CN107022775A - A kind of preparation method of nickel plated steel strip - Google Patents
A kind of preparation method of nickel plated steel strip Download PDFInfo
- Publication number
- CN107022775A CN107022775A CN201710261099.4A CN201710261099A CN107022775A CN 107022775 A CN107022775 A CN 107022775A CN 201710261099 A CN201710261099 A CN 201710261099A CN 107022775 A CN107022775 A CN 107022775A
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- CN
- China
- Prior art keywords
- nickel
- steel strip
- plated steel
- treatment
- nickel plating
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
- C25D3/00—Electroplating: Baths therefor
- C25D3/02—Electroplating: Baths therefor from solutions
- C25D3/12—Electroplating: Baths therefor from solutions of nickel or cobalt
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
- C25D7/00—Electroplating characterised by the article coated
- C25D7/06—Wires; Strips; Foils
- C25D7/0614—Strips or foils
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Sealing Battery Cases Or Jackets (AREA)
- Electroplating And Plating Baths Therefor (AREA)
- Electroplating Methods And Accessories (AREA)
Abstract
The invention provides a kind of preparation method of nickel plated steel strip, comprise the following steps：1）Pre-treatment；Steel band is proceeded through into oil removing and processing of rust removing, oil removing mode is ultrasonic oil removal, and derusting mode is acid soak；2）Electro-deposition：Steel band Jing Guo pre-treatment is subjected to electrodeposit nickel plating in nickel plating solution, electroplating time is 15min；3）Heat treatment：After nickel plated steel strip washing drying, it is placed in vacuum annealing furnace, 10 h is incubated at 600 700 DEG C, then furnace cooling；Described step 2）In, described step 2）In, described nickel plating solution, including following composition：Nickel sulfamic acid, nickel chloride and boric acid, the weight ratio of three is 60 100：1：8.Nickel plated steel strip hardness, intensity and fine corrosion resistance prepared by the method for the present invention.
Description
Technical field
The present invention relates to a kind of preparation method of nickel plated steel strip, belong to electroplating technology field.
Background technology
Nickel plated steel strip is a kind of novel nickel-hydrogen, nickel-cadmium battery negative pole plate material, and alkali-manganese cell steel shell needs to have necessarily
Anti-oxidant and corrosive power, generally protects box hat using nickel plating process, and existing nickel plating process has two kinds, and one kind is drawn by steel band
It is stretched into nickel plating after shell；Another is steel band nickel plating after-drawing shell (nickel preplating steel band), and latter production efficiency is high, and quality is equal
One, the battery storage performance being made is good.
Existing nickel plated steel strip has hardness, intensity and decay resistance not enough excellent weak point.
The content of the invention
The purpose of the present invention is to overcome the deficiencies in the prior art there is provided a kind of preparation method of nickel plated steel strip.
The preparation method of the nickel plated steel strip of the present invention, comprises the following steps：
1）Pre-treatment；Steel band is proceeded through into oil removing and processing of rust removing, oil removing mode is ultrasonic oil removal, and derusting mode is acid solution
Immersion；
2）Electro-deposition：Steel band Jing Guo pre-treatment is subjected to electrodeposit nickel plating in nickel plating solution, electroplating time is 15min；
3）Heat treatment：After nickel plated steel strip washing drying, it is placed in vacuum annealing furnace, 10 h is incubated at 600-700 DEG C,
Then furnace cooling.
Described step 2）In,
Described step 2）In, described nickel plating solution, including following composition：Nickel sulfamic acid, nickel chloride and boric acid, three's
Weight ratio is 60-100：1：8.
Nickel plated steel strip hardness, intensity and fine corrosion resistance prepared by the method for the present invention.
Embodiment
Embodiment 1
The preparation method of the nickel plated steel strip of the present embodiment, comprises the following steps：
1）Pre-treatment；Steel band is proceeded through into oil removing and processing of rust removing, oil removing mode is ultrasonic oil removal, and derusting mode is acid solution
Immersion；
2）Electro-deposition：Steel band Jing Guo pre-treatment is subjected to electrodeposit nickel plating in nickel plating solution, electroplating time is 15min；
3）Heat treatment：After nickel plated steel strip washing drying, it is placed in vacuum annealing furnace, 10 h is incubated at 600-700 DEG C,
Then furnace cooling.
Described step 2）In, described nickel plating solution, including following composition：Nickel sulfamic acid, nickel chloride and boric acid, three
The weight ratio of person is 60：1：8.
Embodiment 2
The preparation method of the nickel plated steel strip of the present embodiment, step step 2 same as Example 1, described）In, described nickel electricity
Plating solution, including following composition：Nickel sulfamic acid, nickel chloride and boric acid, the weight ratio of three is 100：1：8.
Embodiment 3
The preparation method of the nickel plated steel strip of the present embodiment, step step 2 same as Example 1, described）In, described nickel electricity
Plating solution, including following composition：Nickel sulfamic acid, nickel chloride and boric acid, the weight ratio of three is 80：1：8.
Claims (1)
1. a kind of preparation method of nickel plated steel strip, it is characterised in that comprise the following steps：
1）Pre-treatment；Steel band is proceeded through into oil removing and processing of rust removing, oil removing mode is ultrasonic oil removal, and derusting mode is acid solution
Immersion；
2）Electro-deposition：Steel band Jing Guo pre-treatment is subjected to electrodeposit nickel plating in nickel plating solution, electroplating time is 15min；
3）Heat treatment：After nickel plated steel strip washing drying, it is placed in vacuum annealing furnace, 10 h is incubated at 600-700 DEG C,
Then furnace cooling；
Described step 2）In, described nickel plating solution, including following composition：Nickel sulfamic acid, nickel chloride and boric acid, three's
Weight ratio is 60-100：1：8.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710261099.4A CN107022775A (en) | 2017-04-20 | 2017-04-20 | A kind of preparation method of nickel plated steel strip |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710261099.4A CN107022775A (en) | 2017-04-20 | 2017-04-20 | A kind of preparation method of nickel plated steel strip |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107022775A true CN107022775A (en) | 2017-08-08 |
Family
ID=59527247
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710261099.4A Pending CN107022775A (en) | 2017-04-20 | 2017-04-20 | A kind of preparation method of nickel plated steel strip |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107022775A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110721999A (en) * | 2019-10-17 | 2020-01-24 | 湖南科罗德新材料有限公司 | Copper-aluminum composite plate strip added with nickel grid layer and continuous production method thereof |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1861389A (en) * | 2006-06-13 | 2006-11-15 | 无锡市永鑫精密钢带厂 | High precision composite nickel steel band and its prodn. technique |
| CN105543918A (en) * | 2016-01-21 | 2016-05-04 | 燕山大学 | Method for preparing nickel plating steel strip by utilizing sulfamate pulse electronickelling |
-
2017
- 2017-04-20 CN CN201710261099.4A patent/CN107022775A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1861389A (en) * | 2006-06-13 | 2006-11-15 | 无锡市永鑫精密钢带厂 | High precision composite nickel steel band and its prodn. technique |
| CN105543918A (en) * | 2016-01-21 | 2016-05-04 | 燕山大学 | Method for preparing nickel plating steel strip by utilizing sulfamate pulse electronickelling |
Non-Patent Citations (1)
| Title |
|---|
| 安茂忠: "《电镀技术与应用》", 30 June 2007, 北京：机械工业出版社 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110721999A (en) * | 2019-10-17 | 2020-01-24 | 湖南科罗德新材料有限公司 | Copper-aluminum composite plate strip added with nickel grid layer and continuous production method thereof |
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| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20170808 |
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| RJ01 | Rejection of invention patent application after publication |