mentioned dope is sent into film laminator, film is pressed into, highly-efficient glass thermal isolation film finished product is produced after static cooling.
CN201710366939.3A 2017-05-23 2017-05-23 A kind of highly-efficient glass thermal isolation film Pending CN107033510A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108274860A (en) * 2018-01-26 2018-07-13 德兴市盛仕工贸有限公司 Plank in a kind of internal heat type constant temperature complex heat-preservation case

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106634321A (en) * 2016-09-21 2017-05-10 东莞市联洲知识产权运营管理有限公司 Scratch-proof anti-abrasion heat insulating film of car front windshield and preparation method of scratch-proof anti-abrasion heat insulating film

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106634321A (en) * 2016-09-21 2017-05-10 东莞市联洲知识产权运营管理有限公司 Scratch-proof anti-abrasion heat insulating film of car front windshield and preparation method of scratch-proof anti-abrasion heat insulating film

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108274860A (en) * 2018-01-26 2018-07-13 德兴市盛仕工贸有限公司 Plank in a kind of internal heat type constant temperature complex heat-preservation case

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Application publication date: 20170811